CN1119368C - Process for preparing polyamide resin used for alcohol-soluble ink - Google Patents
Process for preparing polyamide resin used for alcohol-soluble ink Download PDFInfo
- Publication number
- CN1119368C CN1119368C CN 00126683 CN00126683A CN1119368C CN 1119368 C CN1119368 C CN 1119368C CN 00126683 CN00126683 CN 00126683 CN 00126683 A CN00126683 A CN 00126683A CN 1119368 C CN1119368 C CN 1119368C
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- acid
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- polyamide resin
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- alcohol
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- Expired - Fee Related
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- Polyamides (AREA)
Abstract
Description
The test example | Raw material ratio (mol ratio) | Test-results | ||||||||||
Quadrol | M-phthalic acid (ester) sulfonate | Dimeracid | Diprotic acid | Polyamines | Monoprotic acid | Monoamine | Acid number mgKOH/g | Amine value mgKOH/g | Softening temperature (ring and ball method) ℃ | -15 ℃ of frost resistances (40% alcoholic solution) | Color and luster (50% alcoholic solution) Jia Shi, number | |
1 | 1.02 | 0.02, sodium salt | 1 | 0.2, m-phthalic acid | 0.2, hexanediamine | 0.5, stearic acid | 0.5, n-Butyl Amine 99 | 4.8 | 4.9 | 107.8 | Do not freeze in 30 minutes | 6 |
2 | 1.0 | 0.05, methyl esters, sodium salt | 1 | 0.2, hexanodioic acid | 0.1, diethylenetriamine | 0.4, stearic acid | 0.6, n-Butyl Amine 99 | 4.3 | 5.0 | 112.5 | Do not freeze in 35 minutes | 6 |
3 | 1.1 | 0.1, ethyl ester, sodium salt | 1 | 0.2, sebacic acid | 0.1, hexanediamine | 0.4, propionic acid | 0.6, n-Butyl Amine 99 | 3.0 | 4.3 | 117.1 | Do not freeze in 30 minutes | 6 |
4 | 1.02 | 0.02, methyl esters, magnesium salts | 1 | 0.3, m-phthalic acid | 0.2, diethylenetriamine | 0.5, propionic acid | 0.5, thanomin | 3.5 | 3.6 | 120.2 | Do not freeze in 35 minutes | 6 |
5 | 1.15 | 0.05, ethyl ester, magnesium salts | 1 | 0.3, hexanodioic acid | 0.2, hexanediamine | 0.5, stearic acid | 0.5 | 3.0 | 4.9 | 114.5 | Do not freeze in 30 minutes | 6 |
6 | 1.35 | 0.1, magnesium salts | 1 | 0.3, sebacic acid | 0.1, diethylenetriamine | 0.6, stearic acid | 0.4, thanomin | 5.0 | 5.0 | 108.5 | Do not freeze in 30 minutes | 6 |
7 | 0.92 | 0.02, zinc salt | 1 | 0.1, m-phthalic acid | 0.1, hexanediamine | 0.4, propionic acid | 0.6, diethanolamine | 2.6 | 3.4 | 105.2 | Do not freeze in 30 minutes | 6 |
8 | 0.85 | 0.05, methyl esters, zinc salt | 1 | 0.1, hexanodioic acid | 0.2, diethylenetriamine | 0.5, propionic acid | 0.5, diethanolamine | 4.5 | 4.7 | 106.3 | Do not freeze in 35 minutes | 6 |
9 | 1.0 | 0.1, ethyl ester, zinc salt | 1 | 0.1, sebacic acid | 0.1, hexanediamine | 0.4, stearic acid | 0.6, diethanolamine | 3.8 | 4.1 | 112.3 | Do not freeze in 30 minutes | 6 |
10 | 1.0 | 0.02, sodium salt | 1 | 0.2, m-phthalic acid | 0.2, hexanediamine | 0.5, stearic acid | 0.5, thanomin | 5.0 | 3.6 | 116 | Do not freeze in 30 minutes | 6 |
11 | 0.92 | 0.03, methyl esters, calcium salt | 1 | 0.2, hexanodioic acid | 0.2, diethylenetriamine | 0.5, propionic acid | 0.5, n-Butyl Amine 99 | 4.8 | 3.8 | 105 | Do not freeze in 30 minutes | 6 |
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 00126683 CN1119368C (en) | 2000-11-14 | 2000-11-14 | Process for preparing polyamide resin used for alcohol-soluble ink |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 00126683 CN1119368C (en) | 2000-11-14 | 2000-11-14 | Process for preparing polyamide resin used for alcohol-soluble ink |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1353128A CN1353128A (en) | 2002-06-12 |
CN1119368C true CN1119368C (en) | 2003-08-27 |
Family
ID=4591983
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 00126683 Expired - Fee Related CN1119368C (en) | 2000-11-14 | 2000-11-14 | Process for preparing polyamide resin used for alcohol-soluble ink |
Country Status (1)
Country | Link |
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CN (1) | CN1119368C (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6960248B2 (en) * | 2003-05-22 | 2005-11-01 | Arizona Chemical Company | Cyclic bisamides useful in formulating inks for phase-change printing |
CN103554485A (en) * | 2013-10-30 | 2014-02-05 | 安庆市虹泰新材料有限责任公司 | Preparation method of transparent dimer acid type polyamide resin |
CN103554486B (en) * | 2013-10-30 | 2016-01-06 | 安庆市虹泰新材料有限责任公司 | A kind of preparation method of alcohol dissolubility dimer acid type polyamide resin |
CN104788671A (en) * | 2015-04-30 | 2015-07-22 | 河北利晖生物科技股份有限公司 | Preparation method of environment-friendly high-hardness alcohol-soluble polyamide resin |
CN108148200A (en) * | 2016-12-02 | 2018-06-12 | 上海杰事杰新材料(集团)股份有限公司 | Water-soluble polyamide resins and preparation method thereof |
CN107652431A (en) * | 2017-11-09 | 2018-02-02 | 安庆巨元高分子材料科技有限公司 | One kind modeling printing ink alcohol-soluble polyamide resin and preparation method thereof |
CN111234208B (en) * | 2020-04-01 | 2021-07-16 | 中山大学 | Polyester/polyamide copolymer and preparation method and application thereof |
CN115594989A (en) * | 2022-11-28 | 2023-01-13 | 宇虹颜料股份有限公司(Cn) | Preparation method of polyamide pigment preparation |
-
2000
- 2000-11-14 CN CN 00126683 patent/CN1119368C/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
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CN1353128A (en) | 2002-06-12 |
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Legal Events
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C06 | Publication | ||
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ASS | Succession or assignment of patent right |
Owner name: CHINA PETROCHEMICAL CORPORATION PETROCHEMICAL CO. Free format text: FORMER OWNER: YUEYANG PETROCHEMICAL PLANT, BALING PETROCHEMICAL CORP. Effective date: 20030214 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20030214 Address after: 414014 Yunxi District, Hunan, Yueyang Applicant after: Sinopec Group Petrochemical Co., Ltd. Address before: 414014 Yunxi District, Hunan, Yueyang Applicant before: Yueyang Chemical General Plant, Baling Petrochemical |
|
ASS | Succession or assignment of patent right |
Owner name: BALING PETROCHEMICAL CO., LTD., SINOPEC Free format text: FORMER OWNER: CHINA PETROCHEMICAL CORPORATION PETROCHEMICAL CO., LTD. Effective date: 20030317 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20030317 Address after: 414014 Yunxi District, Hunan, Yueyang Applicant after: Baling Petrochemical Co., Ltd., SINOPEC Address before: 414014 Yunxi District, Hunan, Yueyang Applicant before: Sinopec Group Petrochemical Co., Ltd. |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C19 | Lapse of patent right due to non-payment of the annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |