CN111925871B - Peppermint oil distillation tower - Google Patents
Peppermint oil distillation tower Download PDFInfo
- Publication number
- CN111925871B CN111925871B CN202010934369.5A CN202010934369A CN111925871B CN 111925871 B CN111925871 B CN 111925871B CN 202010934369 A CN202010934369 A CN 202010934369A CN 111925871 B CN111925871 B CN 111925871B
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- CN
- China
- Prior art keywords
- distillation tower
- hollowed
- fretwork
- round hole
- distillation column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
- B01D19/0052—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/42—Regulation; Control
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a peppermint oil distillation tower, which comprises a distillation tower body and a Roots vacuum pump, wherein a rotary piercing mechanism is arranged at the joint of the distillation tower body and a distillation kettle, the rotary piercing mechanism comprises a limiting plate fixedly arranged at the bottom of the distillation tower body, a round hole is formed in the limiting plate, a hollowed-out ball body is arranged above the limiting plate, the diameter of the hollowed-out ball body is larger than that of the round hole, a part of the hollowed-out ball body penetrates through the round hole, two ends of the hollowed-out ball body are respectively and rotatably connected with the inner side wall of the distillation tower body, an asynchronous motor for driving the hollowed-out ball body to rotate is arranged at the outer side of the distillation tower body, the rotation axis of the hollowed-out ball body is perpendicular to the central line of the round hole, a current transformer for detecting current of the hollow-out ball body is arranged on the asynchronous motor, a frequency converter is arranged on the Roots vacuum pump, and the current transformer is electrically connected with a controller of the frequency converter.
Description
Technical Field
The invention relates to menthol processing, in particular to a peppermint oil distillation tower.
Background
The natural peppermint crude oil has more components and similar components, is difficult to separate, is a thermosensitive spice, has low distillation temperature, does not evaporate unnecessary fractions, has overhigh temperature, easily decomposes menthol which needs to be reserved, increases byproducts and has deep color, so as to prevent oil from decomposing, reduced pressure distillation is needed, a Roots vacuum pump is adopted in the prior art for vacuumizing, and the peppermint oil is easily foamed, so that liquid in a distillation kettle is easily flushed into a distillation column during boiling, vapor-liquid mass transfer is influenced, the technical problems are mainly caused by the following reasons, namely, the suction force of the existing vacuum pump is constant, the capacity of the distillation kettle is constant, the amount of air entering is increased when the feeding amount is increased, the vacuum pump cannot timely pump the menthol out, and bubbles easily gush into the distillation column after the liquid level in the distillation kettle is increased, so that the existing distillation column is required to be improved.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides a peppermint oil distillation tower, wherein a rotary hollow sphere is arranged at the joint of the distillation tower and a distillation kettle, and the peppermint oil distillation tower cannot enter the distillation tower after bubbles are generated.
In order to achieve the technical effects, the technical scheme of the invention is as follows: the utility model provides a peppermint oil distillation column, includes distillation column body, roots vacuum pump, distillation column body and stills's junction is provided with rotatory piercing mechanism, rotatory piercing mechanism including fixed set up in the limiting plate of distillation column body bottom, the round hole has been seted up on the limiting plate, the top of limiting plate is provided with the fretwork spheroid, the spheroidal diameter of fretwork is greater than the diameter of round hole just fretwork spheroidal part passes the round hole, fretwork spheroidal both ends respectively with distillation column body's inside wall rotates to be connected, distillation column body's outside is provided with the drive fretwork spheroid pivoted asynchronous motor, fretwork spheroidal axis of rotation with the central line of round hole is mutually perpendicular, be provided with the current transformer who detects its electric current on the asynchronous motor, be provided with the converter on the roots vacuum pump, the current transformer with the controller of converter is connected mutually electricity.
Further improved is that the outer surface of the hollowed-out sphere is provided with a plurality of spike parts extending along the radial direction of the hollowed-out sphere.
Further improved is that the spike is needle-shaped or conical.
The further improvement is that the two ends of the hollowed-out sphere are respectively connected with the distillation tower body in a rotating way through a rotating joint.
Further improved is that the hollowed-out sphere is in a grid shape.
The invention has the advantages and beneficial effects that: firstly, the rotary hollow sphere is arranged at the joint of the distillation tower and the distillation kettle, after bubbles are generated, the hollow sphere which is rotated is intercepted and cannot enter the distillation tower, in addition, the spike part on the hollow sphere punctures the bubbles, peppermint oil is adhered to the hollow sphere, the whole weight of the hollow sphere is gradually heavier, the load of the asynchronous motor is increased, the current transformer transmits the detected current increasing signal to the frequency converter of the vacuum pump, and therefore the adsorption force of the vacuum pump is improved, and the generation of the bubbles is reduced.
Drawings
Fig. 1 is a schematic structural view of the present invention.
In the figure: 1. a distillation column body; 2. a limiting plate; 3. a distillation still; 4. hollow spheres; 5. an asynchronous motor; 6. and rotating the joint.
Detailed Description
The following describes the embodiments of the present invention further with reference to the drawings and examples. The following examples are only for more clearly illustrating the technical aspects of the present invention, and are not intended to limit the scope of the present invention.
As shown in fig. 1, the peppermint oil distillation tower comprises a distillation tower body 1 and a roots vacuum pump, and is characterized in that a rotary piercing mechanism is arranged at the joint of the distillation tower body 1 and a distillation kettle 2, the rotary piercing mechanism comprises a limiting plate 3 fixedly arranged at the bottom of the distillation tower body 1, a round hole is formed in the limiting plate 3, a hollowed ball 4 is arranged above the limiting plate 3, the diameter of the hollowed ball 4 is larger than that of the round hole, the part of the hollowed ball 4 penetrates through the round hole, two ends of the hollowed ball 4 are respectively connected with the inner side wall of the distillation tower body 1 in a rotary mode, an asynchronous motor 5 for driving the hollowed ball 4 to rotate is arranged at the outer side of the distillation tower body 1, the axis of rotation of the hollowed ball 4 is perpendicular to the central line of the round hole, a current transformer for detecting current of the hollowed ball is arranged on the asynchronous motor 5, a frequency converter is arranged on the roots vacuum pump, and the current transformer is electrically connected with a controller of the frequency converter.
In order to facilitate puncturing the bubbles and prevent the bubbles from entering the distillation tower, the outer surface of the hollow sphere 4 is provided with a plurality of spike parts extending along the radial direction of the hollow sphere, preferably, the spike parts are needle-shaped or conical, the hollow sphere 4 punctures the bubbles after the bubbles contact with the spike parts in the rotation process, and the punctured oil gas bubbles are adhered to the surface of the hollow sphere 4.
In this embodiment, preferably, two ends of the hollow sphere 4 are respectively rotatably connected with the distillation tower body 1 through a rotary joint 6.
In this embodiment, preferably, the hollow sphere 4 is in a grid shape.
The foregoing is merely a preferred embodiment of the present invention, and it should be noted that it will be apparent to those skilled in the art that several modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the scope of the invention.
Claims (4)
1. The utility model provides a peppermint oil distillation column, includes distillation column body, roots vacuum pump, its characterized in that, distillation column body and stills's junction is provided with rotatory piercing mechanism, rotatory piercing mechanism including fixed set up in the limiting plate of distillation column body bottom, the round hole has been seted up on the limiting plate, the top of limiting plate is provided with the fretwork spheroid, the spheroidal diameter of fretwork is greater than the diameter of round hole just fretwork spheroidal part passes the round hole, fretwork spheroidal both ends respectively with distillation column body's inside wall rotates to be connected, distillation column body's outside is provided with the drive fretwork spheroid pivoted asynchronous motor, the spheroidal axis of rotation of fretwork with the central line of round hole is mutually perpendicular, be provided with the current transformer who detects its electric current on the asynchronous motor, be provided with the converter on the roots vacuum pump, the current transformer with the controller of converter is connected, the spheroidal surface of fretwork is provided with a plurality of spines along its radial extension.
2. The peppermint oil distillation tower of claim 1, wherein the spike is needle-shaped or cone-shaped.
3. The peppermint oil distillation tower of claim 1, wherein two ends of the hollowed-out sphere are respectively rotatably connected with the distillation tower body through a rotary joint.
4. The peppermint oil distillation column of claim 1, wherein said hollowed-out spheres are in the form of a grid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010934369.5A CN111925871B (en) | 2020-09-08 | 2020-09-08 | Peppermint oil distillation tower |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010934369.5A CN111925871B (en) | 2020-09-08 | 2020-09-08 | Peppermint oil distillation tower |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111925871A CN111925871A (en) | 2020-11-13 |
| CN111925871B true CN111925871B (en) | 2023-04-21 |
Family
ID=73309239
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010934369.5A Active CN111925871B (en) | 2020-09-08 | 2020-09-08 | Peppermint oil distillation tower |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111925871B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201825929U (en) * | 2010-09-14 | 2011-05-11 | 南通薄荷厂有限公司 | Mentha arvensis oil distillation device |
| CN205109076U (en) * | 2015-11-25 | 2016-03-30 | 安徽爱迪香料股份有限公司 | Menthol production stills |
| CN206081696U (en) * | 2016-09-27 | 2017-04-12 | 江苏华创检测技术服务有限公司 | Antifoaming foam rotary evaporato |
-
2020
- 2020-09-08 CN CN202010934369.5A patent/CN111925871B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201825929U (en) * | 2010-09-14 | 2011-05-11 | 南通薄荷厂有限公司 | Mentha arvensis oil distillation device |
| CN205109076U (en) * | 2015-11-25 | 2016-03-30 | 安徽爱迪香料股份有限公司 | Menthol production stills |
| CN206081696U (en) * | 2016-09-27 | 2017-04-12 | 江苏华创检测技术服务有限公司 | Antifoaming foam rotary evaporato |
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| Publication number | Publication date |
|---|---|
| CN111925871A (en) | 2020-11-13 |
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