CN111875461A - Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon - Google Patents

Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon Download PDF

Info

Publication number
CN111875461A
CN111875461A CN201811256871.4A CN201811256871A CN111875461A CN 111875461 A CN111875461 A CN 111875461A CN 201811256871 A CN201811256871 A CN 201811256871A CN 111875461 A CN111875461 A CN 111875461A
Authority
CN
China
Prior art keywords
curing agent
binder
mass
mixed powder
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811256871.4A
Other languages
Chinese (zh)
Inventor
王浩静
马俊
黄阳飞
黄微波
樊黎君
李尚尉
张博寅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xi'an Hangke Plasma Technology Co ltd
Original Assignee
Xi'an Hangke Plasma Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xi'an Hangke Plasma Technology Co ltd filed Critical Xi'an Hangke Plasma Technology Co ltd
Priority to CN201811256871.4A priority Critical patent/CN111875461A/en
Publication of CN111875461A publication Critical patent/CN111875461A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B43/00—Compositions characterised by explosive or thermic constituents not provided for in groups C06B25/00 - C06B41/00
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
    • C06B21/0008—Compounding the ingredient
    • C06B21/0025—Compounding the ingredient the ingredient being a polymer bonded explosive or thermic component
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B33/00—Compositions containing particulate metal, alloy, boron, silicon, selenium or tellurium with at least one oxygen supplying material which is either a metal oxide or a salt, organic or inorganic, capable of yielding a metal oxide
    • C06B33/04—Compositions containing particulate metal, alloy, boron, silicon, selenium or tellurium with at least one oxygen supplying material which is either a metal oxide or a salt, organic or inorganic, capable of yielding a metal oxide the material being an inorganic nitrogen-oxygen salt
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B33/00—Compositions containing particulate metal, alloy, boron, silicon, selenium or tellurium with at least one oxygen supplying material which is either a metal oxide or a salt, organic or inorganic, capable of yielding a metal oxide
    • C06B33/12—Compositions containing particulate metal, alloy, boron, silicon, selenium or tellurium with at least one oxygen supplying material which is either a metal oxide or a salt, organic or inorganic, capable of yielding a metal oxide the material being two or more oxygen-yielding compounds
    • C06B33/14—Compositions containing particulate metal, alloy, boron, silicon, selenium or tellurium with at least one oxygen supplying material which is either a metal oxide or a salt, organic or inorganic, capable of yielding a metal oxide the material being two or more oxygen-yielding compounds at least one being an inorganic nitrogen-oxygen salt

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention relates to a medicament formula and a preparation method of an ultrahigh-energy broadband electromagnetic pulse weapon, wherein the medicament comprises metal powder, alkali metal salt, a binder and a curing agent, wherein the metal powder accounts for 5-60% of the total mass of the mixed powder of the metal powder and the alkali metal salt; the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder. The raw materials of the medicament are wide in source; the process is simple to operate, and is safe and reliable.

Description

Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon
Technical Field
The invention belongs to the field of energetic materials, relates to an energetic plasma working medium formula, and aims to provide a medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon.
Background
The electromagnetic pulse weapon is a weapon system which can intensively project electromagnetic spectrum energy, and is characterized by that the energy is concentrated, so that the energy density projected to target object is very high, and the target object can be damaged by direct irradiation and coupling invasion heat energy accumulation effect, and can cause serious interference of microwave in same frequency band. Electromagnetic pulses are transient electromagnetic phenomena that propagate in the form of spatial radiation, and through which electromagnetic waves can damage electronic, information, electrical, photovoltaic, microwave, etc. devices, burning of semiconductor insulating layers or integrated circuits of electronic devices, and even equipment failure or permanent damage can occur. The main body is as follows: the electric field in the communication system is redistributed by the instant electric field established by the strong electromagnetic pulse to form surge voltage, so that the communication signal system is damaged; the electric field in the communication system is instantly redistributed to form inrush current, which damages the communication signal system; the strong electromagnetic field penetrates through an internal circuit of the communication system to generate large or larger induced current, so that differential mode interference of communication signals is caused, and the system is damaged; the microelectronic device is very easy to generate resonance heating damage due to abundant frequency spectrum in strong electromagnetic pulse.
The electromagnetic pulse weapon mainly comprises a nuclear electromagnetic pulse bomb and an uncore electromagnetic pulse bomb. The nuclear electromagnetic pulse bomb is a novel nuclear weapon which is mainly characterized by enhancing the electromagnetic pulse effect, and is an non-nuclear electromagnetic pulse bomb which is an electromagnetic pulse weapon generating high-power microwaves by utilizing a method of compressing magnetic flux by explosion at present; due to the use limitation of the core, the non-nuclear electromagnetic pulse bomb is more excellent, the commonly used non-nuclear electromagnetic pulse bomb mainly comprises three modes of explosive chemical explosion type, electric field acceleration plasma type under study and direct generation of plasma type, and the electromagnetic pulse generated by the explosive chemical explosion type electromagnetic pulse bomb has low conversion efficiency, relatively small electromagnetic field peak intensity, limited transmission distance and weaker destruction capability, so the use of the electromagnetic pulse is limited; the electric field accelerating plasma type electromagnetic pulse bomb under study supplies power to the virtual cathode oscillator through the magnetic flux compression generator or the magnetohydrodynamic generator to generate microwave with gigawatt level, and then the microwave is emitted outwards in a directional way through the antenna, which belongs to a typical narrow band, the hitting target is relatively fixed, and the problems of overlarge power supply, complex system structure and the like exist; therefore, the research on the direct generation of the plasma type electromagnetic pulse weapon has important significance.
The plasma generation mainly comprises methods of thermal ionization, gas discharge, laser irradiation, high-power microwave excitation and the like. Which is the simplest and most suitable method for the use of weaponry to generate a plasma. The ionization energy of alkali metal elements in nature is the lowest, but the alkali metal elements can not be easily used for actual operation due to the active chemical characteristics, so the alkali metal salts can be selected as substitutes. The alkali metal salt is added to design a new formula, so that high-density plasma can be directly generated, and the plasma generates a high electromagnetic field, thereby generating strong electromagnetic pulse and damaging a target object. Therefore, the research on the working medium for directly generating the plasma type electromagnetic pulse weapon provides energetic plasma working medium guarantee for developing high-energy density, wide-frequency band and large-area damage electromagnetic pulse weapons.
Disclosure of Invention
The invention aims to provide a medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon. In order to meet the required requirements, the invention adopts the following technical scheme:
a medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon is characterized in that: comprises metal powder, alkali metal salt, a binder and a curing agent,
wherein the metal powder accounts for (5-60)% of the total mass of the metal powder and alkali metal salt mixed powder;
the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder.
Further, the adhesive is bisphenol A type epoxy resin, and the curing agent is any one of triethylene tetramine and ethylenediamine;
or the binder is unsaturated polyester resin, and the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, and the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI).
The invention provides a medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon, which comprises metal powder, alkali metal salt, a binder, a curing agent and an accelerator,
wherein the metal powder accounts for (5-60)% of the total mass of the metal powder and alkali metal salt mixed powder;
the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder, and the mass of the accelerator is (10-50)% of the mass of the curing agent.
Further, the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, and the accelerator is any one of triethylamine, dimethylol butyric acid (DMBA) and tris- (dimethylaminomethyl) phenol (DMP-30);
or the adhesive is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, and the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12);
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), and the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12).
Further, the alkali metal salt is cesium nitrate (CsNO)3) Cesium carbonate (Cs)2CO3) Cesium chloride (CsCl), cesium sulfate (Cs)2SO4) Potassium nitrate (KNO)3) Potassium chloride (KCl) and potassium sulfate (K)2SO4) Potassium carbonate (K)2CO3) Sodium nitrate (NaNO)3) Sodium carbonate (Na)2CO3) Sodium chloride (NaCl), sulfurSodium acid (Na)2SO4) Any one or a mixture of several of them.
The invention relates to a preparation method of a medicament of an ultrahigh-energy broadband electromagnetic pulse weapon, which comprises the following steps:
1) mixing metal powder and alkali metal salt to obtain mixed powder, wherein the metal powder accounts for 5-60% of the total mass of the mixed powder;
2) weighing the mixed powder;
3) preparing a binder system:
weighing a binder, a curing agent and a solvent, and mixing and dissolving to obtain a binder system; the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder; the amount of the solvent is (5-20) mL/50g of the mixed powder;
4) and (3) pouring the binder system prepared in the step 3) into the mixed powder weighed in the step 2), and stirring until the solvent is completely volatilized to obtain the medicament.
Further, the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, and the solvent is any one of acetone, xylene and n-butyl alcohol;
or the binder is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, and the solvent is any one of ethyl acetate, styrene and methyl methacrylate;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), and the solvent is any one of tetrahydrofuran and dichloromethane.
The invention provides a preparation method of a medicament of an ultrahigh-energy broadband electromagnetic pulse weapon, which is characterized by comprising the following steps:
1) mixing metal powder and alkali metal salt to obtain mixed powder, wherein the metal powder accounts for 5-60% of the total mass of the mixed powder;
2) weighing the mixed powder;
3) preparing a binder system:
weighing the binder, the curing agent, the accelerator and the solvent, and mixing and dissolving to obtain a binder system; the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder; the amount of the solvent is (5-20) mL/50g of the mixed powder; the mass of the accelerator is 10-50% of that of the curing agent.
4) And (3) pouring the binder system prepared in the step 3) into the mixed powder weighed in the step 2), and stirring until the solvent is completely volatilized to obtain the medicament.
Further, the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, the accelerant is any one of triethylamine, dimethylol butyric acid (DMBA) and tris- (dimethylaminomethyl) phenol (DMP-30), and the solvent is any one of acetone, xylene and n-butyl alcohol;
or the binder is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12), and the solvent is any one of ethyl acetate, styrene and methyl methacrylate;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12), and the solvent is any one of tetrahydrofuran and dichloromethane.
Further, the alkali metal salt is cesium nitrate (CsNO)3) Cesium carbonate (Cs)2CO3) Cesium chloride (CsCl), cesium sulfate (Cs)2SO4) Potassium nitrate (KNO)3) Potassium chloride (KCl) and potassium sulfate (K)2SO4) Potassium carbonate and potassium carbonate(K2CO3) Sodium nitrate (NaNO)3) Sodium carbonate (Na)2CO3) Sodium chloride (NaCl), sodium sulfate (Na)2SO4) Any one or a mixture of several of them.
The invention has the technical effects that:
the invention relates to a medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon, which has wide raw material sources; the process comprises the following steps: the operation is simple, safe and reliable; the peak field intensity measured by tests on an ultrahigh-energy broadband electromagnetic pulse bomb is (20-1000) KV/m, and the use requirement of an electromagnetic pulse weapon is met. The concrete beneficial effects are embodied in the following aspects: after the mixture is pressed into a grain and ignited, the plasma density measured is more than or equal to 1013/cm3(ii) a The adhesive commonly used in the explosive industry is introduced into the formula, so that the sufficiency of the reaction is improved, and the plasticity of the explosive is enhanced.
Drawings
FIG. 1 Electron Density scattergram of example 1.
Detailed description of the invention
The invention is further illustrated by the following 4 specific examples, which are not intended to be limiting. The example used for mixing is a brass industry standard screen (100 mesh).
Example 1
Weighing 5g of aluminum powder and 90g of cesium chloride, and then uniformly mixing; weighing 50g of mixed powder and pouring the mixed powder into a beaker for later use; weighing 0.5g of epoxy resin, adding 0.1g of ethylenediamine, adding 0.01g of triethylamine, weighing 5mL of acetone, pouring into a beaker, and uniformly stirring; putting the wood chopsticks into a beaker and stirring, pouring the uniformly stirred binder solvent into the beaker filled with the mixed powder while stirring, stopping stirring after the solvent is volatilized along with the stirring, pressing the mixture into a powder column through a special tool, and measuring the density of the generated plasma, wherein the density of the generated plasma is shown in the attached figure 1.
Example 2
Weighing 60g of titanium powder and 40g of potassium nitrate, and then uniformly mixing; weighing 50g of mixed powder and pouring the mixed powder into a beaker for later use; weighing 15g of unsaturated polyester resin, adding 0.225g of methyl ethyl ketone peroxide, adding 0.075g of cobalt naphthenate, weighing 10mL of ethyl acetate, pouring into a beaker, and uniformly stirring; and (3) putting the wood chopsticks into a beaker for stirring, pouring the uniformly stirred binder solution into the beaker filled with the mixed powder while stirring, stopping stirring after the solvent is volatilized along with the stirring, pressing the mixture into a medicine column through a special tool, and measuring the field intensity to be 54328.4V/m.
Example 3
Weighing 15g of aluminum powder, 15g of magnesium powder and 70g of cesium nitrate, and then uniformly mixing; weighing 50g of mixed powder and pouring the mixed powder into a beaker for later use; 2.5g of GAP is weighed in a beaker, then 0.25g of IPDI is added, 8mL of tetrahydrofuran is weighed and poured into the beaker, and the mixture is stirred uniformly; and (3) putting the wood chopsticks into a beaker for stirring, pouring the uniformly stirred binder solution into the beaker filled with the mixed powder while stirring, stopping stirring after the solvent is volatilized along with the stirring, pressing the mixture into a medicine column through a special tool, and measuring the field intensity to be 76743.8V/m.
Example 4
Weighing 40g of aluminum-based alloy powder and 60g of alkali metal salt (5 g each of cesium nitrate, cesium carbonate, cesium chloride, cesium sulfate, potassium nitrate, potassium chloride, potassium sulfate, potassium carbonate, sodium nitrate, sodium carbonate, sodium chloride and sodium sulfate), and then uniformly mixing them; weighing 50g of mixed powder and pouring the mixed powder into a beaker for later use; weighing 2.5g of HTPB in a beaker, adding 0.5g of TDI, then adding 0.15g of TPB, weighing 20mL of tetrahydrofuran, pouring into the beaker, and uniformly stirring; and (3) putting the wood chopsticks into a beaker for stirring, pouring the uniformly stirred binder solution into the beaker filled with the mixed powder while stirring, stopping stirring after the solvent is volatilized along with the stirring, pressing the mixture into a medicine column through a special tool, and measuring the field intensity to be 58967.3V/m.
Example 5
A method for preparing a medicament of an ultrahigh-energy broadband electromagnetic pulse weapon adopts a process of adding a binder for stirring to prepare a compound medicament formula capable of generating high-energy density plasma. The alkali metal salt is cesium nitrate (CsNO)3) Cesium carbonate (Cs)2CO3) Cesium chloride (CsCl), cesium sulfate (Cs)2SO4) Potassium nitrate (KNO)3) Chlorination ofPotassium (KCl), potassium sulfate (K)2SO4) Potassium carbonate (K)2CO3) Sodium nitrate (NaNO)3) Sodium carbonate (Na)2CO3) Sodium chloride (NaCl), sodium sulfate (Na)2SO4) Any one or a mixture of several of them.
2) Weighing the binder, and adding a solvent for dissolving; the binder can be any one of bisphenol A epoxy resin, unsaturated polyester resin, polyaziridine glycidyl ether (GAP) and hydroxyl-terminated polybutadiene (HTPB).
When the adhesive is bisphenol A epoxy resin, a curing agent is required to be added for curing and crosslinking, and the curing agent can be any one of triethylene tetramine and ethylenediamine; in order to shorten the reaction time, a promoter can be selectively added, and the promoter can be any one of triethylamine, dimethylolbutyric acid (DMBA) and tris- (dimethylaminomethyl) phenol (DMP-30); the solvent can be any one of acetone, xylene and n-butanol.
When the binder is unsaturated polyester resin, a curing agent is required to be added for curing and crosslinking, and the curing agent can be any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide; in order to shorten the reaction time, an accelerant can be selectively added, and the accelerant can be any one of cobalt naphthenate, dodecyl mercaptan and dimethylaniline; the solvent is any one of ethyl acetate, styrene and methyl methacrylate.
When the binder is selected from polyaziridine glycidyl ether, a curing agent is added to carry out curing crosslinking, and the curing agent can be any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI); in order to shorten the reaction time, an accelerator can be optionally added, and the accelerator can be any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12); the solvent can be any one of tetrahydrofuran and dichloromethane.
When the adhesive is hydroxyl-terminated polybutadiene, a curing agent is added for curing and crosslinking, wherein the curing agent can be any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI); in order to shorten the reaction time, an accelerator can be optionally added, and the accelerator can be any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12); the solvent can be any one of tetrahydrofuran and dichloromethane.
All the solvents are analytical pure reagents; the addition mass of the binder is (1-30)% of the total mass of the mixed powder. The mass of the curing agent is (1-20)% of the mass of the binder, and the mass of the accelerator is (10-50)% of the mass of the curing agent.
3) And (3) after the binder solution is completely dissolved, adding the binder solution into the weighed mixed powder, stirring until the solvent is completely volatilized, and thus obtaining the medicament.

Claims (10)

1. A medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon is characterized in that: comprises metal powder, alkali metal salt, a binder and a curing agent,
wherein the metal powder accounts for (5-60)% of the total mass of the metal powder and alkali metal salt mixed powder;
the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder.
2. The formulation of the ultra high energy broadband electromagnetic pulse weapon according to claim 1, wherein:
the adhesive is bisphenol A type epoxy resin, and the curing agent is any one of triethylene tetramine and ethylenediamine;
or the binder is unsaturated polyester resin, and the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, and the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI).
3. A medicament formula of an ultrahigh-energy broadband electromagnetic pulse weapon is characterized in that: comprises metal powder, alkali metal salt, a binder, a curing agent and an accelerator,
wherein the metal powder accounts for (5-60)% of the total mass of the metal powder and alkali metal salt mixed powder;
the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder, and the mass of the accelerator is (10-50)% of the mass of the curing agent.
4. The formulation of the ultra high energy broadband electromagnetic pulse weapon of claim 3 wherein:
the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, and the accelerant is any one of triethylamine, dimethylol butyric acid (DMBA) and tris- (dimethylamino methyl) phenol (DMP-30);
or the adhesive is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, and the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12);
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), and the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12).
5. The formulation of the ultra high energy broadband electromagnetic pulse weapon according to claim 1 or 2 or 3 or 4 wherein: the alkali metal salt is cesium nitrate (CsNO)3) Cesium carbonate (Cs)2CO3) Cesium chloride (CsCl), cesium sulfate (Cs)2SO4) Potassium nitrate (KNO)3) Potassium chloride (KCl), potassium sulfate(K2SO4) Potassium carbonate (K)2CO3) Sodium nitrate (NaNO)3) Sodium carbonate (Na)2CO3) Sodium chloride (NaCl), sodium sulfate (Na)2SO4) Any one or a mixture of several of them.
6. A preparation method of a medicament of an ultrahigh-energy broadband electromagnetic pulse weapon is characterized by comprising the following steps:
1) mixing metal powder and alkali metal salt to obtain mixed powder, wherein the metal powder accounts for 5-60% of the total mass of the mixed powder;
2) weighing the mixed powder;
3) preparing a binder system:
weighing a binder, a curing agent and a solvent, and mixing and dissolving to obtain a binder system; the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder; the amount of the solvent is (5-20) mL/50g of the mixed powder;
4) and (3) pouring the binder system prepared in the step 3) into the mixed powder weighed in the step 2), and stirring until the solvent is completely volatilized to obtain the medicament.
7. The method of claim 6 for preparing a pharmaceutical formulation for an ultra high energy broadband electromagnetic pulse weapon, wherein:
the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, and the solvent is any one of acetone, xylene and n-butyl alcohol;
or the binder is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, and the solvent is any one of ethyl acetate, styrene and methyl methacrylate;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), and the solvent is any one of tetrahydrofuran and dichloromethane.
8. A preparation method of a medicament of an ultrahigh-energy broadband electromagnetic pulse weapon is characterized by comprising the following steps:
1) mixing metal powder and alkali metal salt to obtain mixed powder, wherein the metal powder accounts for 5-60% of the total mass of the mixed powder;
2) weighing the mixed powder;
3) preparing a binder system:
weighing the binder, the curing agent, the accelerator and the solvent, and mixing and dissolving to obtain a binder system; the mass of the binder is (1-30)% of the total mass of the mixed powder; the mass of the curing agent is (1-20)% of the mass of the binder; the amount of the solvent is (5-20) mL/50g of the mixed powder; the mass of the accelerator is 10-50% of that of the curing agent.
4) And (3) pouring the binder system prepared in the step 3) into the mixed powder weighed in the step 2), and stirring until the solvent is completely volatilized to obtain the medicament.
9. The method of claim 8 for preparing a pharmaceutical formulation for an ultra high energy broadband electromagnetic pulse weapon, wherein:
the adhesive is bisphenol A type epoxy resin, the curing agent is any one of triethylene tetramine and ethylenediamine, the accelerant is any one of triethylamine, dimethylol butyric acid (DMBA) and tris- (dimethylaminomethyl) phenol (DMP-30), and the solvent is any one of acetone, xylene and n-butyl alcohol;
or the binder is unsaturated polyester resin, the curing agent is any one of methyl ethyl ketone peroxide, dibenzoyl peroxide and cyclohexanone peroxide, the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12), and the solvent is any one of ethyl acetate, styrene and methyl methacrylate;
or the adhesive is polyaziridine glycidyl ether or hydroxyl-terminated polybutadiene, the curing agent is any one of Toluene Diisocyanate (TDI), diphenylmethane diisocyanate (MDI), Hexamethylene Diisocyanate (HDI) and isophorone diisocyanate (IPDI), the accelerator is any one of triphenyl bismuth (TPB) and dibutyltin dilaurate (T12), and the solvent is any one of tetrahydrofuran and dichloromethane.
10. The method for preparing a pharmaceutical formulation for an ultra high energy broadband electromagnetic pulse weapon according to claim 6 or 7 or 8 or 9 wherein: the alkali metal salt is cesium nitrate (CsNO)3) Cesium carbonate (Cs)2CO3) Cesium chloride (CsCl), cesium sulfate (Cs)2SO4) Potassium nitrate (KNO)3) Potassium chloride (KCl) and potassium sulfate (K)2SO4) Potassium carbonate (K)2CO3) Sodium nitrate (NaNO)3) Sodium carbonate (Na)2CO3) Sodium chloride (NaCl), sodium sulfate (Na)2SO4) Any one or a mixture of several of them.
CN201811256871.4A 2018-10-13 2018-10-13 Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon Pending CN111875461A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811256871.4A CN111875461A (en) 2018-10-13 2018-10-13 Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811256871.4A CN111875461A (en) 2018-10-13 2018-10-13 Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon

Publications (1)

Publication Number Publication Date
CN111875461A true CN111875461A (en) 2020-11-03

Family

ID=73153790

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811256871.4A Pending CN111875461A (en) 2018-10-13 2018-10-13 Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon

Country Status (1)

Country Link
CN (1) CN111875461A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107459918A (en) * 2017-07-18 2017-12-12 阜南县民安人防工程设备有限公司 Coated material for tempest door
CN108586171A (en) * 2018-07-18 2018-09-28 中国科学院西安光学精密机械研究所 Nitrate refining treatment method
CN110343027A (en) * 2019-07-16 2019-10-18 中国工程物理研究院化工材料研究所 It is a kind of based on containing can metal organic frame without orange pyrotechnic compound of chlorine and preparation method thereof
CN110358103A (en) * 2019-07-16 2019-10-22 中国工程物理研究院化工材料研究所 Insensitive metal organic frame containing energy of one kind and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107459918A (en) * 2017-07-18 2017-12-12 阜南县民安人防工程设备有限公司 Coated material for tempest door
CN108586171A (en) * 2018-07-18 2018-09-28 中国科学院西安光学精密机械研究所 Nitrate refining treatment method
CN110343027A (en) * 2019-07-16 2019-10-18 中国工程物理研究院化工材料研究所 It is a kind of based on containing can metal organic frame without orange pyrotechnic compound of chlorine and preparation method thereof
CN110358103A (en) * 2019-07-16 2019-10-22 中国工程物理研究院化工材料研究所 Insensitive metal organic frame containing energy of one kind and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DUDNIKOV V: "Carbon film in RF surface plasma source with cesiation", 《AIP CONFERENCE PROCEEDINGS. AIP PUBLISHING LLC》 *
李俊: "高温高压下CsNO3电离产生等离子体规律试验研究", 《装甲兵工程学院学报》 *
沈瑞琪: "激光烧蚀硼-硝酸钾的等离子体特性", 《中国激光》 *

Similar Documents

Publication Publication Date Title
Kemp et al. Hot-electron energy coupling in ultraintense laser-matter interaction
Raman et al. Electromagnetic particle injector for fast time response disruption mitigation in tokamaks
US5835545A (en) Compact intense radiation system
CN111875461A (en) Medicament formula and preparation method of ultrahigh-energy broadband electromagnetic pulse weapon
Taylor Third-generation nuclear weapons
Rachen et al. Cosmic rays and neutrinos from gamma-ray bursts
Shmatov Some problems related to heating the compressed thermonuclear fuel through the cone
Itoh et al. X-ray emission from SN 1987A
Venable Phermex
WO2003044806A1 (en) Methods and systems for generating high-energy photons or quantum energy
US20030058980A1 (en) Method and apparatus for the transmutation of nuclear waste with tandem production of tritium
Kikuchi Ball lightning
Cui et al. Nuclear diagnosis of the fuel areal density for direct-drive deuterium fuel implosion at the Shenguang-II Upgrade laser facility
Lewis et al. Antiproton-boosted microfission
Ganley et al. Enhancement of CO2 laser power and efficiency by neutron irradiation
Hamm Multipurpose neutron generators based on the radio frequency quadrupole linear accelerator
Ives et al. The new RF sources for accelerators
Ding et al. Oscillation-induced gamma-ray emission from dead pulsars: a model for the delayed GeV emission in gamma-ray bursts
CN111875460A (en) Pyrotechnic agent containing potassium nitrate salt and preparation method thereof
Galper et al. Phases of Charged Particles Acceleration during Powerful Solar Gamma-Flares Detected by the Gamma-1
Sinars Radiation Effects Pulsed Power and Future HED Capabilities.
Tang et al. Review of dense plasma focus technology for intense and directional neutron sources
Wei et al. High-power accelerators in China: status and outlook
Chopra et al. E–BOMB
Bluhm et al. Light ion beam driven inertial confinement fusion: Requirements and achievements

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20201103

RJ01 Rejection of invention patent application after publication