CN111790281A - Ammonia water and alkali adding mixer - Google Patents

Ammonia water and alkali adding mixer Download PDF

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Publication number
CN111790281A
CN111790281A CN202010656739.3A CN202010656739A CN111790281A CN 111790281 A CN111790281 A CN 111790281A CN 202010656739 A CN202010656739 A CN 202010656739A CN 111790281 A CN111790281 A CN 111790281A
Authority
CN
China
Prior art keywords
inlet section
ammonia water
section
water inlet
alkali liquor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010656739.3A
Other languages
Chinese (zh)
Inventor
于振东
段有龙
曲斌
于涛
曹培城
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Acre Coking and Refractory Engineering Consulting Corp MCC
Original Assignee
Acre Coking and Refractory Engineering Consulting Corp MCC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Acre Coking and Refractory Engineering Consulting Corp MCC filed Critical Acre Coking and Refractory Engineering Consulting Corp MCC
Priority to CN202010656739.3A priority Critical patent/CN111790281A/en
Publication of CN111790281A publication Critical patent/CN111790281A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/45Mixing liquids with liquids; Emulsifying using flow mixing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/45Mixing liquids with liquids; Emulsifying using flow mixing
    • B01F23/451Mixing liquids with liquids; Emulsifying using flow mixing by injecting one liquid into another
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/45Mixing liquids with liquids; Emulsifying using flow mixing
    • B01F23/453Mixing liquids with liquids; Emulsifying using flow mixing by moving the liquids in countercurrent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/314Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced at the circumference of the conduit
    • B01F25/3141Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced at the circumference of the conduit with additional mixing means other than injector mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/314Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced at the circumference of the conduit
    • B01F25/3143Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced at the circumference of the conduit characterised by the specific design of the injector
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/42Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4314Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor with helical baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/42Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/433Mixing tubes wherein the shape of the tube influences the mixing, e.g. mixing tubes with varying cross-section or provided with inwardly extending profiles
    • B01F25/4334Mixers with a converging cross-section
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application

Abstract

The invention relates to the technical field of coking mixers, in particular to an ammonia water and alkali adding mixer. Comprises an ammonia water inlet section, an alkali liquor inlet section and a mixing section; the ammonia water inlet section is connected with the alkali liquor inlet section, and the alkali liquor inlet section is connected with the mixing section; the ammonia water inlet section comprises an ammonia water inlet section pipe body and a seal head connected with the ammonia water inlet section pipe body, and spiral jet-shaped openings are formed in the connection part of the tail end of the ammonia water inlet section pipe body and the seal head; the alkali liquor inlet section comprises an alkali liquor inlet section pipe body and a spiral sheet, and the spiral sheet is fixedly connected to the outer pipe wall of the ammonia water inlet section pipe body; the spiral jet-shaped opening is opposite to the spiral direction of the spiral sheet. And residual ammonia water is sprayed through the spiral spraying type opening of the mixer, the flow rate is accelerated, and the residual ammonia water and NaOH solution entering along the spiral piece are sprayed reversely to decompose and fix ammonium salt and be uniformly mixed. The mixing section is a conical section, the mixing space is a conical section, the space is small, the flow speed is high, and the blockage is reduced. The ammonia water inlet section and the alkali liquor inlet section are connected through flange bolts, so that the ammonia water inlet section is convenient to disassemble and easy to overhaul.

Description

Ammonia water and alkali adding mixer
Technical Field
The invention relates to the technical field of coking mixers, in particular to an ammonia water and alkali adding mixer.
Background
The national requirements on the indexes of the coking wastewater are increasingly strict, and the residual ammonia water accounts for about 60 percent of the total amount of the wastewater of coking enterprises. The residual ammonia water is industrial wastewater which has complex components, high toxicity and difficult degradation, and mainly comprises free ammonia and fixed ammonium. The ammonia still system is an indispensable link for treating the residual ammonia water, the long-term stable operation of the ammonia still and the qualification of the indexes of the wastewater at the bottom of the ammonia still are inseparable with the addition amount and the uniform mixing degree of the liquid caustic soda, the non-uniform mixing of the liquid caustic soda and the residual ammonia water can directly influence the operation efficiency of the ammonia still, the ammonia nitrogen content of the ammonia still wastewater exceeds the standard, and the impact is caused to a coking wastewater biochemical treatment system.
At present, in the coking industry, residual ammonia water is generally used for ammonia distillation, and NaOH solution is added into a residual ammonia water inlet through a mixer to decompose and fix ammonium salt. The existing mixer has the defect of uneven mixing, so that excessive liquid caustic soda enters the ammonia still to react with calcium and magnesium ions in ammonia water to generate precipitates, block tower plates and influence the long-term stable operation of the ammonia still.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides an ammonia water and alkali adding mixer. So that NaOH and the residual ammonia water are uniformly mixed, the tower plate is prevented from being blocked, and the stable operation of the ammonia still is ensured.
In order to achieve the purpose, the invention adopts the following technical scheme:
an ammonia water alkali-adding mixer comprises an ammonia water inlet section, an alkali liquor inlet section and a mixing section; the ammonia water inlet section is connected with the alkali liquor inlet section, and the alkali liquor inlet section is connected with the mixing section; the ammonia water inlet section comprises an ammonia water inlet section pipe body and a seal head connected with the ammonia water inlet section pipe body, and spiral jet-shaped openings are formed in the connection part of the tail end of the ammonia water inlet section pipe body and the seal head; the alkali liquor inlet section comprises an alkali liquor inlet section pipe body and a spiral sheet, and the spiral sheet is fixedly connected to the outer pipe wall of the ammonia water inlet section pipe body; the spiral jet-shaped opening is opposite to the spiral direction of the spiral sheet.
The ammonia water inlet section comprises an ammonia water inlet section flange, an ammonia water inlet section flange cover, an ammonia water inlet section pipe body and an end enclosure; ammonia water inlet section flange links to each other with ammonia water inlet section body one end, and the ammonia water inlet section body other end links to each other with the head, and ammonia water inlet section flange cover rigid coupling is on the outer pipe wall of ammonia water inlet section body.
The seal head is a spherical seal head or an elliptical seal head or a conical seal head.
The alkali liquor inlet section comprises an alkali liquor inlet section flange, an alkali liquor inlet section flange cover, an alkali liquor inlet section inlet pipe, an alkali liquor inlet section pipe body and a spiral sheet; the alkali lye inlet section flange links to each other with alkali lye inlet section inlet tube, and alkali lye inlet section inlet tube links to each other with the pipe wall of alkali lye inlet section body, and alkali lye inlet section flange cover rigid coupling is in the one end of alkali lye inlet section body, and the other end of alkali lye inlet section body links to each other with the mixing section.
And the ammonia water inlet section flange cover is connected with the alkali liquor inlet section flange cover through bolts.
The mixing section comprises a conical section, a straight section and a mixing section flange; the conical section is a conical pipe, the straight section is a straight pipe, one end of the conical section is connected with the alkali liquor inlet section pipe body, the other end of the conical section is connected with the straight section, and the straight section is connected with the mixing section flange.
The ammonia water inlet section pipe body and the alkali liquor inlet section pipe body are both made of seamless steel pipes.
Compared with the prior art, the invention has the beneficial effects that:
1) the spiral jet-shaped openings are formed in the connecting part of the tail end of the ammonia water inlet section pipe body and the end socket, the spiral sheet is fixedly connected to the outer pipe wall of the ammonia water inlet section pipe body, and the spiral direction of the spiral jet-shaped openings is opposite to that of the spiral sheet;
and residual ammonia water is sprayed through the spiral spraying type opening of the mixer, the flow rate is accelerated, and the residual ammonia water and NaOH solution entering along the spiral piece are sprayed reversely to decompose and fix ammonium salt and be uniformly mixed.
2) The mixing section is a conical section, the mixing space is a conical section, the space is small, the flow speed is high, and the blockage is reduced.
3) The ammonia water inlet section and the alkali liquor inlet section are connected through flange bolts, so that the ammonia water inlet section is convenient to disassemble and easy to overhaul.
Drawings
FIG. 1 is a schematic diagram of the present invention.
In the figure: 1-ammonia water inlet section flange 2-ammonia water inlet section flange cover 3-ammonia water inlet section pipe body 4-end enclosure 5-spiral sheet 6-alkali liquor inlet section flange 7-alkali liquor inlet section inlet pipe 8-alkali liquor inlet section pipe body 9-alkali liquor inlet section flange cover 10-conical section 11-straight section 12-mixing section flange
Detailed Description
The following further describes embodiments of the present invention with reference to the accompanying drawings:
as shown in figure 1, an ammonia-alkali mixer comprises an ammonia inlet section, an alkali liquor inlet section and a mixing section.
The aqueous ammonia inlet section includes aqueous ammonia inlet section flange 1, aqueous ammonia inlet section flange cover 2, aqueous ammonia inlet section body 3 and head 4. Ammonia water inlet section body 3 adopts seamless steel pipe preparation, and 1 welding of ammonia water inlet section flange is in the one end of ammonia water inlet section body 3, and 3 other ends of ammonia water inlet section body link to each other with head 4, and 2 welding of ammonia water inlet section flange lids are on the outer pipe wall of ammonia water inlet section body 3. The end socket 4 is a spherical end socket or an elliptical end socket or a conical end socket. The connection part of the tail end of the ammonia water inlet section pipe body 3 and the seal head 4 are both provided with spiral jet-shaped openings.
The alkali liquor inlet section comprises an alkali liquor inlet section flange 6, an alkali liquor inlet section flange cover 9, an alkali liquor inlet section inlet pipe 7, an alkali liquor inlet section pipe body 8 and a spiral sheet 5. Alkali lye inlet section inlet tube 7 all adopts seamless steel pipe preparation with alkali lye inlet section body 8, and alkali lye inlet section flange 6 links to each other with 7 one end of alkali lye inlet section inlet tube, and the 7 other end of alkali lye inlet section inlet tube links to each other with the pipe wall of alkali lye inlet section body 8 to communicate with it, 9 welding of alkali lye inlet section flange cover are in the one end of alkali lye inlet section body 8, and the other end of alkali lye inlet section body 8 links to each other with the mixing section.
The helical fin 5 is welded on the outer wall of the ammonia water inlet section pipe body 3, and the tail end of the ammonia water inlet section pipe body 3 is opposite to the spiral spraying-shaped hole of the seal head 4 and the spiral direction of the helical fin 5.
Ammonia water inlet section flange cover 2 passes through the bolt with alkali lye inlet section flange cover 9 and links to each other, and then is connected ammonia water inlet section and alkali lye inlet section, and it is convenient to dismantle, easily overhauls.
The mixing section comprises a conical section 10, a straight section 11 and a mixing section flange 12. The conical section 10 is a conical pipe, the straight section 11 is a straight pipe, one end of the conical section 10 is connected with the alkali liquor inlet section pipe body 8, the other end of the conical section is connected with the straight section 11, and the straight section 11 is connected with the mixing section flange 12.
The residual ammonia water is sprayed through the spiral spray-shaped opening of the mixer, the flow rate is accelerated, and the residual ammonia water and NaOH solution entering along the spiral piece 5 are sprayed reversely to decompose and fix ammonium salt, and the ammonium salt is uniformly mixed. The main part of the mixing section is a conical section 10, the mixing space is a conical section, the space is small, the flow speed is high, and the blockage is reduced. The ammonia water inlet section and the alkali liquor inlet section are connected through flange bolts, so that the ammonia water inlet section is convenient to disassemble and easy to overhaul.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (7)

1. The utility model provides an aqueous ammonia adds alkali blender which characterized in that: comprises an ammonia water inlet section, an alkali liquor inlet section and a mixing section; the ammonia water inlet section is connected with the alkali liquor inlet section, and the alkali liquor inlet section is connected with the mixing section; the ammonia water inlet section comprises an ammonia water inlet section pipe body and a seal head connected with the ammonia water inlet section pipe body, and spiral jet-shaped openings are formed in the connection part of the tail end of the ammonia water inlet section pipe body and the seal head; the alkali liquor inlet section comprises an alkali liquor inlet section pipe body and a spiral sheet, and the spiral sheet is fixedly connected to the outer pipe wall of the ammonia water inlet section pipe body; the spiral jet-shaped opening is opposite to the spiral direction of the spiral sheet.
2. The mixer of claim 1, wherein: the ammonia water inlet section comprises an ammonia water inlet section flange, an ammonia water inlet section flange cover, an ammonia water inlet section pipe body and an end enclosure; ammonia water inlet section flange links to each other with ammonia water inlet section body one end, and the ammonia water inlet section body other end links to each other with the head, and ammonia water inlet section flange cover rigid coupling is on the outer pipe wall of ammonia water inlet section body.
3. The mixer of claim 1, wherein: the seal head is a spherical seal head or an elliptical seal head or a conical seal head.
4. The mixer of claim 1, wherein: the alkali liquor inlet section comprises an alkali liquor inlet section flange, an alkali liquor inlet section flange cover, an alkali liquor inlet section inlet pipe, an alkali liquor inlet section pipe body and a spiral sheet; the alkali lye inlet section flange links to each other with alkali lye inlet section inlet tube, and alkali lye inlet section inlet tube links to each other with the pipe wall of alkali lye inlet section body, and alkali lye inlet section flange cover rigid coupling is in the one end of alkali lye inlet section body, and the other end of alkali lye inlet section body links to each other with the mixing section.
5. An aqueous ammonia plus base mixer as claimed in claim 2 or 4, wherein: and the ammonia water inlet section flange cover is connected with the alkali liquor inlet section flange cover through bolts.
6. The mixer of claim 1, wherein: the mixing section comprises a conical section, a straight section and a mixing section flange; the conical section is a conical pipe, the straight section is a straight pipe, one end of the conical section is connected with the alkali liquor inlet section pipe body, the other end of the conical section is connected with the straight section, and the straight section is connected with the mixing section flange.
7. The mixer of claim 1, wherein: the ammonia water inlet section pipe body and the alkali liquor inlet section pipe body are both made of seamless steel pipes.
CN202010656739.3A 2020-07-09 2020-07-09 Ammonia water and alkali adding mixer Pending CN111790281A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010656739.3A CN111790281A (en) 2020-07-09 2020-07-09 Ammonia water and alkali adding mixer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010656739.3A CN111790281A (en) 2020-07-09 2020-07-09 Ammonia water and alkali adding mixer

Publications (1)

Publication Number Publication Date
CN111790281A true CN111790281A (en) 2020-10-20

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010656739.3A Pending CN111790281A (en) 2020-07-09 2020-07-09 Ammonia water and alkali adding mixer

Country Status (1)

Country Link
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112755826A (en) * 2021-01-05 2021-05-07 华东理工大学 Device and method for enhancing liquid-liquid emulsification

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112755826A (en) * 2021-01-05 2021-05-07 华东理工大学 Device and method for enhancing liquid-liquid emulsification

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