CN111751465B - Rapid quantitative screening method and application of liquorice antioxidant active ingredients - Google Patents
Rapid quantitative screening method and application of liquorice antioxidant active ingredients Download PDFInfo
- Publication number
- CN111751465B CN111751465B CN202010581039.2A CN202010581039A CN111751465B CN 111751465 B CN111751465 B CN 111751465B CN 202010581039 A CN202010581039 A CN 202010581039A CN 111751465 B CN111751465 B CN 111751465B
- Authority
- CN
- China
- Prior art keywords
- liquorice
- mobile phase
- antioxidant
- active ingredients
- dpph
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8675—Evaluation, i.e. decoding of the signal into analytical information
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8675—Evaluation, i.e. decoding of the signal into analytical information
- G01N30/8686—Fingerprinting, e.g. without prior knowledge of the sample components
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N2030/042—Standards
- G01N2030/047—Standards external
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Library & Information Science (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010581039.2A CN111751465B (en) | 2020-06-23 | 2020-06-23 | Rapid quantitative screening method and application of liquorice antioxidant active ingredients |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010581039.2A CN111751465B (en) | 2020-06-23 | 2020-06-23 | Rapid quantitative screening method and application of liquorice antioxidant active ingredients |
Publications (2)
Publication Number | Publication Date |
---|---|
CN111751465A CN111751465A (en) | 2020-10-09 |
CN111751465B true CN111751465B (en) | 2022-01-11 |
Family
ID=72676701
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010581039.2A Active CN111751465B (en) | 2020-06-23 | 2020-06-23 | Rapid quantitative screening method and application of liquorice antioxidant active ingredients |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111751465B (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112444592A (en) * | 2020-11-11 | 2021-03-05 | 谱尼测试集团北京检验认证科学研究院有限公司 | Method for rapidly screening active ingredients in liquorice by UPLC-Q-TOF-MS |
CN112666302B (en) * | 2021-01-04 | 2023-02-24 | 上海市农业科学院 | Method for identifying active flavone component group in barley seedling and rapidly detecting active flavone component group |
CN116087394B (en) * | 2023-02-16 | 2023-07-18 | 山东省中医药研究院 | Screening method and application of liquorice honey-fried synergistic active ingredient |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102879499A (en) * | 2012-10-11 | 2013-01-16 | 中国科学院西北高原生物研究所 | Method for detecting antioxidant constituents in nitraria fruit juice by using 1,1-diphenyl-2-picrylhydrazyl (DPPH)-high performance liquid chromatography (HPLC) method |
CN106483215B (en) * | 2016-09-28 | 2019-03-01 | 山东省分析测试中心 | Natural finds online and integrates antioxidant activity evaluation method in pawpaw medicinal material |
-
2020
- 2020-06-23 CN CN202010581039.2A patent/CN111751465B/en active Active
Also Published As
Publication number | Publication date |
---|---|
CN111751465A (en) | 2020-10-09 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN111751465B (en) | Rapid quantitative screening method and application of liquorice antioxidant active ingredients | |
CN105606734B (en) | A kind of quick high separation liquid chromatographic detection honeysuckle and the method for Honeysuckle flower medicinal material | |
Liu et al. | Rapid analysis of 27 components of Isodon serra by LC–ESI-MS–MS | |
Zhang et al. | Pharmacokinetics difference of multiple active constituents from decoction and maceration of Fuzi Xiexin Tang after oral administration in rat by UPLC–MS/MS | |
CN112444592A (en) | Method for rapidly screening active ingredients in liquorice by UPLC-Q-TOF-MS | |
CN114152705B (en) | HPLC fingerprint quality evaluation method for rhizoma atractylodis stem and leaf | |
He et al. | Differentiation of Cuscuta chinensis and Cuscuta australis by HPLC-DAD-MS analysis and HPLC-UV quantitation | |
CN114184704B (en) | Construction method and application of UPLC fingerprint of Xiaoyao pill | |
CN113759003A (en) | Licorice origin distinguishing method based on UPLC fingerprint spectrum and chemometrics method | |
Qi et al. | HPLC fingerprint and LC-TOF-MS analysis on extract from roots of Gentiana macrophylla | |
CN107561192A (en) | R accuses the method accused according to spring and S according to spring content in a kind of measure chromatogram of Radix Isatidis and its product | |
Li et al. | Identification of kukoamines as the novel markers for quality assessment of Lycii Cortex | |
CN112798724B (en) | Method for establishing chromatographic fingerprint of saponins component suitable for ginseng traditional Chinese medicine and medicinal material extract | |
CN111721880A (en) | Method for establishing fingerprint of sarcandra glabra by using double-column tandem HPLC-MS | |
CN110146611B (en) | Method for rapidly identifying chemical components in donkey-hide gelatin blood-enriching particles | |
CN109374788B (en) | Method for constructing and detecting UPLC characteristic spectrum of fructus cnidii medicinal material | |
CN112198253B (en) | Quality control method for ginger magnolia bark formula granules | |
CN113759011B (en) | Method for establishing characteristic spectrum of starwort root and preparation thereof | |
CN111551662B (en) | Quality detection method of angelica sinensis blood-enriching soup | |
CN109187820B (en) | Method for establishing UPLC fingerprint of compound formula chinaroot greenbrier granules | |
CN113640432A (en) | Quality evaluation method of loins strengthening and body building pills | |
CN110646528A (en) | Method for detecting multiple components in rhizoma drynariae based on HPLC/UPLC-QTOF-MS | |
CN110927292A (en) | Characteristic spectrum based on gleditsia sinensis extract and construction method and application thereof | |
CN108593787A (en) | A kind of assay method of cucurbitacin and B prime | |
Zhang et al. | Simultaneous Determination of Thirteen Iridoid Glycosides in Crude and Processed Fructus Corni from Different Areas by UPLC–MS/MS Method |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information |
Inventor after: Zhou Meng Inventor after: Zhou Qian Inventor after: Dai Yanpeng Inventor after: Jiang Haiqiang Inventor after: Chemosensitivity Inventor before: Zhou Qian Inventor before: Dai Yanpeng Inventor before: Zhou Meng Inventor before: Jiang Haiqiang Inventor before: Chemosensitivity |
|
CB03 | Change of inventor or designer information | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20211214 Address after: 247 Beiyuan street, Jinan City, Shandong Province Applicant after: THE SECOND HOSPITAL OF SHANDONG University Address before: 250014, swallow Road, Lixia District, Ji'nan, Shandong, 7, Shanxi Applicant before: SHANDONG ACADEMY OF CHINESE MEDICINE |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant |