CN111704819A - Washable gold powder adhesive and preparation method thereof - Google Patents
Washable gold powder adhesive and preparation method thereof Download PDFInfo
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- CN111704819A CN111704819A CN202010692346.8A CN202010692346A CN111704819A CN 111704819 A CN111704819 A CN 111704819A CN 202010692346 A CN202010692346 A CN 202010692346A CN 111704819 A CN111704819 A CN 111704819A
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- powder
- washable
- temperature
- gold powder
- polyvinyl alcohol
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D129/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Coating compositions based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Coating compositions based on derivatives of such polymers
- C09D129/02—Homopolymers or copolymers of unsaturated alcohols
- C09D129/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses washable gold powder glue which comprises, by weight, polyvinyl alcohol BP17, polyvinyl alcohol PVA24, carbomer resin, xanthan gum, glycerol, propylene glycol, a preservative, glitter powder and the balance of deionized water. The preparation method comprises the following steps: adding deionized water, polyvinyl alcohol BP17, polyvinyl alcohol PVA24 and carbomer resin into a reaction kettle at normal temperature, stirring for dissolving, heating to 85-90 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, and sealing the reaction kettle; adding xanthan gum, glycerol and propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, and cooling to 50-60 ℃; adding antiseptic while stirring, mixing, and continuously cooling to below 40 deg.C to obtain colloid; adding glitter powder and mixing completely to obtain washable gold powder glue. The obtained washable gold powder glue is not easy to be tinged, is environment-friendly and harmless, and is convenient to clean.
Description
Technical Field
The invention belongs to the technical field of children coatings, and particularly relates to washable gold powder glue and a preparation method thereof.
Background
The gold powder painting brush is more in types on the market at present, is generally used for paper, but does not yet coat on textile cloth, clothes and has two main reasons: 1. is not easy to dry and easy to be tinged; 2. certain damage to human body; 3. it is difficult to clean. According to market analysis and investigation, the current woven golden pastel is not common in the market, and in some DIY paintings, a part of the golden pastel is painted on clothes, but the common oil painting pigment or water color pigment is not easy to dry and can not be reused. Therefore, it is necessary to develop a washable gold powder paste.
Disclosure of Invention
The invention aims to provide washable gold powder glue and a preparation method thereof, so as to solve the problems.
The invention has a technical scheme that: the washable gold powder adhesive comprises, by weight, 173-8 parts of polyvinyl alcohol BP, 1-15 parts of polyvinyl alcohol PVA 2411-15 parts, 0.6-1.5 parts of carbomer resin, 0.6-1.5 parts of xanthan gum, 0.5-2 parts of glycerol, 1.5-2.5 parts of propylene glycol, 0.1-0.3 part of preservative, 0.2-0.5 part of glitter powder and the balance of deionized water.
Further, 0.6-1.5 parts of xanthan gum is replaced by 1.1-2.1 parts of wheat flour.
The other technical scheme of the invention is as follows:
the preparation method of the washable gold powder adhesive comprises the following steps:
(1) adding deionized water, polyvinyl alcohol BP17, polyvinyl alcohol PVA24 and carbomer resin into a reaction kettle at normal temperature, stirring for dissolving, heating to 85-90 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, and sealing the reaction kettle;
(2) adding xanthan gum, glycerol and propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, and cooling to 50-60 ℃;
(3) adding antiseptic while stirring, mixing, and continuously cooling to below 40 deg.C to obtain colloid;
(4) putting the colloid into an open stirrer, and adding glitter powder for complete mixing to obtain washable gold powder colloid.
Further, the rotation speed of the stirring in the steps (1) to (3) is 300 to 600 r/min.
Further, the xanthan gum is replaced by wheat grain powder in the step (2).
Further, the wheat grain powder comprises wheat grain powder and straw powder, the wheat grain powder is obtained by crushing wheat grains, the crushing rotation speed is 800-1000 r/min, the time is 10-20 min, the temperature is-5 ℃, the straw powder is obtained by crushing straws, the crushing rotation speed is 2000-2500 r/min, the time is 30-50 min, and the temperature is 5-10 ℃.
Further, the grain size of the wheat grain powder is 150-300 meshes, and the grain size of the straw powder is 500-800 meshes.
Further, the weight ratio of the wheat grain powder to the straw powder is 10-15: 2 to 3.
Further, in the step (3), the preservative is any one of benzoic acid, sodium benzoate, sorbic acid, potassium sorbate and calcium propionate.
Further, in the step (4), the rotation speed of the mixing is 1200-1500 r/min, the time is 20-30 min, and the temperature is 15-25 ℃.
The invention provides washable gold powder glue and a preparation method thereof, and the washable gold powder glue has the main advantages that: is not easy to be tinged, is environment-friendly and harmless, and is convenient to clean.
Detailed Description
In order to make the aforementioned objects, features and advantages of the present invention more comprehensible, embodiments accompanying the present invention are further described below. The invention is not limited to the embodiments listed but also comprises any other known variations within the scope of the invention as claimed.
First, reference herein to "one embodiment" or "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment is included in at least one implementation of the invention. The appearances of the phrase "in one embodiment" in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments.
Example 1
Checking whether related production equipment such as a reaction kettle and the like is normal or not at a normal temperature of 23 ℃, adding 82.5% of deionized water into the reaction kettle after the detection is qualified, adding 3% of polyvinyl alcohol BP17, adding 11% of polyvinyl alcohol PVA24, adding 0.6% of carbomer resin, stirring and dissolving at the normal temperature, heating to 85 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing the vacuum kettle, adding 0.6% of xanthan gum, 0.5% of glycerol and 1.5% of propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, cooling to 50 ℃, adding 0.1% of preservative while stirring, uniformly stirring, continuously cooling to below 40 ℃, detecting discharging, and then adding 0.2% of gold powder into an open type stirrer to completely mix to obtain the gold-washable powder glue.
Example 2
Checking whether related production equipment such as a reaction kettle and the like is normal or not at the normal temperature of 24 ℃, adding 76.4% of deionized water into the reaction kettle after the detection is qualified, adding 5% of polyvinyl alcohol BP17, adding 13% of polyvinyl alcohol PVA24, adding 1% of carbomer resin, stirring and dissolving at the normal temperature, then heating up to 88 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing the vacuum kettle, adding 1% of xanthan gum, 1% of glycerol and 2% of propylene glycol, uniformly stirring, heating up to 90 ℃, keeping the temperature for 2 hours, cooling to 55 ℃, adding 0.2% of preservative while stirring, uniformly stirring and mixing, continuously cooling to the temperature below 40 ℃, detecting and discharging, and then adding 0.4% of glitter powder into an open type stirrer to completely mix to obtain the washable gold powder adhesive.
Example 3
Checking whether related production equipment such as a reaction kettle and the like is normal or not at the normal temperature of 25 ℃, adding 68.7% of deionized water into the reaction kettle after the detection is qualified, adding 8% of polyvinyl alcohol BP17, adding 15% of polyvinyl alcohol PVA24, adding 1.5% of carbomer resin, stirring and dissolving at the normal temperature, heating to 90 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing the vacuum kettle, adding 1.5% of xanthan gum, 2% of glycerol and 2.5% of propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, cooling to 60 ℃, adding 0.3% of preservative while stirring, uniformly stirring, continuously cooling to below 40 ℃, detecting and discharging, and then adding 0.5% of glitter powder into an open stirrer for complete mixing to obtain the washable gold powder adhesive.
Example 4
Checking whether related production equipment such as a reaction kettle and the like is normal or not at a normal temperature of 23 ℃, adding 82% of deionized water into the reaction kettle after the detection is qualified, adding 3% of polyvinyl alcohol BP17, adding 11% of polyvinyl alcohol PVA24, adding 0.6% of carbomer resin, stirring and dissolving at the normal temperature, heating to 85 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing a vacuum kettle, adding 1.1% of wheat flour, 0.5% of glycerol and 1.5% of propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, cooling to 50 ℃, adding 0.1% of preservative while stirring, uniformly stirring, continuously cooling to below 40 ℃, detecting discharging, and then adding 0.2% of gold powder into an open type stirrer to completely mix to obtain the gold-washable powder adhesive. The wheat grain powder is prepared from the following components in percentage by weight of 10: 3, the wheat grain powder is obtained by crushing wheat grains at the rotating speed of 800r/min for 10min and at the temperature of-5 ℃, the straw powder is obtained by crushing straws at the rotating speed of 2000r/min for 30min and at the temperature of 5 ℃, the grain size of the wheat grain powder is 150 meshes, and the grain size of the straw powder is 500 meshes.
Example 5
Checking whether related production equipment such as a reaction kettle and the like is normal or not at the normal temperature of 24 ℃, adding deionized water into the reaction kettle after the detection is qualified, adding 6% of polyvinyl alcohol BP17, adding 13% of polyvinyl alcohol PVA24, adding 1.2% of carbomer resin, stirring and dissolving at the normal temperature, then heating to 88 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing a vacuum kettle, adding 1.8% of wheat flour, 1.5% of glycerol and 2% of propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, cooling to 55 ℃, adding 0.2% of preservative while stirring, uniformly stirring, continuously cooling to below 40 ℃, detecting and discharging, and then adding 0.4% of glitter powder into an open type stirrer for complete mixing to obtain washable gold powder glue. The wheat grain powder is prepared from the following components in percentage by weight of 12: 2.5, the wheat grain powder is obtained by crushing wheat grains at the rotation speed of 900r/min for 15min and at the temperature of 1 ℃, the straw powder is obtained by crushing straws at the rotation speed of 2200r/min for 40min and at the temperature of 7 ℃, the particle size of the wheat grain powder is 210 meshes, and the particle size of the straw powder is 700 meshes.
Example 6
Checking whether related production equipment such as a reaction kettle and the like is normal or not at the normal temperature of 25 ℃, adding deionized water into the reaction kettle after the detection is qualified, adding 8% of polyvinyl alcohol BP17, adding 15% of polyvinyl alcohol PVA24, adding 1.5% of carbomer resin, stirring and dissolving at the normal temperature, heating to 90 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, sealing the vacuum kettle, adding 2.1% of wheat flour, 2% of glycerol and 2.5% of propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, cooling to 60 ℃, adding 0.3% of preservative while stirring, uniformly stirring, continuously cooling to below 40 ℃, detecting and discharging, and then adding 0.5% of glitter powder into an open type stirrer for complete mixing to obtain washable gold powder glue. The wheat grain powder is prepared from the following components in parts by weight: 2, the wheat grain powder is obtained by crushing wheat grains at the rotating speed of 1000r/min for 20min and at the temperature of 5 ℃, the straw powder is obtained by crushing straws at the rotating speed of 2500r/min for 50min and at the temperature of 10 ℃, the particle size of the wheat grain powder is 300 meshes, and the particle size of the straw powder is 800 meshes.
The products obtained in the examples 1-6 have washability for textiles and a three-dimensional effect, and the main technical indexes of the products are detailed in the following table 1:
TABLE 1
Comparison of examples 1 to 6 with the prior art table 2:
TABLE 2
Compared with the prior art, the washable gold powder adhesive has the beneficial effects that: the components have stable performance, safe storage, high efficiency, convenience, difficult halation, environmental protection, harmlessness and convenient cleaning.
It should be noted that the above-mentioned embodiments are only for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the claims of the present invention.
Claims (10)
1. The washable gold powder adhesive is characterized in that: the adhesive comprises, by weight, 173-8 parts of polyvinyl alcohol BP, 1-15 parts of polyvinyl alcohol PVA 2411-15 parts of carbomer resin, 0.6-1.5 parts of xanthan gum, 0.5-2 parts of glycerol, 1.5-2.5 parts of propylene glycol, 0.1-0.3 part of preservative, 0.2-0.5 part of glitter powder and the balance of deionized water.
2. The washable gold powder glue of claim 1, characterized in that: 0.6-1.5 parts of xanthan gum are replaced by 1.1-2.1 parts of wheat grain powder.
3. The method for preparing washable gold powder glue according to claim 1 or 2, comprising the following steps:
(1) adding deionized water, polyvinyl alcohol BP17, polyvinyl alcohol PVA24 and carbomer resin into a reaction kettle at normal temperature, stirring for dissolving, heating to 85-90 ℃, stopping heating after complete dissolution, keeping the temperature for 2 hours, cooling to 50 ℃, uniformly mixing, and sealing the reaction kettle;
(2) adding xanthan gum, glycerol and propylene glycol, uniformly stirring, heating to 90 ℃, keeping the temperature for 2 hours, and cooling to 50-60 ℃;
(3) adding antiseptic while stirring, mixing, and continuously cooling to below 40 deg.C to obtain colloid;
(4) putting the colloid into an open stirrer, and adding glitter powder for complete mixing to obtain washable gold powder colloid.
4. The method for preparing washable gold powder glue according to claim 3, characterized in that: the rotating speed of stirring in the steps (1) - (3) is 300-600 r/min.
5. The method for preparing washable gold powder glue according to claim 3, characterized in that: and (3) replacing the xanthan gum with wheat flour in the step (2).
6. The method for preparing washable gold powder glue according to claim 5, characterized in that: the wheat grain powder comprises wheat grain powder and straw powder, wherein the wheat grain powder is obtained by crushing wheat grains, the crushing rotation speed is 800-1000 r/min, the time is 10-20 min, the temperature is-5 ℃, the straw powder is obtained by crushing straws, the crushing rotation speed is 2000-2500 r/min, the time is 30-50 min, and the temperature is 5-10 ℃.
7. The method for preparing washable gold powder glue according to claim 6, characterized in that: the grain size of the wheat grain powder is 150-300 meshes, and the grain size of the straw powder is 500-800 meshes.
8. The method for preparing washable gold powder glue according to claim 6, characterized in that: the weight ratio of the wheat grain powder to the straw powder is 10-15: 2 to 3.
9. The method for preparing washable gold powder glue according to claim 3, characterized in that: in the step (3), the preservative is any one of benzoic acid, sodium benzoate, sorbic acid, potassium sorbate and calcium propionate.
10. The method for preparing washable gold powder glue according to claim 3, characterized in that: in the step (4), the rotation speed of the mixing is 1200-1500 r/min, the time is 20-30 min, and the temperature is 15-25 ℃.
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CN202010692346.8A CN111704819A (en) | 2020-07-17 | 2020-07-17 | Washable gold powder adhesive and preparation method thereof |
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CN202010692346.8A CN111704819A (en) | 2020-07-17 | 2020-07-17 | Washable gold powder adhesive and preparation method thereof |
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Cited By (1)
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---|---|---|---|---|
CN114058294A (en) * | 2021-11-25 | 2022-02-18 | 江苏兴达文具集团有限公司 | Preparation process of degradable gold powder glue |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN114058294A (en) * | 2021-11-25 | 2022-02-18 | 江苏兴达文具集团有限公司 | Preparation process of degradable gold powder glue |
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Application publication date: 20200925 |