CN111648152A - Production method of high-density mica paper - Google Patents

Production method of high-density mica paper Download PDF

Info

Publication number
CN111648152A
CN111648152A CN202010466687.3A CN202010466687A CN111648152A CN 111648152 A CN111648152 A CN 111648152A CN 202010466687 A CN202010466687 A CN 202010466687A CN 111648152 A CN111648152 A CN 111648152A
Authority
CN
China
Prior art keywords
mica
paper
mica paper
pulp
carrying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010466687.3A
Other languages
Chinese (zh)
Inventor
潘渡江
朱淼
李海相
潘斌海
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pamica Electric Material Hubei Co ltd
Original Assignee
Pamica Electric Material Hubei Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pamica Electric Material Hubei Co ltd filed Critical Pamica Electric Material Hubei Co ltd
Priority to CN202010466687.3A priority Critical patent/CN111648152A/en
Publication of CN111648152A publication Critical patent/CN111648152A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/02Pretreatment of the raw materials by chemical or physical means
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D5/00Purification of the pulp suspension by mechanical means; Apparatus therefor
    • D21D5/02Straining or screening the pulp
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21FPAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F1/00Wet end of machines for making continuous webs of paper
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21FPAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F3/00Press section of machines for making continuous webs of paper
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21GCALENDERS; ACCESSORIES FOR PAPER-MAKING MACHINES
    • D21G1/00Calenders; Smoothing apparatus
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/36Inorganic fibres or flakes
    • D21H13/38Inorganic fibres or flakes siliceous
    • D21H13/44Flakes, e.g. mica, vermiculite

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Paper (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

The invention belongs to the field of mica paper production, and provides a production method of high-density mica paper, which comprises the following steps: carrying out heat treatment on the selected mica material for two times; carrying out secondary crushing; grading by a three-way cyclone and a three-way grading sieve; adsorbing with 12000 Gauss high magnet; introducing mica pulp sheets into a fine pulp tank; extracting mica pulp in the fine pulp tank to a cylinder paper machine for papermaking; pressing the manufactured mica paper for multiple times, drying the mica paper by a drying cylinder of a paper machine, cooling the mica paper by a cooling cylinder, and then performing calendaring treatment; and reeling and slitting the calendered mica paper. The mica paper prepared by the production method has higher density, smaller volume and uniform thickness after being made into a plate-shaped or strip-shaped high-temperature-resistant insulating material, and can meet the development requirement of a new energy industry; the safety of industrial and household appliances is improved; the efficiency of production operation is improved, the cost of labor has been saved for enterprise's production.

Description

Production method of high-density mica paper
Technical Field
The invention belongs to the field of mica paper production, and particularly relates to a production method of high-density mica paper.
Background
The new energy industry in China is the development focus, a large number of industries and household appliances need a large number of products such as high-density insulating mica paper and the like, the insulating mica paper has excellent electrical performance and high-temperature resistance, has good permeability and air permeability, can be impregnated and pressed into high-quality plate-shaped heat-resistant insulating materials by epoxy resin, organic silicon resin and the like, and can also be impregnated and pressed into high-quality belt-shaped high-temperature-resistant insulating materials by glass fiber cloth, films, ceramic fibers and the like through epoxy or organic silicon resin. The existing mica paper has low density, large volume, uneven thickness and low mica content after being made into a plate-shaped or strip-shaped high-temperature-resistant insulating material.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide a production method of high-density mica paper, the mica paper produced by the method has higher density, smaller volume and uniform thickness after being made into a plate-shaped or belt-shaped high-temperature-resistant insulating material, and can meet the development requirements of new energy industry.
The purpose of the invention is realized by the following technical scheme.
A production method of high-density mica paper comprises the following steps:
(1) selecting a clean mica material with uniform sheet diameter and no spots, and carrying out heat treatment on the selected mica material for two times;
(2) crushing the mica material after heat treatment by a secondary crushing system;
(3) grading the mica pulp sheet after the secondary crushing by a three-way cyclone and a three-way grading sieve;
(4) carrying out adsorption treatment on mica pulp sheets which are graded by a cyclone and a grading sieve by using a 12000 Gauss high magnetism;
(5) introducing the mica pulp sheets subjected to adsorption treatment into a fine pulp tank;
(6) extracting mica pulp in the fine pulp tank to a cylinder paper machine for papermaking;
(7) the manufactured mica paper is subjected to multiple times of pressing treatment, so that the thickness is reduced, and the density is increased;
(8) drying the pressed mica paper by a drying cylinder of a paper machine, cooling by a cooling cylinder and then carrying out press polishing treatment;
(9) and (4) reeling and slitting the calendered mica paper.
In the technical scheme, the temperature of the two heat treatments in the step (1) is 720 ℃ and 350 ℃, and the holding time is 2 hours and 1 hour.
In the technical scheme, the cloud master batch in the step (2) is crushed by a secondary crushing system, wherein the crushing pressure is 6MPa and 4MPa respectively.
In the technical scheme, the cyclone pressure of the cyclone in the step (3) is 3MPa, and the grading sieve mesh number is 250 meshes.
The mica paper prepared by the production method has higher density, smaller volume and uniform thickness after being made into a plate-shaped or strip-shaped high-temperature-resistant insulating material, and can meet the development requirement of a new energy industry; the safety of industrial and household appliances is improved; the efficiency of production operation is improved, the cost of labor has been saved for enterprise's production.
Detailed Description
The present invention is further described in detail below with reference to examples so that those skilled in the art can practice the invention with reference to the description.
The embodiment provides a production method of high-density mica paper, which comprises the following steps:
(1) selecting a clean mica material with uniform sheet diameter and no spots, and carrying out two heat treatments on the selected mica material, wherein the temperature of the two heat treatments is 720 ℃ and 350 ℃, and the holding time is 2 hours and 1 hour respectively;
(2) crushing the mica material subjected to heat treatment by a secondary crushing system, wherein the crushing pressure is 6MPa and 4MPa respectively;
(3) grading the mica pulp sheets subjected to secondary crushing by using a three-way cyclone and a three-way grading sieve, wherein the cyclone pressure of the cyclone is 3MPa, and the grading sieve mesh number is 250 meshes;
(4) carrying out adsorption treatment on mica pulp sheets which are graded by a cyclone and a grading sieve by using a 12000 Gauss high magnetism;
(5) introducing the mica pulp sheets subjected to adsorption treatment into a fine pulp tank;
(6) extracting mica pulp in the fine pulp tank to a cylinder paper machine for papermaking;
(7) the manufactured mica paper is pressed by three pairs of rollers, so that the thickness is reduced and the density is increased;
(8) drying the pressed mica paper by a drying cylinder of a paper machine, cooling by a cooling cylinder and then carrying out press polishing treatment;
(9) and (4) reeling and slitting the calendered mica paper.
Performance analysis:
TABLE 1 high Density mica paper Properties
Figure 878730DEST_PATH_IMAGE001
As can be seen from Table 1, the mica paper produced by the production method of this example can achieve the high temperature resistance and high insulation performance of the existing mica paper, and has high density.
Details not described in this specification are within the skill of the art that are well known to those skilled in the art.
While embodiments of the invention have been described above, it is not limited to the applications set forth in the description and the embodiments, which are fully applicable in various fields of endeavor to which the invention pertains, and further modifications may readily be made by those skilled in the art, it being understood that the invention is not limited to the details shown and described herein without departing from the general concept defined by the appended claims and their equivalents.

Claims (5)

1. A production method of high-density mica paper is characterized by comprising the following steps:
(1) selecting a clean mica material with uniform sheet diameter and no spots, and carrying out heat treatment on the selected mica material for two times;
(2) crushing the mica material after heat treatment by a secondary crushing system;
(3) grading the mica pulp sheet after the secondary crushing by a three-way cyclone and a three-way grading sieve;
(4) carrying out adsorption treatment on mica pulp sheets which are graded by a cyclone and a grading sieve by using a 12000 Gauss high magnetism;
(5) introducing the mica pulp sheets subjected to adsorption treatment into a fine pulp tank;
(6) extracting mica pulp in the fine pulp tank to a cylinder paper machine for papermaking;
(7) the manufactured mica paper is subjected to multiple times of pressing treatment, so that the thickness is reduced, and the density is increased;
(8) drying the pressed mica paper by a drying cylinder of a paper machine, cooling by a cooling cylinder and then carrying out press polishing treatment;
(9) and (4) reeling and slitting the calendered mica paper.
2. The method of producing a high density mica paper as set forth in claim 1, characterized in that: the temperature of the two heat treatments in the step (1) is 720 ℃ and 350 ℃, and the holding time is 2 hours and 1 hour.
3. The method of producing a high density mica paper as set forth in claim 1, characterized in that: and (3) crushing the mica masterbatch in the step (2) by using a secondary crushing system, wherein the crushing pressures are 6MPa and 4MPa respectively.
4. The method of producing a high density mica paper as set forth in claim 1, characterized in that: in the step (3), the cyclone pressure of the cyclone is 3MPa, and the grading sieve mesh number is 250 meshes.
5. The method of producing a high density mica paper as set forth in claim 1, characterized in that: and (7) carrying out three-stage pressing treatment on the manufactured mica paper.
CN202010466687.3A 2020-05-28 2020-05-28 Production method of high-density mica paper Pending CN111648152A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010466687.3A CN111648152A (en) 2020-05-28 2020-05-28 Production method of high-density mica paper

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010466687.3A CN111648152A (en) 2020-05-28 2020-05-28 Production method of high-density mica paper

Publications (1)

Publication Number Publication Date
CN111648152A true CN111648152A (en) 2020-09-11

Family

ID=72350939

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010466687.3A Pending CN111648152A (en) 2020-05-28 2020-05-28 Production method of high-density mica paper

Country Status (1)

Country Link
CN (1) CN111648152A (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4219383A (en) * 1977-02-18 1980-08-26 Valkama P J Press section of a paper machine
US4526655A (en) * 1982-09-15 1985-07-02 Valmet Oy Press section with separate press nips in a paper machine
CN1738941A (en) * 2002-11-19 2006-02-22 美卓造纸机械公司 Press section in a paper or board machine
CN102535252A (en) * 2012-01-09 2012-07-04 富阳华利纸业有限公司 Method for producing environment-friendly white cardboard
CN103741541A (en) * 2014-01-11 2014-04-23 湖北平安电工材料有限公司 Method for manufacturing mica paper by low-temperature calcining
CN104452428A (en) * 2014-11-17 2015-03-25 通城县中天云母制品有限公司 Production method of calcining type high-voltage-resisting mica paper
CN105070350A (en) * 2015-06-30 2015-11-18 平江县兴科云母制品有限公司 Manufacture process of low-flourine mica tape
CN105239443A (en) * 2014-07-12 2016-01-13 平江县威派云母绝缘材料有限公司 Environment-friendly preparation process for calcined-mica paper
CN106739270A (en) * 2016-11-24 2017-05-31 东台银信钢结构工程有限公司 A kind of high density steel plate and its production technology
CN106996053A (en) * 2017-03-17 2017-08-01 湖北平安电工材料有限公司 A kind of high heat conduction mica paper manufacture method

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4219383A (en) * 1977-02-18 1980-08-26 Valkama P J Press section of a paper machine
US4526655A (en) * 1982-09-15 1985-07-02 Valmet Oy Press section with separate press nips in a paper machine
CN1738941A (en) * 2002-11-19 2006-02-22 美卓造纸机械公司 Press section in a paper or board machine
CN102535252A (en) * 2012-01-09 2012-07-04 富阳华利纸业有限公司 Method for producing environment-friendly white cardboard
CN103741541A (en) * 2014-01-11 2014-04-23 湖北平安电工材料有限公司 Method for manufacturing mica paper by low-temperature calcining
CN105239443A (en) * 2014-07-12 2016-01-13 平江县威派云母绝缘材料有限公司 Environment-friendly preparation process for calcined-mica paper
CN104452428A (en) * 2014-11-17 2015-03-25 通城县中天云母制品有限公司 Production method of calcining type high-voltage-resisting mica paper
CN105070350A (en) * 2015-06-30 2015-11-18 平江县兴科云母制品有限公司 Manufacture process of low-flourine mica tape
CN106739270A (en) * 2016-11-24 2017-05-31 东台银信钢结构工程有限公司 A kind of high density steel plate and its production technology
CN106996053A (en) * 2017-03-17 2017-08-01 湖北平安电工材料有限公司 A kind of high heat conduction mica paper manufacture method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
J.P.凯西: "《制浆造纸化学工艺学》", 31 March 1988, 轻工业出版社 *

Similar Documents

Publication Publication Date Title
CN102127882A (en) Manufacturing method of ultra-high voltage insulation cooked mica paper
CN103757977A (en) Inorganic powder mica paper and preparation method and use thereof
CN103820883A (en) Preparation method of bacterial cellulose based carbon nanofibers
CN103184586A (en) Preparation method of bacterial-cellulose-fiber-based nano-grade carbon fiber
CN109534343A (en) A method of high-specific surface area nitrogen-preparing carbon molecular sieves are prepared by raw material of bagasse
CN111648152A (en) Production method of high-density mica paper
CN113043686B (en) Electromagnetic shielding composite film with sandwich structure and preparation method thereof
CN106223104A (en) A kind of method using PSA fiber to prepare aramid fiber extrusion coating paper
CN109019576A (en) A kind of technique of physical method production graphene
CN110670392B (en) Processing technology for producing refractory plate by modified kraft paper
CN102211766A (en) Rapid low-cost preparation method of high heat conduction carbon material
CN111778765A (en) High-heat-resistance mica paper and manufacturing method thereof
CN107326723B (en) A kind of aromatic polyamide paper and preparation method thereof
US20230416989A1 (en) Carbon fiber paper, flexible rollable carbon paper made from the carbon fiber base paper and the preparation methods and systems thereof
CN104594094B (en) A kind of method of continuous seepage PPTA-pulp
CN106299211B (en) A kind of preparation method of nickel-hydrogen battery separator
CN107385564A (en) A kind of preparation method of starch base carbon fibre
CN1108712A (en) Low-temp. plasma-treating technology for wool fiber material and apparatus thereof
CN106245392A (en) A kind of preparation method of high-performance Powerleader synthetic fibre aramid fiber extrusion coating paper
CN104098081B (en) A kind of preparation technology of little length-to-diameter ratio carbon fiber powder
CN115621475A (en) Gas diffusion layer and preparation method thereof
CN202638141U (en) Composite needle filtering felt
CN110344287A (en) A kind of renewable fiberboard of high-penetration intensity and its environment-friendly preparation method thereof
CN109467084A (en) A kind of preparation method of superhigh specific surface area nitrogen carbon molecular sieve
CN116695289A (en) Method for manufacturing short fibers from carbon fiber leftover materials

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
CB02 Change of applicant information

Address after: No. 242, Tongcheng Avenue, Tongcheng County, Xianning City, Hubei Province 437400

Applicant after: Hubei Ping'an Electric Technology Co.,Ltd.

Address before: 437400 Building 1, 226 Yuli Avenue, junshui Town, Tongcheng County, Xianning City, Hubei Province

Applicant before: PAMICA ELECTRIC MATERIAL (HUBEI) Co.,Ltd.

CB02 Change of applicant information
RJ01 Rejection of invention patent application after publication

Application publication date: 20200911

RJ01 Rejection of invention patent application after publication