CN111617704A - Hydrogenation reactor inlet diffuser - Google Patents

Hydrogenation reactor inlet diffuser Download PDF

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Publication number
CN111617704A
CN111617704A CN202010394946.6A CN202010394946A CN111617704A CN 111617704 A CN111617704 A CN 111617704A CN 202010394946 A CN202010394946 A CN 202010394946A CN 111617704 A CN111617704 A CN 111617704A
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China
Prior art keywords
inlet
mounting plate
hydrogenation reactor
guide post
injection
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CN202010394946.6A
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CN111617704B (en
Inventor
邓矛
陈崇刚
李立权
晁君瑞
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China Petroleum and Chemical Corp
Sinopec Engineering Group Co Ltd
Sinopec Guangzhou Engineering Co Ltd
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China Petroleum and Chemical Corp
Sinopec Engineering Group Co Ltd
Sinopec Guangzhou Engineering Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278Feeding reactive fluids
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

The invention discloses an inlet diffuser of a hydrogenation reactor, which comprises an inlet conical body, a mounting plate and an injection cover, wherein the inlet conical body is provided with a conical surface; the inlet cone is integrally a conical frustum, the lower part of the inlet cone is a flange-shaped flange, a guide post is arranged on the flange, cyclone tubes are uniformly distributed on the upper surface of the inlet cone, the upper parts of the cyclone tubes are inverted cone-shaped closing-up structures, the lower parts of the cyclone tubes are guide tubes for guiding, and rotary guide vanes are arranged in the inverted cone-shaped closing-up structures; the mounting plate is a circular ring plate, the inner side of the mounting plate is sleeved outside the inlet conical body, the guide post penetrates through the cylindrical hole of the mounting plate, the guide post is sleeved with a spring, the upper end of the guide post is provided with a gasket and a nut, and two ends of the spring are fixed on the gasket and the mounting plate; the bottom of the injection cover is uniformly provided with injection holes, and the injection cover covers the lower part of the inlet conical body and is fixed on the lower surface of the mounting plate. The invention can fully mix gas and liquid, has large spraying area, effectively avoids liquid phase bias flow, can greatly improve the initial distribution of oil gas entering the reactor, improves the reaction operation condition and improves the product quality.

Description

Hydrogenation reactor inlet diffuser
Technical Field
The invention relates to the technical field of diffusers, in particular to a diffuser at an inlet of a hydrogenation reactor.
Background
In recent years, with the gradual upgrade of quality standards of petrochemical products and the stricter of environmental regulations, the hydrogenation technology plays an increasingly important role in the oil refining industry, and in addition, the requirement of 'eating, drying and squeezing out' of raw oil, and oil refining enterprises at home and abroad rapidly expand the hydrotreating capability of various oil products in order to improve the economic benefit and meet the requirement of environmental protection.
The key core equipment of hydrotreating is a hydrogenation reactor, and inside the hydrogenation reactor, a mixture of hydrogen and raw oil in a certain proportion is subjected to various hydrogenation reactions under the action of a catalyst at a certain temperature and pressure. Because the hydrogenation reaction is a strong exothermic reaction existing in three phases of gas, liquid and solid, if the gas and the liquid are not uniformly distributed in a catalyst bed, the reaction of a part with a large amount of liquid phase is violent, the generated heat is large, the local temperature of the catalyst is high, and a hot spot is formed, so that the catalyst is inactivated prematurely, local coking and hardening of the catalyst are caused in serious conditions, and materials cannot normally pass through, so that the service life of the catalyst and the start-up period of the device are reduced, the pressure drop of the bed is increased, and the energy consumption of the device is increased. Therefore, in order to make the hydrogenation apparatus operate smoothly, the temperature difference in the radial direction of the reactor needs to be small, in other words, the liquid distribution in the radial direction of the reactor needs to be as uniform as possible. With the upsizing of equipment caused by the upsizing of the device, the radial temperature difference of the reactor with larger diameter is kept small, and new challenges are provided for the internal components of the hydrogenation reactor.
Fixed bed hydrogenation reactors, a common type of hydrogenation reactor, are typically internally provided with reactor internals such as inlet diffusers, scale depositing baskets, distribution trays, catalyst support grids, discharge tubes, hydrogen cooling tanks, thermocouple protection tubes, and outlet collectors. The fixed bed hydrogenation reactor is generally fed from the top center of the hydrogenation reactor, because the diameter of the reactor inlet is usually smaller than that of the reactor, a gas-liquid two-phase medium from the reactor inlet needs to enter the reactor through an inlet diffuser, and the inlet diffuser has the functions of mixing the gas phase and the liquid phase on one hand, and dispersing the gas phase and the liquid phase into the reactor to realize pre-distribution of the gas phase and the liquid phase, so the inlet diffuser plays an important role in internal parts of the hydrogenation reactor and uniform distribution of the medium. With the upsizing of equipment caused by the upsizing of the device, the increase of the diameter of the reactor inlet has certain limitation, so that the ratio of the diameter of the reactor to the diameter of the reactor inlet reaches 5 or more, and higher requirements are put forward on an inlet diffuser of a hydrogenation reactor.
Present common diffuser is mostly simple two-layer or multilayer conical body, the gas-liquid is double-phase to be short through the conical body time, mix insufficiently, the conical body leads to the material to be the tilt line at the streamline that reactor head space formed simultaneously, the liquid layer on the material distributes the dish with the top is rushed to the reactor all around and is sent, form "push away unrestrained" phenomenon, reactor distribution dish liquid layer height presents from central point to border position and increases the distribution promptly, reactor distribution dish central point puts the liquid level less, there is not the liquid layer even, reactor boundary wall department liquid layer height is big, cause the whole cross-section of material evenly distributed to the reactor that can not be better after the reposition of redundant personnel, there is more serious deviation in the distribution.
Patent publication No. CN202015610U discloses an inlet diffuser for a hydrogenation reactor. The structure mainly comprises an outer cylinder body, a spherical spray head, a hemispheroid, a pipe flange and a flow crushing plate, wherein the spherical spray head, the hemispheroid and the flow crushing plate play a role in slowing down the impact force of fluid, and a medium is sprayed into a reactor through a flow crushing hole connecting pipe on the flow crushing plate. Although the diffuser can slow down the vertical impact force of materials to a certain degree, the gas-liquid two phases mainly spray media into the reactor through the crushed flow hole connecting pipe vertical to the crushed flow plate, the spraying area is small, and meanwhile, the gas-liquid two phases pass through the nozzle once and the connecting pipe twice, and the pressure drop is large. In addition, the use of the hydrogenation reactor with a larger diameter is also limited, because the gas-liquid two-phase feeding amount is increased after the scale of the device is increased, but because the size of the inlet pipe is smaller, the flow velocity of the gas-liquid two-phase in the inlet pipe and at the outlet of the spray head is very high, on one hand, the impact on the semisphere is very large, on the other hand, the impact counter force and the vibration of the inlet pipe are also very large, and the sealing of the pipe flange is easy to lose.
Patent No. CN106268524A discloses a diffuser and a fixed bed reactor. This diffuser mainly includes structures such as barrel, whirl board, well core rod, and the whirl board is fixed at the barrel middle part through well core rod, and the whirl board presents the curved plate that the heliciform extends for following the barrel axial. The gas-liquid material entering the diffuser flows in the cylinder along the extending direction of the rotational flow plate and is diffused along the direction at the gas-liquid material diffusion opening. Although this diffuser enables the gas-liquid material and produces certain mixture, and the pressure drop is less, but the material mainly flows and diffuses along the extending direction of whirl board, leads to the material to concentrate, spray the area little, easily appears local high concentration and most low concentration region.
In order to enable gas-liquid two-phase feeding to be more uniformly dispersed into the reactor, avoid the phenomenon of 'pushing waves', enlarge the spraying area of the gas-liquid two-phase, promote the mixing of the gas-liquid two-phase, enable the gas-liquid two-phase to react with a catalyst more stably and promote the stable operation of a hydrogenation device, a novel hydrogenation reactor inlet diffuser is needed.
Disclosure of Invention
The invention provides an inlet diffuser of a hydrogenation reactor, aiming at solving the technical problems that the inlet diffuser of the fixed bed hydrogenation reactor in the prior art is small in liquid phase distribution area, uneven in radial liquid phase distribution, easy to cause flow deviation and wall flow and the like.
The invention provides an inlet diffuser of a hydrogenation reactor, which comprises an inlet conical body, a mounting plate and an injection cover; the inlet cone is integrally a conical frustum, the lower part of the inlet cone is a flange-shaped flange, a guide post which is erected upwards is arranged on the flange, cyclone tubes are uniformly distributed on the upper surface of the inlet cone, the upper parts of the cyclone tubes are of inverted cone-shaped closing-up structures, the lower parts of the cyclone tubes are guide tubes which play a role in guiding, outlets of the guide tubes are fixed on the lower surface of the inlet cone, and rotary guide vanes are arranged in the inverted cone-shaped closing-up structures; the mounting plate is a circular annular plate, a cylindrical hole matched with the guide post is formed in the mounting plate, the mounting plate is sleeved outside the inlet conical body by the inner ring of the mounting plate, the guide post penetrates through the cylindrical hole, the guide post is sleeved with a spring, a gasket and a nut are arranged at the upper end of the guide post, two ends of the spring are fixed on the gasket and the mounting plate, and the inlet conical body is suspended on the mounting plate through the guide post and the spring and can move up and down relative to the mounting plate; the spraying cover is a cup-shaped body with a spherical or ellipsoidal bottom, spray holes are uniformly distributed at the bottom of the cup-shaped body, and the spraying cover is covered below the inlet conical body and fixed on the lower surface of the mounting plate.
The guide post generally sets up 3 ~ 12, and the entry conical body passes through the combined action of guide post, nut and spring and installs on the mounting panel.
The spiral-flow tube that sets up in the entry conical body is 4 ~ 90, and the main aspects trompil diameter 10 ~ 200mm of back taper binding off structure is preferably 12 ~ 100mm, and the tip trompil diameter after binding off is 5 ~ 100mm, preferably 8 ~ 50 mm. The gas-liquid two-phase medium is in the cyclone tube, as the flow area is reduced, the flow speed is increased, the flowing turbulence degree is increased, and the mixing of the gas phase and the liquid phase is promoted; the gas-liquid two-phase contact time and the pressure drop of the inlet diffuser are comprehensively considered, and the distance between every two adjacent rotary guide vanes is 1.1-5 times of the diameter of the small end opening. The swirl tube lower part is the stand pipe, and the stand pipe can be the straight tube, also can be the return bend, and such purpose is through the guide effect of stand pipe, ensures the gas-liquid two-phase even dispersion on spraying the whole region that covers from the swirl tube outflow.
The bottom of the injection cover is uniformly provided with injection holes along the radial direction on the circumference, the injection holes are distributed in a concentric circle shape, the injection holes spray mixed media to the periphery, and the diameter of the injection holes is preferably 5-50 mm. The bottom of the spraying cover is arranged to be spherical or ellipsoidal, so that the spraying range is wide, the mixed medium can be uniformly sprayed to the periphery, the contact area of the medium and the catalyst in the reactor is increased, and the uniform distribution of the medium in the reactor is promoted. The principle of the hole opening of the jet hole is to ensure enough spraying area and to ensure the uniform distribution of the gas-liquid medium on the cross section of the reactor.
As an improved scheme, a partition plate can be arranged on the inner side of the bottom of the spraying cover and can be divided into an annular partition plate and a vertical partition plate. The annular partition plate is concentrically distributed around the center of the bottom of the injection shield, the bottom of the injection shield is divided into annular areas containing injection holes with different numbers by the annular partition plate, the inner side of the bottom of the injection shield can also be provided with vertical partition plates which are vertically crossed with the annular partition plate along the radial direction of the bottom of the injection shield, and the annular areas are further divided into fan-shaped areas with smaller areas and containing the injection holes with different numbers. The height of the partition plate is 5-200 mm, and the partition plate is used for ensuring that each area on the bottom of the spraying cover is filled with certain liquid. When the liquid in a certain area is too high, the liquid overflows to other areas through the partition plate, so that the free flow and uniform distribution of the liquid on the bottom of the spray hood are realized, the inlet diffuser is ensured to uniformly flow out of the liquid phase to the radial section of the reactor, and bias flow is avoided.
According to the condition of processing raw materials (mainly considering fluidity), holes can be formed in the partition plate or not, the raw materials with good fluidity can not be formed, the raw materials with poor fluidity can be formed with holes, and the holes are preferably round holes or slots.
As a further improvement, the gas-liquid spray head can be arranged at the spray hole at the bottom of the spray cover, the gas-liquid spray head arranged at the bottom of the spray cover can increase the range of spraying the medium to the periphery, and simultaneously increase the contact of gas and liquid phases. The outlet type of the gas-liquid spray head can be an expanding type, a flat type or a closing type so as to ensure that the gas-liquid spray heads at different positions can uniformly distribute the medium to the cross section of the reactor.
The gas-liquid nozzle is fixed at the jet hole part by a tangent plane perpendicular to the jet hole part, the gas-liquid nozzle is a tubular body with two open ends, round holes or slots can be uniformly formed in the pipe wall of the gas-liquid nozzle on the inner side of the bottom of the jet cover along the circumferential direction to serve as a fluid channel, the round holes or the slots can be one layer or two layers or multiple layers, and the diameter of the round holes is 2-30 mm, preferably 4-25 mm. Generally, due to the gravity difference between the gas phase and the liquid phase, the liquid phase accumulated by the partition plate enters the gas-liquid spray head from single-row or multi-row openings on the gas-liquid spray head, the gas phase enters from the top of the gas-liquid spray head and is further contacted and cut with the liquid phase entering from the openings, and the gas phase and the liquid phase are more fully mixed. Under extreme circumstances, the liquid phase also can get into from the gas-liquid shower nozzle top, and the liquid phase leaves with higher speed, and such beneficial part is the mixture that further increases gas-liquid two-phase medium, and the gas-liquid shower nozzle has great operation elasticity simultaneously, and the higher region of liquid level can flow to other regions through the overflow on the one hand, also can leave the injection cover fast from the gas-liquid shower nozzle top, guarantees to have more even liquid height in every subregion by the baffle on the injection cover bottom.
The working principle of the invention is as follows:
when the material flow is small, the medium from the hydrogenation reactor inlet enters the inlet diffuser through the inlet of the inlet conical body cyclone pipe, the rectification of the mixed medium is realized in the cyclone pipe through the cyclone effect of the rotary guide vanes, the contact time of the gas phase and the liquid phase is increased, the medium is further uniformly dispersed in the whole area on the bottom of the injection shield through the guide effect of the guide pipe, and the medium entering the bottom space of the injection shield is radially and uniformly distributed in the reactor through the injection effect of the gas-liquid spray nozzle and enters the catalyst bed layer.
When the material flow is increased, the impact force of the material on the inlet conical body is increased, the stress of the spring is increased, the deformation quantity of the spring is increased, the downward compression quantity of the spring is increased, and the inlet conical body moves downwards under the action of the spring and the guide post; because the appearance of the inlet conical body is conical, the mounting plate is circular, the annular space between the inlet conical body and the mounting plate becomes large after the inlet conical body moves downwards, gas and liquid phases can enter the injection cover through the annular space between the inlet conical body and the mounting plate, and the uniform distribution of materials in the inlet diffuser is realized again after the adjustment of the partition plate on the injection cover.
The invention has the following beneficial effects:
1) oil gas leaves the space between the injection cover and the inlet conical body after entering the inlet conical body, and because the sectional area is increased, the flow velocity of fluid is reduced, the pressure is increased, a pressurizing chamber is formed at the position, the pressure of a mixed medium is increased by utilizing the conversion of the kinetic energy and the pressure of the medium, and the uniform ejection of the medium is facilitated.
2) The inlet of the cyclone tube is in an inverted cone shape or an inverted trumpet shape, so that the mixed medium is accelerated; the inlet of the swirl tube is provided with the rotary guide vane to realize rectification of the mixed medium, increase the turbulence degree of the flow and promote the mixing of gas phase and liquid phase; the guiding action of the guide tube ensures that the liquid phase is uniformly distributed over the entire spray hood.
3) The spraying cover with the spherical or ellipsoidal bottom is used for increasing the spraying range of the medium and increasing the contact area between the medium and the catalyst in the reactor; the flow of the liquid phase is strictly and accurately controlled through the separation effect of the partition plate on the bottom of the injection cover, so that the liquid phase is ensured to exist in each area, and bias flow is avoided from the source; the gas-liquid spray heads are arranged at the bottom of the spray cover, and liquid phase in each area enters the reactor from the gas-liquid spray heads, so that the mixing of gas phase and liquid phase can be further promoted, and the operation flexibility is high.
4) Through the setting of guide post and spring, make the entry conical body can do for the mounting panel and reciprocate, make the entry diffuser have the cushioning effect, can effectively reduce the impact of material to the entry diffuser, furthest has reduced because the impact that the feeding inhomogeneity brought and distribute inhomogeneous, has still realized entry diffuser aperture along with the increase automatically regulated of processingquantity.
In a word, the invention can fully mix gas and liquid, has large spraying area, effectively avoids liquid phase bias flow, can greatly improve the initial distribution of oil gas entering a reactor, improves the reaction operation condition and improves the product quality.
Drawings
FIG. 1 is a schematic view of the inlet diffuser of the present invention;
FIG. 2 is a schematic view of the bottom of the spray hood;
FIG. 3 is a schematic view of the structure of the gas-liquid shower head and its assembly structure;
fig. 4 is a schematic view of the assembled structure of the inlet diffuser of the present invention.
In the figure: 1-inlet cone, 2-mounting plate, 3-injection cover, 4-annular partition plate, 5-gas-liquid spray head, 6-cyclone tube, 7-rotary guide vane, 8-guide column, 9-nut, 10-gasket, 11-spring, 12-jet hole, 13-vertical partition plate, 14-round hole, 15-reactor inlet, 16-reactor shell.
Detailed Description
The invention will be further explained with reference to the drawings.
As shown in fig. 1, the hydrogenation reactor inlet diffuser of the present invention mainly comprises an inlet cone 1, a mounting plate 2 and an injection hood 3; the inlet conical body 1 is integrally a conical frustum-shaped body, the lower part of the inlet conical body is a flange-shaped flange, a guide post 8 which is vertically upwards is arranged on the flange, a cyclone tube 6 is uniformly distributed on the upper surface of the inlet conical body 1, the upper part of the cyclone tube 6 is of an inverted cone-shaped closing-up structure, the lower part of the cyclone tube is of a guide tube which plays a role in guiding, the outlet of the guide tube is fixed on the lower surface of the inlet conical body, and a rotary guide vane 7 is arranged; the mounting plate 2 is a circular annular plate, a cylindrical hole matched with the guide post 8 is formed in the mounting plate, the mounting plate 2 is sleeved outside the inlet conical body 1 through the inner side of the mounting plate, the guide post 8 penetrates through the cylindrical hole, the guide post 8 is sleeved with a spring 11, the upper end of the guide post 8 is provided with a gasket 10 and a nut 9, two ends of the spring 11 are fixed on the gasket 10 and the mounting plate 2, and the inlet conical body 1 is suspended on the mounting plate 2 through the guide post 8 and the spring 11 and can move up and down relative to the mounting plate 2; the injection cover 3 is a cup-shaped body with a spherical or ellipsoidal bottom, spray holes are uniformly distributed at the bottom of the cup-shaped body, and the injection cover 3 covers the lower part of the inlet conical body 1 and is fixed on the lower surface of the mounting plate 2. The inner side of the bottom of the injection cover 3 is provided with an annular clapboard 4 and the injection hole at the bottom is provided with a gas-liquid nozzle 5.
As shown in fig. 2, the bottom of the injection hood is uniformly distributed with injection holes 12, and the bottom of the injection hood is divided into different fan-shaped areas by the annular partition plate 4 arranged in a concentric circle shape and the vertical partition plate 13 vertically crossed with the annular partition plate 4 along the radial direction of the bottom of the injection hood. Of course, the annular partition 4 and the vertical partition 13 may also be perforated, and the perforations may be circular holes or slots.
As shown in fig. 3, the gas-liquid nozzle 5 is disposed at the injection hole at the bottom of the injection hood 3, and a circular hole 14 serving as a fluid passage is disposed on the pipe wall of the gas-liquid nozzle 5, but the fluid passage may be formed in a slit shape, and the outlet pattern of the gas-liquid nozzle 5 in the drawing is a flat type.
As shown in fig. 4, the inlet diffuser of the present invention is installed at the reactor inlet 15 of the reactor housing 16, and the inlet diffuser is fixed to the lower portion of the reactor inlet 15 by the installation plate 2.
The working process of the invention is as follows: as shown in fig. 4 and 1, the arrows indicate the flow direction of the medium in the cyclone tube 6.
When the flow rate is low, the reaction medium external to the hydrogenation reactor enters the inlet diffuser of the present invention through the hydrogenation reactor inlet 15. Firstly, a medium enters an inlet diffuser through an inlet of a cyclone tube 6 of an inlet conical body 1, the rectification of a mixed medium is realized through the cyclone effect of a rotary guide vane 7 in the cyclone tube 6, the contact time of a gas phase and a liquid phase is increased, the medium is further uniformly dispersed in the whole area on the bottom of an injection cover 3 through the guide effect of a guide tube, the medium entering the bottom space of the injection cover 3 is uniformly distributed in a fan-shaped area divided by an annular partition plate 4 and a vertical partition plate 13, and the medium is sprayed out by a gas-liquid spray nozzle 5 and uniformly enters a catalyst bed layer in a reactor. When the material flow is increased, the impact force of the material on the inlet conical body 1 is increased, the stress of the spring 11 is increased, the deformation amount of the spring 11 is increased, the downward compression amount of the spring 11 is increased, and the inlet conical body 1 moves downwards under the action of the spring 11 and the guide column 8; because the shape of the inlet conical body 1 is conical, the mounting plate 2 is circular, the annular space between the inlet conical body 1 and the mounting plate 2 becomes large after the inlet conical body 1 moves downwards, gas and liquid phases can enter the injection cover 3 through the annular space between the inlet conical body 1 and the mounting plate 2, and the uniform distribution of materials in the inlet diffuser is realized again after the adjustment of the partition plate on the bottom of the injection cover 3.

Claims (9)

1. A hydrogenation reactor inlet diffuser characterized by: comprises an inlet cone, a mounting plate and an injection cover; the inlet cone is integrally a conical frustum, the lower part of the inlet cone is a flange-shaped flange, a guide post which is erected upwards is arranged on the flange, cyclone tubes are uniformly distributed on the upper surface of the inlet cone, the upper parts of the cyclone tubes are of inverted cone-shaped closing-up structures, the lower parts of the cyclone tubes are guide tubes which play a role in guiding, outlets of the guide tubes are fixed on the lower surface of the inlet cone, and rotary guide vanes are arranged in the inverted cone-shaped closing-up structures; the mounting plate is a circular annular plate, a cylindrical hole matched with the guide post is formed in the mounting plate, the mounting plate is sleeved outside the inlet conical body by the inner ring of the mounting plate, the guide post penetrates through the cylindrical hole, the guide post is sleeved with a spring, a gasket and a nut are arranged at the upper end of the guide post, two ends of the spring are fixed on the gasket and the mounting plate, and the inlet conical body is suspended on the mounting plate through the guide post and the spring and can move up and down relative to the mounting plate; the spraying cover is a cup-shaped body with a spherical or ellipsoidal bottom, spray holes are uniformly distributed at the bottom of the cup-shaped body, and the spraying cover is covered below the inlet conical body and fixed on the lower surface of the mounting plate.
2. The hydrogenation reactor inlet diffuser of claim 1 wherein: the quantity of whirl pipe is 4 ~ 90, and the main aspects trompil diameter 10 ~ 200mm of back taper binding off structure, and the tip trompil diameter after the binding off is 5 ~ 100 mm.
3. The hydrogenation reactor inlet diffuser of claim 2 wherein: the diameter of a large-end opening of the inverted cone-shaped closing-up structure is 12-100 mm, and the diameter of a small-end opening after closing up is 8-50 mm.
4. The hydrogenation reactor inlet diffuser of claim 1 wherein: the distance between two adjacent rotary guide vanes is 1.1-5 times of the diameter of the small end opening.
5. The hydrogenation reactor inlet diffuser of claim 1 wherein: the inner side of the bottom of the injection cover is provided with an annular partition plate, the annular partition plate is concentrically distributed around the center of the bottom of the injection cover, and the annular partition plate divides the bottom of the injection cover into annular areas containing injection holes with different numbers.
6. The hydrogenation reactor inlet diffuser of claim 5 wherein: the inner side of the bottom of the injection cover is provided with a vertical partition plate which is vertically crossed with the annular partition plate along the radial direction of the bottom of the injection cover, and the annular area is divided into fan-shaped areas with smaller areas and containing injection holes with different numbers.
7. The hydrogenation reactor inlet diffuser of claim 6 wherein: the annular partition plate and the vertical partition plate are provided with holes.
8. The hydrogenation reactor inlet diffuser of any one of claims 1 to 7, wherein: and the gas-liquid spray head is arranged at the spray hole at the bottom of the spray cover and is vertical to the tangent plane at the spray hole.
9. The hydrogenation reactor inlet diffuser of claim 8 wherein: the gas-liquid spray head is a tubular body with two open ends, round holes or slots are uniformly arranged on the pipe wall of the gas-liquid spray head positioned on the inner side of the bottom of the spray cover along the circumferential direction to serve as fluid channels, and the round holes or the slots are one layer or two layers or more layers.
CN202010394946.6A 2020-05-12 2020-05-12 Hydrogenation reactor inlet diffuser Active CN111617704B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010394946.6A CN111617704B (en) 2020-05-12 2020-05-12 Hydrogenation reactor inlet diffuser

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010394946.6A CN111617704B (en) 2020-05-12 2020-05-12 Hydrogenation reactor inlet diffuser

Publications (2)

Publication Number Publication Date
CN111617704A true CN111617704A (en) 2020-09-04
CN111617704B CN111617704B (en) 2022-07-12

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0595056A1 (en) * 1992-10-24 1994-05-04 DIEHL GMBH & CO. Watercraft propulsion by a jet produced by the reaction of water with a chemical
CN101099954A (en) * 2007-07-25 2008-01-09 成都胜东科技有限公司 Atomized spray head
CN205495530U (en) * 2016-03-18 2016-08-24 兰州兰石集团有限公司 Spiral -flow type entry diffuser
CN106268524A (en) * 2015-06-05 2017-01-04 中国石油化工股份有限公司 Bubbler and fixed bed reactors
CN108114670A (en) * 2016-11-30 2018-06-05 中国石油化工股份有限公司 A kind of telescopic subtract rushes equal flow table

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0595056A1 (en) * 1992-10-24 1994-05-04 DIEHL GMBH & CO. Watercraft propulsion by a jet produced by the reaction of water with a chemical
CN101099954A (en) * 2007-07-25 2008-01-09 成都胜东科技有限公司 Atomized spray head
CN106268524A (en) * 2015-06-05 2017-01-04 中国石油化工股份有限公司 Bubbler and fixed bed reactors
CN205495530U (en) * 2016-03-18 2016-08-24 兰州兰石集团有限公司 Spiral -flow type entry diffuser
CN108114670A (en) * 2016-11-30 2018-06-05 中国石油化工股份有限公司 A kind of telescopic subtract rushes equal flow table

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