CN111579342B - A gas-bearing sample preparation device for coal and rock experiments - Google Patents
A gas-bearing sample preparation device for coal and rock experiments Download PDFInfo
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- CN111579342B CN111579342B CN202010489876.2A CN202010489876A CN111579342B CN 111579342 B CN111579342 B CN 111579342B CN 202010489876 A CN202010489876 A CN 202010489876A CN 111579342 B CN111579342 B CN 111579342B
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- 239000003245 coal Substances 0.000 title claims abstract description 33
- 239000011435 rock Substances 0.000 title claims abstract description 29
- 238000002474 experimental method Methods 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000001179 sorption measurement Methods 0.000 claims abstract description 5
- 238000003825 pressing Methods 0.000 claims description 44
- 238000000465 moulding Methods 0.000 claims description 14
- 238000007789 sealing Methods 0.000 claims description 6
- 239000007921 spray Substances 0.000 claims description 4
- 230000006835 compression Effects 0.000 abstract description 6
- 238000007906 compression Methods 0.000 abstract description 6
- 238000000748 compression moulding Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 239000010720 hydraulic oil Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 7
- 239000000843 powder Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000003826 uniaxial pressing Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
- G01N2001/366—Moulds; Demoulding
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Abstract
Description
技术领域technical field
本发明属于煤岩实验技术领域,具体涉及一种煤岩实验的含气样品制备装置。The invention belongs to the technical field of coal and rock experiments, and in particular relates to a gas-containing sample preparation device for coal and rock experiments.
背景技术Background technique
煤矿安全生产关系到国家能源供应,必然对煤岩进行物理力学性质基础研究。在针对我国广泛的、发育程度不同的、变形各异的构造煤进行研究时,由于煤层较软往往不易取大块样品切割加工,因此通常煤粉或岩粉压制成块状以方便展开相关工作。The safe production of coal mines is related to the national energy supply, so it is necessary to carry out basic research on the physical and mechanical properties of coal rocks. When conducting research on a wide range of tectonic coals with different development levels and deformations in my country, it is often difficult to take large samples for cutting and processing because the coal seam is soft, so coal powder or rock powder is usually pressed into blocks to facilitate related work .
目前煤岩实验样品压制方法主要分为单轴压制、三轴压制两种。其中单轴压制煤岩实验样品是对破碎煤岩样施加单方向的力进而使样品固结成型,但在压制过程中可能存在样品受力不均匀、样品不易取出、仅能实现一种尺寸样品的制备从而影响后续实验结果。三轴压制方法是从三个方向进行施压从而使煤岩样固结成型,但三轴压制方法操作繁琐,装置复杂且仅能实现单一尺寸的样品压制过程。At present, the compression methods of coal and rock experimental samples are mainly divided into two types: uniaxial pressing and triaxial pressing. Among them, the uniaxial compression of the coal rock sample is to apply a unidirectional force to the broken coal rock sample to consolidate the sample, but there may be uneven force on the sample during the pressing process, the sample is not easy to take out, and only one size sample can be realized. The preparation will affect the results of subsequent experiments. The triaxial pressing method is to apply pressure from three directions to consolidate the coal rock sample, but the triaxial pressing method is cumbersome to operate, the device is complicated, and it can only realize the sample pressing process of a single size.
现有煤岩样品压制技术存在问题主要有:1、忽略了气体在煤岩成型过程中的影响,2、单轴压制或三轴压制方式难以制备煤岩实验样品,特别是三轴压制方法较难对长方体形状的试验样品压制成型。The main problems in the existing coal rock sample pressing technology are: 1. The influence of gas in the coal rock forming process is ignored. 2. It is difficult to prepare coal rock experimental samples by uniaxial pressing or triaxial pressing, especially the triaxial pressing method It is difficult to press-form a test sample in the shape of a cuboid.
发明内容Contents of the invention
针对现有技术存在的问题,本发明所要解决的技术问题就是提供一种煤岩实验的含气样品制备装置,它能替代单轴或三轴加载条件,实现多种尺寸、含气状态煤岩样品的压制成型,且压制成型方便快捷。Aiming at the problems existing in the prior art, the technical problem to be solved by the present invention is to provide a gas-containing sample preparation device for coal and rock experiments, which can replace uniaxial or triaxial loading conditions, and realize various sizes and gas-bearing states of coal and rock The compression molding of the sample is convenient and quick.
本发明所要解决的技术问题是通过这样的技术方案实现的,它包括从上到下依次设置的上液压油缸、成型模具和下液压油缸,上液压油缸、成型模具和下液压油缸固定在至少两根对称立柱上;成型模具包括壳体、上盖板和下盖板,壳体固定在立柱中段,上盖板和下盖板封盖壳体上下两面,且用第二密封圈密封,盖板边缘的凸耳滑动贯套在立柱上用螺母压紧,壳体内部嵌有第一模具;第一模具内部嵌有第二模具,第二模具内部嵌有第三模具;The technical problem to be solved by the present invention is achieved through such a technical scheme, which includes an upper hydraulic cylinder, a molding die and a lower hydraulic cylinder arranged sequentially from top to bottom, and the upper hydraulic cylinder, forming mold and lower hydraulic cylinder are fixed on at least two on a symmetrical column; the forming mold includes a housing, an upper cover and a lower cover, the housing is fixed in the middle of the column, the upper and lower covers cover the upper and lower sides of the housing, and are sealed with a second sealing ring, the cover The lugs on the edge slide through and fit on the column and are pressed with nuts, the first mold is embedded inside the shell; the second mold is embedded inside the first mold, and the third mold is embedded inside the second mold;
上液压油缸的第一压杆向下通过上盖板的穿孔伸入成型模具上部;下液压油缸的第二压杆向上通过下盖板的穿孔伸入成型模具下部,第一压杆与第二下压杆同轴安装,上盖板和下盖板的穿孔中设置第一密封圈;成型模具侧壁上开有进气管连通吸附气源。The first pressure rod of the upper hydraulic cylinder extends downwards into the upper part of the forming mold through the perforation of the upper cover plate; the second pressure rod of the lower hydraulic cylinder extends upwards into the lower part of the forming mold through the perforation of the lower cover plate. The lower pressing rod is coaxially installed, and the first sealing ring is arranged in the perforation of the upper cover plate and the lower cover plate; an air inlet pipe is opened on the side wall of the forming mold to communicate with the adsorption gas source.
与现有煤岩制样装置相比,本发明具有以下技术效果:Compared with the existing coal rock sample preparation device, the present invention has the following technical effects:
由于成型模具包含有多种型腔,能够实现多种尺寸含气状态松散煤岩样品的压制成型,能够满足单轴或三轴煤岩实验加载条件下的样品制备功能,保证实验样品制备的成功率,且考虑气体对煤岩成型过程的影响。Since the forming mold contains a variety of cavities, it can realize the compression molding of loose coal rock samples in a gas-bearing state of various sizes, and can meet the sample preparation function under the loading conditions of uniaxial or triaxial coal rock experiments, ensuring the success of experimental sample preparation rate, and consider the influence of gas on the formation process of coal rock.
附图说明Description of drawings
本发明的附图说明如下:The accompanying drawings of the present invention are as follows:
图1为本发明装置的结构示意图;Fig. 1 is the structural representation of device of the present invention;
图2为本发明装置的立体图;Fig. 2 is the perspective view of device of the present invention;
图3为成型模具的结构示意图;Fig. 3 is the structural representation of molding die;
图4为压板组件的结构示意图Figure 4 is a structural schematic diagram of the platen assembly
图5为装有十字型管路的下部输油管图。Fig. 5 is a diagram of the lower oil pipeline equipped with a cross-shaped pipeline.
图中,A1、上液压油缸;A2、下液压油缸;1、第一压杆;2、立柱;3、连接块;4、圆柱压头;5、上部输油管;51、下部输油管;6、第一密封圈;13、螺母;14、第二压杆;In the figure, A1, the upper hydraulic cylinder; A2, the lower hydraulic cylinder; 1, the first pressure rod; 2, the column; 3, the connection block; 4, the cylindrical pressure head; A seal ring; 13, nut; 14, the second pressure rod;
B、成型模具;7、第三模具;8、上盖板;9、第二模具;10、第一模具;11、进气管;12、下盖板; 15、第二密封圈;16、第三压块;17、第二压块;18、第一压块。B. Forming mold; 7. Third mold; 8. Upper cover plate; 9. Second mold; 10. First mold; 11. Air intake pipe; 12. Lower cover plate; 15. Second sealing ring; 16. Second mold Three briquetting blocks; 17, the second briquetting block; 18, the first briquetting block.
具体实施方式Detailed ways
下面结合附图和实施例对本发明作进一步说明:Below in conjunction with accompanying drawing and embodiment the present invention will be further described:
如图1和图2所示,本发明包括从上到下依次设置的上液压油缸A1、成型模具B和下液压油缸A2;上液压油缸A1、成型模具B和下液压油缸A2固定在至少两根对称立柱2上,As shown in Figures 1 and 2, the present invention includes an upper hydraulic cylinder A1, a molding die B and a lower hydraulic cylinder A2 arranged sequentially from top to bottom; the upper hydraulic cylinder A1, the molding die B and the lower hydraulic cylinder A2 are fixed on at least two On the root symmetrical column 2,
成型模具B包括壳体、上盖板8和下盖板12,壳体固定在立柱2中段,上盖板8和下盖板12封盖在壳体上下两面,且用第二密封圈15密封,盖板边缘的凸耳滑动贯套在立柱上用螺母压紧,壳体内部嵌有第一模具10;如图3所示,第一模具10内部嵌有第二模具9,第二模具9内部嵌有第三模具7;The molding die B includes a shell, an upper cover 8 and a lower cover 12, the shell is fixed on the middle section of the column 2, the upper cover 8 and the lower cover 12 are sealed on the upper and lower sides of the shell, and are sealed with a second sealing ring 15 , the lugs on the edge of the cover plate are slid through and sleeved on the column and pressed with nuts, and the first mold 10 is embedded inside the housing; as shown in Figure 3, the second mold 9 is embedded inside the first mold 10, and the second mold 9 A third mold 7 is embedded inside;
上液压油缸的第一压杆1向下通过上盖板8的穿孔伸入成型模具B上部;下液压油缸的第二压杆14向上通过下盖板12的穿孔伸入成型模具B下部,第一压杆1与第二压杆14同轴安装,上盖板8和下盖板12的穿孔中设置第一密封圈6;成型模具B侧壁上开有进气管11连通吸附气源。The first pressure rod 1 of the upper hydraulic cylinder extends downward through the perforation of the upper cover plate 8 into the upper part of the forming mold B; the second pressure rod 14 of the lower hydraulic cylinder extends upward through the perforation of the lower cover plate 12 into the lower part of the forming mold B. A pressure rod 1 is coaxially installed with the second pressure rod 14, and the first sealing ring 6 is arranged in the perforation of the upper cover plate 8 and the lower cover plate 12; an air inlet pipe 11 is provided on the side wall of the forming mold B to communicate with the adsorption gas source.
所述成型模具B的壳体为直径50cm、高30cm的筒体;如图3所示,所述第一模具10为直径40cm、高25cm的槽口柱体;第二模具9为长20cm×宽20cm×高25cm的槽口立方体;第三模具7两块芯板合模,每块芯板长10cm×宽5cm×高25cm,每块芯板顶面开有半径为2.5cm、深10cm的半圆柱槽,两块芯板下底面开有长5cm×宽2.5cm×高10cm的方槽;两块芯板合模后,上顶面合成底面直径为5cm、高为10cm的圆柱槽;两块芯板翻转组合成底面为5×5cm正方形、高为10cm的方槽,适配第三压板。The shell of described molding die B is the cylindrical shell of diameter 50cm, high 30cm; As shown in Figure 3, described first mold 10 is the notch cylinder of diameter 40cm, high 25cm; Second mold 9 is long 20cm× A notch cube with a width of 20cm×a height of 25cm; the third mold 7 is molded with two core boards, each core board is 10cm long×width 5cm×height 25cm, and the top surface of each core board has a radius of 2.5cm and a depth of 10cm. Semi-cylindrical groove, the bottom surface of the two core boards has a square groove with a length of 5cm x width 2.5cm x height of 10cm; after the two core boards are molded together, the upper top surface is synthesized into a cylindrical groove with a diameter of 5cm and a height of 10cm; The core boards are turned over and combined to form a square groove with a bottom surface of 5×5cm square and a height of 10cm, suitable for the third platen.
第三模具7的两块芯板翻转过来使用两块芯板组合形成的方槽模腔,能压制5×5×10cm的长方体试样,上液压油缸A1结合压板主动压制,下液压油缸A2辅助配合固定。The two core plates of the third mold 7 are turned over to use the square groove mold cavity formed by the combination of the two core plates, which can press a cuboid sample of 5×5×10 cm. The upper hydraulic cylinder A1 is actively pressed with the pressure plate, and the lower hydraulic cylinder A2 is assisted. Fit fixed.
如图1和图4所示,上液压油缸A1用螺母13固定装在立柱顶端,上液压油缸的第一压杆1还包括有连接块3和圆柱压头4,第一压杆1通过连接块3与圆柱压头4连接,圆柱压头4穿过上盖板8,上部输油管5连通圆柱压头4的中心孔,圆柱压头4底面中心孔接有下部输油管51。As shown in Figures 1 and 4, the upper hydraulic cylinder A1 is fixed on the top of the column with a nut 13. The first pressure rod 1 of the upper hydraulic cylinder also includes a connecting block 3 and a cylindrical pressure head 4. The first pressure rod 1 is connected to Block 3 is connected with cylindrical indenter 4, and cylindrical indenter 4 passes upper cover plate 8, and upper fuel delivery pipe 5 communicates with the central hole of cylindrical indenter 4, and the central hole of cylindrical indenter 4 bottom surface is connected with lower oil delivery pipe 51.
如图5所示,下部输油管51可拆卸地装接有长为8cm的十字型管路,十字型管路端部均设置喷雾喷孔伸入成型模具B内部。十字型管路适用于模腔为20cm×20cm×20cm,直管型下部输油管不能给方形成型模具内表面均匀喷洒润滑油,十字型更加均匀。As shown in FIG. 5 , the lower oil delivery pipe 51 is detachably connected with a cross-shaped pipeline with a length of 8 cm, and the ends of the cross-shaped pipeline are provided with spray holes extending into the inside of the forming mold B. The cross-shaped pipeline is suitable for the mold cavity of 20cm×20cm×20cm. The straight-type lower oil delivery pipe cannot evenly spray lubricating oil on the inner surface of the square forming mold, and the cross-shaped pipeline is more uniform.
如图4和图5所示,圆柱压头4底面连接的下部输油管51上穿套有与成型模具配合的压板组件,压板组件包括有第一压板18、第二压板17和第三压板16,第一压板18内框嵌套第二压板17,第二压板17内框嵌套第三压板16,第三压板顶面凹槽契合圆柱压头4。压板组件既叠合在一起,又可拆卸分离,使用时选择对应尺寸的压板与成型模具B的模腔适配。三个压板与成型模具B的三个方形模腔配合,圆柱压头4与第三模具7合模后的圆柱槽配合。上液压油缸A1通过圆柱压头向下提供作用力,圆柱压头贴合压板,作用力传递到下方所选相应尺寸的压板,压板直接接触煤岩散碎物料,加压成型。As shown in Fig. 4 and Fig. 5, the lower oil delivery pipe 51 connected to the bottom surface of the cylindrical indenter 4 is covered with a pressing plate assembly matched with the molding die, and the pressing plate assembly includes a first pressing plate 18, a second pressing plate 17 and a third pressing plate 16, The inner frame of the first pressing plate 18 nests the second pressing plate 17 , the inner frame of the second pressing plate 17 nests the third pressing plate 16 , and the groove on the top surface of the third pressing plate fits the cylindrical indenter 4 . The pressing plate assembly is not only stacked together, but also can be disassembled and separated. When in use, the pressing plate of the corresponding size is selected to fit the mold cavity of the forming mold B. The three pressing plates cooperate with the three square die cavities of the molding die B, and the cylindrical indenter 4 cooperates with the cylindrical groove after the third mold 7 is closed. The upper hydraulic cylinder A1 provides downward force through the cylindrical pressure head. The cylindrical pressure head fits the pressure plate, and the force is transmitted to the pressure plate of the corresponding size selected below. The pressure plate directly contacts the coal and rock scattered materials, and is pressurized and formed.
圆柱压头4底面直径为5cm,第一压板18为长20cm×宽20cm×高3cm的方块,第一压板上方开边长10cm深2mm的正方形槽契合第二压板;第二压板17为长10cm×宽10cm×高3cm的方块,第二压板上方开边长5cm深2mm的正方形槽契合第三压板;第三压板16为长5cm×宽5cm×高3cm的方块,第三压板上方开直径为5cm深2mm的正圆槽契合圆柱压头;所有的压板中心开孔能够使下部输油管51通过。Cylindrical indenter 4 bottom surface diameters are 5cm, and the first pressing plate 18 is the square of long 20cm * wide 20cm * high 3cm, and the square groove of opening side length 10cm deep 2mm fits the second pressing plate above the first pressing plate; The second pressing plate 17 is long 10cm ×Width 10cm×Height 3cm square, the square groove of length 5cm and depth 2mm above the second pressing plate fits the third pressing plate; The third pressing plate 16 is a square of length 5cm×Width 5cm×High 3cm, and the opening diameter above the third pressing plate is A perfect circular groove with a depth of 5 cm and a depth of 2 mm fits the cylindrical pressure head; all central openings of the pressure plate can allow the lower oil delivery pipe 51 to pass through.
下液压油缸A2用螺母13固定装在立柱底端;下液压油缸A2以及第二压杆14的作用是:1、仅有上液压油缸A1压制会导致20cm×20cm×20cm这样大的煤样下方松散,所以需要下液压油缸A2互相施力;2、煤样制成之后需要用下液压油缸A2将模具顶出来。The lower hydraulic cylinder A2 is fixed on the bottom of the column with a nut 13; the functions of the lower hydraulic cylinder A2 and the second pressure rod 14 are: 1. Only the pressing of the upper hydraulic cylinder A1 will result in a coal sample as large as 20cm×20cm×20cm. Loose, so the lower hydraulic cylinder A2 needs to apply force to each other; 2. After the coal sample is made, the lower hydraulic cylinder A2 needs to be used to push the mold out.
使用上述装置制备煤岩试验样品的过程是:The process of using the above-mentioned device to prepare coal rock test samples is:
步骤1、选择与组装配套成型模具,选取实验需求尺寸的样品制作模具进行组装,其中,第三模具有制备直径为5cm×高10cm的圆柱体试样和长5cm×宽5cm×高10cm的长方体试样的内腔,第一模具有制备长20cm宽×20cm×高20cm的立方体煤岩试样的内腔,第二模具有制备长10cm×宽10cm×高25cm的立方体煤岩试样的内腔;Step 1. Select and assemble the supporting molding mold, select the sample of the size required for the experiment to make a mold for assembly, and the third mold has a cylindrical sample with a diameter of 5cm x 10cm in height and a cuboid with a length of 5cm x width 5cm x 10cm in height For the inner cavity of the sample, the first mold has an inner cavity for preparing a cubic coal rock sample with a length of 20 cm wide × 20 cm × a height of 20 cm, and the second mold has an inner cavity for preparing a cubic coal rock sample with a length of 10 cm × width 10 cm × height 25 cm. Cavity;
步骤2、安装压板组件、上部输油管和下部输油管,选择模具相应的压板安装在圆柱压头底面,连接相应输油管均匀喷少量油至模具内壁;Step 2. Install the pressure plate assembly, the upper oil delivery pipe and the lower oil delivery pipe, select the corresponding pressure plate of the mold and install it on the bottom surface of the cylindrical indenter, connect the corresponding oil delivery pipe and spray a small amount of oil evenly to the inner wall of the mold;
步骤3、将配好的实验所需松散煤粉或岩粉放入模具中,利用下部输油管搅拌均匀物料,取下下部输油管;Step 3. Put the loose coal powder or rock powder required for the experiment into the mold, use the lower oil delivery pipe to stir the material evenly, and remove the lower oil delivery pipe;
步骤4、用螺母固定上、下盖板,从充气孔充入吸附气体稳定压力至1MPa并稳定30min。Step 4. Fix the upper and lower cover plates with nuts, fill the gas filling hole with adsorption gas to stabilize the pressure to 1MPa and stabilize it for 30min.
步骤5、利用上、下液压油缸对上、下压板双侧加压,使根据实验需要采用恒压压制或位移控制压制煤岩样成型。Step 5. Use the upper and lower hydraulic cylinders to pressurize both sides of the upper and lower platens, so that the coal rock sample is formed by constant pressure pressing or displacement control pressing according to the experimental requirements.
步骤6、气体释压,打开上侧盖板,使用下液压油缸将试样顶出模具,完成取样与含气试样的制备。Step 6: Release the pressure of the gas, open the upper side cover, and use the lower hydraulic cylinder to push the sample out of the mold to complete the sampling and the preparation of the gas-containing sample.
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