CN111567842A - Cigarette without burning by heating and method for producing cut tobacco thereof - Google Patents

Cigarette without burning by heating and method for producing cut tobacco thereof Download PDF

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Publication number
CN111567842A
CN111567842A CN202010407475.8A CN202010407475A CN111567842A CN 111567842 A CN111567842 A CN 111567842A CN 202010407475 A CN202010407475 A CN 202010407475A CN 111567842 A CN111567842 A CN 111567842A
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CN
China
Prior art keywords
heating
tobacco
atomizing agent
cigarette
drying
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Pending
Application number
CN202010407475.8A
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Chinese (zh)
Inventor
胡素霞
王娜
杨俊鹏
刘文婷
程占刚
潘婷婷
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China Tobacco Hubei Industrial LLC
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China Tobacco Hubei Industrial LLC
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Publication date
Application filed by China Tobacco Hubei Industrial LLC filed Critical China Tobacco Hubei Industrial LLC
Priority to CN202010407475.8A priority Critical patent/CN111567842A/en
Publication of CN111567842A publication Critical patent/CN111567842A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/36Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
    • A24B15/40Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
    • A24B15/403Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/10Roasting or cooling tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The application discloses a cigarette which is not burnt by heating and a method for manufacturing cut tobacco thereof. According to the manufacturing method of the tobacco shreds, after the atomizing agent is coated, the first heating at 50-60 ℃ and the second heating at 80-100 ℃ are sequentially carried out. By adopting the multi-section heating and low-temperature mode, the drying is milder, the volatilization loss of the atomizing agent attached to the surface of the cut tobacco leaves before the atomizing agent is permeated into the interior is reduced, and the high content of the atomizing agent after the storage is stable is improved. The cigarette made of the tobacco shreds obtained by the method has the advantages of sufficient cigarette taste, strong satisfaction, obvious flue-cured tobacco fragrance and good smoking quality.

Description

Cigarette without burning by heating and method for producing cut tobacco thereof
Technical Field
The invention relates to the technical field of cigarettes, in particular to a cigarette which is not combusted by heating and a method for manufacturing cut tobacco thereof.
Background
Along with international and domestic smoking control is becoming more and more strict, the attention of consumers to health problems is continuously promoted, the research strength of international and domestic cigarette enterprises is increased in the aspect of heating non-combustible novel tobacco, companies such as Fei Mo, English and American, Reynolds and the like successively release novel tobacco products, and a plurality of domestic cigarette enterprises also obtain achievements in the aspect of novel tobacco research and release novel tobacco products.
The novel tobacco which is not burnt by heating has the characteristic of heating tobacco shreds or tobacco extracts but not burning the tobacco shreds, a heating appliance and a cigarette bullet are needed when the novel tobacco is smoked, the tobacco shreds in the cigarette bullet are heated by a special heating source of the appliance, so that nicotine and fragrant substances in the tobacco shreds are volatilized, and smoke is generated to meet the requirements of smokers. The traditional tobacco shreds are not enough in applying amount of the atomizing agent due to insufficient absorption capacity, and generally cannot be directly used for novel tobacco, so that the heating non-combustible material used by the conventional novel tobacco product is basically reconstituted tobacco which takes tobacco components as main materials and applies a large amount of atomizing agent.
However, the reconstituted tobacco has a large difference from the traditional tobacco shreds in the aspect of physical characteristics, so that a series of problems of raw material hardening, large cigarette weight fluctuation, tobacco shred agglomeration of the reconstituted tobacco and the like in the rolling process are solved, the quality control in the cigarette process is not facilitated, and meanwhile, a large amount of adhesive needs to be applied while the atomizing agent is applied in the processing process of the reconstituted tobacco, so that certain non-tobacco smell is generated in the heating process, and the smoking quality of cigarettes which are not burnt during heating is reduced.
Disclosure of Invention
In order to solve the problems, the application provides a cigarette which is not burnt by heating and a method for manufacturing the cut tobacco, and the cut tobacco has higher content of an atomizing agent and better smoking quality after being stored stably.
The tobacco shreds obtained by the novel manufacturing method can be suitable for heating non-combustible cigarettes and can completely replace cigarettes adopting reconstituted tobacco sheets in the prior art. The inventors of the present application have surprisingly found that the rapid drying of the tobacco shreds coated with the atomizing agent by heating at a high temperature can accelerate the penetration of the atomizing agent into the tobacco shreds, i.e. have a faster absorption rate, but the high absorption rate is based on a high loss rate. The loss of the atomizing agent during drying after application of the atomizing agent is particularly high, so that a low retention in the cut tobacco leaves results. In order to improve the aerosol retention without particularly damaging the aerosol absorption rate, the inventor of the application overcomes the conventional thinking bias and reduces the heating temperature by adopting a multi-stage heating mode. Based on this, the invention of the present application has been completed.
According to a first embodiment of the present application, there is provided a method of manufacturing a tobacco shred for heat non-combustible cigarette, comprising the steps of:
(1) coating the surface of tobacco shred with atomizing agent;
(2) heating the cut tobacco leaves treated in the step (1) for the first time at 50-60 ℃, for example, the temperature is preferably 52-58 ℃, particularly preferably 56 ℃;
(3) the tobacco shreds after the primary tobacco shred drying are heated for the second time at the temperature of 80-100 ℃, for example, the temperature range is preferably 85-95 ℃, and particularly preferably 92 ℃.
The above-mentioned "atomizing agent" may employ a conventional atomizing agent such as glycerin, propylene glycol and the like. The solvent used for the atomizing agent may be water or ethanol, etc. However, the inventors of the present application have surprisingly found that the solvent of the nebulant is preferably water. Compared with the mode of using alcohol such as ethanol and the like as a solvent, on one hand, the molecular size of water is smaller than that of the alcohol solvent, on the other hand, the compatibility of pectin and fibers which are main components contained in the tobacco shreds to water is better, so that the atomizing agent using water as the solvent has higher absorption rate and higher permeability, the touch feeling of the prepared tobacco shreds is smoother, and the touch feeling stickiness of the tobacco shreds prepared by the atomizing agent using alcohol as the solvent is avoided.
Here, the mode of applying the atomizing agent is preferably spraying. As the equipment for spraying, a conventional spraying device can be used. As regards the size of the spray, it can be adjusted according to the actual rate of spraying. The spraying mode can obtain a coating mode with a milder speed, and avoids the phenomenon that the atomization absorption exceeds the saturated absorption amount due to the excessively high coating speed, so that the phenomenon of're-spitting' occurs in the drying process, namely the atomization agent in the tobacco shreds seeps outwards.
It will be readily appreciated by those skilled in the art that the coating may also be by dipping.
The time for the first heating and the second heating is preferably 0.4-0.7 min, preferably 0.5-0.6 min, and particularly preferably 0.52min, based on 1kg of tobacco shred. If the heating time exceeds the range, the continuous absorption of the atomizing agent cannot be obviously improved, and the atomizing agent cannot be obviously reduced; if the heating time is too short, the absorption of the atomizing agent is not thorough.
The tobacco shreds to be coated with the atomising agent preferably have a suitable moisture content. On the basis of the above, some conventional operations, such as the method described in patent CN102524936A, can be performed, specifically: after the tobacco leaves are loosened and moistened, the water content of the tobacco leaves is controlled to be 16-19%, the water content of the tobacco leaves is reduced by 1-3% by applying a flexible winnowing process, then the tobacco leaves are subjected to microwave drying, and the microwave frequency is set as follows: 2450 +/-50 MHz, microwave output power: 10-50 KW, drying time: 1-3 min, and the discharging temperature is 40-60 ℃.
Intermediate heating at 60-70 ℃ can be further included between the step (2) and the step (3), and the temperature of the intermediate heating is preferably 62-68 ℃, particularly preferably 65 ℃.
It is known to those skilled in the art that the heating devices involved in the first heating, the intermediate heating and the second heating are preferably multi-stage thin-plate machines common to cut-tobacco drying processes.
Before the step (1), the tobacco shreds are soaked in a soaking solution, wherein the soaking solution comprises 45-62 wt% of carboxymethyl chitosan, 0-8 wt% of a binder and the balance of a solvent according to parts by mass. The content of the carboxymethyl chitosan is preferably 50 to 60wt%, particularly preferably 55wt%, and the content of the adhesive is preferably 2 to 5wt%, particularly preferably 3 wt%.
It is understood that the "balance" is specifically calculated from 100wt% to carboxymethyl chitosan content wt% to binder content wt%.
The carboxymethyl chitosan can endow the surface of tobacco shreds with hydrophilic groups of carboxyl, has better compatibility with solute alcohol contained in the atomizing agent after the atomizing agent, promotes the alcohol to permeate into the tobacco shreds more easily, and improves the absorption rate of the carboxymethyl chitosan on the solute alcohol component contained in the atomizing agent. In addition, carboxyl contained in the carboxymethyl chitosan can partially form intermolecular hydrogen bonds with solute alcohol of the atomizing agent, and the chemical adsorption with the solute alcohol is improved. In the heating process of the step (2) and the step (3), the solute alcohol adsorbed by the carboxymethyl chitosan is not desorbed. However, in the pumping process, under the pumping heating (generally 250-300 ℃), the carboxymethyl chitosan can be desorbed.
Specific types of carboxymethyl chitosan (e.g., acetyl degree, etc.) are not particularly required, and these do not particularly impair the function of carboxymethyl chitosan.
The adhesive is used for forming a coating film on the surface of the tobacco shreds by the impregnation liquid, so that the adhesive force of the carboxymethyl chitosan on the surface of the tobacco shreds is improved. It is understood that the carboxyl group in carboxymethyl chitosan also has an affinity with the hydrophilic group of tobacco leaf thread to attach to it without the addition of a binder.
Examples of the adhesive include CMC and PVA, and other hydrophilic adhesive substances.
The solvent is C1-C4 alcohol and/or water, and the C1-C4 alcohol is methanol, ethanol or isopropanol, preferably water.
The method comprises the steps of soaking in a soaking solution such as carboxymethyl chitosan and drying, wherein the drying temperature is 20-40 ℃. The drying may be natural drying or drying.
According to a second embodiment of the present application, there is provided a heat-nonflammable cigarette having the tobacco shred obtained by the above-described production method.
According to the manufacturing method of the tobacco shreds, after the atomizing agent is coated, the first heating at 50-60 ℃ and the second heating at 80-100 ℃ are sequentially carried out. By adopting the multi-section heating and low-temperature mode, the drying is milder, the volatilization loss of the atomizing agent attached to the surface of the cut tobacco leaves before the atomizing agent is permeated into the interior is reduced, and the high content of the atomizing agent after the storage is stable is improved.
Detailed Description
The following are specific examples of the present application and further describe the technical solutions of the present application, but the present application is not limited to these examples.
Example 1
10kg of cut tobacco leaves which have been subjected to water-controlling treatment are dipped in a dipping solution (containing 45wt% of carboxymethyl chitosan and the balance of water) and dipped at 20 ℃ for 30 min. After the impregnation is completed, the residual liquid is fully absorbed by using filter paper, and then the air is dried.
The surface of the tobacco shreds thus impregnated was sprayed with an atomizing agent (a mixture of glycerin and water, the glycerin volume concentration being 25 vol%) using a spray gun. The remaining liquid was thoroughly aspirated off with filter paper.
And putting the tobacco shreds sprayed with the atomizing agent into a thin plate for drying, adjusting the temperature of the tobacco shreds to 50 ℃ for first heating, and stopping heating after 7 min. And adjusting the drying temperature of the thin plate to 60 ℃ for second heating, and stopping heating after 7 min. And then adjusting the drying temperature of the thin plate to 80 ℃ for secondary heating, and taking out the thin plate after 7 min. Tests show that the content of the fogging agent in the cut tobacco is 30 wt%.
The content of the test atomizing agent in the cut tobacco obtained above is 21wt% after the cut tobacco is stored in an environment of 25 ℃ for 15 hours respectively.
Example 2
10kg of cut tobacco leaves which had been subjected to water-controlling treatment were dipped in a dipping solution (containing 62wt% of carboxymethyl chitosan, 8wt% of PVA and the balance of water) and dipped at 40 ℃ for 10 min. After the impregnation is completed, the residual liquid is fully absorbed by using filter paper, and then the air is dried.
The surface of the tobacco shreds thus impregnated was sprayed with an atomizing agent (a mixture of glycerin and water, the volume concentration of glycerin being 55 vol%) using a spray gun. The remaining liquid was thoroughly aspirated off with filter paper.
And putting the tobacco shreds sprayed with the atomizing agent into a thin plate for drying, adjusting the temperature of the tobacco shreds to 60 ℃ for first heating, and stopping heating after 4 min. And adjusting the drying temperature of the thin plate to 70 ℃ for second heating, and stopping heating after 4 min. And then adjusting the drying temperature of the thin plate to be 100 ℃ for secondary heating, and taking out the thin plate after 7 min. The testing shows that the content of the fogging agent in the cut tobacco is 32 wt%.
The test aerosol retention of the cut tobacco obtained above after storage at 25 ℃ for 15h was 25% (i.e. percentage relative to the aerosol content before storage).
Example 3
10kg of cut tobacco leaves which had been subjected to water-controlling treatment were dipped in a dipping solution (containing 56wt% of carboxymethyl chitosan, 4wt% of PVA and the balance of water) and dipped at 30 ℃ for 20 min. After the impregnation is completed, the residual liquid is fully absorbed by using filter paper, and then the air is dried.
The surface of the tobacco shreds thus impregnated was sprayed with an atomizing agent (a mixture of glycerin and water, the volume concentration of glycerin being 40 vol%) using a spray gun. The remaining liquid was thoroughly aspirated off with filter paper.
And putting the tobacco shreds sprayed with the atomizing agent into a thin plate for drying, adjusting the temperature of the tobacco shreds to 56 ℃ for first heating, and stopping heating after 5 min. And adjusting the drying temperature of the thin plate to 64 ℃ for second heating, and stopping heating after 5 min. And then adjusting the drying temperature of the thin plate to 94 ℃ for secondary heating, and taking out the thin plate from the drying process after 5 min. The testing shows that the content of the fogging agent in the cut tobacco is 34 wt%.
The test aerosol retention of the cut tobacco obtained above after storage at 25 ℃ for 15h was 30% (i.e. percentage relative to the aerosol content before storage).
Example 4
10kg of cut tobacco leaves which had been subjected to water-controlling treatment were dipped in a dipping solution (containing 50wt% of carboxymethyl chitosan, 5wt% of PVA and the balance of water) and dipped at 30 ℃ for 20 min. After the impregnation is completed, the residual liquid is fully absorbed by using filter paper, and then the air is dried.
The surface of the tobacco shreds thus impregnated was sprayed with an atomizing agent (a mixture of glycerin and water, the glycerin volume concentration being 50 vol%) using a spray gun. The remaining liquid was thoroughly aspirated off with filter paper.
And putting the tobacco shreds sprayed with the atomizing agent into a thin plate for drying, adjusting the temperature of the tobacco shreds to 54 ℃ for first heating, and stopping heating after 5 min. And adjusting the drying temperature of the thin plate to 66 ℃ for second heating, and stopping heating after 5 min. And then adjusting the drying temperature of the thin plate to 93 ℃ for secondary heating, and taking out the thin plate after 5 min. Tests show that the content of the fogging agent in the cut tobacco is 35 wt%.
The test aerosol retention of the cut tobacco obtained above after storage at 25 ℃ for 15h was 26% (i.e. percentage relative to the aerosol content before storage).
Example 5
10kg of cut tobacco leaves which had been subjected to water-controlling treatment were dipped in a dipping solution (containing 50wt% of carboxymethyl chitosan, 5wt% of PVA and the balance of water) and dipped at 30 ℃ for 20 min. After the impregnation is completed, the residual liquid is fully absorbed by using filter paper, and then the air is dried.
The surface of the tobacco shreds thus impregnated was sprayed with an atomizing agent (a mixture of glycerin and water, the volume concentration of glycerin being 40 vol%) using a spray gun. The remaining liquid was thoroughly aspirated off with filter paper.
And putting the tobacco shreds sprayed with the atomizing agent into a thin plate for drying, adjusting the temperature of the tobacco shreds to 55 ℃ for first heating, and stopping heating after 6 min. And adjusting the drying temperature of the thin plate to 65 ℃ for second heating, and stopping heating after 6 min. And then adjusting the drying temperature of the thin plate to 90 ℃ for secondary heating, and taking out the thin plate after 6 min. The testing shows that the content of the fogging agent in the cut tobacco is 34 wt%.
The cut tobacco obtained above was stored at 25 ℃ for 15 hours and the test aerosol content was 27% (i.e. percentage relative to the aerosol content before storage).
Comparative example 1
In this example, the cut tobacco leaves sprayed with the atomizing agent were dried at 300 ℃ for the same time as the first heating, the intermediate heating and the second heating in example 3, and the other conditions were the same as in example 5. The testing shows that the content of the fogging agent in the cut tobacco is 34 wt%. The test nebulant content was 18wt% after storage for 15h at 25 ℃.
As can be seen from the data of examples 1-5 and comparative example 1, the content of the atomizing agent after being stored for 15 hours in the environment of 25 ℃ in the application example 3 is significantly higher than that in the comparative example 1, which shows that the multi-stage heating mode in the application can significantly improve the content of the atomizing agent after being stored stably.
The specific embodiments described herein are merely illustrative of the spirit of the application. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the present application as defined by the appended claims.

Claims (9)

1. A method for manufacturing tobacco shreds for cigarette by heating and non-burning is characterized by comprising the following steps:
(1) coating the surface of tobacco shred with atomizing agent;
(2) heating the cut tobacco leaves treated in the step (1) for the first time at 50-60 ℃;
(3) and heating the tobacco shreds subjected to the primary tobacco shred drying for the second time at the temperature of 80-100 ℃.
2. The manufacturing method according to claim 1, further comprising an intermediate heating at 60-70 ℃ between the step (2) and the step (3).
3. The method of claim 1, wherein the coating is by spraying.
4. The preparation method according to claim 1, wherein the step (1) is further carried out before dipping the cut tobacco leaves in dipping solution, and the dipping solution comprises 45-62 wt% of carboxymethyl chitosan, 0-8 wt% of adhesive and the balance of solvent.
5. The method of manufacturing according to claim 4, wherein the binder is CMC and/or PVA.
6. The method according to claim 4, wherein the step of drying is further carried out after the step of dipping, and the temperature of drying is 20-40 ℃.
7. The method according to claim 4, wherein the solvent is C1-C4 alcohol and/or water.
8. The method according to claim 1, wherein the first heating and the second heating are carried out for 0.4 to 0.7min, based on 1kg of cut tobacco leaves.
9. A cigarette which is not burned by heating, characterized by comprising the tobacco shreds obtained by the production method according to any one of claims 1 to 8.
CN202010407475.8A 2020-05-14 2020-05-14 Cigarette without burning by heating and method for producing cut tobacco thereof Pending CN111567842A (en)

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CN202010407475.8A CN111567842A (en) 2020-05-14 2020-05-14 Cigarette without burning by heating and method for producing cut tobacco thereof

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CN202010407475.8A CN111567842A (en) 2020-05-14 2020-05-14 Cigarette without burning by heating and method for producing cut tobacco thereof

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4449541A (en) * 1981-06-02 1984-05-22 R. J. Reynolds Tobacco Company Tobacco treatment process
CN104910444A (en) * 2015-04-08 2015-09-16 湖北中烟工业有限责任公司 Humectant for paper-making reconstituted tobacco and application thereof
CN109602061A (en) * 2018-12-18 2019-04-12 湖北中烟工业有限责任公司 A kind of novel tobacco pipe tobacco processing technology
CN109820233A (en) * 2019-03-18 2019-05-31 云南中烟工业有限责任公司 A kind of preparation method heating the cigarette shreds that do not burn for periphery
CN110150710A (en) * 2019-04-30 2019-08-23 安徽中烟工业有限责任公司 A method of cigarette pipe tobacco is prepared by tobacco leaf or raw material pipe tobacco
CN110679977A (en) * 2019-10-24 2020-01-14 湖北中烟工业有限责任公司 Novel tobacco shred raw material preparation process
CN110771937A (en) * 2019-11-18 2020-02-11 福建中烟工业有限责任公司 Tobacco shred and preparation method and application thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4449541A (en) * 1981-06-02 1984-05-22 R. J. Reynolds Tobacco Company Tobacco treatment process
CN104910444A (en) * 2015-04-08 2015-09-16 湖北中烟工业有限责任公司 Humectant for paper-making reconstituted tobacco and application thereof
CN109602061A (en) * 2018-12-18 2019-04-12 湖北中烟工业有限责任公司 A kind of novel tobacco pipe tobacco processing technology
CN109820233A (en) * 2019-03-18 2019-05-31 云南中烟工业有限责任公司 A kind of preparation method heating the cigarette shreds that do not burn for periphery
CN110150710A (en) * 2019-04-30 2019-08-23 安徽中烟工业有限责任公司 A method of cigarette pipe tobacco is prepared by tobacco leaf or raw material pipe tobacco
CN110679977A (en) * 2019-10-24 2020-01-14 湖北中烟工业有限责任公司 Novel tobacco shred raw material preparation process
CN110771937A (en) * 2019-11-18 2020-02-11 福建中烟工业有限责任公司 Tobacco shred and preparation method and application thereof

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Title
于广利 等: "《糖药物学》", 31 October 2012, 中国海洋大学出版社 *

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Application publication date: 20200825