CN111514062A - Liquid crystal type amino acid facial cleanser - Google Patents
Liquid crystal type amino acid facial cleanser Download PDFInfo
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- CN111514062A CN111514062A CN202010205223.7A CN202010205223A CN111514062A CN 111514062 A CN111514062 A CN 111514062A CN 202010205223 A CN202010205223 A CN 202010205223A CN 111514062 A CN111514062 A CN 111514062A
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- liquid crystal
- amino acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0295—Liquid crystals
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a liquid crystal form amino acid facial cleanser, which comprises the following components in percentage by weight: 15-18 parts of cocoyl sodium glycinate, 20-25 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3-5 parts of modified corn starch, 15-18 parts of glycerol, 2.5-4 parts of acrylic copolymer, 1.5-2 parts of stearic acid, 3-5 parts of sodium citrate, 2-2.5 parts of pearlescent diester, 22-25 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.3-0.6 part of phenoxyethanol and the balance of water. According to the liquid crystal amino acid facial cleanser and the preparation method thereof, phenoxyethanol is used as a preservative, essence and pigment are not added, the nature is mild, skin allergy and irritation are not caused, the pH value of the formula is weakly acidic, foams are fine and rich, and the cleansing effect is good. The formula of the invention has simple process and is convenient for production.
Description
Technical Field
The invention relates to the technical field of daily chemical products, and in particular relates to a liquid crystal type amino acid facial cleanser and a preparation method thereof.
Background
With the continuous improvement of living standard, cosmetics are changed from luxury products to common consumer products, and the requirements of people on facial cleansing products are also developed from daily cleaning to requirements of mildness, safety, stability and the like.
The amino acid cleansing products on the market are diversified and have different qualities.
The viscosity of the amino acid surfactant changes greatly along with the temperature, and after the amino acid surfactant is stored for a period of time, the product can have the defects of coarseness, water discharge and the like; in addition, the preparation process of the amino acid face cleaning product is difficult to control, particles are easy to generate after the raw materials are circulated in a cold and hot mode, paste is easy to coarsen, particles can be generated when the raw materials are improperly controlled, the preparation is quite difficult, the requirement on process control is extremely high, and the production difficulty is greatly increased.
Aiming at the defects in the prior art, the invention provides the liquid crystal amino acid facial cleanser with easily controlled preparation process and good stability and the preparation process thereof.
The amino acid facial cleanser has safe components and good cleaning effect, and is suitable for any skin.
The invention content is as follows:
in order to achieve the purpose, the liquid crystal amino acid facial cleanser provided by the invention comprises the following raw materials in parts by weight: 15-18 parts of cocoyl sodium glycinate, 20-25 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3-5 parts of modified corn starch, 15-18 parts of glycerol, 2.5-4 parts of acrylic copolymer, 1.5-2 parts of stearic acid, 3-5 parts of sodium citrate, 2-2.5 parts of pearlescent diester, 22-25 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.3-0.6 part of phenoxyethanol and the balance of water.
Example 1: the material is prepared from the following raw materials in parts by weight: 15 parts of cocoyl sodium glycinate, 20 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3 parts of modified corn starch, 15 parts of glycerol, 3 parts of acrylic copolymer, 1.5 parts of stearic acid, 3 parts of sodium citrate, 2 parts of pearlescent diester, 22 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.5 part of phenoxyethanol and 15 parts of water.
A preparation method of liquid crystal type amino acid facial cleanser comprises the following steps:
(1) adding 3 parts of modified corn starch into a beaker, adding a proper amount of deionized water, stirring for 2min, adding 15 parts of glycerol, stirring uniformly, adding 3 parts of acrylic copolymer, stirring for 2min, and dispersing uniformly.
(2) Adding 15 parts of cocoyl sodium glycinate, uniformly stirring, adding 20 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, placing a beaker in a water bath device at 93 ℃, starting stirring, wherein the stirring speed is 120-150 rpm;
(3) after the temperature of the materials in the beaker rises to 90 ℃, stirring (at 150 rpm) for 40min, adding 1.5 parts of stearic acid, 3 parts of sodium citrate and 2 parts of pearlescent diester, stirring until the materials are completely dissolved, adding 22 parts of liquid crystal thickener, and continuously keeping the temperature of 90 ℃ constant at the stirring speed of 50-60 rpm;
when the liquid crystal thickener is completely dissolved, stirring at the constant temperature of 90 ℃ (at 150 rpm) for 50min, stopping heating, and stirring at room temperature to cool (at 60-80 rpm);
(4) cooling to 45 deg.C, adding phase D, stirring at low speed (60-70 rpm), cooling to 42 deg.C, and discharging.
Example 2: the material is prepared from the following raw materials in parts by weight: 18 parts of cocoyl sodium glycinate, 22 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3 parts of modified corn starch, 15 parts of glycerol, 3 parts of acrylic copolymer, 1.5 parts of stearic acid, 3 parts of sodium citrate, 2 parts of pearlescent diester, 22 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.5 part of phenoxyethanol and 10 parts of water.
A preparation method of liquid crystal type amino acid facial cleanser comprises the following steps:
(1) adding 3 parts of modified corn starch into a beaker, adding a proper amount of deionized water, stirring for 2min, adding 15 parts of glycerol, stirring uniformly, adding 3 parts of acrylic copolymer, stirring for 2min, and dispersing uniformly.
(2) Adding 18 parts of sodium cocoyl glycinate, uniformly stirring, adding 22 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, placing a beaker in a water bath device at 93 ℃, starting stirring, wherein the stirring speed is 120-150 rpm;
(3) after the temperature of the materials in the beaker rises to 90 ℃, stirring (at 150 rpm) for 40min, adding 1.5 parts of stearic acid, 3 parts of sodium citrate and 2 parts of pearlescent diester, stirring until the materials are completely dissolved, adding 22 parts of liquid crystal thickener, and continuously keeping the temperature of 90 ℃ constant at the stirring speed of 50-60 rpm;
when the liquid crystal thickener is completely dissolved, stirring at the constant temperature of 90 ℃ (at 150 rpm) for 50min, stopping heating, and stirring at room temperature to cool (at 60-80 rpm);
(4) cooling to 45 deg.C, adding phase D, stirring at low speed (60-70 rpm), cooling to 42 deg.C, and discharging.
Example 3: the material is prepared from the following raw materials in parts by weight: 15 parts of cocoyl sodium glycinate, 22 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3 parts of modified corn starch, 16 parts of glycerol, 3 parts of acrylic copolymer, 1.5 parts of stearic acid, 3 parts of sodium citrate, 2 parts of pearlescent diester, 22 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.5 part of phenoxyethanol and 12 parts of water.
A preparation method of liquid crystal type amino acid facial cleanser comprises the following steps:
(1) adding 3 parts of modified corn starch into a beaker, adding a proper amount of deionized water, stirring for 2min, adding 16 parts of glycerol, stirring uniformly, adding 3 parts of acrylic copolymer, stirring for 2min, and dispersing uniformly.
(2) Adding 15 parts of sodium cocoyl glycinate, uniformly stirring, adding 22 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, placing a beaker in a water bath device at 93 ℃, starting stirring, wherein the stirring speed is 120-150 rpm;
(3) after the temperature of the materials in the beaker rises to 90 ℃, stirring (at 150 rpm) for 40min, adding 1.5 parts of stearic acid, 3 parts of sodium citrate and 2 parts of pearlescent diester, stirring until the materials are completely dissolved, adding 22 parts of liquid crystal thickener, and continuously keeping the temperature of 90 ℃ constant at the stirring speed of 50-60 rpm;
when the liquid crystal thickener is completely dissolved, stirring at the constant temperature of 90 ℃ (at 150 rpm) for 50min, stopping heating, and stirring at room temperature to cool (at 60-80 rpm);
(5) cooling to 45 deg.C, adding phase D, stirring at low speed (60-70 rpm), cooling to 42 deg.C, and discharging.
The amino acid facial cleanser disclosed by the invention has the advantages of easiness in control of the preparation process, good stability, faintly acid, easiness in foaming and washing in use, rich foam, and fresh and clean skin which is not tight after washing.
Claims (2)
1. The liquid crystal type amino acid facial cleanser is characterized in that: the amino acid facial cleanser comprises the following components: water, sodium cocoyl glycinate, sodium lauroyl sarcosinate/sodium lauroyl glutamate, modified corn starch, glycerol, acrylic acid copolymer, stearic acid, sodium citrate, pearlescent diester, liquid crystal thickener and phenoxyethanol.
2. The weight percentage of each component is as follows: 15-18 parts of cocoyl sodium glycinate, 20-25 parts of sodium lauroyl sarcosinate/sodium lauroyl glutamate, 3-5 parts of modified corn starch, 15-18 parts of glycerol, 2.5-4 parts of acrylic copolymer, 1.5-2 parts of stearic acid, 3-5 parts of sodium citrate, 2-2.5 parts of pearlescent diester, 22-25 parts of liquid crystal thickener (sodium taurate laurate/modified corn starch/lauric acid/myristic acid), 0.3-0.6 part of phenoxyethanol and the balance of water.
Priority Applications (1)
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CN202010205223.7A CN111514062A (en) | 2020-03-23 | 2020-03-23 | Liquid crystal type amino acid facial cleanser |
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CN202010205223.7A CN111514062A (en) | 2020-03-23 | 2020-03-23 | Liquid crystal type amino acid facial cleanser |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
CN113786360A (en) * | 2021-09-23 | 2021-12-14 | 广州欧米亚生物科技有限公司 | Red mud amino acid facial cleanser and preparation method thereof |
CN114306131A (en) * | 2022-01-27 | 2022-04-12 | 广州百孚润化工有限公司 | Washing composition based on modified corn starch and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103655240A (en) * | 2013-11-28 | 2014-03-26 | 广州百孚润化工有限公司 | Liquid crystal thickener, preparation method and application thereof |
CN105616188A (en) * | 2016-03-09 | 2016-06-01 | 广州千百度化妆品有限公司 | Acne-removal facial cleanser and preparation method thereof |
CN106491381A (en) * | 2016-12-06 | 2017-03-15 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle pure amino acid facial cleaning cream of crystal type |
-
2020
- 2020-03-23 CN CN202010205223.7A patent/CN111514062A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103655240A (en) * | 2013-11-28 | 2014-03-26 | 广州百孚润化工有限公司 | Liquid crystal thickener, preparation method and application thereof |
CN105616188A (en) * | 2016-03-09 | 2016-06-01 | 广州千百度化妆品有限公司 | Acne-removal facial cleanser and preparation method thereof |
CN106491381A (en) * | 2016-12-06 | 2017-03-15 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle pure amino acid facial cleaning cream of crystal type |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112494342A (en) * | 2020-12-28 | 2021-03-16 | 广州天翼化妆品有限公司 | Liquid crystal amino acid facial cleanser and preparation method thereof |
CN113786360A (en) * | 2021-09-23 | 2021-12-14 | 广州欧米亚生物科技有限公司 | Red mud amino acid facial cleanser and preparation method thereof |
CN114306131A (en) * | 2022-01-27 | 2022-04-12 | 广州百孚润化工有限公司 | Washing composition based on modified corn starch and preparation method thereof |
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Application publication date: 20200811 |