CN111458247A - Automatic liquid changing device and method based on buffer material erosion test - Google Patents

Automatic liquid changing device and method based on buffer material erosion test Download PDF

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CN111458247A
CN111458247A CN202010434053.XA CN202010434053A CN111458247A CN 111458247 A CN111458247 A CN 111458247A CN 202010434053 A CN202010434053 A CN 202010434053A CN 111458247 A CN111458247 A CN 111458247A
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liquid
subsystem
changing
erosion
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谢敬礼
曹胜飞
刘月妙
高玉峰
马利科
李娜娜
张奇
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Beijing Research Institute of Uranium Geology
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Abstract

本发明公开了一种基于缓冲材料冲蚀试验的自动换液装置及方法。该装置包括多个换液子系统;每一换液子系统的出液端口均与冲蚀实验装置的进液端连接;每一换液子系统的进液端口均与冲蚀实验装置的出液端连接;换液子系统设置有定时阀,换液子系统根据定时阀的开合状态交替进行换液操作;换液子系统中的检测装置用于检测装液容器内溶液的参数。本发明提供的基于缓冲材料冲蚀试验的自动换液装置及方法,能够在自动换液过程中实现自动测定溶液的浊度、电导率。

Figure 202010434053

The invention discloses an automatic liquid changing device and method based on a buffer material erosion test. The device includes a plurality of liquid exchange subsystems; the liquid outlet port of each liquid exchange subsystem is connected with the liquid inlet end of the erosion experimental device; the liquid inlet port of each liquid exchange subsystem is connected with the outlet of the erosion experimental device. The liquid end is connected; the liquid exchange subsystem is provided with a timing valve, and the liquid exchange subsystem alternately performs liquid exchange operations according to the opening and closing states of the timing valve; the detection device in the liquid exchange subsystem is used to detect the parameters of the solution in the liquid container. The automatic liquid exchange device and method based on the buffer material erosion test provided by the invention can realize automatic determination of the turbidity and conductivity of the solution during the automatic liquid exchange process.

Figure 202010434053

Description

一种基于缓冲材料冲蚀试验的自动换液装置及方法A kind of automatic liquid exchange device and method based on buffer material erosion test

技术领域technical field

本发明涉及高放废物地质处置缓冲材料性能试验技术领域,特别是涉及一种基于缓冲材料冲蚀试验的自动换液装置及方法。The invention relates to the technical field of buffer material performance test for geological disposal of high-level radioactive waste, in particular to an automatic liquid exchange device and method based on a buffer material erosion test.

背景技术Background technique

地下水是高放废物向处置库外界空间泄漏的载体。缓冲材料作为填充在废物罐和地质体之间的最后一道人工屏障,起着水力学屏障的重要作用,阻滞地下水(可能含有腐蚀物质)流到废物罐表面,同时阻滞废物罐水溶化合物和核素渗漏到围岩中。大量研究表明,膨润土是适宜的缓冲材料的基材,因此必须了解膨润土在不同溶液条件下的冲蚀特性。Groundwater is the carrier for the leakage of high-level radioactive waste to the external space of the repository. As the last artificial barrier filled between the waste tank and the geological body, the buffer material plays an important role as a hydraulic barrier, blocking the flow of groundwater (which may contain corrosive substances) to the surface of the waste tank, while blocking the waste tank water-soluble compounds and Nuclides seep into the surrounding rock. Numerous studies have shown that bentonite is a suitable substrate for buffer materials, so it is necessary to understand the erosion characteristics of bentonite under different solution conditions.

研究膨润土的冲蚀实验不仅需要每天手动测定其溶液的参数,参数包括浊度、电导率,还需要不定期更换溶液。现有的设备比较分散,每次更换溶液及测定其浊度和电导率都比较费时费力。Studying the erosion experiment of bentonite not only requires manual determination of the parameters of its solution every day, including turbidity and electrical conductivity, but also needs to change the solution from time to time. The existing equipment is relatively scattered, and it is time-consuming and laborious to change the solution and measure its turbidity and conductivity each time.

发明内容SUMMARY OF THE INVENTION

本发明的目的是提供一种基于缓冲材料冲蚀试验的自动换液装置及方法,能够在自动换液过程中实现自动测定溶液的参数。The purpose of the present invention is to provide an automatic liquid exchange device and method based on the erosion test of buffer materials, which can realize the automatic determination of the parameters of the solution during the automatic liquid exchange process.

为实现上述目的,本发明提供了如下方案:For achieving the above object, the present invention provides the following scheme:

本发明提供了一种基于缓冲材料冲蚀试验的自动换液装置,包括:The invention provides an automatic liquid exchange device based on the erosion test of buffer material, comprising:

多个换液子系统;Multiple fluid exchange subsystems;

每一所述换液子系统的出液端口均与冲蚀实验装置进液端连接;每一所述换液子系统的进液端口均与所述冲蚀实验装置出液端连接;所述冲蚀实验装置内置有缓冲材料;The liquid outlet port of each of the liquid exchange subsystems is connected to the liquid inlet end of the erosion experiment device; the liquid inlet port of each of the liquid exchange subsystems is connected to the liquid outlet end of the erosion experiment device; the The erosion experiment device has a built-in buffer material;

所述换液子系统的加液端口用于对所述换液子系统中的装液容器添加冲蚀实验所用溶液;所述换液子系统的出液端口用于将所述装液容器中的溶液排入所述冲蚀实验装置进液端;所述换液子系统的进液端口用于将所述冲蚀实验装置出液端流出的冲蚀溶液流入所述装液容器;所述换液子系统的排液端口用于将所述装液容器中的溶液排出;所述换液子系统设置有定时阀,所述换液子系统根据所述定时阀的开合状态交替进行换液操作;所述换液子系统中的检测装置用于检测所述装液容器内溶液的参数。The liquid addition port of the liquid exchange subsystem is used to add the solution used in the erosion experiment to the liquid filling container in the liquid exchange subsystem; the liquid outlet port of the liquid exchange subsystem is used to add the liquid filling container to the liquid container. The solution is discharged into the liquid inlet end of the erosion experiment device; the liquid inlet port of the liquid exchange subsystem is used to flow the erosion solution from the outlet end of the erosion experiment device into the liquid container; the The discharge port of the liquid exchange subsystem is used to discharge the solution in the liquid container; the liquid exchange subsystem is provided with a timing valve, and the liquid exchange subsystem alternately changes according to the opening and closing states of the timing valve. liquid operation; the detection device in the liquid exchange subsystem is used to detect the parameters of the solution in the liquid container.

可选的,optional,

所述换液子系统,具体包括:The liquid exchange subsystem specifically includes:

设置有进液定时阀的进液管、设置有出液定时阀的出液管、设置有加液定时阀的加液管、设置有排液定时阀的排液管和装液容器;The liquid inlet pipe is provided with the liquid inlet timing valve, the liquid outlet pipe is provided with the liquid outlet timing valve, the liquid addition pipe is provided with the liquid addition timing valve, the liquid discharge pipe and the liquid filling container are provided with the liquid discharge timing valve;

所述进液管的出液端口与所述冲蚀实验装置进液端连接,所述进液管的进液端置于所述装液容器内;The liquid outlet port of the liquid inlet pipe is connected with the liquid inlet end of the erosion experiment device, and the liquid inlet end of the liquid inlet pipe is placed in the liquid container;

所述出液管的进液端口与所述冲蚀实验装置出液端连接,所述出液管的出液端置于所述装液容器内;The liquid inlet port of the liquid outlet pipe is connected with the liquid outlet end of the erosion experiment device, and the liquid outlet end of the liquid outlet pipe is placed in the liquid container;

所述加液管的出液端置于所述装液容器内,所述加液管的加液端口用于加入冲蚀实验所用溶液;The liquid outlet end of the liquid addition pipe is placed in the liquid filling container, and the liquid addition port of the liquid addition pipe is used for adding the solution used in the erosion experiment;

所述排液管的进液端设置在所述装液容器的底部,所述排液管的排液端口用于将所述装液容器内的溶液排出。The liquid inlet end of the liquid discharge pipe is arranged at the bottom of the liquid filling container, and the liquid discharge port of the liquid discharge pipe is used for discharging the solution in the liquid filling container.

可选的,所述检测装置,具体包括:Optionally, the detection device specifically includes:

浊度检测装置和电导率检测装置;Turbidity detection device and conductivity detection device;

所述浊度检测装置的检测部置于所述装液容器的内部,所述浊度检测装置用于检测所述装液容器内溶液的浊度;The detection part of the turbidity detection device is placed inside the liquid container, and the turbidity detection device is used to detect the turbidity of the solution in the liquid container;

所述电导率检测装置的检测部置于所述装液容器的内部,所述电导率检测装置用于检测所述装液容器内溶液的电导率。The detection part of the conductivity detection device is placed inside the liquid container, and the conductivity detection device is used to detect the conductivity of the solution in the liquid container.

可选的,所述自动换液装置,还包括:Optionally, the automatic liquid exchange device further includes:

集液装置;liquid collecting device;

所述排液管的排液端口置于所述集液装置内,所述集液装置用于收集从所述装液容器中排出的溶液。The liquid discharge port of the liquid discharge pipe is placed in the liquid collecting device, and the liquid collecting device is used for collecting the solution discharged from the liquid filling container.

可选的,所述集液装置,具体包括:Optionally, the liquid collecting device specifically includes:

集液箱和加热装置;Collection tank and heating device;

所述排液管的排液端口置于所述集液箱内,所述加热装置位于所述集液箱内部,所述加热装置用于加热蒸发所述集液箱中的溶液。The liquid discharge port of the liquid discharge pipe is placed in the liquid collecting tank, and the heating device is located inside the liquid collecting tank, and the heating device is used for heating and evaporating the solution in the liquid collecting tank.

可选的,所述自动换液装置,还包括:Optionally, the automatic liquid exchange device further includes:

搅拌器;agitator;

所述搅拌器的搅拌部置于所述装液容器内部,所述搅拌器用于搅拌所述装液容器内的液体。The stirring part of the stirrer is placed inside the liquid-filling container, and the stirrer is used for stirring the liquid in the liquid-filling container.

本发明还提供一种基于缓冲材料冲蚀试验的自动换液方法,应用于上述的基于缓冲材料冲蚀试验的自动换液装置,包括:The present invention also provides an automatic liquid exchange method based on the buffer material erosion test, which is applied to the above-mentioned automatic liquid exchange device based on the buffer material erosion test, including:

获取定时时间;所述定时时间为控制定时阀开启和关闭的时间;Acquire the timing time; the timing time is the time for controlling the opening and closing of the timing valve;

根据所述定时时间对进行冲蚀实验的换液子系统进行切换,并在切换后的换液子系统进行冲蚀实验时对切换前的换液子系统进行换液操作;Switch the liquid exchange subsystem for the erosion experiment according to the timing time, and perform the liquid exchange operation on the liquid exchange subsystem before the switching when the switched liquid exchange subsystem performs the erosion experiment;

判断是否接收到停止换液操作指令;若接收到指令,则停止换液操作;若未收到指令,则返回步骤“根据所述定时时间对进行冲蚀实验的换液子系统进行切换,并在切换后的换液子系统进行冲蚀实验时对切换前的换液子系统进行换液操作”。Determine whether the instruction to stop the liquid exchange operation is received; if the instruction is received, the liquid exchange operation is stopped; if the instruction is not received, return to the step "switch the liquid exchange subsystem for the erosion experiment according to the timing time, and During the erosion experiment of the switched liquid exchange subsystem, the liquid exchange operation of the pre-switched liquid exchange subsystem is carried out”.

可选的,在所述根据所述定时时间对进行冲蚀实验的换液子系统进行切换,之前还包括:Optionally, before the switching of the liquid exchange subsystem for performing the erosion experiment according to the timing time, the method further includes:

将当前换液子系统中的加液定时阀打开,向当前换液子系统中的装液容器添加冲蚀实验所用溶液,开始计时;Open the liquid addition timing valve in the current liquid exchange subsystem, add the solution used in the erosion experiment to the liquid filling container in the current liquid exchange subsystem, and start timing;

超过预设加液时间后关闭所述当前换液子系统中的加液定时阀;After the preset liquid addition time is exceeded, the liquid addition timing valve in the current liquid exchange subsystem is closed;

打开当前换液子系统中的进液定时阀和当前换液子系统中的出液定时阀;Open the liquid inlet timing valve in the current liquid exchange subsystem and the liquid outlet timing valve in the current liquid exchange subsystem;

当前换液子系统中的搅拌器根据预设搅拌时间搅拌所述当前换液子系统中的装液容器内的溶液,当前换液子系统中的检测装置根据预设检测时间检测溶液参数。The stirrer in the current liquid exchange subsystem stirs the solution in the liquid container in the current liquid exchange subsystem according to the preset stirring time, and the detection device in the current liquid exchange subsystem detects the solution parameters according to the preset detection time.

可选的,所述根据所述定时时间对进行冲蚀实验的换液子系统进行切换,并在切换后的换液子系统进行冲蚀实验时对切换前的换液子系统进行换液操作,具体包括:Optionally, switching the liquid exchange subsystem that performs the erosion experiment according to the timing, and performs a liquid exchange operation on the liquid exchange subsystem before the switching when the switched liquid exchange subsystem performs the erosion experiment. , including:

根据所述定时时间打开待切换子系统的加液定时阀并开始计时,在超过预设加液时间后关闭所述待切换子系统的加液定时阀;Open the liquid addition timing valve of the subsystem to be switched according to the timing time and start timing, and close the liquid addition timing valve of the to-be-switched subsystem after the preset liquid addition time is exceeded;

根据所述定时时间关闭所述当前换液子系统中的进液定时阀和所述当前换液子系统中的出液定时阀,同时打开待切换子系统的进液定时阀和待切换子系统的出液定时阀;Close the liquid inlet timing valve in the current liquid exchange subsystem and the liquid outlet timing valve in the current liquid exchange subsystem according to the timing time, and simultaneously open the liquid inlet timing valve of the sub-system to be switched and the sub-system to be switched The liquid outlet timing valve;

待切换子系统中的搅拌器根据所述预设搅拌时间搅拌待切换子系统中的装液容器内的溶液,待切换子系统中的检测装置根据所述预设检测时间检测溶液参数;The stirrer in the subsystem to be switched stirs the solution in the liquid container in the subsystem to be switched according to the preset stirring time, and the detection device in the subsystem to be switched detects the solution parameter according to the preset detection time;

打开当前换液子系统中的排液定时阀并开始计时,超出预设排液时间后关闭所述当前换液子系统中的排液定时阀。Open the liquid discharge timing valve in the current liquid exchange subsystem and start timing, and close the liquid discharge timing valve in the current liquid exchange subsystem after the preset liquid discharge time is exceeded.

与现有技术相比,本发明的有益效果是:Compared with the prior art, the beneficial effects of the present invention are:

本发明提出了一种基于缓冲材料冲蚀试验的自动换液装置及方法,该装置包括多个换液子系统;每一换液子系统的出液端口均与冲蚀实验装置的进液端连接;每一换液子系统的进液端口均与冲蚀实验装置的出液端连接;换液子系统设置有定时阀,换液子系统根据定时阀的开合状态交替进行换液操作;换液子系统中的检测装置用于检测装液容器内溶液的参数,能够在自动换液过程中实现自动测定溶液的浊度、电导率。The invention proposes an automatic liquid exchange device and method based on a buffer material erosion test. The device includes a plurality of liquid exchange subsystems; the liquid outlet port of each liquid exchange subsystem is connected to the liquid inlet end of the erosion test device. connection; the liquid inlet port of each liquid exchange subsystem is connected with the liquid outlet end of the erosion experiment device; the liquid exchange subsystem is provided with a timing valve, and the liquid exchange subsystem performs liquid exchange operations alternately according to the opening and closing states of the timing valve; The detection device in the liquid exchange subsystem is used to detect the parameters of the solution in the liquid container, and can automatically measure the turbidity and conductivity of the solution during the automatic liquid exchange process.

附图说明Description of drawings

为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the accompanying drawings required in the embodiments will be briefly introduced below. Obviously, the drawings in the following description are only some of the present invention. In the embodiments, for those of ordinary skill in the art, other drawings can also be obtained according to these drawings without creative labor.

图1为本发明实施例中基于缓冲材料冲蚀试验的自动换液装置结构图。FIG. 1 is a structural diagram of an automatic liquid exchange device based on a buffer material erosion test in an embodiment of the present invention.

具体实施方式Detailed ways

下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, but not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

本发明的目的是提供一种基于缓冲材料冲蚀试验的自动换液装置及方法,能够在自动换液过程中实现自动测定溶液的浊度、电导率。The purpose of the present invention is to provide an automatic liquid exchange device and method based on a buffer material erosion test, which can automatically measure the turbidity and conductivity of the solution during the automatic liquid exchange process.

为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图和具体实施方式对本发明作进一步详细的说明。In order to make the above objects, features and advantages of the present invention more clearly understood, the present invention will be described in further detail below with reference to the accompanying drawings and specific embodiments.

本发明提供的一种基于缓冲材料冲蚀试验的自动换液装置包括多个换液子系统。每一换液子系统的出液端口均与冲蚀实验装置的进液端口连接;每一换液子系统的进液端口均与冲蚀实验装置的出液端口连接;冲蚀实验装置内置有缓冲材料;换液子系统的加液端口用于对换液子系统中的装液容器添加冲蚀实验所用溶液;换液子系统的出液端口用于将装液容器中的溶液排入冲蚀实验装置进液端;换液子系统的进液端口用于将冲蚀实验装置出液端流出的冲蚀溶液流入装液容器;换液子系统的排液端口用于将装液容器中的溶液排出;换液子系统设置有定时阀,换液子系统根据定时阀的开合状态交替进行换液操作;换液子系统中的检测装置用于检测装液容器内溶液的参数。An automatic liquid exchange device based on a buffer material erosion test provided by the present invention includes a plurality of liquid exchange subsystems. The liquid outlet port of each liquid exchange subsystem is connected with the liquid inlet port of the erosion experiment device; the liquid inlet port of each liquid exchange subsystem is connected with the liquid outlet port of the erosion experiment device; the erosion experiment device has a built-in Buffer material; the liquid filling port of the liquid exchange subsystem is used to add the solution used in the erosion experiment to the liquid filling container in the liquid exchange subsystem; the liquid outlet port of the liquid exchange subsystem is used to discharge the solution in the liquid filling container into the flushing system. The liquid inlet end of the erosion experiment device; the liquid inlet port of the liquid exchange subsystem is used to flow the erosion solution flowing out of the liquid outlet end of the erosion experiment device into the liquid container; The liquid exchange subsystem is provided with a timing valve, and the liquid exchange subsystem alternately performs liquid exchange operations according to the opening and closing states of the timing valve; the detection device in the liquid exchange subsystem is used to detect the parameters of the solution in the liquid container.

换液子系统,具体包括:设置有进液定时阀的进液管、设置有出液定时阀的出液管、设置有加液定时阀的加液管、设置有排液定时阀的排液管和装液容器。进液管的出液端口(即换液子系统的出液端口)与冲蚀实验装置的进液管的进液端口连接,进液管的进液端置于装液容器内;出液管的进液端口(即换液子系统的进液端口)与冲蚀实验装置出液管的出液端口连接,出液管的出液端口置于装液容器内;加液管的出液端置于装液容器内,加液管的加液端口(即换液子系统的加液端口)用于加入冲蚀实验所用溶液;排液管的进液端设置在装液容器的底部,排液管的排液端口(即换液子系统的排液端口)用于将装液容器内的溶液排出。The liquid exchange subsystem specifically includes: a liquid inlet pipe provided with a liquid inlet timing valve, a liquid outlet pipe provided with a liquid outlet timing valve, a liquid addition pipe provided with a liquid addition timing valve, and a liquid discharge pipe provided with a liquid discharge timing valve Tubes and liquid containers. The liquid outlet port of the liquid inlet pipe (that is, the liquid outlet port of the liquid exchange subsystem) is connected with the liquid inlet port of the liquid inlet pipe of the erosion experiment device, and the liquid inlet end of the liquid inlet pipe is placed in the liquid container; the liquid outlet pipe The liquid inlet port (that is, the liquid inlet port of the liquid exchange subsystem) is connected to the liquid outlet port of the liquid outlet pipe of the erosion experiment device, and the liquid outlet port of the liquid outlet pipe is placed in the liquid container; the liquid outlet end of the liquid addition pipe It is placed in the liquid filling container, and the liquid filling port of the liquid filling pipe (that is, the liquid filling port of the liquid exchange subsystem) is used to add the solution used in the erosion experiment; the liquid inlet end of the liquid discharge pipe is set at the bottom of the liquid filling container, and drain The liquid discharge port of the liquid pipe (ie, the liquid discharge port of the liquid exchange subsystem) is used to discharge the solution in the liquid filling container.

检测装置,具体包括:浊度检测装置和电导率检测装置。浊度检测装置的检测部置于装液容器的内部,浊度检测装置用于检测装液容器内溶液的浊度。电导率检测装置的检测部置于装液容器的内部,电导率检测装置用于检测装液容器内溶液的电导率。The detection device specifically includes: a turbidity detection device and a conductivity detection device. The detection part of the turbidity detection device is arranged inside the liquid container, and the turbidity detection device is used to detect the turbidity of the solution in the liquid container. The detection part of the conductivity detection device is arranged inside the liquid container, and the conductivity detection device is used to detect the conductivity of the solution in the liquid container.

自动换液装置,还包括:集液装置。排液管的排液端口置于集液装置内,集液装置用于收集从装液容器中排出的溶液。The automatic liquid changing device also includes: a liquid collecting device. The discharge port of the discharge pipe is placed in the liquid collecting device, and the liquid collecting device is used to collect the solution discharged from the liquid filling container.

集液装置,具体包括:集液箱和加热装置。加热装置位于集液箱内部,加热装置用于加热蒸发集液箱中的溶液。The liquid collecting device specifically includes: a liquid collecting tank and a heating device. The heating device is located inside the collecting tank, and the heating device is used to heat the solution in the evaporating liquid collecting tank.

自动换液装置,还包括:搅拌器。搅拌器的搅拌部置于装液容器内部,搅拌器用于搅拌装液容器内的液体。The automatic liquid changing device also includes: a stirrer. The stirring part of the stirrer is placed inside the liquid container, and the stirrer is used to stir the liquid in the liquid container.

以自动换液装置包括2个换液子系统为例,进一步说明本发明的装置结构。图1为本发明实施例中基于缓冲材料冲蚀试验的自动换液装置结构图,如图1所示,一种用于缓冲材料冲蚀试验的自动换液装置,主要包括:进液管1、加液管2、出液管3、排液管4、浊度探头5和6、电导率探头7和8、搅拌器9和10、加液定时阀11和12、进液定时阀13和14、出液定时阀15和16、排液定时阀17和18、集液箱19、500ml装液容器20和21。Taking the automatic liquid exchange device including two liquid exchange subsystems as an example, the device structure of the present invention is further described. FIG. 1 is a structural diagram of an automatic liquid exchange device based on a buffer material erosion test in an embodiment of the present invention. As shown in FIG. 1 , an automatic liquid exchange device for a buffer material erosion test mainly includes: a liquid inlet pipe 1 , liquid addition pipe 2, liquid outlet pipe 3, liquid discharge pipe 4, turbidity probe 5 and 6, conductivity probe 7 and 8, agitator 9 and 10, liquid addition timing valve 11 and 12, liquid inlet timing valve 13 and 14. Liquid discharge timing valves 15 and 16, liquid discharge timing valves 17 and 18, liquid collecting tank 19, and 500ml liquid containers 20 and 21.

进液管1用三通管接头连接,一端连接装好的冲蚀实验的进液管,另两端分别连接500ml装液容器20和21。将进液定时阀13、14装在通往500ml装液容器20和21的进液管1上。The liquid inlet pipe 1 is connected with a three-way pipe joint, one end is connected to the liquid inlet pipe of the erosion experiment, and the other two ends are respectively connected to 500ml liquid filling containers 20 and 21. The liquid inlet timing valves 13 and 14 are installed on the liquid inlet pipe 1 leading to the 500ml liquid filling containers 20 and 21 .

加液管2用三通管接头连接,一端连接装好的冲蚀实验所需溶液的容器,另两端分别连接500ml装液容器20和21;将加液定时阀11和12装在通往500ml装液容器20和21的加液管2上。The liquid addition pipe 2 is connected with a three-way pipe joint, one end is connected to the container of the solution required for the erosion experiment, and the other two ends are connected to the 500ml liquid container 20 and 21 respectively; 500ml liquid container 20 and 21 on the filling pipe 2.

出液管3用三通管接头连接,一端连接装好的冲蚀实验的出液管,另两端分别连接500ml装液容器20和21;将出液定时阀15、16装在通往500ml装液容器20和21的出液管3上。The liquid outlet pipe 3 is connected with a three-way pipe joint, one end is connected to the installed liquid outlet pipe of the erosion experiment, and the other two ends are respectively connected to the 500ml liquid filling containers 20 and 21; on the liquid outlet pipes 3 of the liquid containers 20 and 21.

排液管4用三通管接头连接,一端连接集液箱19,另两端分别连接500ml装液容器20和21;将排液定时阀17、18装在通往500ml装液容器20和21的排液管4上。The drain pipe 4 is connected with a three-way pipe joint, one end is connected to the liquid collecting tank 19, and the other two ends are respectively connected to the 500ml liquid filling containers 20 and 21; on the drain pipe 4.

将浊度探头5与电导率探头7安装在500ml装液容器20内,浊度探头6与电导率探头8安装在500ml装液容器21内,同时做好密封措施,防止漏水。将搅拌器9与10分别安装在500ml装液容器20和21内,同时调整搅拌器处于合适位置和高度,防止旋转时碰到500ml装液容器20和21中的管子和内壁。The turbidity probe 5 and the conductivity probe 7 are installed in the 500ml liquid container 20, the turbidity probe 6 and the conductivity probe 8 are installed in the 500ml liquid container 21, and sealing measures are taken to prevent water leakage. Install the stirrers 9 and 10 in the 500ml liquid containers 20 and 21 respectively, and adjust the stirrers to be at the proper position and height to prevent them from hitting the tubes and inner walls of the 500ml liquid containers 20 and 21 during rotation.

本发明还提供一种基于缓冲材料冲蚀试验的自动换液方法,包括:The present invention also provides an automatic liquid exchange method based on the erosion test of the buffer material, comprising:

步骤一:获取定时时间;定时时间为控制定时阀开启和关闭的时间。Step 1: Obtain the timing time; the timing time is the time for controlling the opening and closing of the timing valve.

将当前换液子系统中的加液定时阀打开,向当前换液子系统中的装液容器添加冲蚀实验所用溶液,开始计时;Open the liquid addition timing valve in the current liquid exchange subsystem, add the solution used in the erosion experiment to the liquid filling container in the current liquid exchange subsystem, and start timing;

超过预设加液时间后关闭当前换液子系统中的加液定时阀;After the preset liquid addition time is exceeded, close the liquid addition timing valve in the current liquid exchange subsystem;

打开当前换液子系统中的进液定时阀和当前换液子系统中的出液定时阀;Open the liquid inlet timing valve in the current liquid exchange subsystem and the liquid outlet timing valve in the current liquid exchange subsystem;

当前换液子系统中的搅拌器根据预设搅拌时间搅拌当前换液子系统中的装液容器内的溶液,当前换液子系统中的检测装置根据预设检测时间检测溶液参数。The stirrer in the current liquid exchange subsystem stirs the solution in the liquid container in the current liquid exchange subsystem according to the preset stirring time, and the detection device in the current liquid exchange subsystem detects the solution parameters according to the preset detection time.

步骤二:根据定时时间对进行冲蚀实验的换液子系统进行切换,并在切换后的换液子系统进行冲蚀实验时对切换前的换液子系统进行换液操作。Step 2: Switch the liquid exchange subsystem for the erosion experiment according to the timing time, and perform the liquid exchange operation on the liquid exchange subsystem before the switch when the exchanged liquid exchange subsystem performs the erosion experiment.

步骤二具体包括:Step 2 specifically includes:

根据定时时间打开待切换子系统的加液定时阀并开始计时,在超过预设加液时间后关闭待切换子系统的加液定时阀;Open the liquid addition timing valve of the subsystem to be switched according to the timing time and start timing, and close the liquid addition timing valve of the to-be-switched subsystem after the preset liquid addition time is exceeded;

根据定时时间关闭当前换液子系统中的进液定时阀和当前换液子系统中的出液定时阀,同时打开待切换子系统的进液定时阀和待切换子系统的出液定时阀;Close the liquid inlet timing valve in the current liquid exchange subsystem and the liquid outlet timing valve in the current liquid exchange subsystem according to the timing time, and open the liquid inlet timing valve of the to-be-switched subsystem and the liquid-out timing valve of the to-be-switched subsystem at the same time;

待切换子系统中的搅拌器根据预设搅拌时间搅拌待切换子系统中的装液容器内的溶液,待切换子系统中的检测装置根据预设检测时间检测溶液参数;The stirrer in the subsystem to be switched stirs the solution in the liquid container in the subsystem to be switched according to the preset stirring time, and the detection device in the subsystem to be switched detects the solution parameters according to the preset detection time;

打开当前换液子系统中的排液定时阀并开始计时,超出预设排液时间后关闭当前换液子系统中的排液定时阀。Open the liquid discharge timing valve in the current liquid exchange subsystem and start timing, and close the liquid discharge timing valve in the current liquid exchange subsystem after the preset liquid discharge time is exceeded.

步骤三:判断是否接收到停止换液操作指令;若接收到指令,则执行步骤四;若未收到指令,则返回步骤二。Step 3: determine whether an instruction to stop the liquid exchange operation is received; if an instruction is received, execute step 4; if no instruction is received, return to step 2.

步骤四:停止换液操作。Step 4: Stop the liquid change operation.

以自动换液装置包括2个换液子系统为例,进一步说明本发明的方法流程,该方法流程是基于图1自动换液装置的自动换液方法,该方法包括:Taking the automatic liquid exchange device including two liquid exchange subsystems as an example, the method flow of the present invention is further described. The method flow is based on the automatic liquid exchange method of the automatic liquid exchange device in FIG. 1 , and the method includes:

(1)将组装好的冲蚀实验装置连接进液管1、出液管3;(1) Connect the assembled erosion test device to the liquid inlet pipe 1 and the liquid outlet pipe 3;

(2)将加液管2连接到装液容器;(2) Connect the liquid filling pipe 2 to the liquid filling container;

(3)将加液定时阀11打开,其他阀门全部关闭后,向500ml装液容器20中注入500ml冲蚀实验所用溶液;(3) opening the liquid addition timing valve 11, and after all other valves are closed, inject 500ml of the solution used in the erosion experiment into the 500ml liquid filling container 20;

(4)将浊度探头5与6、电导率探头7与8和搅拌器9与10分别接通电源。(4) Power on the turbidity probes 5 and 6, the conductivity probes 7 and 8, and the stirrers 9 and 10, respectively.

(5)进液定时阀13、出液定时阀15打开24小时;(5) The liquid inlet timing valve 13 and the liquid outlet timing valve 15 are opened for 24 hours;

(6)设置搅拌器9每隔30分钟搅拌一次,浊度探头5和电导率探头7每30分钟记录一次;(6) set the stirrer 9 to stir every 30 minutes, and record the turbidity probe 5 and the conductivity probe 7 every 30 minutes;

(7)23小时后(即在进液定时阀13、出液定时阀15打开23小时后)打开加液定时阀12,向500ml装液容器21中注入500ml冲蚀实验所用溶液后关闭;(7) after 23 hours (that is, after the liquid inlet timing valve 13 and the liquid outlet timing valve 15 are opened for 23 hours), the liquid addition timing valve 12 is opened, and the solution used in the 500ml erosion experiment is injected into the 500ml liquid container 21 and closed;

(8)24小时后(即在进液定时阀13、出液定时阀15打开24小时后),进液定时阀13、出液定时阀15关闭,进液定时阀14、出液定时阀16打开24小时;(8) After 24 hours (that is, 24 hours after the liquid inlet timing valve 13 and the liquid outlet timing valve 15 are opened), the liquid inlet timing valve 13 and the liquid outlet timing valve 15 are closed, and the liquid inlet timing valve 14 and the liquid outlet timing valve 16 open for 24 hours;

(9)设置搅拌器10每隔30分钟搅拌一次,浊度探头6和电导率探头8每30分钟记录一次;(9) set the stirrer 10 to stir every 30 minutes, and record the turbidity probe 6 and the conductivity probe 8 every 30 minutes;

(10)打开排液定时阀17,集液箱19开始加热蒸发500ml装液容器20流入的冲蚀实验所用溶液;(10) Open the drain timing valve 17, and the liquid collecting tank 19 starts to heat and evaporate the solution used in the erosion experiment that the 500ml liquid container 20 flows into;

(11)1小时后(即打开排液定时阀17的1小时后)关闭排液定时阀17;(11) After 1 hour (that is, 1 hour after opening the drain timing valve 17), close the drain timing valve 17;

(12)23小时后(即进液定时阀14、出液定时阀16打开23小时后)打开加液定时阀11,向500ml装液容器20中注入500ml冲蚀实验所用溶液后关闭;(12) after 23 hours (that is, after the liquid inlet timing valve 14 and the liquid outlet timing valve 16 are opened for 23 hours), the liquid addition timing valve 11 is opened, and the solution used in the 500ml erosion experiment is injected into the 500ml liquid container 20 and closed;

(13)24小时后(即进液定时阀14、出液定时阀16打开24小时后),进液定时阀14、出液定时阀16关闭,进液定时阀13、出液定时阀15打开24小时;(13) After 24 hours (that is, 24 hours after the liquid inlet timing valve 14 and the liquid outlet timing valve 16 are opened), the liquid inlet timing valve 14 and the liquid outlet timing valve 16 are closed, and the liquid inlet timing valve 13 and the liquid outlet timing valve 15 are opened. 24 hours;

(14)排液定时阀18打开,集液箱19开始加热蒸发500ml装液容器21流入的冲蚀实验所用溶液;(14) The drain timing valve 18 is opened, and the liquid collecting tank 19 starts to heat and evaporate the solution used in the erosion experiment that flows into the 500ml liquid container 21;

(15)1小时后(即排液定时阀18打开1小时后)关闭排液定时阀18,并且从第(7)步循环操作,直至整个冲蚀试验结束。(15) After 1 hour (that is, 1 hour after the drain timing valve 18 is opened), close the drain timing valve 18, and cycle from step (7) until the entire erosion test ends.

本发明提供的自动换液方法,通过对膨润土的冲蚀实验进行等间隔时间更换溶液,减少人为时间差对实验测试结果的影响。The automatic liquid changing method provided by the present invention reduces the influence of artificial time difference on the experimental test results by changing the solution at equal intervals in the erosion experiment of bentonite.

本文中应用了具体个例对本发明的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处。综上,本说明书内容不应理解为对本发明的限制。In this paper, specific examples are used to illustrate the principles and implementations of the present invention. The descriptions of the above embodiments are only used to help understand the methods and core ideas of the present invention; meanwhile, for those skilled in the art, according to the present invention There will be changes in the specific implementation and application scope. In conclusion, the contents of this specification should not be construed as limiting the present invention.

Claims (9)

1. The utility model provides an automatic liquid device that trades based on buffer material erosion test which characterized in that includes:
a plurality of liquid change subsystems;
the liquid outlet port of each liquid changing subsystem is connected with the liquid inlet end of the erosion experimental device; the liquid inlet port of each liquid changing subsystem is connected with the liquid outlet end of the erosion experimental device; a buffer material is arranged in the erosion experimental device;
the liquid adding port of the liquid changing subsystem is used for adding a solution for an erosion experiment to a liquid container in the liquid changing subsystem; the liquid outlet port of the liquid changing subsystem is used for discharging the solution in the liquid container into the liquid inlet end of the erosion experimental device; the liquid inlet port of the liquid changing subsystem is used for enabling the erosion solution flowing out of the liquid outlet end of the erosion experimental device to flow into the liquid container; the liquid discharge port of the liquid changing subsystem is used for discharging the solution in the liquid container; the liquid changing subsystem is provided with a timing valve and alternately carries out liquid changing operation according to the opening and closing state of the timing valve; and the detection device in the liquid change subsystem is used for detecting the parameters of the solution in the liquid container.
2. The automatic liquid changing device based on the buffer material erosion test according to claim 1,
the liquid changing subsystem specifically comprises:
the liquid feeding device comprises a liquid feeding pipe provided with a liquid feeding timing valve, a liquid discharging pipe provided with a liquid discharging timing valve and a liquid container;
the liquid outlet end of the liquid inlet pipe is connected with the liquid inlet end of the erosion experimental device, and the liquid inlet end of the liquid inlet pipe is arranged in the liquid container;
the liquid inlet end of the liquid outlet pipe is connected with the liquid outlet end of the erosion experimental device, and the liquid outlet end of the liquid outlet pipe is arranged in the liquid container;
the liquid outlet end of the liquid adding pipe is arranged in the liquid container, and the liquid adding port of the liquid adding pipe is used for adding a solution used in an erosion experiment;
the liquid inlet end of the liquid discharge pipe is arranged at the bottom of the liquid container, and the liquid discharge port of the liquid discharge pipe is used for discharging the solution in the liquid container.
3. The automatic liquid changing device based on the buffer material erosion test according to claim 1, wherein the detection device specifically comprises:
a turbidity detecting means and a conductivity detecting means;
the detection part of the turbidity detection device is arranged in the liquid container, and the turbidity detection device is used for detecting the turbidity of the solution in the liquid container;
the detection part of the conductivity detection device is arranged in the liquid container, and the conductivity detection device is used for detecting the conductivity of the solution in the liquid container.
4. The automatic liquid changing device based on the buffer material erosion test according to claim 2, further comprising:
a liquid collecting device;
and the liquid discharge port of the liquid discharge pipe is arranged in the liquid collecting device, and the liquid collecting device is used for collecting the solution discharged from the liquid container.
5. The automatic liquid changing device based on the buffer material erosion test is characterized in that the liquid collecting device specifically comprises:
a liquid collecting tank and a heating device;
the liquid discharge port of the liquid discharge pipe is arranged in the liquid collection box, the heating device is positioned in the liquid collection box, and the heating device is used for heating and evaporating the solution in the liquid collection box.
6. The automatic liquid changing device based on the buffer material erosion test of claim 1, further comprising:
a stirrer;
the stirring part of the stirrer is arranged in the liquid container, and the stirrer is used for stirring the liquid in the liquid container.
7. An automatic liquid changing method based on a buffer material erosion test is applied to the automatic liquid changing device based on the buffer material erosion test, which is characterized by comprising the following steps:
acquiring timing time; the timing time is the time for controlling the opening and closing of the timing valve;
switching the liquid-changing subsystem for carrying out the erosion experiment according to the timing time, and carrying out liquid-changing operation on the liquid-changing subsystem before switching when the switched liquid-changing subsystem carries out the erosion experiment;
judging whether a liquid change stopping operation instruction is received or not; if receiving the instruction, stopping the liquid changing operation; and if the command is not received, returning to the step of switching the liquid changing subsystem for carrying out the erosion experiment according to the timing time, and carrying out liquid changing operation on the liquid changing subsystem before switching when the switched liquid changing subsystem carries out the erosion experiment.
8. The automatic liquid changing method based on the buffer material erosion test as claimed in claim 7, wherein before the switching the liquid changing subsystem for conducting the erosion test according to the timing time, further comprising:
opening a liquid adding timing valve in the current liquid changing subsystem, adding a solution used in an erosion experiment into a liquid container in the current liquid changing subsystem, and starting timing;
closing the liquid adding timing valve in the current liquid changing subsystem after the preset liquid adding time is exceeded;
opening a liquid inlet timing valve in the current liquid changing subsystem and a liquid outlet timing valve in the current liquid changing subsystem;
the stirrer in the current liquid changing subsystem stirs the solution in the liquid container in the current liquid changing subsystem according to preset stirring time, and the detection device in the current liquid changing subsystem detects solution parameters according to preset detection time.
9. The automatic liquid switching method based on the buffer material erosion test of claim 8, wherein the switching of the liquid switching subsystem for the erosion test is performed according to the timing time, and the liquid switching operation is performed on the liquid switching subsystem before switching when the switched liquid switching subsystem performs the erosion test, specifically comprising:
opening a liquid adding timing valve of the subsystem to be switched according to the timing time, starting timing, and closing the liquid adding timing valve of the subsystem to be switched after the preset liquid adding time is exceeded;
closing a liquid inlet timing valve in the current liquid changing subsystem and a liquid outlet timing valve in the current liquid changing subsystem according to the timing time, and simultaneously opening a liquid inlet timing valve of the subsystem to be switched and a liquid outlet timing valve of the subsystem to be switched;
a stirrer in the subsystem to be switched stirs the solution in the liquid container in the subsystem to be switched according to the preset stirring time, and a detection device in the subsystem to be switched detects the solution parameters according to the preset detection time;
and opening a liquid drainage timing valve in the current liquid changing subsystem and starting timing, and closing the liquid drainage timing valve in the current liquid changing subsystem after the preset liquid drainage time is exceeded.
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