CN111388442A - Gel candy type plant soft capsule - Google Patents

Gel candy type plant soft capsule Download PDF

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Publication number
CN111388442A
CN111388442A CN202010212938.5A CN202010212938A CN111388442A CN 111388442 A CN111388442 A CN 111388442A CN 202010212938 A CN202010212938 A CN 202010212938A CN 111388442 A CN111388442 A CN 111388442A
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CN
China
Prior art keywords
starch
soft capsule
carrageenan
gelling agent
type plant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010212938.5A
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Chinese (zh)
Inventor
原敏敏
汤绮庭
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Guangzhou Procept Biotech Co ltd
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Guangzhou Procept Biotech Co ltd
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Publication date
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Priority to CN202010212938.5A priority Critical patent/CN111388442A/en
Publication of CN111388442A publication Critical patent/CN111388442A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/48Preparations in capsules, e.g. of gelatin, of chocolate
    • A61K9/4816Wall or shell material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/30Encapsulation of particles, e.g. foodstuff additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a gel candy type plant soft capsule, which comprises the following raw materials by weight percent of 100 percent: 20-40% of first gelling agent, 1-10% of second gelling agent, 10-40% of plasticizer, 0.2-10% of water holding agent, 0.1-2% of food additive and 30-50% of water; the first gelling agent is starch, and comprises natural starch and modified starch; the second gelling agent comprises one or more of carrageenan, high-acyl gellan gum, low-acyl gellan gum, konjac gum and pullulan; the plasticizer comprises one or more of glycerol, xylitol, sorbitol, mannitol, maltitol and trehalose; the water holding agent comprises one or more of carboxymethyl cellulose, hydroxypropyl methyl cellulose and microcrystalline cellulose. The chewable soft capsule has high chewiness and good taste, and solves the technical problem that the plant soft capsule in the prior art cannot be chewed.

Description

Gel candy type plant soft capsule
The technical field is as follows:
the invention relates to a gel candy type plant soft capsule.
Background art:
the soft capsule is one of the most widely applied formulations in the fields of medicine, health care products and big health, can well ensure the stability of nutrients and medicinal components in the capsule, has the advantages of portability, peculiar smell shielding and the like, is prepared from gelatin as a raw material in the traditional soft capsule, is totally a gelatin soft capsule by observing products on the market, has great limitation on vegetarians and people who swallow the soft capsule, has great limitation on people who swallow the soft capsule, and cannot be eaten as candy food.
CN 103750523B discloses a method for preparing candy soft capsule, the components of the capsule skin include animal glue and vegetable glue, compared with the soft capsule which mainly uses gelatin, glycerin and other raw materials, the capsule has the advantages of reasonable proportion, low cost, portability, high bioavailability and no side effect, the production and preparation process is easy to master and is suitable for production, the product quality is stable, and the capsule is a health care nutrition food which is safe to eat and has wide application range, but because of the animal glue, the capsule does not conform to the dietary habit and requirement of halal or vegetarian, and the development of vegetable soft capsule has important significance based on the reasons.
CN 110075081A discloses a plant soft capsule with industrial application and a preparation method thereof, wherein the plant soft capsule with excellent performance is prepared by controlling the weight average molecular weight of carrageenan, starch, plasticizer and water; compared with the plant soft capsule in the prior art, the plant soft capsule has lower production cost, and the product quality meets the requirements of the gelatin soft capsule; on the premise of high production efficiency, the low oil leakage rate is realized, and the fracture time reaches the standard of United States Pharmacopoeia (USP). However, the plant soft capsule is like the common soft capsule, and can only be swallowed but not be chewed.
If the plant-flavored health-care soft capsule is made into a soft capsule made of pure plant raw materials and is made into a gel candy form, the health-care soft capsule can be chewed, so that the requirements of vegetarians can be met, the crowd with dysphagia can be met, and the taste of the product can be improved.
The invention content is as follows:
the invention aims to provide a gel candy type plant soft capsule which has high chewiness and good taste Q elasticity and solves the technical problem that the plant soft capsule in the prior art can not be chewed.
The invention is realized by the following technical scheme:
the gel candy type plant soft capsule comprises an inclusion and a rubber sheet wrapping the inclusion, wherein the inclusion is oil or oil powder suspension, and the rubber sheet comprises the following raw materials in percentage by weight of 100 percent: 20-40% of first gelling agent, 1-10% of second gelling agent, 10-40% of plasticizer, 0.2-10% of water holding agent, 0.1-2% of food additive and 30-50% of water; the first gelling agent is starch, and comprises natural starch and modified starch, wherein the modified starch comprises one or more of a series of modified starches such as hydroxypropyl starch, acetate starch, oxidized starch and the like; the second gelling agent comprises one or more of carrageenan, high-acyl gellan gum, low-acyl gellan gum, konjac gum and pullulan; the carrageenan comprises one or two of k-carrageenan and l-carrageenan; the plasticizer comprises one or more of glycerol, xylitol, sorbitol, mannitol, maltitol and trehalose; the water holding agent comprises one or more of carboxymethyl cellulose, hydroxypropyl methyl cellulose and microcrystalline cellulose; the food additive comprises any one of pigment, sweetener, sour agent, essence, etc.
The preparation method of the gel candy type plant soft capsule comprises the following steps: adding the first gel, the second gel, the plasticizer and the water holding agent into water, stirring and mixing uniformly, heating to 85-100 ℃, adding the food additive after completely dissolving, vacuumizing for 1h (the vacuum degree is less than or equal to-0.6 MPa), checking that the glue solution is free of bubbles, and pressing into the gel candy type plant soft capsule.
The invention has the following beneficial effects: the gel candy type plant soft capsule disclosed by the invention has the advantages that all the components forming the capsule skin are pure plant raw materials, and the components are synergistic to prepare the gel candy form, so that the obtained gel candy type plant soft capsule has high chewiness and Q elastic mouthfeel, can be chewed, meets the requirements of vegetarians, meets the requirements of dysphagia people, and can increase the taste of the product. Solves the technical problem that the plant soft capsule in the prior art can not be chewed.
Description of the drawings:
FIG. 1 is a TPA test hardness comparison graph of comparative and examples conducted by Stable Micro Systems TA. Xtplus texture analyzer;
FIG. 2 is a graph comparing the elasticity of TPA tests conducted on comparative and examples by Stable Micro Systems TA. Xtplus texture analyzer;
FIG. 3 is a TPA test chew comparison chart of comparative and examples conducted by Stable Micro Systems TA. Xtplus texture analyzer.
The specific implementation mode is as follows:
the following is a further description of the invention and is not intended to be limiting.
Example 1:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent: 30% of hydroxypropyl starch, 1% of K-carrageenan, 20% of glycerol, 5% of trehalose, 0.2% of carboxymethyl cellulose, 0.2% of essence and 43.6% of water; the contents are as follows: DHA algae oil
The preparation method of the gel candy type plant soft capsule comprises the following steps: adding hydroxypropyl starch, K-carrageenan, glycerol, trehalose, and carboxymethyl cellulose into water, stirring, heating to 85-100 deg.C, adding essence until completely dissolved, vacuumizing for 1 hr (vacuum degree is less than or equal to-0.6 MPa), checking that the glue solution is free of bubbles, and making into gel candy type plant soft capsule.
Example 2:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent:
20% of acetic ester starch, 2% of K-carrageenan, 2% of l-carrageenan, 30% of glycerol, 7% of xylitol, 0.5% of hydroxypropyl methyl cellulose, 0.2% of essence and 38.3% of water; inclusion of: oil powder suspension milk calcium
Example 3:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent: 35 percent of oxidized starch, 0.5 percent of low-acyl gellan gum, 1 percent of l-carrageenan, 20 percent of sorbitol, 4 percent of microcrystalline cellulose, 0.2 percent of sweetening agent and 39.3 percent of water
Inclusion of: oil powder suspension probiotics.
Example 4:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent: 25% of hydroxypropyl starch, 0.2% of high-acyl gellan gum, 2% of K-carrageenan, 5% of pullulan, 15% of glycerol, 10% of maltitol, 4% of trehalose, 0.5% of hydroxypropyl methyl cellulose, 0.2% of pigment and 38.1% of water; inclusion of: the fruit and vegetable iron is mixed with the oil powder suspension.
Example 5:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent: 20% of hydroxypropyl starch, 20% of acetate starch, 1% of K-carrageenan, 20% of glycerin, 5% of sorbitol, 0.5% of carboxymethyl cellulose, 0.2% of pigment and 33.3% of water; inclusion of: the oil powder suspension seaweed powder is high in calcium.
Example 6:
the gel candy type plant soft capsule comprises an inclusion and a rubber for wrapping the inclusion, wherein the rubber comprises the following raw materials in percentage by weight of 100 percent: 20% of acetic ester starch, 2% of K-carrageenan, 5% of konjac glucomannan, 10% of glycerin, 5% of sorbitol, 5% of maltitol, 0.5% of carboxymethyl cellulose, 5% of trehalose, 0.2% of essence and 47.3% of water
Inclusion of: rose oil
Comparative example: referring to example 2 of CN 110075081 a, the rubber comprises, by weight, 100% hydroxypropyl starch 30%, l-carrageenan 8%, glycerin 15%, and water 47%, and is heated to 80-90 ℃ to swell the rubber solution, then the temperature is maintained for 20-120 min, and the rubber is degassed until the rubber solution is clear and transparent to obtain the rubber solution.
To better illustrate the effects of the gel candy type soft capsules of the present invention, sensory evaluation and texture analysis were performed on samples of examples and comparative examples.
Sensory evaluation: 20 sensory evaluators were selected and trained according to GB/T16860-1997 sensory analysis method-texture profiling, and sensory scores were made on 3 aspects of hardness, elasticity, chewiness of the samples of the examples and the control, see GB/T16860-1997 for reference standards, and specific scores are shown in the following table:
table 1: the examples and comparative examples were scored for hardness, elasticity, chewiness 3
Sample (I) Hardness of Elasticity Chewiness of the product
Comparative example 10 1.2 10
Example 1 5.1 7.5 4.8
Example 2 4.7 8.0 5.1
Example 3 4.5 8.2 4.6
Example 4 5.6 7.8 5.2
Example 5 5.8 8.3 5.1
Example 6 5.2 7.6 4.9
Remarking: the above scores were averaged over 20 evaluators
A higher hardness score indicates a harder product, a higher elasticity score indicates a more elastic product, a higher chewiness score indicates a less chewy product, and a lower chewiness score indicates a less chewy product. As can be seen from the above scores, the comparative samples were generally perceived by the panelists as being too hard, and not elastic, and difficult to chew, consistent with the properties of conventional soft gelatin capsules, indicating that the product was taken by swallowing. As can be seen from the scores of examples 1-6, the samples of the examples had moderate hardness, high elasticity, and moderate chewiness, and were suitable for consumption by chewing.
And (3) texture analysis: the TPA test of the comparative examples and examples (two bite test, simulating bite of human mouth) was performed by Stable Micro Systems ta. xtplus texture analyzer, and the results are shown in fig. 1, 2, and 3, and it is known that the comparative examples have much higher hardness, much lower elasticity, and much lower chewiness than the examples (in TPA test system, the higher chewiness score, the more chewy the product is), which are consistent with the results of sensory test.

Claims (2)

1. The gel candy type plant soft capsule is characterized by comprising an inclusion and a rubber sheet wrapping the inclusion, wherein the inclusion is oil or oil powder suspension, and the rubber sheet comprises the following raw materials in percentage by weight of 100 percent: 20-40% of first gelling agent, 1-10% of second gelling agent, 10-40% of plasticizer, 0.2-10% of water holding agent, 0.1-2% of food additive and 30-50% of water; the first gelling agent is starch selected from any one of natural starch and modified starch; the modified starch comprises one or more of hydroxypropyl starch, acetate starch and oxidized starch; the second gelling agent comprises one or more of carrageenan, high-acyl gellan gum, low-acyl gellan gum, konjac gum and pullulan; the carrageenan comprises one or two of k-carrageenan and l-carrageenan; the plasticizer comprises one or more of glycerol, xylitol, sorbitol, mannitol, maltitol and trehalose; the water holding agent comprises one or more of carboxymethyl cellulose, hydroxypropyl methyl cellulose and microcrystalline cellulose; the food additive comprises any one of pigment, sweetener, sour agent and essence.
2. The process for preparing gelose type plant soft capsules according to claim 1, which comprises the following steps: adding the first gel, the second gel, the plasticizer and the water holding agent into water, stirring and mixing uniformly, heating to 85-100 ℃, adding the food additive after completely dissolving, vacuumizing until the vacuum degree is less than or equal to-0.6 MPa, keeping for 1h, checking that the glue solution is free of bubbles, and pressing into gel candy type plant soft capsules.
CN202010212938.5A 2020-03-24 2020-03-24 Gel candy type plant soft capsule Pending CN111388442A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112273651A (en) * 2020-11-07 2021-01-29 润科生物工程(福建)有限公司 Soft capsule rich in microalgae oil DHA, DPA and EPA and preparation method thereof
CN112294775A (en) * 2020-12-10 2021-02-02 浙江艾兰得生物科技有限公司 Plant-based soft capsule rubber with anti-adhesion function
CN112401045A (en) * 2020-11-10 2021-02-26 江南大学 Preparation method of vegetable gum gel soft sweets
CN112569204A (en) * 2020-12-30 2021-03-30 湖北人福药用辅料股份有限公司 Pullulan polysaccharide and starch plant enteric-coated capsule and preparation method thereof
CN112603905A (en) * 2020-12-30 2021-04-06 湖北人福药用辅料股份有限公司 Preparation process of pullulan plant capsules
CN113180136A (en) * 2021-04-13 2021-07-30 浙江新维士生物科技有限公司 Preparation method of gel soft sweets
CN114642648A (en) * 2022-04-26 2022-06-21 仙乐健康科技股份有限公司 Starch film-forming composition and application thereof in soft capsules
CN115364068A (en) * 2022-08-23 2022-11-22 青岛至纯生物科技有限公司 Temperature-sensitive capsule and preparation method thereof
CN117281259A (en) * 2023-09-19 2023-12-26 广东润智源健康科技有限公司 Fish oil soft capsule with stable storage and easy disintegration and preparation method thereof
EP4074191A4 (en) * 2020-12-31 2024-04-10 Sirio Pharma Co Ltd Starch film-forming composition and method for preparing capsule shell

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CN105434397A (en) * 2015-12-31 2016-03-30 厦门金达威生物科技有限公司 Vegetable soft capsule shell composition and preparation method thereof
CN109601678A (en) * 2019-01-10 2019-04-12 广州富诺健康科技股份有限公司 A kind of pure plant type calcium D gel candy and preparation method thereof
CN109619250A (en) * 2019-01-14 2019-04-16 广州富诺健康科技股份有限公司 A kind of natural plant gum integumentary pattern seawood meal gel candy
CN110169955A (en) * 2019-07-05 2019-08-27 陕西中医药大学 A kind of production method of the soft capsule shell based on modified starch

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Publication number Priority date Publication date Assignee Title
WO2004091529A2 (en) * 2003-04-14 2004-10-28 Fmc Corporation Homogeneous, thermoreversible low viscosity polymannan gum films and soft capsules made therefrom
CN104644609A (en) * 2015-01-28 2015-05-27 龙标兵 Functional chewing type soft capsule coating
CN105434397A (en) * 2015-12-31 2016-03-30 厦门金达威生物科技有限公司 Vegetable soft capsule shell composition and preparation method thereof
CN109601678A (en) * 2019-01-10 2019-04-12 广州富诺健康科技股份有限公司 A kind of pure plant type calcium D gel candy and preparation method thereof
CN109619250A (en) * 2019-01-14 2019-04-16 广州富诺健康科技股份有限公司 A kind of natural plant gum integumentary pattern seawood meal gel candy
CN110169955A (en) * 2019-07-05 2019-08-27 陕西中医药大学 A kind of production method of the soft capsule shell based on modified starch

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112273651A (en) * 2020-11-07 2021-01-29 润科生物工程(福建)有限公司 Soft capsule rich in microalgae oil DHA, DPA and EPA and preparation method thereof
CN112401045A (en) * 2020-11-10 2021-02-26 江南大学 Preparation method of vegetable gum gel soft sweets
CN112294775A (en) * 2020-12-10 2021-02-02 浙江艾兰得生物科技有限公司 Plant-based soft capsule rubber with anti-adhesion function
CN112569204A (en) * 2020-12-30 2021-03-30 湖北人福药用辅料股份有限公司 Pullulan polysaccharide and starch plant enteric-coated capsule and preparation method thereof
CN112603905A (en) * 2020-12-30 2021-04-06 湖北人福药用辅料股份有限公司 Preparation process of pullulan plant capsules
EP4074191A4 (en) * 2020-12-31 2024-04-10 Sirio Pharma Co Ltd Starch film-forming composition and method for preparing capsule shell
CN113180136A (en) * 2021-04-13 2021-07-30 浙江新维士生物科技有限公司 Preparation method of gel soft sweets
CN114642648A (en) * 2022-04-26 2022-06-21 仙乐健康科技股份有限公司 Starch film-forming composition and application thereof in soft capsules
CN114642648B (en) * 2022-04-26 2023-10-03 仙乐健康科技股份有限公司 Starch film forming composition and application thereof in soft capsules
CN115364068A (en) * 2022-08-23 2022-11-22 青岛至纯生物科技有限公司 Temperature-sensitive capsule and preparation method thereof
CN117281259A (en) * 2023-09-19 2023-12-26 广东润智源健康科技有限公司 Fish oil soft capsule with stable storage and easy disintegration and preparation method thereof
CN117281259B (en) * 2023-09-19 2024-03-22 广东润智源健康科技有限公司 Fish oil soft capsule with stable storage and easy disintegration and preparation method thereof

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