CN111298743A - Vertical reaction kettle for surfactant - Google Patents
Vertical reaction kettle for surfactant Download PDFInfo
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- CN111298743A CN111298743A CN201911066815.9A CN201911066815A CN111298743A CN 111298743 A CN111298743 A CN 111298743A CN 201911066815 A CN201911066815 A CN 201911066815A CN 111298743 A CN111298743 A CN 111298743A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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Abstract
The invention provides a vertical surfactant reaction kettle which comprises a kettle body, a kettle cover, a motor and a stirring structure, wherein a feeding hole is formed in the kettle cover, a discharging hole is formed in the bottom of the kettle body, the stirring structure comprises a main rotating shaft and a plurality of stirring assemblies arranged on the main rotating shaft, the upper end of the main rotating shaft is connected with a power output end of the motor, and the lower end of the main rotating shaft extends into the kettle body; the stirring subassembly includes a plurality of stirring leaves of stacking in proper order down from last, the relative angle of two adjacent stirring leaves can be adjusted. Through setting up the stirring subassembly, under the prerequisite of ensureing to mix the degree of consistency, realize stirring the adjustable of degree of consistency.
Description
Technical Field
The invention relates to the technical field of surfactant processing, in particular to a vertical surfactant reaction kettle.
Background
The surfactant is a substance which is added in a small amount and can cause the interface state of a solution system to change obviously. Has fixed hydrophilic and lipophilic groups and can be directionally arranged on the surface of the solution. The surfactant has a series of physical and chemical effects of wetting or anti-sticking, emulsifying or demulsifying, foaming or defoaming, solubilizing, dispersing, washing, corrosion prevention, antistatic and the like and corresponding practical application, so that the surfactant becomes a flexible and diversified fine chemical product with wide application. Besides being used as detergents in daily life, surfactants can cover almost all areas of fine chemistry.
In the surfactant processing process, a reaction kettle is generally adopted to fully mix reactants. In the prior art, in order to improve the uniformity of mixing, the stirring mode of a reaction kettle is generally adjusted, for example, a reaction kettle related to a novel green surfactant, which is disclosed in chinese patent publication No. CN203494517U and application No. 201320638794.5, discloses the following technical contents: including the cauldron body, kettle cover, main shaft, main motor, feed inlet, horizontal stirring frame, horizontal axle, external motor, electric heater, singlechip, discharge gate, temperature sensor, alarm, vertical stirring frame, kettle cover and cauldron body coupling, the main shaft is located the internal portion of cauldron, main motor is connected with the main shaft, the feed inlet is located the cauldron body, horizontal stirring frame is connected with the main shaft, horizontal axle is located the internal portion of cauldron, external motor is located the external portion of cauldron, the electric heater is located the cauldron body, the singlechip is connected with the electric heater, the discharge gate is located the downside of the cauldron body, temperature sensor is located the cauldron body, the alarm is located the temperature sensor upside, vertical stirring frame is connected with horizontal axle. The defect that such structure setting exists is that make reation kettle inner structure more complicated to, in order to realize two-way stirring action, be located the external motor outside the cauldron body, horizontal axle is located the cauldron internal portion, and the requirement can be higher in the aspect of the leakproofness, otherwise can influence reation kettle's mixing quality. In other reaction kettles, the structure of the stirring shaft is fixed, namely the matching of the rotating shaft and the stirring blade, and the stirring uniformity is not adjustable within a set time by the conventional structure; in view of this situation, improvements are urgently needed.
Disclosure of Invention
Based on this, the invention aims to provide a vertical surfactant reaction kettle, which is provided with a stirring assembly to realize the adjustment of the stirring uniformity on the premise of ensuring the mixing uniformity.
The invention provides a vertical surfactant reaction kettle which comprises a kettle body, a kettle cover, a motor and a stirring structure, wherein a feeding hole is formed in the kettle cover, a discharging hole is formed in the bottom of the kettle body, the stirring structure comprises a main rotating shaft and a plurality of stirring assemblies arranged on the main rotating shaft, the upper end of the main rotating shaft is connected with a power output end of the motor, and the lower end of the main rotating shaft extends into the kettle body; the stirring subassembly includes a plurality of stirring leaves of stacking in proper order down from last, the relative angle of two adjacent stirring leaves can be adjusted.
As a preferred scheme, the stirring subassembly includes first stirring leaf, second stirring leaf, third stirring leaf, first stirring leaf includes the lantern ring, fixed setting is in the stirring leaf A of the relative both sides of lantern ring, the second stirring leaf includes the lantern ring, fixed setting is in the stirring leaf B of the relative both sides of lantern ring, the third stirring leaf includes the lantern ring, fixed setting is in the stirring leaf C of the relative both sides of lantern ring, each the lantern ring all corresponds the cover and establishes in the main pivot, the position that corresponds with the stirring subassembly in the main pivot all is provided with the external screw thread, each the inner wall of lantern ring all be provided with external screw thread complex internal thread.
As a preferred scheme, a plurality of positioning pins are convexly arranged on the lower surface of the lantern ring of the first stirring blade, and a plurality of slots are arranged on the upper surface of the lantern ring of the second stirring blade; the lower surface of the lantern ring of second stirring leaf is protruding to be equipped with a plurality of locating pins, the upper surface of the lantern ring of third stirring leaf is provided with a plurality of slots.
As a preferable scheme, an upper fixing lantern ring is arranged on the upper surface of the first stirring blade, a bolt hole is arranged on the upper surface of the lantern ring of the first stirring blade, and a bolt fixedly connected with the first stirring blade penetrates through the upper fixing lantern ring; the lower surface of the third stirring blade is provided with a lower fixing sleeve ring, the lower surface of the third stirring blade is provided with a bolt hole, and a connecting bolt fixed with the third stirring blade penetrates through the lower fixing sleeve ring.
Preferably, the stirring blades a, B and C are stirring blades with different shapes.
As a preferred scheme, the shape of the stirring blade A is a strip plate body; the stirring blade B is a plate body with a V-shaped cross section; the stirring blade C is arranged in a columnar shape.
Preferably, the upper surface of the stirring blade B is irregularly distributed with a plurality of convex particles along the V-shaped surface.
Preferably, the stirring blade C is provided with a plurality of convex columns along the columnar outer surface array thereof.
As a preferred scheme, a backing material stirring component is arranged at the lower end of the main rotating shaft; the backing material stirring assembly comprises a mounting sleeve and stirring blocks arranged on the outer side surface of the mounting sleeve in a circumferential array mode.
Preferably, the part of the stirring block extending out of the mounting sleeve is obliquely arranged.
The invention has the beneficial effects that:
1. the stirring assembly comprises a plurality of stirring blades which are sequentially overlapped from top to bottom, the relative angle of two adjacent stirring blades can be adjusted, the number of the stirring blades can be set according to the required stirring uniformity, and the stirring uniformity can be influenced by adjusting the relative expansion angle between the two adjacent stirring blades, so that the internal structure of the reaction kettle is not required to be complicated, the mixing uniformity is improved by adjusting the relative expansion angle between the stirring blades in a set time, and the operation is simple and convenient;
2. stirring leaf A, stirring leaf B, stirring leaf C set up to the stirring leaf that the shape is different, and the stirring leaf of multiple shape carries out stirring operation simultaneously to further strengthen mixing the degree of consistency.
Drawings
Fig. 1 is a structural view of the present invention.
Fig. 2 is a structural view of the stirring assembly.
Fig. 3 is a structural view of the first agitating blade.
Fig. 4 is a structural view of the second agitating blade.
Fig. 5 is a structural view of a third agitating blade.
Fig. 6 is a sectional view of the second agitating blade.
Fig. 7 is a sectional view of the third agitating blade.
Fig. 8 is a schematic view of the first stirring blade 15, the second stirring blade 16, and the third stirring blade 17 in a developed state.
The reference signs are: the device comprises a motor 10, a feed inlet 11, a kettle cover 12, a main rotating shaft 13, an upper fixing sleeve ring 14, a first stirring blade 15, a second stirring blade 16, a third stirring blade 17, a lower fixing sleeve ring 18, an installation sleeve 19, a stirring block 20, a discharge port 21, a kettle body 22, a bolt 24, a positioning pin 25, a slot 26, a sleeve ring 27, convex particles 28, a convex column 29, a stirring blade A30, a stirring blade B31, a stirring blade C32 and a flange 23.
Detailed Description
For further understanding of the features and technical means of the present invention, as well as the specific objects and functions attained by the present invention, the present invention will be described in further detail with reference to the accompanying drawings and detailed description.
Please refer to fig. 1-8: a vertical reaction kettle for a surfactant comprises a kettle body 22, a kettle cover 12, a motor 10 and a stirring structure, wherein a feeding hole 11 is formed in the kettle cover 12, and a discharging hole 21 is formed in the bottom of the kettle body 22. The kettle body 22 and the kettle cover 12 are connected through a flange 23, and a sealing structure is arranged at the connection part.
The stirring structure comprises a main rotating shaft 13 and a plurality of stirring components arranged on the main rotating shaft 13, the upper end of the main rotating shaft 13 is connected with the power output end of the motor 10, and the lower end of the main rotating shaft 13 penetrates through the kettle cover 12 and extends into the kettle body 22; the stirring assembly comprises a plurality of stirring blades which are sequentially overlapped from top to bottom, and the relative angle between two adjacent stirring blades can be adjusted. The motor drives the main rotating shaft 13 to rotate in the kettle body 22.
The stirring subassembly includes first stirring leaf 15, second stirring leaf 16, third stirring leaf 17, first stirring leaf 15 includes the lantern ring 27, the fixed stirring leaf A30 that sets up in the relative both sides of lantern ring 27, second stirring leaf 16 includes lantern ring 27, the fixed stirring leaf B31 that sets up in the relative both sides of lantern ring, third stirring leaf 17 includes the lantern ring 27, the fixed stirring leaf C32 that sets up in the relative both sides of lantern ring, each lantern ring 27 all corresponds the cover and establishes on main pivot 13, the position that corresponds with the stirring subassembly on main pivot 13 all is provided with the external screw thread, the inner wall of each lantern ring all be provided with external screw thread complex internal thread.
The lower surface of the lantern ring of first stirring leaf 15 is protruding to be equipped with a plurality of locating pins 25, and in this embodiment, the quantity of locating pin 25 sets up to 2. The upper surface of the collar of the second stirring blade 16 is provided with a plurality of slots 26, and in the present embodiment, the number of the slots 26 is set to 6. The lower surface of the lantern ring of second stirring leaf 16 is protruding to be equipped with a plurality of locating pins 25, and in this embodiment, the quantity of locating pin 25 sets up to 2. The upper surface of the collar of the third stirring vane 17 is provided with a plurality of slots 26. In the present embodiment, the number of slots 26 is set to 6. The positioning pins 25 are correspondingly inserted into different slots 26, and the spreading angles between two adjacent stirring blades are different.
An upper fixing lantern ring 14 is arranged on the upper surface of the first stirring blade 15, a bolt hole is formed in the upper surface of the lantern ring of the first stirring blade 15, and a bolt 24 fixedly connected with the first stirring blade 15 penetrates through the upper fixing lantern ring 14; the lower surface of the third stirring blade 17 is provided with a lower fixing lantern ring 18, the lower surface of the third stirring blade 17 is provided with a bolt hole, and a connecting bolt 24 fixed with the third stirring blade 17 penetrates through the lower fixing lantern ring 18. The first stirring blade 15, the second stirring blade 16 and the third stirring blade 17 are respectively connected together through an upper fixing lantern ring 14 and a lower fixing lantern ring 18.
The stirring blades A30, B31 and C32 are provided as stirring blades with different shapes. The stirring blade A30 is shaped into a strip plate body; the stirring blade B31 is a plate body with a V-shaped cross section; the stirring blade C32 was provided in a columnar shape.
In a preferred embodiment, the upper surface of the stirring blade B31 is provided with a plurality of protruding grains 28 distributed irregularly along the V-shaped surface.
As a preferred embodiment, the stirring blade C32 is provided with a plurality of convex columns 29 along its cylindrical outer surface array.
The lower end of the main rotating shaft 13 is provided with a backing material stirring component; the backing material stirring assembly comprises a mounting sleeve 19 and stirring blocks 20 arranged on the outer side surface of the mounting sleeve 19 in a circumferential array mode, and the mounting sleeve 19 is fixedly connected with the main rotating shaft 13. The part of the stirring block 20 extending out of the mounting sleeve is obliquely arranged. Through the structural arrangement, the materials accumulated at the bottom can be stirred, and the stirring uniformity is improved.
In the embodiment, the stirring assembly comprises a plurality of stirring blades which are sequentially stacked from top to bottom, the relative angle between two adjacent stirring blades can be adjusted, through the mode, the number of the stirring blades can be set according to the required stirring uniformity in a set time, in addition, the stirring uniformity can be influenced by adjusting the relative unfolding angle between the two adjacent stirring blades, the improvement of the mixing uniformity can be realized by adjusting the relative unfolding angle between the stirring blades in a set time, and the operation is simple and convenient; stirring leaf A, stirring leaf B, stirring leaf C set up to the stirring leaf that the shape is different, and the stirring leaf of multiple shape carries out stirring operation simultaneously to further strengthen mixing the degree of consistency.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. The utility model provides a vertical reation kettle of surfactant, includes the cauldron body (22), kettle cover (12), motor (10), stirring structure, be provided with feed inlet (11) on kettle cover (12), the bottom of the cauldron body (22) is provided with discharge gate (21), its characterized in that: the stirring structure comprises a main rotating shaft (13) and a plurality of stirring assemblies arranged on the main rotating shaft (13), the upper end of the main rotating shaft (13) is connected with the power output end of the motor (10), and the lower end of the main rotating shaft (13) extends into the kettle body (22); the stirring subassembly includes a plurality of stirring leaves of stacking in proper order down from last, the relative angle of two adjacent stirring leaves can be adjusted.
2. The vertical surfactant reaction kettle according to claim 1, wherein: the stirring subassembly includes first stirring leaf (15), second stirring leaf (16), third stirring leaf (17), first stirring leaf (15) are including lantern ring (27), fixed setting the stirring leaf A (30) of the relative both sides of lantern ring (27), second stirring leaf (16) are including lantern ring (27), fixed setting the stirring leaf B (31) of the relative both sides of lantern ring, third stirring leaf (17) are including lantern ring (27), fixed setting the stirring leaf C (32) of the relative both sides of lantern ring, each lantern ring (27) all correspond the cover and establish on main pivot (13), on main pivot (13) with the position that the stirring subassembly corresponds all is provided with the external screw thread, each the inner wall of the lantern ring all be provided with external screw thread complex internal thread.
3. The vertical surfactant reaction kettle according to claim 2, wherein: a plurality of positioning pins (25) are convexly arranged on the lower surface of the lantern ring of the first stirring blade (15), and a plurality of slots (26) are arranged on the upper surface of the lantern ring of the second stirring blade (16); the lower surface of the lantern ring of second stirring leaf (16) protruding is equipped with a plurality of locating pins (25), the upper surface of the lantern ring of third stirring leaf (17) is provided with a plurality of slots (26).
4. The vertical surfactant reaction kettle according to claim 3, wherein: an upper fixing lantern ring (14) is arranged on the upper surface of the first stirring blade (15), bolt holes are formed in the upper surface of the lantern ring of the first stirring blade (15), and bolts (24) fixedly connected with the first stirring blade (15) penetrate through the upper fixing lantern ring (14); the lower surface of third stirring leaf (17) is provided with down fixed lantern ring (18), the lower surface of third stirring leaf (17) is provided with the bolt hole, run through on the fixed lantern ring down be provided with connecting bolt (24) that third stirring leaf (17) are fixed.
5. The vertical surfactant reaction kettle according to any one of claims 2 to 4, wherein: the stirring blades A (30), B (31) and C (32) are different in shape.
6. The vertical surfactant reaction kettle according to claim 5, wherein: the stirring blade A (30) is arranged into a strip-shaped plate body; the shape of the stirring blade B (31) is a plate body with a V-shaped cross section; the stirring blade C (32) is provided in a columnar shape.
7. The vertical surfactant reaction kettle according to claim 6, wherein: the upper surface of the stirring blade B (31) is irregularly distributed with a plurality of convex particles (28) along the V-shaped surface.
8. The vertical surfactant reaction kettle according to claim 6, wherein: the stirring blade C (32) is provided with a plurality of convex columns (29) along the columnar outer surface array.
9. The vertical surfactant reaction kettle according to claim 8, wherein: a bottom material stirring component is arranged at the lower end of the main rotating shaft (13); the backing material stirring assembly comprises a mounting sleeve (19) and stirring blocks (20) which are arranged on the outer side surface of the mounting sleeve (19) in a circumferential array mode.
10. The vertical surfactant reaction kettle according to claim 9, wherein: the part of the stirring block (20) extending out of the mounting sleeve is obliquely arranged.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911066815.9A CN111298743B (en) | 2019-11-04 | 2019-11-04 | Vertical reaction kettle for surfactant |
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|---|---|---|---|
| CN201911066815.9A CN111298743B (en) | 2019-11-04 | 2019-11-04 | Vertical reaction kettle for surfactant |
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| CN111298743A true CN111298743A (en) | 2020-06-19 |
| CN111298743B CN111298743B (en) | 2021-10-22 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112958027A (en) * | 2021-03-15 | 2021-06-15 | 西安凯尔文石化助剂制造有限公司 | Novel surfactant/foaming agent reation kettle |
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| CN209451698U (en) * | 2019-01-14 | 2019-10-01 | 武汉德创捷机电技术有限公司 | A kind of coating material agitator |
| CN110252233A (en) * | 2019-07-04 | 2019-09-20 | 南通醋酸纤维有限公司 | The agitating device of precipitating device |
| CN111420625A (en) * | 2020-05-12 | 2020-07-17 | 江门市昆益树脂材料科技有限公司 | High viscosity feed liquid reation kettle and agitating unit |
| CN213013785U (en) * | 2020-07-10 | 2021-04-20 | 河南亚龙智能装备有限公司 | Pitch agitator of stirring arm installation angle adjustable |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112958027A (en) * | 2021-03-15 | 2021-06-15 | 西安凯尔文石化助剂制造有限公司 | Novel surfactant/foaming agent reation kettle |
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