CN111268821A - Fine treatment method for slurry for clay production from building spoil - Google Patents
Fine treatment method for slurry for clay production from building spoil Download PDFInfo
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- 239000004927 clay Substances 0.000 title claims abstract description 78
- 239000002002 slurry Substances 0.000 title claims abstract description 69
- 238000000034 method Methods 0.000 title claims abstract description 31
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 26
- 239000004576 sand Substances 0.000 claims abstract description 148
- 239000000203 mixture Substances 0.000 claims abstract description 92
- 238000000926 separation method Methods 0.000 claims abstract description 83
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 46
- 239000006185 dispersion Substances 0.000 claims abstract description 32
- 230000005484 gravity Effects 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 238000001556 precipitation Methods 0.000 claims abstract description 19
- 238000005189 flocculation Methods 0.000 claims abstract description 16
- 230000016615 flocculation Effects 0.000 claims abstract description 16
- 238000012216 screening Methods 0.000 claims abstract description 16
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 230000008569 process Effects 0.000 claims abstract description 10
- 238000000151 deposition Methods 0.000 claims abstract description 4
- 230000001376 precipitating effect Effects 0.000 claims abstract 3
- 239000012716 precipitator Substances 0.000 claims abstract 3
- 238000004062 sedimentation Methods 0.000 claims description 57
- 238000010276 construction Methods 0.000 claims description 22
- 238000007670 refining Methods 0.000 claims description 10
- 239000012535 impurity Substances 0.000 claims description 8
- 239000002689 soil Substances 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 7
- 239000002699 waste material Substances 0.000 claims description 7
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 6
- 230000003311 flocculating effect Effects 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 5
- 239000002244 precipitate Substances 0.000 claims description 5
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 4
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims description 4
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims description 4
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000002245 particle Substances 0.000 description 39
- 230000000694 effects Effects 0.000 description 8
- 239000002994 raw material Substances 0.000 description 7
- 238000011161 development Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000008394 flocculating agent Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000009418 renovation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000004162 soil erosion Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000000844 transformation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F2001/007—Processes including a sedimentation step
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Treatment Of Sludge (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
Description
技术领域technical field
本发明涉及一种建筑弃土生产黏土的工艺,具体的,涉及一种建筑弃土生产黏土用的泥浆精细化处理方法。The invention relates to a process for producing clay from construction spoil, in particular to a method for refining mud for producing clay from construction spoil.
技术背景technical background
随着我国经济规模发展在国际中的地位越来越重要,对全球经济发展已举足轻重,我国的城镇化速度也越来越快,城镇化比例也越来越高。这主要体现在城市中建筑物越来越多,地下空间的开发规模也与日俱增。但随之而来的是建筑废弃物越来也多,不仅有对旧建筑物的翻新或拆除产生的建筑废弃物,而且还有新建设的建筑物将过量的中间用料直接废弃。为了更好的实现城市的综合治理以及资源的综合化利用,将建筑废弃物回收处理再利用成为了国家倡导、民众需求、可持续发展必须的理念。将建筑废弃物重新利用催生并促进了相关行业的发展,在构筑资源循环利用的同时,也促进了社会经济的正向循环。As my country's economic scale development has become more and more important in the world, it has played a pivotal role in global economic development. my country's urbanization rate is getting faster and faster, and the proportion of urbanization is also getting higher and higher. This is mainly reflected in the increasing number of buildings in the city, and the development scale of underground space is also increasing day by day. However, there is an increasing amount of construction waste, not only from the renovation or demolition of old buildings, but also from newly constructed buildings that directly discard excess intermediate materials. In order to better realize the comprehensive management of the city and the comprehensive utilization of resources, the recycling of construction waste has become a national advocacy, public demand, and a necessary concept for sustainable development. The reuse of construction waste has spawned and promoted the development of related industries. While building resource recycling, it also promotes a positive social and economic cycle.
建筑弃土是常见的建筑废弃物之一,其通过处理后能够应用于多种用途,例如可以用于美化环境的绿化带植物用土,用于填充水土流失部分保持生态环境,用于再此生产建筑材料的原料等。根据不同的用途建筑弃土会进行针对性的不同处理,通常包括杂质的去除,粉碎成需要的粒径,分离并收集目标物质等处理步骤,虽然主要步骤的处理手段和实现的目的相似,但建筑弃土的用途在实际中决定了相关行业人员采用的处理方法。Construction spoil is one of the common construction wastes, which can be used for various purposes after treatment, such as green belt plant soil that can be used for beautifying the environment, used to fill in soil erosion, and partially maintain the ecological environment for re-production. Raw materials for building materials, etc. According to different uses, the construction spoil will be processed differently, usually including the removal of impurities, crushing into the required particle size, separation and collection of target substances and other processing steps. The use of construction spoil actually determines the disposal method adopted by the relevant industry personnel.
目前,在使用建筑弃土生产黏土的工艺中,通常只对泥砂混合物中体积较大的砂石进行清除,而往往不会对泥浆中的细砂进行清理。因为,采用建筑弃土为原料制备的黏土通常被认为由于采用废弃料导致其中的“杂物”无法被处理“干净”,其市场价值与正常原料或正常方法获得的黏土不能同日而语。但建筑弃土的来源并非都是来自废弃建筑,也包括新建设建筑物中的废弃中间料,而且经过精细处理后建筑弃土能够生产品质较高的黏土,其在功能上并未与正常原料或正常方法制备的黏土具有实质性的差距,而且,建筑弃土的来源广泛却越来越多,正常原料或黏土开采资源相对越来越少,使得不同原料在经济上的差距已难以忽略。与此同时,随着城镇化速度越来越快,高品质黏土的需求量也越来越多。因此,越来越多的采用建筑弃土生产黏土的企业开始进军高品质黏土的市场。目前使用建筑弃土生产黏土的工艺中,分离泥浆和砂子的方法主要是利用物理沉淀法,通过泥浆泵和一端较长的倾斜管道,利用砂子的沉淀速度比泥土的沉淀速度快的物理性质将泥浆液和砂子分离,或是采用旋液分离器利用不同比重的物质的离心力不同将泥浆液与砂子分离,上述方法适合连续生产且非常经济,而且能够去除大部分粗颗粒砂子,但是采用这种方法难免会有部分细砂子跟随泥浆一起进入到下一工步中,而且沉淀法主要依靠物质的比重,有些砂子由于种种原因导致粒度较大的同时比重较轻而未能有效分离,最终影响黏土的品质。筛分技术能够很好对泥浆和砂子进行粒径上的分离,但采用大孔径网筛对于去除细砂粒效率低,采用较小孔径的网筛成本较高的同时,生产分离的速率较低,网筛经常被小颗粒堵塞。出于能够综合生产效率和生产高品质黏土的要求,对建筑弃土生产黏土用的泥浆进行精细化处理仍然需要研究改进,使生产企业能够高效的生产高品质黏土。At present, in the process of using construction spoil to produce clay, usually only the larger sand and gravel in the mud-sand mixture are removed, and the fine sand in the mud is often not removed. Because, the clay prepared by using construction spoil as raw material is generally considered to be the "scraps" in it that cannot be treated "cleanly" due to the use of waste materials, and its market value cannot be compared with the clay obtained by normal raw materials or normal methods. However, the sources of construction spoil are not all from abandoned buildings, but also the waste intermediate materials in newly constructed buildings. After fine processing, construction spoil can produce high-quality clay, which is not functionally similar to normal raw materials. There is a substantial gap between the clay prepared by the normal method or the normal method, and the sources of construction spoil are more and more extensive, and the normal raw materials or clay mining resources are relatively less and less, so that the economic gap between different raw materials is difficult to ignore. At the same time, with the speed of urbanization, the demand for high-quality clay is also increasing. Therefore, more and more companies that use construction spoil to produce clay have begun to enter the market of high-quality clay. At present, in the process of using construction spoil to produce clay, the method of separating mud and sand is mainly to use physical precipitation method. Through mud pump and long inclined pipe at one end, the sedimentation speed of sand is faster than that of soil. The mud liquid and sand are separated, or the mud liquid and the sand are separated by using a hydrocyclone by using different centrifugal forces of substances with different specific gravity. The above method is suitable for continuous production and very economical, and can remove most of the coarse sand. It is inevitable that some fine sand will enter the next step with the mud, and the precipitation method mainly depends on the specific gravity of the material. Some sands have large particle size and light specific gravity due to various reasons and cannot be effectively separated, which will eventually affect the clay. quality. The screening technology can well separate the mud and sand in terms of particle size, but the use of a large-aperture mesh screen is inefficient for removing fine sand particles, and the use of a smaller-aperture mesh screen is more costly, and the rate of production separation is low. Screens are often clogged with small particles. Due to the requirements of comprehensive production efficiency and high-quality clay, the refinement of mud used for the production of clay from construction spoil still needs research and improvement, so that production enterprises can efficiently produce high-quality clay.
发明内容SUMMARY OF THE INVENTION
本发明为了解决上述技术问题,提出了一种建筑弃土生产黏土用的泥浆精细化处理方法,其依次采用二次沉降重颗粒、筛滤大颗粒、振动处理、絮凝收集的多级处理步骤,实现了高效率的生产高品质黏土的工艺。具体方案如下:In order to solve the above-mentioned technical problems, the present invention proposes a mud refinement treatment method for producing clay from construction spoil, which sequentially adopts the multi-stage treatment steps of secondary sedimentation of heavy particles, screening of large particles, vibration treatment, and flocculation collection, A highly efficient process for producing high-quality clay is achieved. The specific plans are as follows:
一种建筑弃土生产黏土用的泥浆精细化处理方法,依次包括如下步骤:A mud refinement treatment method for producing clay from construction spoil, comprising the following steps in sequence:
(1)预沉淀处理:通过沉淀池将原始泥砂混合物中部分比重较大的砂子沉淀,得到细砂泥浆混合物;(1) Pre-precipitation treatment: Part of the sand with a larger specific gravity in the original mud-sand mixture is precipitated through a sedimentation tank to obtain a fine-sand mud mixture;
(2)沉淀处理:通过倾斜的泥砂分离管道将细砂泥浆混合物中部分比重较大的细砂沉淀,得到泥浆混合物;(2) Precipitation treatment: Part of the fine sand with larger specific gravity in the fine sand mud mixture is precipitated through the inclined mud sand separation pipeline to obtain a mud mixture;
(3)筛分处理:将泥浆混合物通入高压分离罐中进行筛分,得到泥浆水;(3) Screening treatment: pass the mud mixture into the high-pressure separation tank for screening to obtain mud water;
(4)振动处理:通过振动处理将泥浆水中的至少部分剩余细砂沉淀在振动池底部;(4) Vibration treatment: at least part of the remaining fine sand in the muddy water is deposited at the bottom of the vibrating tank by vibration treatment;
(5)絮凝收集:振动池上部的泥浆分散液送入黏土沉淀池中,通过加入快速絮凝沉淀剂使得泥浆分散液分为下层的黏土浆和上层的清水,收集黏土浆。(5) Flocculation collection: The mud dispersion in the upper part of the vibrating tank is sent to the clay sedimentation tank, and the mud dispersion is divided into the lower clay slurry and the upper water by adding a fast flocculating precipitant, and the clay slurry is collected.
优选的,步骤(1)中,将包含泥浆液和砂子的原始泥砂混合物从长度为10-50m的长条形的沉淀池的一端通入,沉淀池的另一端中部与浆液泵连接,长条形的沉淀池能够将原始泥砂混合物中部分比重较大的砂子沉淀,比重轻的杂质会漂浮在原始泥砂混合物表面,沉淀池中部得到细砂泥浆混合物。Preferably, in step (1), the original mud-sand mixture containing mud slurry and sand is introduced from one end of a long sedimentation tank with a length of 10-50m, and the middle of the other end of the sedimentation tank is connected with the slurry pump, and the long The shaped sedimentation tank can precipitate part of the sand with larger specific gravity in the original mud-sand mixture, the impurities with light specific gravity will float on the surface of the original mud-sand mixture, and the fine sand mud mixture is obtained in the middle of the sedimentation tank.
优选的,步骤(2)中,浆液泵将细砂泥浆混合物送至长度为5-30m倾斜的泥砂分离管道中,由于泥砂分离管道与地面倾斜设置,且分离管道的进料端靠近地面,当浆液泵将细砂泥浆混合物送入泥砂分离管道时,部分比重较大的细砂会沉淀在泥砂分离管道底部,而泥浆混合物则被送至下一工序中;泥砂分离管道的出料端与泥浆罐连接,泥浆混合物从泥砂分离管道中进入到泥浆罐内,泥浆罐能够储存泥浆混合物。Preferably, in step (2), the slurry pump sends the fine sand-mud mixture to the mud-sand separation pipeline with a length of 5-30 m inclined. Since the mud-sand separation pipeline is inclined to the ground, and the feed end of the separation pipeline is close to the ground, when When the slurry pump sends the fine sand-mud mixture into the mud-sand separation pipeline, part of the fine sand with larger specific gravity will settle at the bottom of the mud-sand separation pipeline, and the mud-sand mixture will be sent to the next process; The tank is connected, and the mud mixture enters the mud tank from the mud sand separation pipeline, and the mud tank can store the mud mixture.
优选的,步骤(3)中,高压泵将泥浆罐中的泥浆混合物送至高压分离罐内,高压分离罐内设有筛网,高压泵将泥浆混合物增压,使得泥浆水能够通过筛网,而部分直径较大的细砂则留在高压分离罐内。Preferably, in step (3), the high-pressure pump sends the mud mixture in the mud tank to the high-pressure separation tank, the high-pressure separation tank is provided with a screen, and the high-pressure pump pressurizes the mud mixture so that the mud water can pass through the screen, Part of the fine sand with larger diameter remains in the high-pressure separation tank.
优选的,在步骤(4)中,将高压分离罐分离出的泥浆水通入到振动池的底部,同时振动池底部的振动使得泥浆水中至少部分剩余的细砂被振动沉淀在振动池的底部,而在振动池的上层形成泥浆分散液。Preferably, in step (4), the mud water separated from the high-pressure separation tank is passed into the bottom of the vibrating pool, and the vibration at the bottom of the vibrating pool causes at least part of the remaining fine sand in the mud water to be vibrated and deposited at the bottom of the vibrating pool. , and a slurry dispersion is formed in the upper layer of the vibrating tank.
优选的,在步骤(5)中,振动池上层的泥浆分散液被传送至黏土沉淀池中,向黏土沉淀池中加入泥浆快速絮凝沉淀剂,使得泥浆水中的黏土快速凝聚沉淀;絮凝沉淀完成后,从黏土沉淀池的底部将黏土浆送至压滤机中,从黏土沉淀池的上部将清水送至水循环系统中。Preferably, in step (5), the mud dispersion liquid in the upper layer of the vibrating tank is transferred to the clay sedimentation tank, and a mud fast flocculating precipitant is added to the clay sedimentation tank, so that the clay in the mud water quickly coagulates and precipitates; after the flocculation and sedimentation is completed , the clay slurry is sent to the filter press from the bottom of the clay sedimentation tank, and the clean water is sent to the water circulation system from the upper part of the clay sedimentation tank.
优选的,在步骤(1)中,包含泥浆液和砂子的原始泥砂混合物以0.5m/s-1m/s的速度从长条形的沉淀池的一端通入;在步骤(2)中,细砂泥浆混合物在分离管道内的流动速度小于0.5m/s。Preferably, in step (1), the original mud-sand mixture containing mud slurry and sand is introduced from one end of the elongated sedimentation tank at a speed of 0.5m/s-1m/s; in step (2), fine The flow velocity of the sand-mud mixture in the separation pipe is less than 0.5m/s.
优选的,在步骤(3)中,筛网孔径为0.1-2mm,优选0.5-1mm;泥浆混合物增压至0.15-5Mpa,优选0.5-1Mpa;泥浆混合物从高压分离罐底部进入并通过筛网,泥浆水从高压分离罐上部离开。Preferably, in step (3), the aperture of the screen is 0.1-2mm, preferably 0.5-1mm; the mud mixture is pressurized to 0.15-5Mpa, preferably 0.5-1Mpa; the mud mixture enters from the bottom of the high-pressure separation tank and passes through the screen, Slurry water leaves from the upper part of the high-pressure separation tank.
优选的,在步骤(4)中,在振动池的底部设置防水型声波振动装置,声波频率为50-5000Hz,优选100-500Hz。Preferably, in step (4), a waterproof acoustic wave vibration device is arranged at the bottom of the vibration pool, and the frequency of the acoustic wave is 50-5000 Hz, preferably 100-500 Hz.
优选的,在步骤(5)中,快速絮凝沉淀剂为无机絮凝剂,优选硫酸铝、硫酸铁、氯化铝、氯化铁、聚合硫酸铝、聚合硫酸铁中的一种或多种,将无机絮凝剂配置成质量分数0.5%-5%絮凝剂溶液,絮凝剂溶液与泥浆分散液体积比为1:10-100。Preferably, in step (5), the rapid flocculation precipitation agent is an inorganic flocculant, preferably one or more of aluminum sulfate, ferric sulfate, aluminum chloride, ferric chloride, polyaluminum sulfate, polyferric sulfate, and the The inorganic flocculant is configured into a flocculant solution with a mass fraction of 0.5%-5%, and the volume ratio of the flocculant solution to the mud dispersion liquid is 1:10-100.
本发明的有益效果:Beneficial effects of the present invention:
(1)本发明依次采用预沉淀处理、沉淀处理、筛分处理、振动处理和絮凝收集五级处理步骤对建筑弃土生产黏土用的泥浆进行精细化处理,能够基本去除比重大的砂子、粒径大的砂子,得到含砂量更低的泥浆分散液,从而能够得到纯净度更高的高品质黏土,避免了杂质降低黏土品质,而且各个步骤流程安排合理,能够高效、稳定地生产高品质黏土。(1) The present invention successively adopts the five-level treatment steps of pre-sedimentation treatment, precipitation treatment, screening treatment, vibration treatment and flocculation collection to refine the mud used for the production of clay from the construction spoil, which can basically remove the sand, particles with a large specific gravity. The larger diameter sand can obtain a slurry dispersion with lower sand content, so that high-quality clay with higher purity can be obtained, avoiding impurities to reduce the quality of clay, and the arrangement of each step process is reasonable, which can efficiently and stably produce high-quality clay. clay.
(2)本发明采用长条形沉淀池完成预沉淀处理不仅能够将明显比重或粒径过大的砂子颗粒进行快速沉积,并且能够去除大部分粗砂子颗粒,减少后面步骤流程的处理压力,而且能够去除比重过轻的杂质;采用倾斜的泥砂分离管道能够去除大部分砂子颗粒;经过两级沉淀处理,大部分砂子颗粒已经通过沉淀去除,但仍有少部分砂子(包括比重相似的砂子)残留在泥浆中。采用该泥浆虽然可以制备黏土,但其中的少量砂子使得制备的黏土在品质上下降,而且生产的黏土的性质也不是稳定的。本发明进一步通过筛分处理能够进一步去除粒径较小的砂子。为了能够更好的提高黏土品质以及保障其性质稳定,本发明进一步将过筛后的泥浆水通入振动池的底部,使得少量的砂子由于比重和粒径在振动池底部范围内振动,而泥浆中的小颗粒土以泥浆分散液的形式分散在振动池上层,最后振动池上层的泥浆分散液导入黏土沉淀池中进行絮凝沉淀收集。本发明创造性地在沉淀处理和筛分处理后采用振动处理,使得形成的泥浆分散液作为制备黏土的原料,不仅去除了浆液中至少部分剩余的砂子,而且使得成为泥浆分散液的小颗粒土都是能够通过振动分散至液体上层的,其保证了生产的黏土具有高品质和性质稳定,通过无机絮凝剂进行沉降能够实现对上述小颗粒土的快速收集,保证了制备工艺的效率。(2) The present invention adopts the long-strip sedimentation tank to complete the pre-sedimentation treatment, which can not only rapidly deposit sand particles with obvious specific gravity or excessive particle size, but also remove most of the coarse sand particles, reduce the processing pressure of the subsequent steps, and Impurities with too light specific gravity can be removed; most of the sand particles can be removed by the inclined mud-sand separation pipeline; after two-stage precipitation treatment, most of the sand particles have been removed by precipitation, but a small part of sand (including sand with similar specific gravity) remains in the mud. Although clay can be prepared by using the slurry, a small amount of sand in it makes the quality of the prepared clay deteriorate, and the properties of the produced clay are not stable. The present invention can further remove sand with smaller particle size through screening treatment. In order to better improve the quality of clay and ensure the stability of its properties, the present invention further passes the sieved mud water into the bottom of the vibrating pool, so that a small amount of sand vibrates within the range of the bottom of the vibrating pool due to its specific gravity and particle size, while the mud The small particles in the soil are dispersed in the upper layer of the vibrating tank in the form of mud dispersion, and finally the mud dispersion in the upper layer of the vibrating tank is introduced into the clay sedimentation tank for flocculation and sedimentation collection. The invention creatively adopts vibration treatment after precipitation treatment and screening treatment, so that the formed slurry dispersion liquid is used as the raw material for preparing clay, which not only removes at least part of the remaining sand in the slurry liquid, but also makes the small particles of soil that become the slurry dispersion liquid all disappear. It can be dispersed to the upper layer of the liquid through vibration, which ensures that the produced clay has high quality and stable properties, and sedimentation through inorganic flocculants can realize the rapid collection of the above-mentioned small particles of soil, ensuring the efficiency of the preparation process.
具体实施方式Detailed ways
以下对本发明的技术方案及优点做出更加详细的解释和说明。应当理解的是,说明书、具体实施方式中所呈现的内容,仅仅为了更加清楚地说明本发明的技术方案及其优点,并不对本发明的保护范围构成限制。本领域技术人员能够在说明书公开内容的基础上,针对各种合理的变换得到变化后的技术方案,只要不脱离本发明的精神,各种变化后的技术方案均包括在本发明的保护范围之内。The technical solutions and advantages of the present invention will be explained and described in more detail below. It should be understood that the contents presented in the description and the specific embodiments are only for the purpose of illustrating the technical solutions and advantages of the present invention more clearly, and do not limit the protection scope of the present invention. Those skilled in the art can obtain changed technical solutions for various reasonable transformations on the basis of the disclosure of the description. As long as they do not depart from the spirit of the present invention, various changed technical solutions are included in the protection scope of the present invention. Inside.
本发明的建筑弃土生产黏土用的泥浆精细化处理方法的具体实施方式如下:The specific embodiment of the mud refining treatment method for producing clay from the construction spoil of the present invention is as follows:
(1)预沉淀处理:通过沉淀池将原始泥砂混合物中部分比重较大的砂子沉淀,得到细砂泥浆混合物;(1) Pre-precipitation treatment: Part of the sand with a larger specific gravity in the original mud-sand mixture is precipitated through a sedimentation tank to obtain a fine-sand mud mixture;
将包含泥浆液和砂子的原始泥砂混合物从长度为10-50m的长条形的沉淀池的一端通入,沉淀池的另一端中部与浆液泵连接,长条形的沉淀池能够将原始泥砂混合物中部分比重较大的砂子沉淀,比重轻的杂质会漂浮在原始泥砂混合物表面,沉淀池中部得到细砂泥浆混合物;其中,包含泥浆液和砂子的原始泥砂混合物以0.5m/s-1m/s的速度从长条形的沉淀池的一端通入。The original mud-sand mixture containing mud and sand is introduced from one end of a long sedimentation tank with a length of 10-50m, and the middle of the other end of the sedimentation tank is connected with a slurry pump. The sand with a larger specific gravity in the middle part is precipitated, and the impurities with a light specific gravity will float on the surface of the original mud-sand mixture, and a fine-sand-mud mixture is obtained in the middle of the sedimentation tank; among them, the original mud-sand mixture containing mud liquid and sand is 0.5m/s-1m/s The speed is passed from one end of the elongated sedimentation tank.
本发明采用长条形的沉淀池对原始泥砂混合物进行沉积预处理,在沉淀池的一端通入原始泥砂混合物,在沉淀池的另一端排出,其原理为利用混合物中各物质的比重不同使得较重的粗颗粒砂子沉入沉淀池底部,较轻的杂质漂浮在沉淀池表面。由此,通过预沉淀处理能够使得在后的沉淀处理和筛分处理能够减轻砂子颗粒的处理压力,提高对砂子颗粒的处理效果,而且由于漂浮的杂质在该步骤中基本被去除,沉淀池中部得到了主要由细砂颗粒和土颗粒的细砂泥浆混合物,其保证了制备黏土的高品质。为了保证分离效果并兼顾生产效率,原始泥砂混合物在沉淀池中的运行速度不宜过快或过慢,而且沉淀池的长度也不宜过长或过短,经过试验运行,在长度为10-50m的沉淀池中以0.5m/s-1m/s的速度运行最佳,其既能完成预期的分离效果,而且运行效率较高。The invention adopts a long sedimentation tank to carry out deposition pretreatment on the original mud-sand mixture, and the original mud-sand mixture is introduced into one end of the sedimentation tank and discharged at the other end of the sedimentation tank. Heavy, coarse-grained sand sinks to the bottom of the sedimentation tank, and lighter impurities float on the surface of the sedimentation tank. Therefore, the pre-sedimentation treatment can reduce the processing pressure of the sand particles and improve the treatment effect of the sand particles in the subsequent sedimentation treatment and screening treatment. A fine sand slurry mixture is obtained consisting mainly of fine sand particles and soil particles, which guarantees a high quality of the prepared clay. In order to ensure the separation effect and take into account the production efficiency, the running speed of the original mud-sand mixture in the sedimentation tank should not be too fast or too slow, and the length of the sedimentation tank should not be too long or too short. In the sedimentation tank, the speed of 0.5m/s-1m/s is the best, which can not only complete the expected separation effect, but also has a high operating efficiency.
(2)沉淀处理:通过倾斜的泥砂分离管道将细砂泥浆混合物中部分比重较大的细砂沉淀,得到泥浆混合物;(2) Precipitation treatment: Part of the fine sand with larger specific gravity in the fine sand mud mixture is precipitated through the inclined mud sand separation pipeline to obtain a mud mixture;
浆液泵将细砂泥浆混合物送至长度为5-30m倾斜的泥砂分离管道中,由于泥砂分离管道与地面倾斜设置,且分离管道的进料端靠近地面,当浆液泵将细砂泥浆混合物送入泥砂分离管道时,部分比重较大的细砂会沉淀在泥砂分离管道底部,而泥浆混合物则被送至下一工序中;泥砂分离管道的出料端与泥浆罐连接,泥浆混合物从泥砂分离管道中进入到泥浆罐内,泥浆罐能够储存泥浆混合物;其中,细砂泥浆混合物在分离管道内的流动速度小于0.5m/s。The slurry pump sends the fine sand and mud mixture to the sloping mud and sand separation pipeline with a length of 5-30m. Since the mud and sand separation pipeline is inclined to the ground, and the feeding end of the separation pipeline is close to the ground, when the slurry pump sends the fine sand and mud mixture into the During the mud-sand separation pipeline, part of the fine sand with larger specific gravity will settle at the bottom of the mud-sand separation pipeline, and the mud mixture will be sent to the next process; into the mud tank, and the mud tank can store the mud mixture; wherein, the flow velocity of the fine sand mud mixture in the separation pipeline is less than 0.5m/s.
本发明采用两级沉淀处理原始泥砂混合物,在预沉淀处理后,通过倾斜的泥砂分离管道能够将细颗粒砂子去除。两级沉淀处理能够先去除大颗粒砂子再去除小颗粒砂子,避免了单级处理时大颗粒和小颗粒砂子同时处理使得处理量大,而且倾斜的管道使得大量的砂子在重力作用下下滑至泥砂分离管道入口,减小甚至堵塞泥砂分离管道入口,需要较频繁的清理泥砂分离管道,影响处理效果和效率;而且大颗粒和小颗粒砂子同时处理使得其相互影响,导致较多的砂子颗粒在泥砂分离管道出口处仍未被有效分离,而延长泥砂分离管道或减慢混合物流动速度虽然能够提高分离效率,但生产效率会下降。因此,本发明的针对粗细颗粒的砂子进行两级处理,能够更有效的去除砂子,而且保障了较高的生产效率。进一步,为了保证分离效果并兼顾生产效率,细砂泥浆混合物在倾斜的泥砂分离管道中的运行速度不宜过快或过慢,而且泥砂分离管道的长度也不宜过长或过短,经过试验运行,在长度为5-30m的泥砂分离管道中以小于0.5m/s的速度运行最佳,其既能完成预期的分离效果,而且运行效率较高。将泥浆混合物在储罐中进行储存可以协调两级沉淀处理和筛分处理的步骤衔接,而且静置在储罐中的泥浆混合物也会有一部分物质沉积在底部,实现分离效果。The invention adopts two-stage sedimentation to treat the original mud-sand mixture, and after the pre-precipitation treatment, the fine-grained sand can be removed through the inclined mud-sand separation pipeline. Two-stage sedimentation treatment can first remove large particles of sand and then remove small particles of sand, avoiding the simultaneous treatment of large particles and small particles of sand in single-stage treatment, which makes the processing capacity large, and the inclined pipeline makes a large amount of sand slide down to the mud sand under the action of gravity Separating the inlet of the pipeline, reducing or even blocking the inlet of the silt separation pipeline, requires more frequent cleaning of the silt separation pipeline, which affects the treatment effect and efficiency; and the simultaneous treatment of large particles and small particles of sand makes them affect each other, resulting in more sand particles in the mud and sand The outlet of the separation pipeline is still not effectively separated, and although extending the mud-sand separation pipeline or slowing down the flow rate of the mixture can improve the separation efficiency, the production efficiency will decrease. Therefore, the two-stage treatment of the coarse and fine particles of the present invention can remove the sand more effectively and ensure higher production efficiency. Further, in order to ensure the separation effect and take into account the production efficiency, the running speed of the fine sand mud mixture in the inclined mud sand separation pipeline should not be too fast or too slow, and the length of the mud sand separation pipeline should not be too long or too short. It is best to operate at a speed of less than 0.5m/s in a silt and sand separation pipeline with a length of 5-30m, which can not only achieve the expected separation effect, but also has a high operating efficiency. Storing the mud mixture in the storage tank can coordinate the steps of the two-stage sedimentation treatment and the screening treatment, and the mud mixture left in the storage tank will also have a part of the material deposited at the bottom to achieve the separation effect.
(3)筛分处理:将泥浆混合物通入高压分离罐中进行筛分,得到泥浆水;(3) Screening treatment: pass the mud mixture into the high-pressure separation tank for screening to obtain mud water;
高压泵将泥浆罐中的泥浆混合物送至高压分离罐内,高压分离罐内设有筛网,高压泵将泥浆混合物增压,使得泥浆水能够通过筛网,而部分直径较大的细砂则留在高压分离罐内;其中,泥浆混合物从高压分离罐底部进入并通过筛网,泥浆水从高压分离罐上部离开;筛网孔径为0.1-2mm,优选0.5-1mm;泥浆混合物增压至0.15-5Mpa,优选0.5-1Mpa。The high-pressure pump sends the mud mixture in the mud tank to the high-pressure separation tank. There is a screen in the high-pressure separation tank. The high-pressure pump pressurizes the mud mixture so that the mud water can pass through the screen, while some fine sand with a larger diameter is stay in the high-pressure separation tank; wherein, the mud mixture enters from the bottom of the high-pressure separation tank and passes through the screen, and the mud water leaves from the upper part of the high-pressure separation tank; the aperture of the screen is 0.1-2mm, preferably 0.5-1mm; the mud mixture is pressurized to 0.15 -5Mpa, preferably 0.5-1Mpa.
经过两级沉淀处理的泥浆混合物是通过比重进行的物质分离,而大粒径且比重相对低的砂子仍然存在于泥浆混合物中,而且粒径分布的不均匀也无法更好实现对制备黏土品质的提高。因此,通过高压分离罐能够获得粒径分布更为均一的泥浆水。为了更好实现泥浆混合物的分离以及考虑减小对筛网的堵塞或方便筛网清理,本发明在高压分离罐底部通入泥浆混合物,使其从下到上通过筛网,避免了物质沉积在筛网上,实现了保障制备黏土品质的同时实现高效生产。根据所要去除的物质的粒径以及维持较高生产效率的要求,筛网的孔径不宜设置过小或过大,相应的压力也需要达到一定程度,经过试验运行,筛网孔径为0.5-1mm;泥浆混合物增压至0.5-1Mpa运行最佳,其既能完成预期的分离效果,而且运行效率较高。The mud mixture after the two-stage precipitation treatment is separated by specific gravity, while the sand with large particle size and relatively low specific gravity still exists in the mud mixture, and the uneven particle size distribution cannot better achieve the quality of the prepared clay. improve. Therefore, slurry water with more uniform particle size distribution can be obtained through the high-pressure separation tank. In order to better realize the separation of the mud mixture and consider reducing the blockage of the screen or facilitate the cleaning of the screen, the present invention passes the mud mixture at the bottom of the high-pressure separation tank, so that it passes through the screen from the bottom to the top, so as to avoid the deposition of substances on the screen. On the screen, the high-efficiency production can be achieved while ensuring the quality of the prepared clay. According to the particle size of the substance to be removed and the requirement of maintaining high production efficiency, the aperture of the screen should not be set too small or too large, and the corresponding pressure also needs to reach a certain level. After the test operation, the aperture of the screen is 0.5-1mm; The best operation is when the slurry mixture is pressurized to 0.5-1Mpa, which can not only achieve the expected separation effect, but also has a high operating efficiency.
(4)振动处理:通过振动处理将泥浆水中的至少部分剩余细砂沉淀在振动池底部;(4) Vibration treatment: at least part of the remaining fine sand in the muddy water is deposited at the bottom of the vibrating tank by vibration treatment;
将高压分离罐分离出的泥浆水通入到振动池的底部,同时振动池底部的振动使得泥浆水中至少部分剩余的细砂被振动沉淀在振动池的底部,而在振动池的上层形成泥浆分散液,其中,在振动池的底部设置防水型声波振动装置,声波频率为50-5000Hz,优选100-500Hz。The mud water separated by the high-pressure separation tank is passed to the bottom of the vibrating pool, and the vibration at the bottom of the vibrating pool causes at least part of the remaining fine sand in the mud water to be vibrated and sedimented at the bottom of the vibrating pool, and the upper layer of the vibrating pool forms a mud dispersion. liquid, wherein a waterproof sonic vibration device is arranged at the bottom of the vibration pool, and the sonic frequency is 50-5000 Hz, preferably 100-500 Hz.
本发明为了提高制备黏土的品质,设置了振动池对泥浆水进行振动处理,振动装置设置在振动池底部,受到振动的泥浆水向上扩散,砂子颗粒由于自身密度原因或自身性质能够较快的落回沉淀池底部,而土颗粒由于自身比重轻能够比砂子颗粒更容易扩散至振动池上部,而回落的驱动力较低且路程长,因此,振动池的上部为几乎没有砂子颗粒的泥浆分散液。该步骤保证了制备黏土的品质,使得制备的黏土中非常少或几乎不存在砂子。根据上述振动原理,为了避免剧烈的振动导致各种物质在振动池各个位置都有分散,在将振动装置设置在振动池底部的同时,应注意振动的频率要适当,频率过小影响生产效率,频率过大则影响产品品质,经过试验运行,底部设置的防水型声波振动装置的声波频率为100-500Hz运行最佳,能够确保获得高品质黏土的基础上,具有较好的生产效率。In order to improve the quality of the prepared clay, a vibrating tank is set up to vibrate the mud water. The vibrating device is arranged at the bottom of the vibrating tank, and the vibrated mud water diffuses upward, and the sand particles can fall down faster due to their own density or their own properties. Return to the bottom of the sedimentation tank, and the soil particles can diffuse to the upper part of the vibrating tank more easily than the sand particles due to their light weight, and the driving force for falling back is low and the distance is long. Therefore, the upper part of the vibrating tank is a mud dispersion with almost no sand particles. This step ensures the quality of the prepared clay so that very little or no sand is present in the prepared clay. According to the above vibration principle, in order to avoid the violent vibration causing various substances to be scattered in various positions of the vibration pool, when setting the vibration device at the bottom of the vibration pool, it should be noted that the frequency of vibration should be appropriate, and the frequency is too small to affect the production efficiency. If the frequency is too large, the quality of the product will be affected. After the test operation, the sound wave frequency of the waterproof acoustic wave vibration device set at the bottom is 100-500Hz.
(5)絮凝收集:振动池上部的泥浆分散液送入黏土沉淀池中,通过加入快速絮凝沉淀剂使得泥浆分散液分为下层的黏土浆和上层的清水,收集黏土浆;(5) flocculation collection: the mud dispersion liquid in the upper part of the vibrating tank is sent into the clay sedimentation tank, and the mud dispersion liquid is divided into the clay slurry of the lower layer and the clear water of the upper layer by adding a fast flocculating precipitant, and the clay slurry is collected;
振动池上层的泥浆分散液被传送至黏土沉淀池中,向黏土沉淀池中加入泥浆快速絮凝沉淀剂,使得泥浆水中的黏土快速凝聚沉淀;絮凝沉淀完成后,从黏土沉淀池的底部将黏土浆送至压滤机中,从黏土沉淀池的上部将清水送至水循环系统中,其中,快速絮凝沉淀剂为无机絮凝剂,优选硫酸铝、硫酸铁、氯化铝、氯化铁、聚合硫酸铝、聚合硫酸铁中的一种或多种,将无机絮凝剂配置成质量分数0.5%-5%絮凝剂溶液,絮凝剂溶液与泥浆分散液体积比为1:10-100。The mud dispersion liquid in the upper layer of the vibrating tank is transferred to the clay sedimentation tank, and the mud fast flocculating precipitant is added to the clay sedimentation tank, so that the clay in the mud water quickly coagulates and settles; It is sent to the filter press, and the clear water is sent from the upper part of the clay sedimentation tank to the water circulation system, wherein the fast flocculating precipitant is an inorganic flocculant, preferably aluminum sulfate, ferric sulfate, aluminum chloride, ferric chloride, polyaluminum sulfate , one or more of polymeric ferric sulfate, the inorganic flocculant is configured into a flocculant solution with a mass fraction of 0.5%-5%, and the volume ratio of the flocculant solution to the mud dispersion liquid is 1:10-100.
经过振动处理获得的泥浆分散液以及能够保证生产粘土的高品质,而将其快速收回能够保证生产的效率。本发明采用絮凝处理实现悬浮颗粒的快速沉淀,由于制备物质为无机粘土,为了避免采用有机絮凝剂对产品造成影响,本发明采用常规的无机絮凝剂;为了实现高效的絮凝沉淀以及避免过多的絮凝剂对产品造成影响,本发明经过试验运行,确定将无机絮凝剂配置成质量分数0.5%-5%絮凝剂溶液,并以絮凝剂溶液与泥浆分散液体积比为1:10-100的比例加入泥浆分散液。由此,能够将经过多级分离处理的泥浆分散液快速转化成黏土浆,即保证了制备黏土的高品质,有保障了高效的生产效率。The slurry dispersion obtained by vibrating treatment can ensure the high quality of the produced clay, and its rapid recovery can ensure the efficiency of the production. The present invention adopts flocculation treatment to realize the rapid precipitation of suspended particles. Since the preparation material is inorganic clay, in order to avoid the use of organic flocculants to affect the product, the present invention adopts conventional inorganic flocculants; in order to achieve efficient flocculation and sedimentation and avoid excessive The flocculant has an impact on the product. After the test operation of the present invention, it is determined that the inorganic flocculant is configured into a flocculant solution with a mass fraction of 0.5%-5%, and the volume ratio of the flocculant solution to the mud dispersion liquid is 1:10-100. Add the slurry dispersion. As a result, the slurry dispersion liquid subjected to the multi-stage separation treatment can be quickly converted into clay slurry, that is, the high quality of the prepared clay is ensured, and the efficient production efficiency is guaranteed.
实施例1Example 1
(1)将包含泥浆液和砂子的原始泥砂混合物从长度为30m的长条形的沉淀池的一端以0.8m/s的速度通入,沉淀池的另一端中部与浆液泵连接,长条形的沉淀池能够将原始泥砂混合物中部分比重较大的砂子沉淀,比重轻的杂质会漂浮在原始泥砂混合物表面,沉淀池中部得到细砂泥浆混合物;(1) Pass the original mud-sand mixture containing mud slurry and sand at a speed of 0.8m/s from one end of a long strip sedimentation tank with a length of 30m. The sedimentation tank can precipitate some of the sand with larger specific gravity in the original mud-sand mixture, the impurities with light specific gravity will float on the surface of the original mud-sand mixture, and the fine sand mud mixture is obtained in the middle of the sedimentation tank;
(2)浆液泵将细砂泥浆混合物送至长度为15m的倾斜的泥砂分离管道中,细砂泥浆混合物在分离管道内的流动速度为0.3m/s;由于泥砂分离管道与地面倾斜设置,且分离管道的进料端靠近地面,当浆液泵将细砂泥浆混合物送入泥砂分离管道时,部分比重较大的细砂会沉淀在泥砂分离管道底部,而泥浆混合物则被送至下一工序中;泥砂分离管道的出料端与泥浆罐连接,泥浆混合物从泥砂分离管道中进入到泥浆罐内,泥浆罐能够储存泥浆混合物;(2) The slurry pump sends the fine sand and mud mixture to the inclined mud and sand separation pipeline with a length of 15m, and the flow velocity of the fine sand mud mixture in the separation pipeline is 0.3m/s; because the mud and sand separation pipeline is inclined to the ground, and The feed end of the separation pipe is close to the ground. When the slurry pump sends the fine sand and mud mixture into the mud and sand separation pipe, part of the fine sand with larger specific gravity will settle at the bottom of the mud and sand separation pipe, and the mud mixture will be sent to the next process. ; The discharge end of the mud-sand separation pipeline is connected to the mud tank, and the mud mixture enters the mud tank from the mud-sand separation pipeline, and the mud tank can store the mud mixture;
(3)高压泵将泥浆罐中的泥浆混合物从高压分离罐底部送至高压分离罐内,高压分离罐内设有孔径为0.8mm的筛网,高压泵将泥浆混合物增压至0.6Mpa,使得泥浆水能够通过筛网从高压分离罐上部离开,而部分直径较大的细砂则留在高压分离罐内;(3) The high-pressure pump sends the mud mixture in the mud tank from the bottom of the high-pressure separation tank to the high-pressure separation tank. The high-pressure separation tank is provided with a screen with an aperture of 0.8 mm, and the high-pressure pump pressurizes the mud mixture to 0.6 Mpa, so that Slurry water can leave the upper part of the high-pressure separation tank through the screen, while part of the fine sand with larger diameter remains in the high-pressure separation tank;
(4)将高压分离罐分离出的泥浆水通入设置有防水型声波振动装置的振动池的底部,声波频率为300Hz,同时振动池底部的振动使得泥浆水中至少部分剩余的细砂被振动沉淀在振动池的底部,而在振动池的上层形成泥浆分散液;(4) The mud water separated by the high-pressure separation tank is passed into the bottom of the vibrating pool provided with the waterproof sonic vibration device, and the sound wave frequency is 300 Hz, and the vibration at the bottom of the vibrating pool causes at least part of the remaining fine sand in the mud water to be vibrated and precipitated At the bottom of the vibrating pool, a slurry dispersion is formed in the upper layer of the vibrating pool;
(5)振动池上层的泥浆分散液被传送至黏土沉淀池中,按照絮凝剂溶液与泥浆水体积比为1:80向黏土沉淀池中加入质量分数1%的无聚合硫酸铝溶液,使得泥浆水中的黏土快速凝聚沉淀;絮凝沉淀完成后,从黏土沉淀池的底部将黏土浆送至压滤机中,从黏土沉淀池的上部将清水送至水循环系统中。(5) The slurry dispersion in the upper layer of the vibrating tank is transferred to the clay sedimentation tank, and a 1% mass fraction of non-polymerized aluminum sulfate solution is added to the clay sedimentation tank according to the volume ratio of the flocculant solution to the slurry water of 1:80 to make the slurry The clay in the water quickly coagulates and settles; after the flocculation and sedimentation is completed, the clay slurry is sent to the filter press from the bottom of the clay sedimentation tank, and the clean water is sent to the water circulation system from the upper part of the clay sedimentation tank.
取步骤(2)的泥浆混合物、步骤(3)的泥浆水和步骤(4)的泥浆分散液进行测试比较,其中,将上述三种样品超声分散成悬浮液,然后静置1h,通过比较沉积层高度可以发现,泥浆混合物产生的沉积层最厚,泥浆水次之,泥浆分散液的沉积层最薄。上述结果说明本发明通过沉淀处理、筛分处理和振动处理后得到的泥浆分散液含有的砂粒最少甚至被全部去除,由此,能够最大化保证制备黏土的品质以及性质,实现对泥浆的精细化处理。Take the mud mixture of step (2), the mud water of step (3) and the mud dispersion of step (4) for testing and comparison, wherein, the above three samples are ultrasonically dispersed into suspension, and then left standing for 1h, by comparing sedimentation The layer height can be found that the sediment layer produced by the mud mixture is the thickest, followed by the mud water, and the sediment layer of the mud dispersion is the thinnest. The above results show that the mud dispersion liquid obtained by the present invention through precipitation treatment, screening treatment and vibration treatment contains at least or even removes all sand particles, thus, the quality and properties of the prepared clay can be guaranteed to the greatest extent, and the refinement of the mud can be realized. deal with.
虽然本发明内容包括具体的实施例,但是对本领域的技术人员明显的是在不偏离本权利要求和其等同技术方案的发明要点和范围的情况下,可以对这些实施例做出各种形式上和细节上的替换或变动。本文中描述的实施例应被认为只在说明意义上,并非为了限制的目的。在每一个实施例中的特征和方面的描述被认为适用于其他实施例中的相似特征和方面。因此,本发明的范围不应受到具体的描述的限定,而是受权利要求技术方案的限定,并且在本权利要求和其等同物的范围内的所有变化被解释为包含在本发明的技术方案之内。Although the content of the present invention includes specific embodiments, it is obvious to those skilled in the art that these embodiments can be made in various forms without departing from the spirit and scope of the invention of the claims and the equivalent technical solutions thereof. and substitutions or changes in details. The embodiments described herein should be considered in an illustrative sense only and not for purposes of limitation. Descriptions of features and aspects in each embodiment are considered to be applicable to similar features and aspects in other embodiments. Therefore, the scope of the present invention should not be limited by the specific description but by the technical solutions of the claims, and all changes within the scope of the claims and their equivalents are to be construed as being included in the technical solutions of the present invention within.
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