CN111205129A - Pesticide carrier added with mineral substances and preparation method thereof - Google Patents

Pesticide carrier added with mineral substances and preparation method thereof Download PDF

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Publication number
CN111205129A
CN111205129A CN202010020621.1A CN202010020621A CN111205129A CN 111205129 A CN111205129 A CN 111205129A CN 202010020621 A CN202010020621 A CN 202010020621A CN 111205129 A CN111205129 A CN 111205129A
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parts
mixing
sulfate
phosphate
manganese
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刘晓旭
吴立圣
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Zhongbo Soil Environmental Engineering Technology Jiangsu Co ltd
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Zhongbo Soil Environmental Engineering Technology Jiangsu Co ltd
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Priority to CN202010020621.1A priority Critical patent/CN111205129A/en
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a pesticide carrier added with mineral substances, which comprises the following raw materials in parts by weight: 14-28 parts of medical stone, 10-25 parts of calcite, 15-25 parts of chrysolite, 10-20 parts of zeolite, 7-12 parts of quartz, 12-25 parts of sodium carbonate, 13-25 parts of potassium phosphate, 10-30 parts of calcium phosphate, 7-15 parts of manganese phosphate, 12-20 parts of magnesium nitrate, 11-23 parts of sodium nitrate, 8-16 parts of manganese sulfate, 10-20 parts of magnesium sulfate, 6-14 parts of copper sulfate, 2-4 parts of triethylhexyl phosphoric acid, 1.5-3 parts of polyacrylamide, 3-8 parts of emulsifier, 4-10 parts of adhesive, 6-10 parts of synergist and 48-90 parts of water. According to the invention, the natural mineral fertilizers are selected, ground and mixed, and are combined with various metal salt compounds to serve as pesticide carriers, so that the soil fertility can be improved and the soil structure can be improved in the pesticide spraying process, and the integral preparation method is simple and environment-friendly.

Description

Pesticide carrier added with mineral substances and preparation method thereof
Technical Field
The invention relates to the technical field of pesticide preparation, in particular to a pesticide carrier added with mineral substances and a preparation method thereof.
Background
The pesticide is chemical for preventing and controlling diseases and pests and regulating plant growth. It is widely used in agriculture, forestry and animal husbandry production, environment and household sanitation, pest and disease control, and industrial product mildew and moth prevention. The pesticide has various varieties, and can be mainly divided into insecticide, acaricide, rodenticide, nematicide, molluscicide, bactericide, herbicide, plant growth regulator and the like according to the application; according to the raw material source, the pesticide can be divided into mineral source pesticides (inorganic pesticides), biological source pesticides (natural organic matters, microorganisms, antibiotics and the like) and chemical synthetic pesticides; according to chemical structure, mainly comprises organic chlorine, organic phosphorus, organic nitrogen, organic sulfur, carbamate, pyrethroid, amide compounds, urea compounds, ether compounds, phenolic compounds, phenoxy carboxylic acids, amidines, triazoles, heterocycles, benzoic acids, organic metal compounds and the like, which are all organic synthetic pesticides; it can be divided into powder, wettable powder, emulsion, emulsifiable concentrate, cream, paste, colloid agent, fumigant, aerosol, granule, microgranule and oil agent according to the preparation formulation.
The pesticide carrier is a pesticide adjuvant, is an auxiliary substance for improving the physicochemical property of a medicament during the processing or using of a pesticide preparation, can improve the pesticide effect, and is convenient to transport, store and the like.
At present, most pesticide carriers on the market need to be mixed with pesticides and then sprayed to serve as the pesticide carriers, however, the traditional pesticide carriers are less and rich in mineral elements and cannot be used for fertilizing crops, and in order to solve the problems, a pesticide carrier added with mineral substances and a preparation method thereof are provided.
Disclosure of Invention
The invention provides a pesticide carrier added with mineral substances and a preparation method thereof, aiming at the technical defects of the prior pesticide carrier and the like.
The invention aims to solve the technical defects, adopts a modified technical scheme, and provides a pesticide carrier added with mineral substances, which comprises the following raw materials in parts by weight: 14-28 parts of medical stone, 10-25 parts of calcite, 15-25 parts of chrysolite, 10-20 parts of zeolite, 7-12 parts of quartz, 12-25 parts of sodium carbonate, 13-25 parts of potassium phosphate, 10-30 parts of calcium phosphate, 7-15 parts of manganese phosphate, 12-20 parts of magnesium nitrate, 11-23 parts of sodium nitrate, 8-16 parts of manganese sulfate, 10-20 parts of magnesium sulfate, 6-14 parts of copper sulfate, 2-4 parts of triethylhexyl phosphoric acid, 1.5-3 parts of polyacrylamide, 3-8 parts of emulsifier, 4-10 parts of adhesive, 6-10 parts of synergist and 48-90 parts of water.
The invention further comprises the following raw materials in parts by weight: 28 parts of medical stone, 25 parts of calcite, 25 parts of chrysolite, 20 parts of zeolite, 12 parts of quartz, 5 parts of sodium carbonate, 25 parts of potassium phosphate, 30 parts of calcium phosphate, 15 parts of manganese phosphate, 20 parts of magnesium nitrate, 23 parts of sodium nitrate, 16 parts of manganese sulfate, 20 parts of magnesium sulfate, 14 parts of copper sulfate, 4 parts of triethylhexyl phosphoric acid, 30 parts of polyacrylamide, 8 parts of an emulsifier, 10 parts of an adhesive, 10 parts of a synergist and 90 parts of water.
The invention further comprises the following raw materials in parts by weight: 14 parts of medical stone, 10 parts of calcite, 15 parts of chrysolite, 10 parts of zeolite, 7 parts of quartz, 12 parts of sodium carbonate, 13 parts of potassium phosphate, 10 parts of calcium phosphate, 7 parts of manganese phosphate, 12 parts of magnesium nitrate, 11 parts of sodium nitrate, 8 parts of manganese sulfate, 10 parts of magnesium sulfate, 6 parts of copper sulfate, 2 parts of triethylhexyl phosphoric acid, 1.5 parts of polyacrylamide, 3 parts of emulsifier, 4 parts of adhesive, 6 parts of synergist and 48 parts of water.
As a further preferable mode of the invention, the preparation process comprises the following steps:
s1, preparing materials, namely weighing the raw materials according to the parts;
s2, crushing ores, fully crushing medical stones, calcite, gold stones, zeolite and quartz, and mixing after crushing;
s3, mixing salt materials, namely firstly heating water to 100 ℃, preserving heat for 10min, cooling to 45 ℃, then adding sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate and copper sulfate, then starting stirring, homogenizing at medium speed for 5min until the mixture is uniformly dispersed, and controlling the temperature at 90 ℃;
s4, mixing ores, respectively pouring the powder of medical stone, calcite, gold stone, zeolite and quartz into the mixed salt material, heating and mixing, controlling the temperature at 110 ℃, and keeping for 5 min;
and S5, mixing the auxiliary agents, respectively pouring triethyl hexyl phosphoric acid, polyacrylamide, an emulsifier, an adhesive and a synergist into the step 4, continuously stirring and mixing for 10min, and cooling to finish the processing.
As a further preferable mode of the invention, in step S4, triethylhexyl phosphoric acid and polyacrylamide are poured, the rotation speed of 150r/min-180r/min is controlled to carry out stirring and mixing treatment for 5min, then the emulsifier, the adhesive and the synergist are injected, and the stirring and mixing are carried out for 5min under the rotation speed of 260r/min-380 r/min.
In a further preferred embodiment of the present invention, in step S1, the ore is primarily pulverized by a grinding and pulverizing method, and then secondarily pulverized by an ultrasonic pulverizing method after the primary pulverization, and the pulverized particle diameter is controlled to be 45 to 60 um.
As a further preferable embodiment of the present invention, in step S3, hydrogen peroxide with a concentration of 45% to 65% may be prepared and washed before mixing sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate, and copper sulfate.
In a further preferred embodiment of the present invention, the synergist is a mixture of a urease inhibitor, an ammonia stabilizer, a biological agent, an insecticide, and a plant growth promoter.
The invention has the following beneficial effects: according to the invention, the natural mineral fertilizers are selected, ground and mixed, and are combined with various metal salt compounds to serve as pesticide carriers, so that the soil fertility can be improved and the soil structure can be improved in the pesticide spraying process, and the integral preparation method is simple and environment-friendly.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a technical scheme that: a pesticide carrier added with mineral substances comprises the following raw materials in parts by weight: 14-28 parts of medical stone, 10-25 parts of calcite, 15-25 parts of chrysolite, 10-20 parts of zeolite, 7-12 parts of quartz, 12-25 parts of sodium carbonate, 13-25 parts of potassium phosphate, 10-30 parts of calcium phosphate, 7-15 parts of manganese phosphate, 12-20 parts of magnesium nitrate, 11-23 parts of sodium nitrate, 8-16 parts of manganese sulfate, 10-20 parts of magnesium sulfate, 6-14 parts of copper sulfate, 2-4 parts of triethylhexyl phosphoric acid, 1.5-3 parts of polyacrylamide, 3-8 parts of emulsifier, 4-10 parts of adhesive, 6-10 parts of synergist and 48-90 parts of water.
The preparation process comprises the following steps:
s1, preparing materials, namely weighing the raw materials according to the parts;
s2, crushing ores, fully crushing medical stones, calcite, gold stones, zeolite and quartz, and mixing after crushing;
s3, mixing salt materials, namely firstly heating water to 100 ℃, preserving heat for 10min, cooling to 45 ℃, then adding sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate and copper sulfate, then starting stirring, homogenizing at medium speed for 5min until the mixture is uniformly dispersed, and controlling the temperature at 90 ℃;
s4, mixing ores, respectively pouring the powder of medical stone, calcite, gold stone, zeolite and quartz into the mixed salt material, heating and mixing, controlling the temperature at 110 ℃, and keeping for 5 min;
and S5, mixing the auxiliary agents, respectively pouring triethyl hexyl phosphoric acid, polyacrylamide, an emulsifier, an adhesive and a synergist into the step 4, continuously stirring and mixing for 10min, and cooling to finish the processing.
In step S4, triethyl hexyl phosphoric acid and polyacrylamide are poured, stirring and mixing treatment is carried out for 5min by controlling the rotating speed of 150r/min-180r/min, then the emulsifying agent, the adhesive and the synergist are injected, and stirring and mixing are carried out for 5min by controlling the rotating speed of 260r/min-380 r/min.
In step S1, the ore is primarily pulverized by a grinding and pulverizing method, and then secondarily pulverized by an ultrasonic pulverizing method, wherein the pulverized particle diameter is controlled to be 45-60 um.
In step S3, hydrogen peroxide with a concentration of 45% to 65% may be added to sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate, and copper sulfate before mixing.
The synergist is prepared by mixing urease inhibitor, ammonia stabilizer, biological agent, pesticide and plant production promoter.
Example 1
Raw materials and weight fraction: 28 parts of medical stone, 25 parts of calcite, 25 parts of chrysolite, 20 parts of zeolite, 12 parts of quartz, 5 parts of sodium carbonate, 25 parts of potassium phosphate, 30 parts of calcium phosphate, 15 parts of manganese phosphate, 20 parts of magnesium nitrate, 23 parts of sodium nitrate, 16 parts of manganese sulfate, 20 parts of magnesium sulfate, 14 parts of copper sulfate, 4 parts of triethylhexyl phosphoric acid, 30 parts of polyacrylamide, 8 parts of an emulsifier, 10 parts of an adhesive, 10 parts of a synergist and 90 parts of water.
Firstly, preparing materials, and weighing the raw materials according to the parts by weight;
crushing the ores, fully crushing medical stones, calcite, gold stones, zeolite and quartz, and mixing after crushing;
then mixing salt materials, namely firstly heating water to 100 ℃, preserving heat for 10min, cooling to 45 ℃, then adding sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate and copper sulfate, then starting stirring, homogenizing at medium speed for 5min until the mixture is uniformly dispersed, and controlling the temperature to be 90 ℃;
mixing the ores, respectively pouring the powders of Maifanitum, Calcite, Chrysanthemum stone, Zeolite and Quartz album into the mixed salt material, heating and mixing, controlling temperature at 110 deg.C, and maintaining for 5 min;
and finally, mixing the auxiliary agents, respectively pouring triethyl hexyl phosphoric acid, polyacrylamide, an emulsifier, an adhesive and a synergist into the step 4, continuously stirring and mixing for 10min, and cooling to finish the processing.
The content of the carrier phosphorus, potassium, calcium, magnesium and manganese ore prepared by the method is 32 percent.
Example 2
Raw materials and weight fraction: 14 parts of medical stone, 10 parts of calcite, 15 parts of chrysolite, 10 parts of zeolite, 7 parts of quartz, 12 parts of sodium carbonate, 13 parts of potassium phosphate, 10 parts of calcium phosphate, 7 parts of manganese phosphate, 12 parts of magnesium nitrate, 11 parts of sodium nitrate, 8 parts of manganese sulfate, 10 parts of magnesium sulfate, 6 parts of copper sulfate, 2 parts of triethylhexyl phosphoric acid, 1.5 parts of polyacrylamide, 3 parts of emulsifier, 4 parts of adhesive, 6 parts of synergist and 48 parts of water.
Firstly, preparing materials, and weighing the raw materials according to the parts by weight;
crushing the ores, fully crushing medical stones, calcite, gold stones, zeolite and quartz, and mixing after crushing;
then mixing salt materials, namely firstly heating water to 100 ℃, preserving heat for 10min, cooling to 45 ℃, then adding sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate and copper sulfate, then starting stirring, homogenizing at medium speed for 5min until the mixture is uniformly dispersed, and controlling the temperature to be 90 ℃;
mixing the ores, respectively pouring the powders of Maifanitum, Calcite, Chrysanthemum stone, Zeolite and Quartz album into the mixed salt material, heating and mixing, controlling temperature at 110 deg.C, and maintaining for 5 min;
and finally, mixing the auxiliary agents, respectively pouring triethyl hexyl phosphoric acid, polyacrylamide, an emulsifier, an adhesive and a synergist into the step 4, continuously stirring and mixing for 10min, and cooling to finish the processing.
The content of the carrier phosphorus, potassium, calcium, magnesium and manganese ore prepared by the method accounts for 26 percent.
Ratio of phosphorus Ratio of potassium Calcium content ratio Ratio of magnesium to magnesium Ratio of manganese Total amount of
10％ 6％ 8％ 4％ 4％ 32％ Example 1
8％ 4％ 6％ 3％ 5％ 26％ Example 2
。
In conclusion, the natural mineral fertilizers are ground and mixed, and are combined with various metal salt compounds to serve as pesticide carriers, so that the soil fertility can be improved and the soil structure can be improved in the pesticide spraying process, and the integral preparation method is simple and environment-friendly.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (8)

1. A pesticide carrier added with mineral substances, which is characterized in that: comprises the following raw materials in parts by weight: 14-28 parts of medical stone, 10-25 parts of calcite, 15-25 parts of chrysolite, 10-20 parts of zeolite, 7-12 parts of quartz, 12-25 parts of sodium carbonate, 13-25 parts of potassium phosphate, 10-30 parts of calcium phosphate, 7-15 parts of manganese phosphate, 12-20 parts of magnesium nitrate, 11-23 parts of sodium nitrate, 8-16 parts of manganese sulfate, 10-20 parts of magnesium sulfate, 6-14 parts of copper sulfate, 2-4 parts of triethylhexyl phosphoric acid, 1.5-3 parts of polyacrylamide, 3-8 parts of emulsifier, 4-10 parts of adhesive, 6-10 parts of synergist and 48-90 parts of water.
2. The pesticide carrier added with mineral substances as claimed in claim 1, further comprising the following raw materials in parts by weight: 28 parts of medical stone, 25 parts of calcite, 25 parts of chrysolite, 20 parts of zeolite, 12 parts of quartz, 5 parts of sodium carbonate, 25 parts of potassium phosphate, 30 parts of calcium phosphate, 15 parts of manganese phosphate, 20 parts of magnesium nitrate, 23 parts of sodium nitrate, 16 parts of manganese sulfate, 20 parts of magnesium sulfate, 14 parts of copper sulfate, 4 parts of triethylhexyl phosphoric acid, 30 parts of polyacrylamide, 8 parts of an emulsifier, 10 parts of an adhesive, 10 parts of a synergist and 90 parts of water.
3. The pesticide carrier added with mineral substances as claimed in claim 1, further comprising the following raw materials in parts by weight: 14 parts of medical stone, 10 parts of calcite, 15 parts of chrysolite, 10 parts of zeolite, 7 parts of quartz, 12 parts of sodium carbonate, 13 parts of potassium phosphate, 10 parts of calcium phosphate, 7 parts of manganese phosphate, 12 parts of magnesium nitrate, 11 parts of sodium nitrate, 8 parts of manganese sulfate, 10 parts of magnesium sulfate, 6 parts of copper sulfate, 2 parts of triethylhexyl phosphoric acid, 1.5 parts of polyacrylamide, 3 parts of emulsifier, 4 parts of adhesive, 6 parts of synergist and 48 parts of water.
4. The preparation method of the pesticide carrier added with the mineral substances as claimed in claim 1, which is characterized by comprising the following steps:
s1, preparing materials, namely weighing the raw materials according to the parts;
s2, crushing ores, fully crushing medical stones, calcite, gold stones, zeolite and quartz, and mixing after crushing;
s3, mixing salt materials, namely firstly heating water to 100 ℃, preserving heat for 10min, cooling to 45 ℃, then adding sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate and copper sulfate, then starting stirring, homogenizing at medium speed for 5min until the mixture is uniformly dispersed, and controlling the temperature at 90 ℃;
s4, mixing ores, respectively pouring the powder of medical stone, calcite, gold stone, zeolite and quartz into the mixed salt material, heating and mixing, controlling the temperature at 110 ℃, and keeping for 5 min;
and S5, mixing the auxiliary agents, respectively pouring triethyl hexyl phosphoric acid, polyacrylamide, an emulsifier, an adhesive and a synergist into the step 4, continuously stirring and mixing for 10min, and cooling to finish the processing.
5. The method for preparing a mineral-added pesticide carrier as set forth in claim 4, wherein: in step S4, triethyl hexyl phosphoric acid and polyacrylamide are poured, stirring and mixing treatment is carried out for 5min by controlling the rotating speed of 150r/min-180r/min, then the emulsifying agent, the adhesive and the synergist are injected, and stirring and mixing are carried out for 5min by controlling the rotating speed of 260r/min-380 r/min.
6. The method for preparing a mineral-added pesticide carrier as set forth in claim 4, wherein: in step S1, the ore is primarily pulverized by a grinding and pulverizing method, and then secondarily pulverized by an ultrasonic pulverizing method, wherein the pulverized particle diameter is controlled to be 45-60 um.
7. The method for preparing a mineral-added pesticide carrier as set forth in claim 4, wherein: in step S3, hydrogen peroxide with a concentration of 45% to 65% may be added to sodium carbonate, potassium phosphate, calcium phosphate, manganese phosphate, magnesium nitrate, sodium nitrate, manganese sulfate, magnesium sulfate, and copper sulfate before mixing.
8. The mineral-supplemented pesticidal carrier of claim 1, characterized in that: the synergist is prepared by mixing urease inhibitor, ammonia stabilizer, biological agent, pesticide and plant production promoter.
CN202010020621.1A 2020-01-09 2020-01-09 Pesticide carrier added with mineral substances and preparation method thereof Withdrawn CN111205129A (en)

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CN202010020621.1A CN111205129A (en) 2020-01-09 2020-01-09 Pesticide carrier added with mineral substances and preparation method thereof

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Application Number Priority Date Filing Date Title
CN202010020621.1A CN111205129A (en) 2020-01-09 2020-01-09 Pesticide carrier added with mineral substances and preparation method thereof

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CN111205129A true CN111205129A (en) 2020-05-29

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