CN111141771A - X-ray diffractometer suspension wire light well bracket and use method thereof - Google Patents

X-ray diffractometer suspension wire light well bracket and use method thereof Download PDF

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Publication number
CN111141771A
CN111141771A CN202010040663.1A CN202010040663A CN111141771A CN 111141771 A CN111141771 A CN 111141771A CN 202010040663 A CN202010040663 A CN 202010040663A CN 111141771 A CN111141771 A CN 111141771A
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suspension wire
axis
well
suspension
light well
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CN111141771B (en
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潘宇观
李伟强
蔡元峰
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Nanjing University
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Nanjing University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G01N23/20008Constructional details of analysers, e.g. characterised by X-ray source, detector or optical system; Accessories therefor; Preparing specimens therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/05Investigating materials by wave or particle radiation by diffraction, scatter or reflection
    • G01N2223/056Investigating materials by wave or particle radiation by diffraction, scatter or reflection diffraction
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/10Different kinds of radiation or particles
    • G01N2223/101Different kinds of radiation or particles electromagnetic radiation
    • G01N2223/1016X-ray
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/30Accessories, mechanical or electrical features

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  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
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Abstract

The invention discloses a wire-suspended light well bracket of an X-ray diffractometer and a use method thereof, wherein the wire-suspended light well comprises a wire suspension and a weight tied at the bottom end of the wire suspension, and the bracket comprises a lockable magnetic base, a three-axis translational fine tuning holder, a sliding device and a stopper positioned below the wire-suspended light well; the upper end of the lockable magnetic base is connected with the three-axis translational fine-tuning holder, and the lower end of the lockable magnetic base is adsorbed on the detector protective cover; the magnetic device is provided with a magnetic knob switch; the sliding device comprises a sliding rail cantilever and a sliding block mechanism, wherein one end of the sliding rail cantilever is fixed on the top surface of the Z-axis vertical displacement table; the sliding block mechanism comprises a sliding block arranged on a sliding rail cantilever, a horizontal rotating mechanism with angle scales and a suspension wire fixing button, wherein the horizontal rotating mechanism and the suspension wire fixing button are arranged in the center of the sliding block; the upper end of the suspension wire is connected with the horizontal rotating mechanism. The invention is convenient to disassemble and assemble, has accurate positioning, can be infinitely and flexibly adjusted, and forms a freely selectable direct light shielding angle.

Description

X-ray diffractometer suspension wire light well bracket and use method thereof
Technical Field
The invention relates to a suspension wire light well bracket of an X-ray diffractometer and a using method thereof, belonging to the technical field of X-ray diffractometers.
Background
Light well: an original used on some types of X-ray diffractometers is to block incident X-rays directed toward the detector to protect the detector from damage from direct radiation exposure.
The existing component is used for a RAPID II type X-ray diffractometer of Japan science company, and adopts a door-shaped bracket, one section of the bracket is connected with a device collimator, and the other end is attached with a light well. The collimator is a replaceable component, and when different collimators are replaced, if the collimator is not reconnected due to omission in the prior art, the device detector component is damaged by direct radiation caused when the radiation is started.
In the prior art, when the device is connected to an equipment collimator, a door-shaped support structure can shield a sample table to a certain degree, so that the sample is difficult to replace, the support is easy to be touched by mistake when the sample is replaced, the light well position deviation can be caused if the sample is replaced, the shielding effect is poor, the collimator can be caused to deviate if the sample is replaced, the precision of the device is directly influenced, and the device is even damaged; the portal frame structure in the prior art shields a part of the detector, can partially block diffraction signals and causes certain loss to the signal acquisition range of equipment; the structural material in the prior art is a stainless steel sheet, the rigidity of the material is insufficient, and the material is easy to bend in the use process, so that the light well is deviated in position, and the shading effect is influenced.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the X-ray diffractometer suspension wire light well bracket and the use method thereof, which are convenient to disassemble and assemble, accurate in positioning, stepless and flexible in adjustment and capable of forming a freely selectable direct light shielding angle.
In order to achieve the purpose, the invention is realized by the following technical scheme:
the invention relates to a wire-suspended light well bracket of an X-ray diffractometer, which comprises a wire-suspended light well fixed at the gravity center of the light well and a weight tied at the bottom end of the wire-suspended light well, wherein the bracket comprises a lockable magnetic base for providing stable support for the light well bracket, a three-axis translational fine-adjustment cradle head, a sliding device and a stopper positioned below the wire-suspended light well and used for enabling the wire-suspended light well to rapidly reach stable and static state in the debugging process; the upper end of the lockable magnetic base is connected with the three-axis translational fine-tuning holder, and the lower end of the lockable magnetic base is adsorbed on the detector protective cover through a magnetic device; the magnetic force knob switch capable of controlling the magnitude of magnetic force is arranged on the magnetic device; the three-axis translational fine tuning holder comprises an upper section and a lower section, wherein the lower section is an X-axis and Y-axis orthogonal horizontal displacement table, and the upper section is a Z-axis vertical displacement table; the sliding device comprises a sliding rail cantilever and a sliding block mechanism, wherein one end of the sliding rail cantilever is fixed on the top surface of the Z-axis vertical displacement table; the sliding block mechanism comprises a sliding block arranged on a sliding rail cantilever, a horizontal direction rotating mechanism with angle scales and arranged in the center of the sliding block, and a suspension wire fixing button which can rotate along a vertical direction rotating shaft without limitation; and the upper end of the suspension wire is connected with the horizontal rotating mechanism and is used for controlling the horizontal direction of the wellhead of the suspension wire light well.
The limiter adopts a tuning fork-shaped structure, two arms which are close to each other are arranged in the horizontal direction of the limiter, a limiter slit is formed between the two arms, a suspension wire of the suspension wire light well penetrates through the limiter slit and is connected with a pendant, horizontal scales are arranged at the position of the limiter slit, and the angle range shielded by the suspension wire light well can be directly read according to the position of the suspension wire.
The three-axis translation fine-tuning holder is used for providing displacement distances which are 10mm in three orthogonal directions, and is manually driven by a micrometer.
The material of the suspension wires is a high polymer material with high transparency to X-rays and is used for equipment signal acquisition.
The upper end of the lockable magnetic base is arranged on the X-axis and Y-axis orthogonal horizontal displacement table through countersunk screws convenient to disassemble and assemble, and the slide rail cantilever is fixed on the top surface of the Z-axis vertical displacement table through two countersunk screws.
The slide rail suspension arm provides 100mm of horizontal travel for the upper slider.
The suspension wire light well is a lead light well.
The use method of the suspension wire optical well bracket of the X-ray diffractometer comprises the following steps:
step 1: assembling the lockable magnetic base, the three-axis translational fine-tuning holder and the slide rail cantilever into a bracket assembly;
step 2: turning off the magnetic knob switch, placing the support assembly on a detector protective cover, and moving the position of the support assembly to enable the Y axis of the three-axis translational fine-tuning holder to fall in a vertical plane where direct X rays of equipment are located; then the magnetic knob switch is set to be turned on, so that the lockable magnetic base is sucked on the detector protection cover;
and step 3: the pre-assembled suspension wire light well penetrates through a suspension wire fixing button in the middle of an upper sliding block of a sliding rail suspension arm, and then a suspension wire is inserted into the suspension wire fixing button;
and 4, step 4: moving a sliding block on a cantilever of the sliding rail, placing the suspension wire light well in a stroke range near a target position, and locking the suspension wire; mounting the limiter to enable the lower end of the suspension wire to penetrate through a limiter slit;
and 5: adjusting an X axis, a Y axis, a Z axis and a suspension wire fixing button on the three-axis translation fine-tuning holder, and adjusting the limiter to enable the suspension wire to pass through a narrow slit of the limiter without contacting with a narrow slit arm when the suspension wire well is static; detecting the position of the light well by using low-power direct X-rays; repeating the steps until the suspension wire light well falls into a required position; and locking the X axis, the Y axis and the Z axis on the three-axis translational fine-tuning holder.
When the light path calibration operation is carried out, the bottom end of the suspension wire light well needs to be moved out of the slit opening of the limiter.
And when the suspension wire light well is shifted to the shading position again from the deviated light path position, if the suspension wire light well is shifted out of the light path and operated properly, only the bottom end of the suspension wire needs to be slightly shifted into the narrow slit of the limiter when the suspension wire light well is reset, and if the light path verification finds that the light well is inaccurate in position, the operation steps of the steps need to be repeated.
The invention is used for blocking the X-ray emitted by the diffractometer from directly irradiating the incident ray detector so as to protect the detector from being damaged by the ray. Compared with a door-shaped light well, the invention has the advantages that:
the invention adopts the suspension wire design, is directly arranged in front of the equipment detector and is completely separated from the equipment collimator pipe part, so that the two parts cannot interfere with each other.
The invention cancels the door-shaped frame, eliminates the shielding problem of the sample table and is convenient for the placement and the replacement of the sample.
The invention uses the design of the suspension wire, and the suspension wire material is a high polymer material with higher transparency to X-rays, thereby being beneficial to the signal acquisition of equipment.
The position of the light well can be infinitely and flexibly adjusted to form a freely selectable direct light shielding angle.
When the optical well is accidentally touched with low intensity, the optical well can be automatically and rapidly reset without debugging, so that the misoperation risk of the equipment is effectively avoided.
The invention is convenient to disassemble and assemble, has accurate positioning, can improve the experimental efficiency and effectively ensure the quality of experimental data.
Drawings
FIG. 1 is a schematic structural diagram of a suspension-wire optical well support of an X-ray diffractometer according to the present invention.
The reference numbers in the figures: the device comprises a lockable magnetic base 1, an X-axis and Y-axis orthogonal horizontal displacement table 2, a Z-axis vertical displacement table 3, a slide rail cantilever 4, a detector protection cover 5, a suspension wire 6, a pendant 7 and a slide block 8.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
Referring to fig. 1, the X-ray diffractometer suspension wire optical well support can be divided into five components.
The upper bearing fine-tuning holder of the magnetic base can be locked and fixed by screws, and the lower bearing fine-tuning holder is connected with the detector protective cover 5 and fixed by magnetic attraction. The base is provided with a knob switch which can control the magnetic force.
The three-axis translational fine tuning holder is divided into an upper section and a lower section, wherein the lower section is an X-axis and Y-axis orthogonal horizontal displacement table, and the upper section is a Z-axis vertical displacement table. The holder can provide displacement distances of about 10mm in three orthogonal directions, and the displacement precision can reach micron level by adopting a micrometer for propulsion.
The sliding rail suspension 4 can provide a horizontal travel of about 100mm for the upper slider 8. The center of the slide block 8 is provided with a horizontal rotating mechanism (without limitation of rotating angle) with angle scales, and the horizontal rotating mechanism is used for connecting the upper end suspension wires 6 of the light well.
The upper end of the suspension wire 6 is connected with the rotating mechanism so as to control the horizontal orientation of the wellhead of the light well. The lower end of the suspension wire 6 is connected with a gravity weight 7. The weight 7 provides a pull-down force to easily stabilize the light well.
A suspension wire 6 between a light well and a weight 7 penetrates through a slit (the width of the slit is 2 mm) on the limiter, so that the light well can rapidly reach a static stable state in the installation and debugging process. The limiter slit is provided with scales for marking the shielding angles of the light-emitting well to the straight rays at different positions.
The component usage workflow is as follows:
step 1: and assembling and integrating the components. As shown in fig. 1, the lockable magnetic base, the three-axis translational fine-tuning pan-tilt and the slide rail cantilever 4 with the slide rail of the device are assembled by fastening screws to form a complete bracket assembly.
Step 2: and mounting the bracket assembly. It is confirmed that the lockable magnetic base switch in the carriage assembly is in the "off" position, in which the base is in a low magnetic state for movement. The component is placed on a top plate of a protective cover 5 of the device detector, the position of the component is moved and adjusted, and the Y axis of a three-axis holder of the component falls in the vertical plane where the direct X-ray of the device is located. After the adjustment is finished, the lockable magnetic base switch is turned to an on position, and at the moment, the base generates strong magnetic force and is attracted to a top plate of the detector protection cover 5.
And step 3: installing a suspension wire light well: and (3) penetrating the lead light well which is assembled in advance through a hole in the middle of a sliding block 8 on a sliding rail cantilever 4 with a sliding rail, and then inserting a knob at the top end of a suspension wire 6 into a rotating hole of the sliding block 8.
And 4, step 4: coarse adjustment: and moving the sliding block 8 on the sliding rail cantilever 4 with the sliding rail, placing the optical well in a fine adjustment stroke range near the target position, and locking and fixing the sliding block 8. And installing a limiter to enable the lower end of the suspension wire 6 to penetrate through the narrow slit of the limiter.
And 5: fine adjustment: three translation shafts on the synchronous adjustment holder and a rotating button at the top end of the suspension wire 6 are matched with the adjustment limiter, so that the suspension wire 6 can pass through the narrow slit of the limiter and can not be contacted with the narrow slit arm when the light well is static. The location of the optical well is detected with low power direct X-rays. Repeating the fine adjustment process until the optical well falls into the required position. Locking pan head X, Y, Z triaxial fixed buttons.
The device performs an optical path calibration operation, sometimes requiring removal of the optical well. And (4) slightly moving the bottom end of the suspension wire 6 of the optical well out of the slit opening of the limiter, and moving the optical well out of the optical path. Note that touching the slit so that the stopper is displaced should be avoided, and pulling the polished rod string so that the string 6 is deformed or the bracket is displaced. If the operation is proper in the step, the bottom end of the suspension wire of the optical well only needs to be slightly moved into the narrow slit of the limiting stopper when the optical well is reset, and the limiting stopper can be deviated without touching the arm of the narrow slit. And if the light path verification finds that the position of the light well is not accurate, repeating the fine adjustment operation process of the step 5. After the fine adjustment is completed, the optical well is shifted to the light shielding position again from the light path deviation position.
The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (10)

1. A kind of X-ray diffractometer hangs the light well support of the silk, the said light well of hanging the silk includes fixing the hanging silk (6) in the centre of gravity of the light well and tying the pendant (7) in the bottom of hanging the silk (6), characterized by that, the said support includes providing the lockable magnetic force base (1) that stably supports for light well support, three-axis translation fine setting cloud terrace, slide gear and locating under hanging the silk light well and being used for making the light well of hanging the silk reach the steady stationary stop rapidly in the course of debugging;
the upper end of the lockable magnetic base (1) is connected with a three-axis translational fine tuning pan-tilt, and the lower end of the lockable magnetic base is adsorbed on a detector protective cover (5) through a magnetic device; the magnetic force knob switch capable of controlling the magnitude of magnetic force is arranged on the magnetic device;
the three-axis translational fine-tuning pan-tilt comprises an upper section and a lower section, wherein the lower section is an X-axis and Y-axis orthogonal horizontal displacement table (2), and the upper section is a Z-axis vertical displacement table (3);
the sliding device comprises a sliding rail cantilever (4) and a sliding block mechanism, wherein one end of the sliding rail cantilever (4) is fixed on the top surface of the Z-axis vertical displacement table (3); the sliding block mechanism comprises a sliding block (8) arranged on the sliding rail cantilever (4), a horizontal direction rotating mechanism with angle scales and arranged in the center of the sliding block (8), and a suspension wire fixing button which can rotate along a vertical direction rotating shaft without limitation; and the upper end of the suspension wire (6) is connected with the horizontal rotating mechanism and is used for controlling the horizontal orientation of the wellhead of the suspension wire light well.
2. The X-ray diffractometer suspension wire light well bracket according to claim 1, characterized in that the stopper is a tuning fork structure, two arms are arranged in the horizontal direction, a stopper slit is formed between the two arms, the suspension wire (6) of the suspension wire light well passes through the stopper slit and is connected with the weight (7), the stopper slit is provided with horizontal scales, and the angle range shielded by the suspension wire light well can be directly read according to the position of the suspension wire (6).
3. The X-ray diffractometer suspension wire light well bracket according to claim 1, wherein the three-axis translational fine tuning holder is used for providing displacement distances of 10mm in each of three orthogonal directions, and is manually driven by a micrometer.
4. The X-ray diffractometer suspension wire optical well bracket according to claim 1, characterized in that the suspension wire (6) is made of a high polymer material with high transparency to X-rays for device signal acquisition.
5. The X-ray diffractometer suspension wire optical well bracket according to claim 1, wherein the upper end of the lockable magnetic base (1) is mounted on the X-axis and Y-axis orthogonal horizontal displacement table (2) through countersunk screws convenient for disassembly, and the slide rail cantilever (4) is fixed on the top surface of the Z-axis vertical displacement table (3) through two countersunk screws.
6. The X-ray diffractometer suspended-wire optical well support according to claim 1, characterized in that the slide rail suspension arm (4) provides 100mm horizontal travel for its upper slide (8).
7. The X-ray diffractometer suspension wire optical well bracket of claim 1, wherein the suspension wire optical well is a lead optical well.
8. The method of using an X-ray diffractometer suspended-wire optical well support according to claim 1, characterized by the following steps:
step 1: assembling the lockable magnetic base (1), the three-axis translational fine-tuning holder and the slide rail cantilever (4) into a bracket assembly;
step 2: turning off the magnetic knob switch, placing the bracket component on a detector protection cover (5), and moving the position of the bracket component to enable the Y axis of the three-axis translational fine tuning holder to fall in a vertical plane where direct X rays of equipment are located; then the magnetic knob switch is set to be turned on, so that the lockable magnetic base (1) is sucked on the detector protective cover (5);
and step 3: the pre-assembled suspension wire light well penetrates through a suspension wire fixing button in the middle of a sliding block (8) on a sliding rail cantilever (4), and then a suspension wire (6) is inserted into the suspension wire fixing button;
and 4, step 4: moving a sliding block (8) on the sliding rail cantilever (4), placing the suspension wire optical well in a stroke range near a target position, and locking the suspension wire (6); mounting the limiter, and enabling the lower end of the suspension wire (6) to penetrate through a narrow slit of the limiter;
and 5: adjusting an X axis, a Y axis, a Z axis and a suspension wire fixing button on the three-axis translation fine-tuning holder, and adjusting the limiter to enable a suspension wire (6) to pass through a narrow slit of the limiter and not to contact with a narrow slit arm when the suspension wire light well is static; detecting the position of the light well by using low-power direct X-rays; repeating the steps until the suspension wire light well falls into a required position; and locking the X axis, the Y axis and the Z axis on the three-axis translational fine-tuning holder.
9. The use of the X-ray diffractometer suspension-wire optical well bracket according to claim 8, characterized in that the optical path calibration operation is performed by moving the bottom end of the suspension wire (6) of the suspension-wire optical well out of the stopper slit opening.
10. The use method of the suspension wire optical well bracket of the X-ray diffractometer according to claim 9, characterized in that when the suspension wire optical well is shifted from the light path deviation position to the light shielding position again, if the suspension wire optical well is shifted out of the light path and operated properly, the suspension wire optical well is reset by only slightly shifting the bottom end of the suspension wire (6) into the stopper slit, and if the light path verification finds that the position of the optical well is not accurate, the operation step of step (5) is repeated.
CN202010040663.1A 2020-01-15 2020-01-15 Suspension wire optical well bracket of X-ray diffractometer and use method thereof Active CN111141771B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112361969A (en) * 2020-11-20 2021-02-12 中国航空工业集团公司北京长城计量测试技术研究所 Detection apparatus for suspension wire angularity for acceleration sensor

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CN2241340Y (en) * 1995-07-30 1996-11-27 谈良知 Fibre-optic bicolour liquid level meter
GB201219021D0 (en) * 2011-11-11 2012-12-05 Rigaku Denki Co Ltd X-Ray intensity correction method and x-ray diffractometer
CN105510366A (en) * 2016-02-03 2016-04-20 中国工程物理研究院材料研究所 Portable X-ray diffractometer
RU2617560C1 (en) * 2016-04-04 2017-04-25 Акционерное общество "Научно-производственное предприятие "Буревестник" Method of adjusting samples in x-ray diffractometer
CN106932419A (en) * 2017-04-19 2017-07-07 南京大学 X-ray diffractometer capillary sample tube rack and its application method
CN108872279A (en) * 2018-05-08 2018-11-23 苏州矩阵光电有限公司 A kind of the light path calibration method and calibrating installation of four brilliant monochromators
CN211955275U (en) * 2020-01-15 2020-11-17 南京大学 X-ray diffractometer suspension wire light well support

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2241340Y (en) * 1995-07-30 1996-11-27 谈良知 Fibre-optic bicolour liquid level meter
GB201219021D0 (en) * 2011-11-11 2012-12-05 Rigaku Denki Co Ltd X-Ray intensity correction method and x-ray diffractometer
CN105510366A (en) * 2016-02-03 2016-04-20 中国工程物理研究院材料研究所 Portable X-ray diffractometer
RU2617560C1 (en) * 2016-04-04 2017-04-25 Акционерное общество "Научно-производственное предприятие "Буревестник" Method of adjusting samples in x-ray diffractometer
CN106932419A (en) * 2017-04-19 2017-07-07 南京大学 X-ray diffractometer capillary sample tube rack and its application method
CN108872279A (en) * 2018-05-08 2018-11-23 苏州矩阵光电有限公司 A kind of the light path calibration method and calibrating installation of four brilliant monochromators
CN211955275U (en) * 2020-01-15 2020-11-17 南京大学 X-ray diffractometer suspension wire light well support

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112361969A (en) * 2020-11-20 2021-02-12 中国航空工业集团公司北京长城计量测试技术研究所 Detection apparatus for suspension wire angularity for acceleration sensor
CN112361969B (en) * 2020-11-20 2022-03-29 中国航空工业集团公司北京长城计量测试技术研究所 Detection apparatus for suspension wire angularity for acceleration sensor

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