CN111141630A - Device for detecting erosion corrosion of reducing pipe and detection method thereof - Google Patents
Device for detecting erosion corrosion of reducing pipe and detection method thereof Download PDFInfo
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Abstract
The invention provides a device for detecting erosion corrosion of a reducing pipe and a detection method thereof, wherein the device comprises a testing device and a reducing pipe part, the testing device comprises a screw pump, a control cabinet, a water tank, an erosion chamber and an electrochemical test recording device, the screw pump is arranged below the control cabinet, a water inlet of the screw pump is communicated with a water outlet of the water tank through a water inlet pipeline, a water outlet of the screw pump is connected with a water inlet of the erosion chamber through an erosion water inlet pipeline, a water outlet of the erosion chamber is communicated with a water inlet of the water tank through an erosion water outlet pipeline, the reducing pipe part is arranged in the erosion chamber, the reducing pipe part is communicated with the erosion water inlet pipeline, and the electrochemical test recording device is connected with the reducing pipe part through a test lead. The device realizes that the erosion corrosion weightlessness test and the electrochemical test of the reducing pipe are carried out simultaneously, and realizes the electrochemical measurement of real time, multiple points and in situ at different positions of the reducing pipe.
Description
Technical Field
The invention relates to the technical field of erosion corrosion detection devices, in particular to a device for detecting erosion corrosion of a reducing pipe and a detection method thereof.
Background
At present, the experimental devices for researching Erosion corrosion of pipelines mainly comprise jet type experimental devices, rotary type experimental devices and pipe type experimental devices (Rajahram S S, Harvey T J, Wood R J K, Erosis-relative resistance of engineering materials in variant conditions, Wear,2009,267(1-4): 244-; different experimental devices, different experimental methods and different research means are used. The jet type experimental device can simulate the erosion corrosion process at any erosion speed and angle, but cannot well simulate the actual working condition, the erosion strength is higher than the actual condition, and the difference between the actual erosion condition and the actual erosion condition of a pump and a pipeline is certain. The rotary experimental device has the advantages of simple equipment, low price, short experimental period and the like, but requires stable rotation of the motor, no vibration of the rotating shaft under high-speed rotation, and incapability of truly simulating the actual working condition conditions of the pipeline (research on the scouring and corrosion synergistic effect of Tang-liquid-solid two-phase flow on the metal surface [ D ]. Welan: Welan university of Petroleum, 2018). The pipe flow type experimental device can well simulate the erosion corrosion of a pipeline under the actual working condition, can accurately control the flow rate, has a good fluid mechanics model, and has strong practical value in the experimental result (ginger dawn Xia, Lishi Zhuo, Lishui. metal erosion and abrasion [ M ]. Beijing: chemical industry Press, 2003).
When a pipeline conveys media, pipe fittings exposed in moving fluid are damaged by erosion in different degrees, particularly the erosion corrosion rate of bent pipes and reducing pipes is dozens of times higher than that of straight pipes, and the erosion corrosion characteristics of the reducing pipes at different positions are different; the damage forms are grooves, thinning and even breaking. In recent years, accidents caused by pipeline erosion damage are endless (Huohua. numerical simulation of typical pipe erosion corrosion [ D ]. Hangzhou: Zhejiang university, 2012). Liu Jian et al studied the Effect of flow rate on erosion corrosion of 90 ° elbows (Liu J G, BaKeDaShi W L, Li Z L, et al, Effect of flow gradient on erosion-corrosion of 90-coarse horizontal elbow, Wear,2017,376: 516. 525), Jin et al studied the Failure of tee pipe under multiphase flow conditions (Jin H, ChenX, Zheng Z, et al, Failure Analysis of multiphase flow erosion-corrosion in the water pipe, Engineering Failure Analysis,2017,73:46-56), but the study on erosion corrosion of reducer pipes was rare and the existing experimental setup could not characterize the erosion characteristics and interaction of erosion and corrosion in different areas of reducer pipes, and the study on erosion corrosion of reducer pipes showed great erosion corrosion limitations.
Disclosure of Invention
The invention overcomes the defects in the prior art, the existing experimental device can not represent the erosion corrosion characteristics of different local areas of the reducing pipe and the interaction of the erosion and the corrosion, and provides a device and a method for detecting the erosion corrosion of the reducing pipe.
The purpose of the invention is realized by the following technical scheme.
A device for detecting erosion corrosion of a reducing pipe comprises a testing device and a reducing pipe part,
the testing device comprises a screw pump, a control cabinet, a water tank, a scouring chamber and an electrochemical testing and recording device, wherein the screw pump is arranged below the control cabinet, a water inlet of the screw pump is communicated with a water outlet of the water tank through a water inlet pipeline, the water outlet of the screw pump is connected with a water inlet of the scouring chamber through a scouring water inlet pipeline, the water outlet of the scouring chamber is communicated with a water inlet of the water tank through a scouring water outlet pipeline, the reducing pipe part is arranged in the scouring chamber and is communicated with the scouring water inlet pipeline, and the electrochemical testing and recording device is connected with the reducing pipe part through a testing lead;
the reducing pipe part comprises a reducing pipe die, a large head groove, a reducing groove, a small head groove and a connecting piece, the large head of the reducing pipe die is provided with the large head groove, the reducing part of the reducing pipe die is provided with the reducing groove, the small head of the reducing pipe die is provided with the small head groove, the large head groove, the reducing groove and a working electrode are packaged in the small head groove, a wire hole is formed in the bottom of the large head groove, a reference electrode mounting hole and a counter electrode mounting hole are formed in the reducing pipe die, each reducing pipe die passes through the connecting piece for fixation, the reducing pipe die after fixation is installed in a scouring chamber, and two ends of the reducing pipe die after fixation are respectively connected with straight pipes with equal diameters.
The electrochemical testing and recording device comprises an electrochemical workstation and a data recording device, wherein a counter electrode in the electrochemical workstation is inserted in the counter electrode mounting hole, a reference electrode in the electrochemical workstation is inserted in the reference electrode mounting hole, the working electrode, the reference electrode and the counter electrode are all connected with the electrochemical workstation through the testing lead, and the electrochemical workstation is connected with the data recording device.
The electrochemical workstation adopts an AutoLab 302N electrochemical workstation, and the impedance test frequency range is 0.1Hz-10 kHz.
The number of the reducing pipe dies is 4, 6 or 8.
The surface of the working electrode is flush with the inner surface of the pipe diameter of the reducing pipe die.
The working electrode is packaged in the big head groove, the reducing groove and the small head groove of the reducing pipe die through epoxy resin.
The screw pump adopts adjustable screw pump, the velocity of flow of medium in the adjustable control pipeline.
A flowmeter is arranged on the flushing water inlet pipeline.
And a stirrer for uniformly mixing the corrosive solution is also arranged in the water tank.
The in-situ detection method for the erosion corrosion of the reducing pipe comprises the following steps:
step 1, encapsulating working electrodes in a large-head groove, a reducing groove and a small-head groove of a reducing pipe mold, installing a reference electrode and a counter electrode in a reference electrode installation hole and a counter electrode installation hole, fixing the reducing pipe mold by using a connecting piece, butting the reducing pipe mold with a pipeline on a testing device, preparing a solution, and adding quartz sand into a water tank;
and 6, obtaining the influence rule of parameters such as different flow rates, sand content, sand grain size and the like on the erosion corrosion of each position of the reducing pipe according to the weight loss amount and the electrochemical impedance spectrum of the working electrode at different positions of the reducing pipe.
The invention has the beneficial effects that: the inner wall of the reducing pipe is provided with a plurality of grooves, and working electrodes can be arranged at each position of the reducing pipe, so that the erosion corrosion weightlessness test and the electrochemical test of the reducing pipe can be simultaneously carried out; the electrochemical measurement in real time, multiple points and in situ can be realized at different positions of the reducing pipe; the erosion corrosion characteristics of different positions of the reducing pipe can be represented, and the erosion corrosion experiment result accords with the field working condition.
Drawings
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is a schematic structural view of the reducing pipe, wherein (a) is a three-dimensional structural view and (b) is a rear structural view;
FIG. 3 is a sample encapsulation view of a reduced diameter tube portion;
FIG. 4 is an assembled view of a reduced diameter tube portion and a three electrode system;
FIG. 5 is an impedance diagram of samples at different positions of the reducing pipe part after 6h of a erosion corrosion test;
in the figure: the device comprises a screw pump 1, a control cabinet 2, a flow meter 3, a water tank 4, a stirrer 5, a scouring chamber 6, a reducing pipe part 7, an electrochemical workstation 8, a data recording device 9, a working electrode 10, a counter electrode 11, a reference electrode 12, a connecting piece 13, an inlet pipeline 14, a scouring inlet pipeline 15, a scouring outlet pipeline 16 and a reducing pipe die 17.
For a person skilled in the art, other relevant figures can be obtained from the above figures without inventive effort.
Detailed Description
The technical solution of the present invention is further illustrated by the following specific examples.
Example one
A device for detecting erosion corrosion of a reducing pipe comprises a testing device and a reducing pipe part,
the testing device comprises a screw pump 1, a control cabinet 2, a water tank 4, a scouring chamber 6 and an electrochemical testing and recording device, wherein the screw pump 1 is arranged below the control cabinet 2, a water inlet of the screw pump 1 is communicated with a water outlet of the water tank 4 through a water inlet pipeline 14, the water outlet of the screw pump 1 is connected with a water inlet of the scouring chamber 6 through a scouring water inlet pipeline 15, the water outlet of the scouring chamber 6 is communicated with a water inlet of the water tank 4 through a scouring water outlet pipeline 16, a reducing pipe part is arranged in the scouring chamber 6, the reducing pipe part is communicated with the scouring water inlet pipeline 15, and the electrochemical testing and recording device is connected with the reducing pipe part through a testing lead;
the reducing pipe part comprises a reducing pipe die 17, a big end groove, a reducing groove, a small end groove and a connecting piece 13, the big end groove is formed in the big end of the reducing pipe die 17, the reducing groove is formed in the reducing position of the reducing pipe die 17, the small end groove is formed in the small end of the reducing pipe die 17, the working electrode 10 is packaged in the big end groove, the reducing groove and the small end groove, wire holes are formed in the bottoms of the big end groove, the reducing groove and the small end groove, a reference electrode mounting hole and a counter electrode mounting hole are formed in the reducing pipe die 17, each reducing pipe die 17 is fixed through the connecting piece 13, the fixed reducing pipe die 17 is installed in the scouring chamber 6, and two ends of the fixed reducing pipe die 17 are respectively connected with straight pipes with equal diameters.
The electrochemical testing and recording device comprises an electrochemical workstation 8 and a data recording device 9, a counter electrode 11 in the electrochemical workstation 8 is inserted in a counter electrode mounting hole, a reference electrode 12 in the electrochemical workstation 8 is inserted in a reference electrode mounting hole, the working electrode 10, the reference electrode 12 and the counter electrode 11 are all connected with the electrochemical workstation 8 through testing leads, the electrochemical workstation 8 is connected with the data recording device 9, the electrochemical workstation 8 adopts an AutoLab 302N electrochemical workstation, and the impedance testing frequency range is 0.1Hz-10 kHz.
Example two
On the basis of the first embodiment, the number of the reducing pipe dies 17 is 4, 6 or 8, the surfaces of the working electrodes 10 are flush with the inner surface of the pipe diameter of the reducing pipe dies 17, and the working electrodes 10 are encapsulated in the large-head grooves, the reducing grooves and the small-head grooves of the reducing pipe dies 17 through epoxy resin.
EXAMPLE III
On the basis of the second embodiment, the screw pump 1 adopts an adjustable screw pump, the flow speed of the medium in the pipeline can be adjusted and controlled, the flushing water inlet pipeline 15 is provided with a flowmeter 3, and the water tank 4 is also provided with a stirrer 5 for uniformly mixing the corrosive solution.
Example four
The in-situ detection method for the erosion corrosion of the reducing pipe comprises the following steps:
step 1, encapsulating working electrodes 10 in a large-head groove, a reducing groove and a small-head groove of a reducing pipe die 17, installing reference electrodes 12 and counter electrodes 11 in a reference electrode installation hole and a counter electrode installation hole, fixing the reducing pipe die 17 by using a connecting piece 13, butting the reducing pipe die with a pipeline on a testing device, preparing a solution, and adding quartz sand into a water tank 4;
and 6, obtaining the influence rule of parameters such as different flow rates, sand contents, sand grain sizes and the like on the erosion corrosion of each position of the reducing pipe according to the weight loss amount and the electrochemical impedance spectrum of the working electrode 10 at different positions of the reducing pipe.
As shown in fig. 5, the complex impedance plan at different positions of the reducing pipe basically presents a flattened capacitive reactance arc characteristic, which is characterized by a single time constant, and the radius of the half arc is different at different positions of the reducing pipe, i.e. the corrosion rate is different at different positions. The radius of the capacitor semi-arc is the largest at the large end part of the reducing pipe, the reducing part is larger, and the small end part of the reducing pipe is the smallest, which means that the charge transfer resistance at the large end part of the reducing pipe is the largest, the corrosion rate is the smallest, the charge transfer resistance at the small end part is the smallest, and the corrosion rate is the largest. Comparing the positions of the top, the side and the bottom of the pipe, the radius of the capacitance half arc at the top is the largest, the side is larger, and the bottom is the smallest, which shows that the corrosion rate at the top of the pipe is the smallest, and the corrosion rate at the bottom is the largest.
Spatially relative terms, such as "upper," "lower," "left," "right," and the like, may be used in the embodiments for ease of description to describe one element or feature's relationship to another element or feature as illustrated in the figures. It will be understood that the spatial terms are intended to encompass different orientations of the device in use or operation in addition to the orientation depicted in the figures. For example, if the device in the figures is turned over, elements described as "below" other elements or features would then be oriented "above" the other elements or features. Thus, the exemplary term "lower" can encompass both an upper and a lower orientation. The device may be otherwise oriented (rotated 90 degrees or at other orientations) and the spatially relative descriptors used herein interpreted accordingly.
Moreover, relational terms such as "first" and "second," and the like, may be used solely to distinguish one element from another element having the same name, without necessarily requiring or implying any actual such relationship or order between such elements.
The present invention has been described in detail, but the above description is only a preferred embodiment of the present invention, and is not to be construed as limiting the scope of the present invention. All equivalent changes and modifications made within the scope of the present invention shall fall within the scope of the present invention.
Claims (10)
1. The utility model provides a device for detecting reducing pipe erosion corrosion which characterized in that: comprises a testing device and a reducing pipe part,
the testing device comprises a screw pump, a control cabinet, a water tank, a scouring chamber and an electrochemical testing and recording device, wherein the screw pump is arranged below the control cabinet, a water inlet of the screw pump is communicated with a water outlet of the water tank through a water inlet pipeline, the water outlet of the screw pump is connected with a water inlet of the scouring chamber through a scouring water inlet pipeline, the water outlet of the scouring chamber is communicated with a water inlet of the water tank through a scouring water outlet pipeline, the reducing pipe part is arranged in the scouring chamber and is communicated with the scouring water inlet pipeline, and the electrochemical testing and recording device is connected with the reducing pipe part through a testing lead;
the reducing pipe part comprises a reducing pipe die, a large head groove, a reducing groove, a small head groove and a connecting piece, the large head of the reducing pipe die is provided with the large head groove, the reducing part of the reducing pipe die is provided with the reducing groove, the small head of the reducing pipe die is provided with the small head groove, the large head groove, the reducing groove and a working electrode are packaged in the small head groove, a wire hole is formed in the bottom of the large head groove, a reference electrode mounting hole and a counter electrode mounting hole are formed in the reducing pipe die, each reducing pipe die passes through the connecting piece for fixation, the reducing pipe die after fixation is installed in a scouring chamber, and two ends of the reducing pipe die after fixation are respectively connected with straight pipes with equal diameters.
2. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 1, wherein: the electrochemical testing and recording device comprises an electrochemical workstation and a data recording device, wherein a counter electrode in the electrochemical workstation is inserted in the counter electrode mounting hole, a reference electrode in the electrochemical workstation is inserted in the reference electrode mounting hole, the working electrode, the reference electrode and the counter electrode are all connected with the electrochemical workstation through the testing lead, and the electrochemical workstation is connected with the data recording device.
3. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 2, wherein: the electrochemical workstation adopts an AutoLab 302N electrochemical workstation, and the impedance test frequency range is 0.1Hz-10 kHz.
4. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 1, wherein: the number of the reducing pipe dies is 4, 6 or 8.
5. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 1, wherein: the surface of the working electrode is flush with the inner surface of the pipe diameter of the reducing pipe die.
6. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 5, wherein: the working electrode is packaged in the big head groove, the reducing groove and the small head groove of the reducing pipe die through epoxy resin.
7. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 1, wherein: the screw pump adopts adjustable screw pump.
8. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 7, wherein: a flowmeter is arranged on the flushing water inlet pipeline.
9. The apparatus for detecting erosion corrosion of a reducer pipe according to claim 1, wherein: and a stirrer for uniformly mixing the corrosive solution is also arranged in the water tank.
10. An in-situ method for detecting erosion corrosion of a reducer by using the apparatus for detecting erosion corrosion of a reducer according to any one of claims 1 to 9, comprising: the method comprises the following steps:
step 1, encapsulating working electrodes in a large-head groove, a reducing groove and a small-head groove of a reducing pipe mold, installing a reference electrode and a counter electrode in a reference electrode installation hole and a counter electrode installation hole, fixing the reducing pipe mold by using a connecting piece, butting the reducing pipe mold with a pipeline on a testing device, preparing a solution, and adding quartz sand into a water tank;
step 2, opening a switch of the control cabinet, operating a screw pump and a stirrer, enabling the solution in the water tank and the quartz sand to be uniformly mixed by the stirrer, enabling the solution in the water tank to flow along a pipeline shown by an arrow by the screw pump, enabling the solution to flow into a scouring chamber through a flowmeter and a reducing pipe part, connecting the scouring chamber with the water tank, and finally enabling the solution to flow back into the water tank to form a circulating pipeline system for a scouring corrosion experiment;
step 3, connecting the working electrode, the counter electrode and the reference electrode with an electrochemical workstation through leads, and sequentially detecting the corrosion potential and the electrochemical impedance spectrum of each working electrode on line;
step 4, after the experiment is finished, turning off a switch of the control cabinet, taking down the reducing pipe part, and taking out the working electrodes in the big-end groove, the reducing groove and the small-end groove;
step 5, carrying out corrosion morphology observation and corrosion product component analysis on the working electrodes, weighing the working electrodes after removing corrosion products on the surfaces of the working electrodes, and determining the weight loss of each working electrode;
and 6, obtaining the influence rule of parameters such as different flow rates, sand content, sand grain size and the like on the erosion corrosion of each position of the reducing pipe according to the weight loss amount and the electrochemical impedance spectrum of the working electrode at different positions of the reducing pipe.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112683154A (en) * | 2020-12-28 | 2021-04-20 | 福州大学 | Indirect measurement method for abrasion of parts which are not easy to disassemble, such as high-speed switch valve and the like |
CN112903576A (en) * | 2021-01-18 | 2021-06-04 | 中国船舶重工集团公司第七二五研究所 | Electrochemical testing device for erosion corrosion of pipeline inner wall special-shaped structure |
CN113324865A (en) * | 2021-05-27 | 2021-08-31 | 中国船舶重工集团公司第七二五研究所 | Liquid-solid two-phase flow pipeline erosion corrosion test device |
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2018
- 2018-11-05 CN CN201811309525.8A patent/CN111141630A/en active Pending
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112683154A (en) * | 2020-12-28 | 2021-04-20 | 福州大学 | Indirect measurement method for abrasion of parts which are not easy to disassemble, such as high-speed switch valve and the like |
CN112683154B (en) * | 2020-12-28 | 2022-05-17 | 福州大学 | Indirect measurement method for abrasion of parts which are not easy to disassemble, such as high-speed switch valve and the like |
CN112903576A (en) * | 2021-01-18 | 2021-06-04 | 中国船舶重工集团公司第七二五研究所 | Electrochemical testing device for erosion corrosion of pipeline inner wall special-shaped structure |
CN113324865A (en) * | 2021-05-27 | 2021-08-31 | 中国船舶重工集团公司第七二五研究所 | Liquid-solid two-phase flow pipeline erosion corrosion test device |
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