CN111085002A - Full-angle glycerol water purification equipment - Google Patents

Full-angle glycerol water purification equipment Download PDF

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Publication number
CN111085002A
CN111085002A CN201911278555.1A CN201911278555A CN111085002A CN 111085002 A CN111085002 A CN 111085002A CN 201911278555 A CN201911278555 A CN 201911278555A CN 111085002 A CN111085002 A CN 111085002A
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CN
China
Prior art keywords
tower body
diversion
mouth
water
water conservancy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911278555.1A
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Chinese (zh)
Inventor
倪震
曾炜
伍海辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Kangning Oil Technology Co Ltd
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Anhui Kangning Oil Technology Co Ltd
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Filing date
Publication date
Application filed by Anhui Kangning Oil Technology Co Ltd filed Critical Anhui Kangning Oil Technology Co Ltd
Priority to CN201911278555.1A priority Critical patent/CN111085002A/en
Publication of CN111085002A publication Critical patent/CN111085002A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention discloses full-angle glycerol water purification equipment. The tower body is provided with a first diversion port for guiding the evaporation gas in a first direction, a second diversion port for guiding the evaporation gas in a second direction, a third diversion port for guiding the evaporation gas in a third direction and a fourth diversion port for guiding the evaporation gas in a fourth direction. The invention can solve the problem that the evaporated water can not be recycled.

Description

Full-angle glycerol water purification equipment
Technical Field
The invention relates to the technical field of glycerol production, in particular to full-angle glycerol water purification equipment.
Background
Purified glycerol water is generally low in concentration, about 7% -8% of the purified glycerol water, and a large amount of water needs to be removed when the content is increased to more than 80%, and the process of removing water is called glycerol evaporation, which is also called purification. The conventional glycerin water purification process is carried out in an open purification tank, and the water in the glycerin water is directly discharged to the atmosphere by using high-temperature steam.
One of the disadvantages of the method is that the water is evaporated in an open way, the heat loss is large, the production cost is high, and the water evaporated out contains a small part of glycerin, the COD value is very high, the requirement of the country for environmental protection production in recent years is not met, and the water evaporated out can not be recycled, so that the resource is seriously wasted.
Disclosure of Invention
Aiming at the defects of the prior art, the invention discloses full-angle glycerin water purification equipment which can solve the problem that evaporated water cannot be recycled.
In order to achieve the purpose, the invention is realized by the following technical scheme:
full angle glycerine water purification equipment, including the tower body that is used for holding the glycerine water, be provided with at the tower body and be used for guiding boil-off gas in the first direction first water conservancy diversion mouth, be used for guiding boil-off gas in the second direction second water conservancy diversion mouth, be used for guiding boil-off gas in the third direction third water conservancy diversion mouth, be used for guiding boil-off gas in the fourth direction fourth water conservancy diversion mouth, first water conservancy diversion mouth is followed the circumference of tower body is extended, the second water conservancy diversion mouth is followed the circumference of tower body is extended, the third water conservancy diversion mouth is followed the circumference of tower body is extended, the fourth water conservancy diversion mouth is followed the circumference of tower body is extended, along the projection of the direction of height of tower body, first water conservancy diversion mouth with second water conservancy diversion mouth partially overlaps, the second water conservancy diversion mouth with third water conservancy diversion mouth partially overlaps, the third water conservancy diversion mouth with fourth water conservancy diversion mouth partially overlaps, the fourth diversion opening and the first diversion opening are partially overlapped.
The preferable technical scheme is that the inner cavity of the tower body is provided with a first guide opening, the bottom of the first guide opening extends along the radial direction of the tower body to form a first protrusion, the first protrusion extends along the circumferential direction of the tower body to guide the condensate on the inner side wall of the tower body to enter the first guide opening, and the first guide opening is connected with a first pipeline connector outside the tower body.
According to the preferable technical scheme, the inner cavity of the tower body is provided with a second guide opening, the bottom of the second guide opening extends along the radial direction of the tower body to form a second protrusion, the second protrusion extends along the circumferential direction of the tower body to guide condensate on the inner side wall of the tower body to enter the second guide opening, and the second guide opening is connected with a second pipeline connector outside the tower body.
According to the preferable technical scheme, the inner cavity of the tower body is provided with a third guide opening, the bottom of the third guide opening extends along the radial direction of the tower body to form a third protrusion, the third protrusion extends along the circumferential direction of the tower body to guide condensate on the inner side wall of the tower body to enter the third guide opening, and the third guide opening is connected with a third pipeline connector outside the tower body.
According to the preferable technical scheme, the inner cavity of the tower body is provided with a fourth flow guide opening, the bottom of the fourth flow guide opening extends along the radial direction of the tower body to form a fourth protrusion, the fourth protrusion extends along the circumferential direction of the tower body to guide the condensate on the inner side wall of the tower body to enter the fourth flow guide opening, and the fourth flow guide opening is connected with a fourth pipeline connector outside the tower body.
In a preferred embodiment, in a height direction of the tower body, a height of the first diversion port is set to H1, a height of the second diversion port is set to H2, a height of the third diversion port is set to H3, and a height of the fourth diversion port is set to H4, where H1 > H2, H4 > H3.
The preferred technical scheme, the tower body is including the inlet that is used for injecting into glycerine water, the pressure release mouth that is used for quick pressure release, the inlet is in the bottom of tower body sets up, the pressure release mouth is in the top of tower body sets up, the internal diameter of inlet sets up to R1, the internal diameter of pressure release mouth sets up to R2, and R1 < R2.
The invention discloses a full-angle glycerol water purification device, which has the following advantages:
the tower body is in four water conservancy diversion mouths that are the platykurtic and extend that four different directions set up, can realize retrieving in multi-direction and release the moisture of effusion to improve the recovery efficiency to the gaseous state moisture of effusion glycerine by a wide margin, and then reduce piling up of moisture in the tower body, with the formation that reduces the inside liquid moisture of tower body, avoided moisture to get back to in the glycerine again and the purification effect that leads to descends.
Four water conservancy diversion mouths overlap the setting each other partially, can realize the continuous arrangement to the tower body lateral wall in the circumference of tower body to carry out all-round release to the gas moisture of effusion in the circumference of tower body, with improve the recovery rate to gas moisture by a wide margin, also can retrieve completely the liquid moisture of the inside wall of tower body, and then avoid moisture to get back to in the glycerine again completely.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below.
It is obvious that the drawings in the following description are only some embodiments of the invention, and that for a person skilled in the art, other drawings can be derived from them without inventive effort.
FIG. 1 is a front view of an embodiment of the present invention;
FIG. 2 is a cross-sectional view of an embodiment of the present invention;
FIG. 3 is an enlarged view of a portion of an embodiment of the present invention;
FIG. 4 is a top view of an embodiment of the invention (with the pipe joint omitted);
FIG. 5 is a top view of an embodiment of the present invention;
fig. 6 is a system block diagram of an embodiment of the invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments.
All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1 to 6, the all-angle glycerin water purifying apparatus according to the embodiment of the present invention includes a tower body 1 for containing glycerin water, the tower body 1 is provided with a first diversion port 11 for guiding an evaporation gas in a first direction, a second diversion port 12 for guiding the evaporation gas in a second direction, a third diversion port 13 for guiding the evaporation gas in a third direction, and a fourth diversion port 14 for guiding the evaporation gas in a fourth direction, the first diversion port 11 extends along a circumferential direction of the tower body 1, the second diversion port 12 extends along the circumferential direction of the tower body 1, the third diversion port 13 extends along the circumferential direction of the tower body 1, the fourth diversion port 14 extends along the circumferential direction of the tower body 1, a projection along a height direction of the tower body 1, the first diversion port 11 and the second diversion port 12 partially overlap, the second diversion port 12 and the third diversion port 13 partially overlap, the third diversion opening 13 and the fourth diversion opening 14 are partially overlapped, and the fourth diversion opening 14 and the first diversion opening 11 are partially overlapped.
In order to further recover the escaped moisture, in the inner cavity of the tower body 1, the bottom of the first diversion opening 11 extends along the radial direction of the tower body 1 to form a first protrusion 110, the first protrusion 110 extends along the circumferential direction of the tower body 1 to guide the condensate on the inner side wall of the tower body 1 to enter the first diversion opening 11, and the first diversion opening 11 is connected with a first pipeline joint 111 outside the tower body 1. The condensation equipment is connected through the pipeline joint 111, so that the simultaneous recovery operation of the gas-state moisture and the liquid-state moisture is realized.
In order to further recover the escaped moisture, in the inner cavity of the tower body 1, the bottom of the second guiding opening 12 extends along the radial direction of the tower body 1 to form a second protrusion 120, the second protrusion 120 extends along the circumferential direction of the tower body 1 to guide the condensate on the inner side wall of the tower body 1 to enter the second guiding opening 12, and the second guiding opening 12 is connected with a second pipeline joint 121 outside the tower body 1. And the second pipeline joint 121 is connected with a condensing device, so that the simultaneous recovery operation of the gas-state and liquid-state moisture is realized.
In order to further recover the escaped moisture, a third protrusion 130 is formed at the bottom of the third guiding opening 13 in the inner cavity of the tower body 1 along the radial direction of the tower body 1, the third protrusion 130 extends along the circumferential direction of the tower body 1 to guide the condensate on the inner side wall of the tower body 1 to enter the third guiding opening 13, and a third pipe joint 131 is connected to the third guiding opening 13 at the outside of the tower body 1. The condensing equipment is connected through the third pipe joint 131, thereby realizing the simultaneous recovery operation of the moisture in the gas state and the liquid state.
In order to further recover the escaped moisture, in the inner cavity of the tower body 1, the bottom of the fourth diversion opening 14 extends along the radial direction of the tower body 1 to form a fourth protrusion 140, the fourth protrusion 140 extends along the circumferential direction of the tower body 1 to guide the condensate on the inner side wall of the tower body 1 to enter the fourth diversion opening 14, and a fourth pipeline joint 141 is connected to the fourth diversion opening 14 at the outer part of the tower body 1. The condensing apparatus is connected through the fourth pipe joint 141, thereby realizing simultaneous recovery of moisture in a gas state and a liquid state.
In order to recover the escaped moisture at different heights, the height of the first diversion port 11 is set to be H1, the height of the second diversion port 12 is set to be H2, the height of the third diversion port 13 is set to be H3, and the height of the fourth diversion port is set to be H4, and H1 > H2 ═ H4 > H3 along the height direction of the tower body 1. Thereby forming a multi-position recovery in the height direction of the tower 1.
In order to avoid the inside too big pressure of tower body 1, tower body 1 is including the inlet 10 that is used for injecting into glycerine water, the pressure release mouth 19 that is used for quick pressure release, inlet 10 is in the bottom of tower body 1 sets up, pressure release mouth 19 is in the top of tower body 1 sets up, the internal diameter of inlet 10 sets up to R1, the internal diameter of pressure release mouth 19 sets up to R2, R1 < R2. Thereby release pressure when tower body 1 internal pressure is too big to guarantee the operation safety.
It will be appreciated that the inlet port 10 and the pressure relief port 19 may be connected to the same basin in which the glycerol water to be treated is stored. After the four diversion ports are connected to the condensing tank, liquid moisture condensed out by the condensing tank can be connected and guided to the recovery tank for other use.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions.
Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.

Claims (7)

1. Full angle glycerine water purification equipment is including being used for holding the tower body of glycerine water, its characterized in that: the tower body is provided with a first diversion opening for guiding the evaporation gas in a first direction, a second diversion opening for guiding the evaporation gas in a second direction, a third diversion opening for guiding the evaporation gas in a third direction, and a fourth diversion opening for guiding the evaporation gas in a fourth direction, wherein the first diversion opening extends along the circumferential direction of the tower body, the second diversion opening extends along the circumferential direction of the tower body, the third diversion opening extends along the circumferential direction of the tower body, the fourth diversion opening extends along the circumferential direction of the tower body, the projection of the height direction of the tower body is formed, the first diversion opening is partially overlapped with the second diversion opening, the second diversion opening is partially overlapped with the third diversion opening, the third diversion opening is partially overlapped with the fourth diversion opening, and the fourth diversion opening is partially overlapped with the first diversion opening.
2. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: the inner chamber of tower body, the bottom of first water conservancy diversion mouth is followed the radial extension of tower body forms first protruding, first protruding edge the circumference of tower body extends to the guide the condensate of tower body inside wall gets into first water conservancy diversion mouth the outside of tower body, first water conservancy diversion mouth is connected with first pipe joint.
3. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: the inner chamber of tower body, the bottom of second water conservancy diversion mouth is followed the radial extension of tower body forms the second and swells, the second is protruding to be followed the circumference of tower body extends to the guide the condensate of tower body inside wall gets into second water conservancy diversion mouth the outside of tower body, second water conservancy diversion mouth is connected with the second pipe joint.
4. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: the inner chamber of tower body, the bottom of third water conservancy diversion mouth is followed the radial extension of tower body forms the third and swells, the third is protruding to be followed the circumference of tower body extends to the guide the condensate of tower body inside wall gets into third water conservancy diversion mouth the outside of tower body, third water conservancy diversion mouth is connected with the third pipe joint.
5. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: the inner chamber of tower body, the bottom of fourth water conservancy diversion mouth is followed the radial extension of tower body forms the fourth and swells, the fourth is protruding to be followed the circumference of tower body extends to the guide the condensate of tower body inside wall gets into fourth water conservancy diversion mouth the outside of tower body, fourth water conservancy diversion mouth is connected with the fourth pipeline and connects.
6. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: in the height direction of the tower body, the height of the first diversion port is set to be H1, the height of the second diversion port is set to be H2, the height of the third diversion port is set to be H3, the height of the fourth backflow port is set to be H4, and H1 is greater than H2, H4 is greater than H3.
7. The apparatus for purifying whole-angle glycerol water as claimed in claim 1, wherein: the tower body is including the inlet that is used for pouring into glycerine water, the pressure release mouth that is used for quick pressure release, the inlet is in the bottom of tower body sets up, the pressure release mouth is in the top of tower body sets up, the internal diameter of inlet sets up to R1, the internal diameter of pressure release mouth sets up to R2, R1 < R2.
CN201911278555.1A 2019-12-13 2019-12-13 Full-angle glycerol water purification equipment Pending CN111085002A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911278555.1A CN111085002A (en) 2019-12-13 2019-12-13 Full-angle glycerol water purification equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911278555.1A CN111085002A (en) 2019-12-13 2019-12-13 Full-angle glycerol water purification equipment

Publications (1)

Publication Number Publication Date
CN111085002A true CN111085002A (en) 2020-05-01

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911278555.1A Pending CN111085002A (en) 2019-12-13 2019-12-13 Full-angle glycerol water purification equipment

Country Status (1)

Country Link
CN (1) CN111085002A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102600627A (en) * 2011-12-23 2012-07-25 安徽国孚润滑油工业有限公司 Cyclone-flash cloth-film-reboiling-type heat-pipe distiller
CN203736872U (en) * 2014-01-07 2014-07-30 昆明理工大学 Dilute glycerin water solution concentrating device
CN106457058A (en) * 2014-01-31 2017-02-22 索拉奎金国际有限公司 Counter current liquid gas evaporation and condensation apparatus with fragmentation plates
CN206203920U (en) * 2016-11-28 2017-05-31 哈尔滨工大金涛科技股份有限公司 Waste water residual heat evaporator
CN208493257U (en) * 2018-05-28 2019-02-15 安徽省瑞芬得油脂深加工有限公司 A kind of explosion-proof type glycerol liquor concentrator

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102600627A (en) * 2011-12-23 2012-07-25 安徽国孚润滑油工业有限公司 Cyclone-flash cloth-film-reboiling-type heat-pipe distiller
CN203736872U (en) * 2014-01-07 2014-07-30 昆明理工大学 Dilute glycerin water solution concentrating device
CN106457058A (en) * 2014-01-31 2017-02-22 索拉奎金国际有限公司 Counter current liquid gas evaporation and condensation apparatus with fragmentation plates
CN206203920U (en) * 2016-11-28 2017-05-31 哈尔滨工大金涛科技股份有限公司 Waste water residual heat evaporator
CN208493257U (en) * 2018-05-28 2019-02-15 安徽省瑞芬得油脂深加工有限公司 A kind of explosion-proof type glycerol liquor concentrator

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Application publication date: 20200501

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