CN111067925A - Production method of fried cowherb seed decoction pieces and determination method of explosion rate of fried cowherb seed decoction pieces - Google Patents

Production method of fried cowherb seed decoction pieces and determination method of explosion rate of fried cowherb seed decoction pieces Download PDF

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CN111067925A
CN111067925A CN202010012304.5A CN202010012304A CN111067925A CN 111067925 A CN111067925 A CN 111067925A CN 202010012304 A CN202010012304 A CN 202010012304A CN 111067925 A CN111067925 A CN 111067925A
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林伟雄
邓李红
田清清
张志鹏
曾昭君
张雪兰
黄瑶
黄梦婷
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Guangdong Yifang Pharmaceutical Co Ltd
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Abstract

The invention discloses a production method of a fried cowherb seed decoction piece, which comprises the following steps: (1) pre-frying or frying the cowherb seeds to obtain fried cowherb seed decoction pieces; (2) taking a preset amount of fried cowherb seed decoction pieces; (3) measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data; (4) establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation for calculation, and solving the explosion rate of the fried cowherb seeds decoction pieces; (5) and setting or adjusting frying parameters according to the popping rate of the fried cowherb seed decoction pieces. Correspondingly, the invention also provides a method for measuring the popping rate of the fried cowherb seed decoction pieces. The method is simple, can quickly and accurately judge the explosion rate of the fried cowherb seed decoction pieces in the frying process, can optimize the frying parameters in time, improves the explosion rate and improves the production efficiency.

Description

Production method of fried cowherb seed decoction pieces and determination method of explosion rate of fried cowherb seed decoction pieces
Technical Field
The invention relates to the technical field of traditional Chinese medicine processing, in particular to a production method of fried cowherb seed decoction pieces and a determination method of a puffing rate of the fried cowherb seed decoction pieces.
Background
The cowherb seed is a dry mature seed of Vaccinium macrocephalum segetalis (Neok.) Garcke of Caryophyllaceae, is a traditional Chinese medicine commonly used in China, and is listed as the superior product from Shennong Ben Cao Jing. Has the effects of promoting blood circulation and stimulating the menstrual flow, promoting lactation and reducing swelling, and inducing diuresis and treating stranguria, and is mainly used for treating amenorrhea, dysmenorrhea, agalactia, stranguria and other symptoms clinically. The main chemical components of the cowherb seed comprise flavonoid glycoside, alkaloid, cyclic peptide, triterpenoid saponin, volatile oil and the like, wherein the cowherb seed flavonoid glycoside and the erythrina are main effective components and have the pharmacological effects of promoting milk secretion, protecting vascular endothelial cells, resisting inflammation, enhancing immunity, resisting liver injury and the like.
Since the seeds of the cowherb seeds are hard, the effective components are not easy to be decocted, and since the Ming dynasty, the cowherb seed decoction pieces are continuously prepared by a frying method, so that the seed coats are cracked, the seeds are exploded and bloomed, the decocting effect of the effective components is improved, and the loose texture of the fried cowherb seeds is beneficial to the effective components to be decocted, has strong dispersing power, and is better than activating blood and stimulating the menstrual flow, promoting lactation and treating stranguria.
In the traditional Chinese pharmacopoeia 2015, the cowherb seeds are required to be fried by a clear frying method until most of the cowherb seeds are exploded and white, the actual production of enterprises at present basically takes the explosion rate of more than 80% as the frying limit, and meanwhile, the traditional manual frying with high labor intensity and low efficiency is replaced by a mechanical frying mode so as to meet the increasing clinical medicine demand. However, the problem that the stir-frying of the cowherb seed decoction pieces is difficult to prepare and low in explosion rate easily occurs, the stir-frying parameter requirement is strict, and the actual production needs trial stir-frying so as to achieve the qualified explosion rate and stable parameters and then carry out normal production, so that the quick and correct control of the actual explosion rate is extremely important.
However, the explosion rate is judged by adopting a visual inspection method in the prior production, a manual calculation method is adopted if necessary, the seed coat of the cowherb seed fried decoction pieces cracks, explodes and blooms, the volume expands, the weight is light, the volume of the cowherb seed decoction pieces which do not explode and whiten flowers is small, but the actual weight is large, a visual error is caused, the visual explosion rate is higher than the actual explosion rate, the inventor uses a plurality of different batches of cowherb seed decoction pieces with known explosion rates for 10-20 people to judge the explosion rate visually through experiments, and the visual judgment value is higher than the actual explosion rate.
The method of manually selecting the stiff seed decoction pieces which are not popped is adopted to calculate the popping rate, the time consumption is too long, the feedback speed is slow, the production progress is influenced, and the timely adjustment of the field frying parameters is not facilitated.
Disclosure of Invention
The technical problem to be solved by the invention is to provide a production method of fried cowherb seed decoction pieces, which is simple, can quickly and accurately judge the popcorn rate of the fried cowherb seed decoction pieces, and can timely and conveniently set and optimize frying parameters.
The invention also aims to solve the technical problem of providing a method for measuring the popping rate of the cowherb seed fried decoction pieces, which is simple, rapid and convenient to measure the popping rate and has accurate result.
In order to achieve the technical effects, the invention provides a production method of a cowherb seed fried decoction piece, which comprises the following steps:
(1) pre-frying or frying the cowherb seeds to obtain fried cowherb seed decoction pieces;
(2) taking a preset amount of fried cowherb seed decoction pieces;
(3) measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data;
(4) establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation for calculation, and solving the explosion rate of the fried cowherb seeds decoction pieces;
(5) and setting or adjusting frying parameters according to the popping rate of the fried cowherb seed decoction pieces.
As an improvement of the scheme, the sampling amount of the fried cowherb seed decoction pieces is 50-5000 g.
As an improvement of the scheme, the linear regression equation of the explosion rate and the volume of the decoction pieces is shown as the formula I:
Y＝(0.0234n)X+1.2215n
wherein, n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
As an improvement of the above scheme, in the step (4), substituting the volume data into the linear regression equation for calculation includes:
and substituting different sampling quantities into different linear regression equations to obtain the explosion rate.
As an improvement of the above scheme, when the sampling amount is 50g, the linear regression equation is that Y is 1.1447X +63.902, and the correlation coefficient r is 0.9991;
when the sampling quantity is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999;
when the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997;
when the sampling amount is 500g, the linear regression equation is that Y is 11.866X +595.23, and the correlation coefficient r is 0.9992;
when the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993;
when the sampling amount is 5000g, the linear regression equation is that Y is 117.02X +6088.6, and the correlation coefficient r is 0.9995;
wherein Y is the volume of the decoction pieces, and X is the bursting rate.
As an improvement of the scheme, when the sampling amount of the fried cowherb seed decoction pieces is 50-5000 g, the linear regression equation of the popping rate and the decoction piece volume is shown as a formula II:
Figure BDA0002357589990000031
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75 g;
or
Figure BDA0002357589990000032
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure BDA0002357589990000033
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure BDA0002357589990000034
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure BDA0002357589990000035
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure BDA0002357589990000036
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
As an improvement of the above scheme, in the step (3), the step of measuring the volume of the parched semen vaccariae decoction pieces comprises:
pouring the decoction pieces into a container with volume scale, compacting, spreading surface, and reading volume V of the decoction piecesaCompacting, spreading the surface, and reading volume V of decoction piecesbCalculating VaAnd VbThe average value of (A) is taken as the reading V of the volume of the decoction piecesab。
As an improvement of the above scheme, in the step (3), the step of measuring the volume of the parched semen vaccariae decoction pieces comprises:
tap readings are carried out by 1-3 persons to respectively obtain V1(Vab)、V2(Vab)、V3(Vab) Reading decoction pieces, and calculating V1、V2And V3The average was taken as the final volume reading of the tablets
Figure BDA0002357589990000041
Correspondingly, the invention also provides a method for measuring the popping rate of the fried cowherb seed decoction pieces, which comprises the following steps:
(1) taking a preset amount of fried cowherb seed decoction pieces;
(2) measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data;
(3) and establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation to calculate the explosion rate of the fried cowherb seeds, wherein the explosion rate is used for setting or adjusting the frying parameters.
As an improvement of the scheme, the linear regression equation of the explosion rate and the volume of the decoction pieces is shown as the formula I:
Y＝(0.0234n)X+1.2215n
wherein n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
As an improvement of the above scheme, when the sampling amount is 50g, the linear regression equation is that Y is 1.1447X +63.902, and the correlation coefficient r is 0.9991;
when the sampling quantity is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999;
when the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997;
when the sampling amount is 500g, the linear regression equation is that Y is 11.866X +595.23, and the correlation coefficient r is 0.9992;
when the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993;
when the sampling amount is 5000g, the linear regression equation is that Y is 117.02X +6088.6, and the correlation coefficient r is 0.9995;
wherein Y is the volume of the decoction pieces, and X is the bursting rate.
As an improvement of the scheme, the sampling amount of the fried cowherb seed decoction pieces is 50-5000 g, and the linear regression equation of the explosion rate and the decoction piece volume is shown as a formula II:
Figure BDA0002357589990000051
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75 g;
or
Figure BDA0002357589990000052
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure BDA0002357589990000053
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure BDA0002357589990000054
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure BDA0002357589990000055
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure BDA0002357589990000056
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
The implementation of the invention has the following beneficial effects:
(1) the invention provides a production method of fried cowherb seed decoction pieces, which establishes a linear regression equation of the popcorn rate and the decoction piece volume, calculates the popcorn rate of the fried cowherb seed decoction pieces by measuring the volume of the fried cowherb seed decoction pieces, and further sets or timely adjusts frying parameters, so that qualified decoction pieces meeting standard requirements can be processed, and the quality of the decoction pieces is ensured. Moreover, the invention rapidly measures the explosion rate of the fried cowherb seed decoction pieces and rapidly feeds back the result, thereby being beneficial to smooth production or rapid adjustment of the processing scheme, optimizing the frying parameters in time, processing qualified decoction pieces meeting the standard requirements, and being capable of monitoring the explosion rate in the whole process in time in the frying process, ensuring the quality of the decoction pieces, improving the production efficiency and meeting the current rapidly-developed mechanical frying speed and the increasing medicine demand.
(2) The invention provides a method for measuring the popcorn rate of the fried cowherb seed decoction pieces, which is simple, quick and convenient, has accurate results, and can quickly and accurately judge the popcorn rate of the fried cowherb seed decoction pieces in the frying process; moreover, misjudgment caused by visual inspection of the explosion rate by naked eyes can be reduced, the stir-frying parameters are adjusted in time to meet the requirements of standard decoction pieces, and the quality of the decoction pieces is improved; in addition, the manpower, material resources and time consumed by manual calculation can be reduced, and the production cost is reduced.
Drawings
FIG. 1 is a flow chart of a method for producing the parched semen Vaccariae decoction pieces of the present invention;
FIG. 2 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 50 g;
FIG. 3 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 100 g;
FIG. 4 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 200 g;
FIG. 5 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 500 g;
FIG. 6 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 1000 g;
FIG. 7 is a linear relationship graph of the decrepitation rate and volume of the parched semen Vaccariae decoction pieces when the sampling amount is 5000 g;
FIG. 8 is a flow chart of the method for determining the popping rate of the fried cowherb seed decoction pieces of the invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail with reference to the accompanying drawings.
The cowherb seed is a seed medicinal material, the active ingredients are difficult to leach, and after the cowherb seed is processed by a processing technology, the medicinal material is heated and explodes, and the explosion is directly proportional to the leaching of the active ingredients of the medicinal material. The popping rate is an index for measuring the popping degree of the cowherb seeds, thereby ensuring the decoction and curative effect of the effective components of the cowherb seeds.
As shown in fig. 1, the invention provides a production method of a cowherb seed stir-fried decoction piece, which comprises the following steps:
s101, pre-frying or frying the cowherb seeds to obtain fried cowherb seed decoction pieces;
the stir-frying in step S101 may be pre-stir-frying before production, or stir-frying during production. The invention can sample in the pre-frying process before production, and set the frying parameters after detecting the explosion rate of the fried cowherb seed decoction pieces so as to carry out the subsequent production sequence. The invention can also carry out sampling in the actual frying process, and adjust the frying parameters after detecting the explosion rate of the fried cowherb seed decoction pieces. The frying method of the cowherb seed is carried out according to the prior art.
S102, taking a preset amount of fried cowherb seed decoction pieces;
wherein, taking decoction pieces of parched semen Vaccariae, sampling according to the sampling method of 0211 medicinal materials and decoction pieces of the four-part general rule of 2015 pharmacopoeia of the people's republic of China.
S103, measuring the volume of the fried cowherb seed decoction pieces, and reading volume data;
the method for measuring the volume of the cowherb seed stir-fried decoction pieces is various as long as the volume can be measured.
Preferably, the present invention provides an embodiment of measuring the volume, wherein the step of measuring the volume of the parched semen vaccariae decoction pieces comprises:
pouring the decoction pieces into a container with volume scale, compacting, spreading surface, and reading volume V of the decoction piecesaCompacting, spreading the surface, and reading volume V of decoction piecesbCalculating VaAnd VbThe average value of (A) is taken as the reading V of the volume of the decoction piecesab。
Preferably, the present invention provides another embodiment of the method for measuring volume, wherein the step of measuring volume of the parched semen vaccariae decoction pieces comprises:
tap readings are carried out by 1-3 persons to respectively obtain V1(Vab)、V2(Vab)、V3(Vab) Reading decoction pieces, and calculating V1、V2And V3The average was taken as the final volume reading of the tablets
Figure BDA0002357589990000071
The method for measuring the explosion rate of the cowherb seed fried decoction pieces by using the volume method is simple, quick and convenient, has accurate result, and can reduce the misjudgment caused by visual inspection of the explosion rate by naked eyes.
S104, establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation for calculation, and solving the explosion rate of the fried cowherb seeds decoction pieces.
According to the invention, the volume of the decoction pieces is used as a vertical coordinate (Y), the explosion rate is used as a horizontal coordinate (X), and linear relations between the explosion rate and the volume of the decoction pieces under different sampling amounts are respectively established to obtain corresponding linear regression equations. The linear regression equation comprises a unified regression equation as shown in equation I, which applies to all samples: the method also comprises a general regression equation shown in the formula II, wherein the general regression equation is suitable for optimizing the sampling quantity of 50-5000 g; the method also comprises a linear regression equation corresponding to the specific sampling amount, wherein the linear regression equation is suitable for the specific sampling amount of 50g, 100g, 200g, 500g, 1000g or 5000g, and the specific sampling amount is as follows:
the linear regression equation of the explosion ratio and the volume of the decoction pieces is shown as the formula I:
Y＝(0.0234n)X+1.2215n
wherein n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
Secondly, when the sampling amount of the fried cowherb seed decoction pieces is 50-5000 g, the linear regression equation of the popping rate and the decoction piece volume is shown as a formula II:
Figure BDA0002357589990000072
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75 g;
or
Figure BDA0002357589990000073
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure BDA0002357589990000074
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure BDA0002357589990000075
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure BDA0002357589990000081
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure BDA0002357589990000082
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
Thirdly, when the sampling amount of the fried cowherb seed decoction pieces is 50g, 100g, 200g, 500g, 1000g or 5000g, the linear regression equation of the popping rate and the decoction piece volume is as follows:
as shown in fig. 2, when the sampling amount is 50g, the linear regression equation is that Y is 1.1447X +63.902, and the correlation coefficient r is 0.9991;
as shown in fig. 3, when the sampling amount is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999;
as shown in fig. 4, when the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997;
as shown in fig. 5, when the sampling amount is 500g, the linear regression equation is that Y is 11.866X +595.23, and the correlation coefficient r is 0.9992;
as shown in fig. 6, when the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993;
as shown in fig. 7, when the sampling amount is 5000g, the linear regression equation is that Y is 117.02X +6088.6, and the correlation coefficient r is 0.9995;
wherein Y is the volume of the decoction pieces, and X is the bursting rate.
The sampling amount of the cowherb seed stir-fried decoction pieces is preferably 50-5000 g, the sampling amount in the range is convenient to operate, the explosion rate of the cowherb seed stir-fried decoction pieces is measured, and the measurement result is relatively accurate.
It should be noted that the correlation coefficient r reflects a statistical indicator of the closeness of the correlation between the variables. The linear correlation coefficients of the invention are all larger than 0.999, the correlation is good, and the invention accords with the pharmacopoeia standard.
When different amounts of the decoction pieces are taken, the volumes of the corresponding decoction pieces are measured and substituted into the unified regression equation, so that the explosion rate can be quickly obtained. The calculation method of the explosion ratio is various and specifically comprises the following steps:
firstly, when any value is measured by a sampling amount for frying the cowherb seed decoction pieces, the following linear regression equation of the explosion rate and the decoction piece volume can be substituted, and the equation is shown as a formula I:
Y＝(0.0234n)X+1.2215n
wherein, n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
The method is suitable for a wide range of occasions and any sampling amount, and the explosion rate of the fried cowherb seed decoction pieces can be quickly calculated by measuring the volume of the fried cowherb seed decoction pieces.
Secondly, when the sampling amount of the cowherb seed stir-fried decoction pieces is measured to obtain an optimal range value, the optimal range value is 50-5000 g, and the calculation method comprises the following steps: substituting different sampling quantities into different linear regression equations to obtain the explosion rate, which is concretely as follows:
when the sampling amount of the cowherb seed stir-fried decoction pieces is 50-5000 g, the linear regression equation of the popping rate and the decoction piece volume is shown as a formula II:
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75 g;
or
Figure BDA0002357589990000092
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure BDA0002357589990000093
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure BDA0002357589990000094
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure BDA0002357589990000095
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure BDA0002357589990000096
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
Thirdly, when the sampling amount of the cowherb seed decoction pieces is preferably determined to be a specific value, the specific value comprises 50g, 100g, 200g, 500g, 1000g and 5000g, the calculation method comprises the following steps: and substituting different sampling quantities into different linear regression equations to obtain the explosion rate.
When the sampling amount is 50g, the linear regression equation is that Y is 1.1447X +63.902, and the correlation coefficient r is 0.9991, wherein Y is the volume of the decoction pieces, and X is the bursting rate.
When the sampling amount is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999, wherein Y is the volume of the decoction pieces, and X is the bursting rate.
When the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997, wherein Y is the volume of the decoction pieces, and X is the popping rate.
When the sampling amount is 500g, the linear regression equation is 11.866X +595.23, and the correlation coefficient r is 0.9992, wherein Y is the volume of the decoction pieces, and X is the bursting rate.
When the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993, wherein Y is the volume of the decoction pieces, and X is the popping rate.
When the sampling amount is 5000g, the linear regression equation is 117.02X +6088.6, and the correlation coefficient r is 0.9995, wherein Y is the volume of the decoction pieces, and X is the popping rate.
The method for measuring the popcorn rate of the fried cowherb seed decoction pieces by using the volume method is simple, quick and convenient, has accurate results, can quickly and accurately judge the popcorn rate of the fried cowherb seed decoction pieces in the frying process, reduces misjudgment caused by visual inspection of the popcorn rate by naked eyes, meets the requirements of standard decoction pieces by adjusting the frying parameters in time, and improves the quality of the decoction pieces. Moreover, the invention reduces the manpower, material resources and time consumed by manual calculation and reduces the production cost by rapidly measuring the popping rate of the fried cowherb seed decoction pieces. In addition, the invention is beneficial to smooth production or rapid adjustment of the processing scheme by rapidly measuring the popping rate of the fried cowherb seed decoction pieces and rapidly feeding back results, optimizes the frying parameters in time, improves the popping rate and improves the production efficiency.
S105, setting or adjusting frying parameters according to the popping rate of the fried cowherb seed decoction pieces.
The stir-frying parameters mainly comprise stir-frying temperature and stir-frying time, but are not limited to the stir-frying temperature and the stir-frying time. The invention can rapidly and accurately measure the explosion rate of the cowherb seed decoction pieces fried in the frying process and timely adjust the frying parameters on site, thereby not only conforming to the current rapidly developed machine frying speed and the increasing medicine demand and continuously improving the production efficiency, but also optimizing the frying parameters in time, improving the explosion rate, processing qualified decoction pieces meeting the standard requirements and ensuring the quality of the decoction pieces. The method of setting and adjusting the stir-frying parameters may be performed with reference to the prior art.
Correspondingly, as shown in fig. 8, the invention also provides a method for measuring the popping rate of the cowherb seed stir-fried decoction pieces, which comprises the following steps:
s201, taking a preset amount of fried cowherb seed decoction pieces;
s202, measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data;
s203, establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation to calculate the explosion rate of the fried cowherb seeds, wherein the explosion rate is used for setting or adjusting frying parameters.
It should be noted that the technical details of step S201, step S102, step S202, step S103, and step S203 are the same as those of step S104, and are not described herein again.
The invention is further illustrated by the following specific examples
Examples 1 to 5 are the method for measuring the popping rate of the fried cowherb seed decoction pieces, comparative examples 1 to 5 are the method for estimating the popping rate by adopting an artificial visual inspection method in the prior art, comparative examples 6 to 10 are the method for measuring the popping rate by adopting an artificial selection calculation method in the prior art, and examples 6 to 10 are the production method of the fried cowherb seed decoction pieces.
Example 1:
a method for rapidly measuring the popping rate of a cowherb seed stir-fried decoction piece comprises the following steps:
a. parching the same batch of semen Vaccariae containing 1 piece of medicinal material, 50kg each;
b. sampling the fried cowherb seed decoction pieces in three parts, sampling each part one by one according to requirements, and randomly sampling 100g, 300g and 500g in multiple points to obtain three parts of decoction pieces of 100g, 300g and 500g for testing;
c. respectively and uniformly mixing the three decoction pieces, respectively pouring the mixture into a container marked with volume scales, compacting, trowelling the surface, reading the volume, compacting again, trowelling the surface, reading the volume again, and obtaining a volume average value;
d. substituting into a unified regression equation, respectively solving the explosion rate of the decoction pieces, and calculating the total time length.
Example 2:
a method for rapidly measuring the popping rate of a cowherb seed stir-fried decoction piece comprises the following steps:
a. parching the same batch of semen Vaccariae containing 2 medicinal materials, 50kg each;
b. sampling the stir-fried cowherb seed decoction pieces respectively in three parts, sampling one by one in each part according to requirements, and randomly sampling 100g, 300g and 500g in each part at multiple points to obtain three parts of decoction pieces of 200g, 600g and 1000g for testing;
c. respectively and uniformly mixing the three decoction pieces, respectively pouring the mixture into a container marked with volume scales, compacting, trowelling the surface, reading the volume, compacting again, trowelling the surface, reading the volume again, and obtaining a volume average value;
d. substituting into a unified regression equation, respectively solving the explosion rate of the decoction pieces, and calculating the total time length.
Example 3:
a method for rapidly measuring the popping rate of a cowherb seed stir-fried decoction piece comprises the following steps:
a. parching the same batch of semen Vaccariae containing 3 medicinal materials, 50kg each;
b. sampling the stir-fried cowherb seed decoction pieces respectively in three parts, sampling each part one by one according to requirements, and randomly sampling 100g, 300g and 500g each part at multiple points to obtain three parts of decoction pieces of 300g, 900g and 1500g for testing;
c. respectively and uniformly mixing the three decoction pieces, respectively pouring the mixture into a container marked with volume scales, compacting, trowelling the surface, reading the volume, compacting again, trowelling the surface, reading the volume again, and obtaining a volume average value;
d. substituting into a unified regression equation, respectively solving the explosion rate of the decoction pieces, and calculating the total time length.
Example 4:
a method for rapidly measuring the popping rate of a cowherb seed stir-fried decoction piece comprises the following steps:
a. parching the same batch of semen Vaccariae containing 4 pieces of medicinal materials, 50kg each;
b. sampling the stir-fried cowherb seed decoction pieces respectively in three parts, sampling each part one by one according to requirements, and randomly sampling 100g, 300g and 500g each part at multiple points to obtain three parts of decoction pieces of 400g, 1200g and 2000g for testing;
c. respectively and uniformly mixing the three decoction pieces, respectively pouring the mixture into a container marked with volume scales, compacting, trowelling the surface, reading the volume, compacting again, trowelling the surface, reading the volume again, and obtaining a volume average value;
d. substituting into a unified regression equation, respectively solving the explosion rate of the decoction pieces, and calculating the total time length.
Example 5:
a method for rapidly measuring the popping rate of a cowherb seed stir-fried decoction piece comprises the following steps:
a. parching the same batch of semen Vaccariae containing 5 pieces of medicinal materials, 50kg each;
b. sampling the stir-fried cowherb seed decoction pieces respectively in three parts, sampling one by one each part according to requirements, and randomly sampling 100g, 300g and 500g at multiple points to obtain 500g, 1500g and 2500g decoction pieces for testing;
c. respectively and uniformly mixing the three decoction pieces, respectively pouring the mixture into a container marked with volume scales, compacting, trowelling the surface, reading the volume, compacting again, trowelling the surface, reading the volume again, and obtaining a volume average value;
d. substituting into a unified regression equation, respectively solving the explosion rate of the decoction pieces, and calculating the total time length.
Comparative example 1: estimating the popping rate by adopting an artificial visual inspection method
The measured volume of the tablets of example 1 were poured into trays and the popping rate was visually estimated by three different persons and recorded.
Comparative example 2: estimating the popping rate by adopting an artificial visual inspection method
The measured volume of the tablets of example 2 were poured into trays and the popping rate was visually estimated by three different persons and recorded.
Comparative example 3: estimating the popping rate by adopting an artificial visual inspection method
The measured volume of the tablets of example 3 were each placed in a tray and the burst rate was visually estimated by three different persons and recorded.
Comparative example 4: estimating the popping rate by adopting an artificial visual inspection method
The measured volume of the tablets of example 4 were each placed in a tray and the burst rate was visually estimated by three different persons and recorded.
Comparative example 5: estimating the popping rate by adopting an artificial visual inspection method
The measured volume of the tablets of example 5 were each poured into a tray and the popping rate was visually estimated by three different persons and recorded.
Comparative example 6: determination of the percentage of popcorn Using a Manual selection calculation
The decoction pieces estimated by visual observation in the comparative example 1 are respectively selected manually, the separated popcorn decoction pieces and the jianzi decoction pieces are respectively weighed, the popcorn rate of the decoction pieces is calculated, and the total duration is calculated at the same time.
Comparative example 7: determination of the percentage of popcorn Using a Manual selection calculation
The decoction pieces estimated by visual observation in the comparative example 2 are respectively selected manually, the separated popcorn decoction pieces and the jianzi decoction pieces are respectively weighed, the popcorn rate of the decoction pieces is calculated, and the total time duration is calculated at the same time.
Comparative example 8: determination of the percentage of popcorn Using a Manual selection calculation
And (3) respectively manually selecting the decoction pieces estimated by visual observation in the comparative example 3, respectively weighing the separated popcorn decoction pieces and the jianzi decoction pieces, calculating the popcorn rate of the decoction pieces, and simultaneously calculating the total time.
Comparative example 9: determination of the percentage of popcorn Using a Manual selection calculation
The decoction pieces estimated by visual observation in the comparative example 4 are respectively selected manually, the separated popcorn decoction pieces and the jianzi decoction pieces are respectively weighed, the popcorn rate of the decoction pieces is calculated, and the total duration is calculated at the same time.
Comparative example 10: determination of the percentage of popcorn Using a Manual selection calculation
The decoction pieces estimated by visual observation in the comparative example 5 are respectively selected manually, the separated popcorn decoction pieces and the jianzi decoction pieces are respectively weighed, the popcorn rate of the decoction pieces is calculated, and the total time duration is calculated at the same time.
The measured data of the examples and the comparative examples are counted and compared, and the results are shown in tables 1-3:
TABLE 1 volume method for fast determination of popping rate of fried cowherb seed decoction pieces
Figure BDA0002357589990000141
TABLE 2 comparative example results of determination of puffing rate of semen Vaccariae preparata decoction pieces by eye measurement method
Figure BDA0002357589990000142
TABLE 3 comparison example results of determination of explosion ratio of parched semen Vaccariae decoction pieces by manual selection calculation method
Figure BDA0002357589990000143
Figure BDA0002357589990000151
As can be seen from the results of the examples 1 to 5 and the comparative examples 6 to 10, the method for rapidly determining the popcorn rate of the fried cowherb seed decoction pieces by using the volume method has the advantages that compared with the traditional manual selection calculation method, the measured values of the popcorn rate of the fried cowherb seed decoction pieces in the same batch are basically consistent, the result accuracy is high, the repeatability is good, the error is small, and the method is really feasible.
Meanwhile, the volume method is short in use time, the explosion rate result can be basically obtained within 10min, the manual selection calculation method consumes longer time along with the increase of the sampling amount, when the production batch is large, the large amount of decoction pieces needs to be taken, the time needs to be consumed for several days, even if multiple persons are used for simultaneously selecting, the time and the labor are consumed for manual selection, and the method for rapidly determining the explosion rate of the decoction pieces of cowherb seeds by adopting the volume method is accurate, simple, rapid and convenient, not only can the production efficiency be remarkably improved, but also the labor cost can be reduced, the accuracy is the same as that of the traditional manual selection calculation method, and the efficiency and the cost are remarkably superior to that of the traditional manual selection calculation method.
The results of examples 1 to 5 and comparative examples 1 to 5 show that the determination result of the volume method for rapidly determining the popping rate of the cowherb seed-fried decoction pieces is basically consistent with the actual popping rate, while the determination result of the visual method is obviously higher than the actual popping rate, because the seeds are heavier and the volume of the cowherb seed-fried decoction pieces is smaller, the seeds are mainly distributed on the lower layer after sampling, the seeds are mainly distributed on the upper layer after sampling, and the seeds are larger in volume and slightly soaked in water, so that the popping decoction pieces with more surfaces are only observed in the visual observation, and the misjudgment of the higher popping rate is caused.
Therefore, the accuracy of the method for rapidly measuring the explosion rate of the fried cowherb seed decoction pieces by adopting the volume method is obviously higher than that of a visual method, the error of visual measurement results can be reduced in the actual production process, the explosion rate is improved by adjusting the frying parameters in time, and the product quality is improved.
Example 6:
a production method of a fried cowherb seed decoction piece comprises the following steps:
(1) stir-frying the cowherb seed according to the embodiment 1, and measuring the popping rate of the stir-fried cowherb seed decoction pieces;
(2) according to the popping rate of the cowherb seed stir-fried decoction pieces prepared in the embodiment 1, setting or adjusting stir-frying parameters, and stir-frying cowherb seeds of the same batch, wherein the cowherb seeds comprise 5-99 medicinal materials, and each medicinal material comprises 50 kg;
(3) sampling the fried cowherb seed decoction pieces, randomly sampling 5 pieces of the decoction pieces according to requirements, and randomly sampling 500g of the decoction pieces at multiple points to obtain 2500g of the decoction pieces;
(4) the sampled decoction pieces are uniformly mixed, and the explosion rate is determined by adopting a rapid determination method.
Example 7:
a production method of a fried cowherb seed decoction piece comprises the following steps:
(1) stir-frying the cowherb seeds according to the embodiment 2, and measuring the popping rate of the stir-fried cowherb seed decoction pieces;
(2) according to the popping rate of the cowherb seed stir-fried decoction pieces prepared in the embodiment 2, setting or adjusting stir-frying parameters, and stir-frying cowherb seeds of the same batch, wherein the cowherb seeds comprise 5-99 medicinal materials, and each medicinal material comprises 50 kg;
(3) sampling the fried cowherb seed decoction pieces, randomly sampling 5 pieces of the decoction pieces according to requirements, and randomly sampling 500g of the decoction pieces at multiple points to obtain 2500g of the decoction pieces;
(4) the sampled decoction pieces are uniformly mixed, and the explosion rate is determined by adopting a rapid determination method.
Example 8:
a production method of a fried cowherb seed decoction piece comprises the following steps:
(1) stir-frying the cowherb seed according to the embodiment 3, and measuring the popping rate of the stir-fried cowherb seed decoction pieces;
(2) according to the popping rate of the cowherb seed stir-fried decoction pieces prepared in the embodiment 3, setting or adjusting stir-frying parameters, and stir-frying the cowherb seeds of the same batch, wherein the cowherb seeds comprise 5-99 medicinal materials, and each medicinal material comprises 50 kg;
(3) sampling the fried cowherb seed decoction pieces, randomly sampling 5 pieces of the decoction pieces according to requirements, and randomly sampling 500g of the decoction pieces at multiple points to obtain 2500g of the decoction pieces;
(4) the sampled decoction pieces are uniformly mixed, and the explosion rate is determined by adopting a rapid determination method.
Example 9:
a production method of a fried cowherb seed decoction piece comprises the following steps:
(1) stir-frying the cowherb seed according to the embodiment 4, and measuring the popping rate of the stir-fried cowherb seed decoction pieces;
(2) according to the popping rate of the cowherb seed stir-fried decoction pieces prepared in the embodiment 4, setting or adjusting stir-frying parameters, and stir-frying cowherb seeds of the same batch, wherein the cowherb seeds comprise 5-99 medicinal materials, and each medicinal material comprises 50 kg;
(3) sampling the fried cowherb seed decoction pieces, randomly sampling 5 pieces of the decoction pieces according to requirements, and randomly sampling 500g of the decoction pieces at multiple points to obtain 2500g of the decoction pieces;
(4) the sampled decoction pieces are uniformly mixed, and the explosion rate is determined by adopting a rapid determination method.
Example 10:
a production method of a fried cowherb seed decoction piece comprises the following steps:
(1) stir-frying the cowherb seeds according to the embodiment 5, and measuring the popping rate of the stir-fried cowherb seed decoction pieces;
(2) setting or adjusting frying parameters according to the popping rate of the cowherb seed frying decoction pieces prepared in the embodiment 5, and frying cowherb seeds of the same batch, wherein the cowherb seeds comprise 5-99 medicinal materials, and each medicinal material is 50 kg;
(3) sampling the fried cowherb seed decoction pieces, randomly sampling 5 pieces of the decoction pieces according to requirements, and randomly sampling 500g of the decoction pieces at multiple points to obtain 2500g of the decoction pieces;
(4) the sampled decoction pieces are uniformly mixed, and the explosion rate is determined by adopting a rapid determination method.
TABLE 4 volume method for fast determination of popping rate of fried cowherb seed decoction pieces
Examples Sample volume/g Va/ml Vb/ml Mean value/ml Percentage of popping/%
6 2500.89 8348 8325 8337 90
7 2501.35 8120 8103 8112 86
8 2501.66 7973 7940 7957 84
9 2501.21 8053 8035 8044 85
10 2500.69 8206 8197 8202 88
From the results of the examples 6 to 10, the volume method is adopted to rapidly measure the explosion rate of the fried cowherb seed decoction pieces, the fried results are fed back in time, the frying parameters can be rapidly adjusted, the qualified decoction pieces meeting the standard requirements are fried, the final explosion rate of each batch of fried decoction pieces reaches more than 80 percent, and the requirements of frying until most of exploded white flowers are fried in 2015 edition of Chinese pharmacopoeia are met.
The method for rapidly measuring the explosion rate of the fried cowherb seed decoction pieces by adopting the volume method not only can be used for timely measuring and feeding back the explosion rate in the trial-frying stage, timely adjusting and optimizing field frying parameters and processing qualified decoction pieces meeting the standard requirements, but also can be used for timely monitoring the explosion rate in the whole frying process and ensuring the quality of the decoction pieces.
While the foregoing is directed to the preferred embodiment of the present invention, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention.

Claims (12)

1. A production method of a cowherb seed stir-fried decoction piece is characterized by comprising the following steps:
(1) pre-frying or frying the cowherb seeds to obtain fried cowherb seed decoction pieces;
(2) taking a preset amount of fried cowherb seed decoction pieces;
(3) measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data;
(4) establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation for calculation, and solving the explosion rate of the fried cowherb seeds decoction pieces;
(5) and setting or adjusting frying parameters according to the popping rate of the fried cowherb seed decoction pieces.
2. The method for producing the parched semen vaccariae decoction piece as claimed in claim 1, wherein the sampling amount of the parched semen vaccariae decoction piece is 50-5000 g.
3. The method for producing the parched semen vaccariae decoction pieces as claimed in claim 1 or 2, wherein the linear regression equation of the explosion ratio and the decoction piece volume is shown as formula i:
Y＝(0.0234n)X+1.2215n
wherein n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
4. The method for producing the parched semen vaccariae decoction pieces as claimed in claim 2, wherein the step (4) of substituting the volume data into the linear regression equation comprises:
and substituting different sampling quantities into different linear regression equations to obtain the explosion rate.
5. The method of claim 4, wherein when the sampling amount is 50g, the linear regression equation is 1.1447X +63.902, and the correlation coefficient r is 0.9991;
when the sampling quantity is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999;
when the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997;
when the sampling amount is 500g, the linear regression equation is that Y is 11.866X +595.23, and the correlation coefficient r is 0.9992;
when the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993;
when the sampling amount is 5000g, the linear regression equation is that Y is 117.02X +6088.6, and the correlation coefficient r is 0.9995;
wherein Y is the volume of the decoction pieces, and X is the bursting rate.
6. The method for producing the parched semen vaccariae decoction piece according to claim 4, wherein when the sampling amount of the parched semen vaccariae decoction piece is 50-5000 g, the linear regression equation of the explosion ratio and the decoction piece volume is shown as formula II:
Figure FDA0002357589980000022
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75g；
Or
Figure FDA0002357589980000023
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure FDA0002357589980000024
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure FDA0002357589980000025
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure FDA0002357589980000026
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure FDA0002357589980000027
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
7. The method for producing the parched semen vaccariae decoction piece according to claim 1, wherein in the step (3), the step of measuring the volume of the parched semen vaccariae decoction piece comprises:
pouring the decoction pieces into a container with volume scale, compacting, spreading surface, and reading volume V of the decoction piecesaCompacting, spreading the surface, and reading volume V of decoction piecesbCalculating VaAnd VbThe average value of (A) is taken as the reading V of the volume of the decoction piecesab。
8. The method for producing the parched semen vaccariae decoction piece according to claim 1, wherein in the step (3), the step of measuring the volume of the parched semen vaccariae decoction piece comprises:
tap readings are carried out by 1-3 persons to respectively obtain V1(Vab)、V2(Vab)、V3(Vab) Reading decoction pieces, and calculating V1、V2And V3The average was taken as the final volume reading of the tablets
Figure FDA0002357589980000021
9. A method for measuring the popping rate of a fried cowherb seed decoction piece is characterized by comprising the following steps:
(1) taking a preset amount of fried cowherb seed decoction pieces;
(2) measuring the volume of the cowherb seed stir-fried decoction pieces, and reading volume data;
(3) and establishing a linear regression equation of the explosion rate of the fried cowherb seeds and the volume of the decoction pieces, substituting the volume data into the linear regression equation to calculate the explosion rate of the fried cowherb seeds, wherein the explosion rate is used for setting or adjusting the frying parameters.
10. The method for determining the popcorn rate of the parched cowherb seed decoction pieces as claimed in claim 9, wherein the linear regression equation of the popcorn rate and the decoction piece volume is shown as formula i:
Y＝(0.0234n)X+1.2215n
wherein n is the sampling amount, Y is the volume of the decoction pieces, and X is the bursting rate.
11. The method of claim 9, wherein when the sampling amount is 50g, the linear regression equation is 1.1447X +63.902, and the correlation coefficient r is 0.9991;
when the sampling quantity is 100g, the linear regression equation is that Y is 2.3477X +122.16, and the correlation coefficient r is 0.9999;
when the sampling amount is 200g, the linear regression equation is that Y is 4.7362X +241.87, and the correlation coefficient r is 0.9997;
when the sampling amount is 500g, the linear regression equation is that Y is 11.866X +595.23, and the correlation coefficient r is 0.9992;
when the sampling amount is 1000g, the linear regression equation is that Y is 23.476X +1211.9, and the correlation coefficient r is 0.9993;
when the sampling amount is 5000g, the linear regression equation is that Y is 117.02X +6088.6, and the correlation coefficient r is 0.9995;
wherein Y is the volume of the decoction pieces, and X is the bursting rate.
12. The method for determining the popcorn rate of the fried cowherb seed decoction pieces as claimed in claim 9, wherein the sampling amount of the fried cowherb seed decoction pieces is 50-5000 g, and the linear regression equation of the popcorn rate and the decoction piece volume is shown as formula II:
Figure FDA0002357589980000031
wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is less than 75 g;
or
Figure FDA0002357589980000032
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 75g and less than 150 g;
or
Figure FDA0002357589980000041
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 150g and less than 350 g;
or
Figure FDA0002357589980000042
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 350g and less than 750 g;
or
Figure FDA0002357589980000043
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is more than or equal to 750g and less than 3000 g;
or
Figure FDA0002357589980000044
Wherein Y is the volume of the decoction pieces, X is the bursting rate, n is the sampling amount, and n is not less than 3000 g.
CN202010012304.5A 2020-01-07 2020-01-07 Production method of fried cowherb seed decoction pieces and determination method of explosion rate of fried cowherb seed decoction pieces Pending CN111067925A (en)

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Citations (1)

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Publication number Priority date Publication date Assignee Title
CN108030799A (en) * 2018-02-11 2018-05-15 宁夏明德中药饮片有限公司 A kind of Semen Vaccariae (parched) medicine materical crude slice and its concocting method

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Publication number Priority date Publication date Assignee Title
CN108030799A (en) * 2018-02-11 2018-05-15 宁夏明德中药饮片有限公司 A kind of Semen Vaccariae (parched) medicine materical crude slice and its concocting method

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Application publication date: 20200428