CN111058141A - TDP fiber cloth and preparation method thereof - Google Patents

TDP fiber cloth and preparation method thereof Download PDF

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Publication number
CN111058141A
CN111058141A CN201911399948.8A CN201911399948A CN111058141A CN 111058141 A CN111058141 A CN 111058141A CN 201911399948 A CN201911399948 A CN 201911399948A CN 111058141 A CN111058141 A CN 111058141A
Authority
CN
China
Prior art keywords
tdp
fiber
cloth
fiber cloth
preparing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911399948.8A
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Chinese (zh)
Inventor
聂长安
袁先洪
向小阳
陈伯龙
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Chongqing Silicate Research Institute
Original Assignee
Chongqing Silicate Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chongqing Silicate Research Institute filed Critical Chongqing Silicate Research Institute
Priority to CN201911399948.8A priority Critical patent/CN111058141A/en
Publication of CN111058141A publication Critical patent/CN111058141A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
    • D03D15/242—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads inorganic, e.g. basalt
    • D03D15/267—Glass
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D9/00—Open-work fabrics
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2101/00—Inorganic fibres
    • D10B2101/02—Inorganic fibres based on oxides or oxide ceramics, e.g. silicates
    • D10B2101/06—Glass
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2509/00—Medical; Hygiene

Abstract

The invention relates to the technical field of TDP preparation, and particularly discloses TDP fiber cloth and a preparation method thereof, wherein the TDP fiber cloth is formed by spinning TDP fiber monofilaments, the diameter of each TDP fiber monofilament is 6-20 microns, and the TDP fiber cloth is prepared by the processes of TDP batching, melting, wire drawing, filament drawing, softening, filament feeding, wire clamping and winding, wire winding, weaving and treating compound removing. Adopt the TDP fibre cloth of this patent preparation to compare with TDP element board, TDP fibre cloth is unanimous basically with TDP element board's relative radiation energy spectrum curve, the treatment of TDP fibre cloth product has been guaranteed, TDP fibre cloth's thickness is little simultaneously, not only weight obtains very big reduction, TDP fibre cloth has better deformability simultaneously, can prepare "physiotherapy area", "wearing formula or wearing formula's TDP", be used for products such as articulated "physiotherapy subsides", potential market is big, can reach more consumer groups.

Description

TDP fiber cloth and preparation method thereof
Technical Field
The invention relates to the technical field of TDP preparation, in particular to TDP fiber cloth and a preparation method thereof.
Background
The invention of specific electromagnetic spectrum therapeutic apparatus (TDP for short) for more than 30 years is widely accepted at home and abroad based on the unique curative effect of non-drug therapy, and is already used as a conventional medical apparatus and is equipped for various medical units at home and known as a "magic lamp". In recent decades, along with the rapid development of domestic economy, the improvement of the living standard of material culture, the increasing attention of people on the development of health, medical treatment and other civilians, the pace of the TDP with broad-spectrum treatment and health care effects entering families is increasing, and the development of TDP products more suitable for families and personal consumption is a great inevitable way for the development of the TDP industry.
The existing TDP products are mainly divided into two types: (1) traditional high temperature TDP therapy devices; (2) low temperature type TDP physiotherapy subsides. Among them, the "low-temperature type TDP physiotherapy patch" is a new product developed in recent years, and is more and more accepted by the market due to its advantages of low price, instant use, convenient use, no influence on daily activities of patients, and the like, and is a main direction for upgrading and updating TDP products.
The core components of the two types of TDP products are TDP element plates, and the TDP element plates are prepared by adopting an enamel technology: spraying the prepared TDP biological enamel glaze on an iron plate substrate and firing to obtain the TDP biological enamel glaze. When the component is used for a 'TDP physical therapy patch', the main defects are as follows: the texture is hard, the weight is heavy, the comfort is not enough, the close-fitting treatment of all parts (particularly joints) of a human body is difficult to meet, the application range of the product is seriously restricted, and the development of series products (particularly products with larger models) is also restricted.
Disclosure of Invention
The invention provides TDP fiber cloth and a preparation method thereof, which aim to solve the core technical problem that the existing TDP product cannot be completely flexible and are convenient for further development of a TDP apparatus for close-fitting treatment.
In order to achieve the purpose, the technical scheme of the invention is as follows:
a TDP fiber cloth and a preparation method thereof are formed by spinning TDP fiber monofilaments, wherein the diameter of each TDP fiber monofilament is 6-20 microns.
The technical principle and the effect of the technical scheme are as follows:
the TDP element plate prepared by the technology is heavy in weight and free of flexibility, and cannot meet close-fitting treatment of various parts (particularly joints) of a human body when being made into a TDP instrument for close-fitting treatment.
And TDP fibre cloth is compared with TDP element board, under the same temperature effect, TDP fibre cloth is unanimous basically with TDP element board's relative radiation energy spectrum curve, the treatment effect of TDP fibre cloth product has been guaranteed, TDP fibre cloth's thickness is little simultaneously, not only weight obtains very big reduction, TDP fibre cloth has better deformability simultaneously, can tailor the concatenation wantonly, accommodation is wide, can prepare products such as "physiotherapy area", "wearing formula or wearing formula's TDP", be used for articulated "physiotherapy subsides", potential market is big, can benefit to more consumer groups.
Furthermore, the TDP fiber cloth can emit electromagnetic waves of 5-22 mu m under heating.
Has the advantages that: the TDP fiber cloth emits electromagnetic waves of 5-22 mu m under heating, and the electromagnetic waves are equivalent to the TDP element plate at the same temperature, so that the physical therapy effect is ensured.
According to another technical scheme, the preparation method of the TDP fiber cloth comprises the following steps of TDP batching, melting, wire drawing, softening, wire feeding, wire clamping and winding, wire winding, weaving and treating size removing.
Has the advantages that: the preparation method is similar to the common preparation method of the glass fiber cloth, the process is mature, and the mass production of the TDP fiber cloth can be ensured, so that the preparation method is rapidly popularized in the market.
Further, raw materials in the TDP ingredient are cleaned and prepared into powder.
Has the advantages that: the raw material is washed to reduce impurities contained in the prepared fiber cloth.
Further, the TDP raw material comprises 11.0-15.0 wt% of SiO2、21.0～24.0wt％B2O3、2.0～8.0wt％MoO3、30.0～36.0wt％MgO216.0 to 22.0 wt% of BaO and 6.0 to 12.0 wt% of ZnO.
Has the advantages that: the TDP for physical therapy can be obtained under the components and the content.
Further, the TDP raw material also comprises 0-4.0 wt% of SnO2。
Has the advantages that: SnO2The addition of (2) can improve the surface gloss of the TDP fiber monofilament.
Further, the melting temperature is 1250-1280 ℃.
Has the advantages that: the melting temperature in the mature glass fiber cloth preparation process is usually 1300-1600 ℃, the formula of the raw materials in the application belongs to the formula of special glass, and the raw materials contain various compounds, so that the melting temperature is reduced compared with that of common glass.
Further, the surface treatment is carried out on the TDP fiber monofilament formed by wire drawing, and the method specifically comprises the following steps: coating a layer of impregnating compound on the surface of the TDP fiber monofilament, and then drying.
Has the advantages that: the TDP fiber monofilament is subjected to surface treatment to increase active groups on the surface of the TDP fiber monofilament and improve the weaving performance of the TDP fiber monofilament.
Further, the impregnating compound comprises a silane coupling agent, epoxy resin, polyvinyl alcohol glue resin and water.
Has the advantages that: the epoxy resin has the function of film formation, and the polyvinyl alcohol glue resin has the adhesive property, so that the weaving performance of the TDP fiber monofilaments is improved.
Further, the prepared TDP fiber cloth is fiber gridding cloth, fiber checkered cloth, fiber plain cloth or fiber electronic cloth.
Has the advantages that: the prepared fiber cloth with different grains can meet different use requirements.
Detailed Description
The following is further detailed by way of specific embodiments:
the parameters of the TDP fiber cloth in the embodiments 1-4 are shown in the following table 1:
table 1 shows the parameters of the TDP fiber cloth preparation method
Example 1 Example 2 Example 3 Example 4
Melting temperature (. degree.C.) 1250 1260 1270 1280
TDP fiber monofilament (mum) 6 10 15 20
The preparation method of a TDP fiber cloth is described in detail by taking example 1 as an example.
A preparation method of TDP fiber cloth comprises the following steps:
step 1: TDP compounding, cleaning the material to obtain powder, wherein the TDP material has the main components and content shown in Table 2, SnO2Is added to improve the surface gloss of the TDP fiber filaments.
Table 2 shows the composition and content of TDP raw material
Composition of SiO2 B2O3 MoO3 MgO2 BaO ZnO SnO2
Content (wt%) 11.0～15.0 21.0～24.0 2.0～8.0 30.0～36.0 16.0～22.0 6.0～12.0 0～4.0
Step 2: and (3) melting, namely adding the powder in the step (1) into a crucible, and melting the powder completely at 1250 ℃.
And step 3: drawing, namely drawing the molten raw material in the step 2 into a TDP fiber monofilament with the diameter of 6 microns, coating a layer of impregnating compound on the TDP fiber monofilament in the drawing process, and then drying, wherein the impregnating compound comprises silane coupling agent, epoxy resin, polyvinyl alcohol glue resin and water.
And 4, step 4: and (3) performing drawing, softening, reeling, clamping, winding and weaving on the fiber monofilaments subjected to the surface treatment in the step (3) according to the prior art to obtain the TDP fiber cloth, wherein the thickness of the TDP fiber cloth is 0.2-0.5 mm.
The TDP fiber cloth can be spun into fiber gridding cloth, fiber plain cloth or fiber electronic cloth according to actual requirements.
And 5: in order to ensure the strength of the TDP fiber cloth, the impregnating compound is removed by a chemical method: according to the composition of the impregnating compound, alkali liquor, soap, organic solvent and the like can be adopted, and ultrasonic vibration is matched to remove the impregnating compound.
Examples 2 to 4 are the same as the production method of example 1 except that the parameters in table 1 are different, and example 5 is the same as the production method of example 1 except that the melting in step 2 is performed in a tank furnace, so that example 5 is more suitable for mass production.
Compared with the TDP element plate prepared by the existing enamel technology, the TDP fiber cloth prepared in the embodiments 1 to 5 has the advantages that under the same temperature, the relative radiation energy spectrum curves of the TDP fiber cloth and the TDP element plate are basically consistent, 5-22 mu m electromagnetic waves can be emitted, the treatment effect of the TDP fiber cloth product is guaranteed, the thickness of the prepared TDP fiber cloth is 0.2-0.5 mm and is far smaller than the thickness of the TDP element plate, the weight is greatly reduced, meanwhile, the TDP fiber cloth has good deformation capacity, can be cut and spliced at will, and is wide in application range, products such as a physiotherapy belt, a wearable or wearable TDP, a physiotherapy patch for joints and the like can be prepared, the potential market is large, and more consumer groups can be benefited.
The foregoing is merely an example of the present invention and common general knowledge of known specific methods and features of the schemes is not described herein. It should be noted that, for those skilled in the art, without departing from the method of the present invention, several variations and modifications can be made, which should also be regarded as the scope of protection of the present invention, and these will not affect the effect of the implementation of the present invention and the applicability of the patent. The scope of the claims of the present application shall be determined by the contents of the claims, and the description of the embodiments and the like in the specification shall be used to explain the contents of the claims.

Claims (10)

1. A TDP fiber cloth is characterized in that: the single fiber is formed by spinning TDP fiber single fibers, and the diameter of each TDP fiber single fiber is 6-20 mu m.
2. A TDP fiber cloth according to claim 1, wherein: the TDP fiber cloth can emit electromagnetic waves of 5-22 mu m under heating.
3. A method for preparing the TDP fiber cloth of claim 2, wherein: the method comprises the following steps of TDP batching, melting, wire drawing, softening, wire feeding, wire clamping and winding, wire winding, weaving and treating size removing.
4. The method for preparing TDP fiber cloth according to claim 3, wherein the TDP fiber cloth comprises the following steps: the TDP ingredient is prepared by cleaning raw materials and preparing the raw materials into powder.
5. The method for preparing TDP fiber cloth according to claim 4, wherein: the TDP raw material comprises 11.0-15.0 wt% of SiO2、21.0～24.0wt％B2O3、2.0～8.0wt％MoO3、30.0～36.0wt％MgO216.0 to 22.0 wt% of BaO and 6.0 to 12.0 wt% of ZnO.
6. The method for preparing TDP fiber cloth according to claim 5, wherein: the TDP raw material also comprises 0-4.0 wt% of SnO2。
7. The method for preparing TDP fiber cloth according to claim 6, wherein: the melting temperature is 1250-1280 ℃.
8. The method for preparing TDP fiber cloth according to claim 7, wherein: the surface treatment is carried out on the TDP fiber monofilament formed by wire drawing, and the method specifically comprises the following steps: coating a layer of impregnating compound on the surface of the TDP fiber monofilament, and then drying.
9. The method for preparing TDP fiber cloth according to claim 8, wherein: the impregnating compound comprises a silane coupling agent, epoxy resin, polyvinyl alcohol glue resin and water.
10. The method for preparing TDP fiber cloth according to claim 9, wherein: the prepared TDP fiber cloth is fiber gridding cloth, fiber checkered cloth, fiber plain cloth or fiber electronic cloth.
CN201911399948.8A 2019-12-30 2019-12-30 TDP fiber cloth and preparation method thereof Pending CN111058141A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911399948.8A CN111058141A (en) 2019-12-30 2019-12-30 TDP fiber cloth and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911399948.8A CN111058141A (en) 2019-12-30 2019-12-30 TDP fiber cloth and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111058141A true CN111058141A (en) 2020-04-24

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911399948.8A Pending CN111058141A (en) 2019-12-30 2019-12-30 TDP fiber cloth and preparation method thereof

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Country Link
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Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04243932A (en) * 1991-01-29 1992-09-01 Nitto Boseki Co Ltd Inorganic fiber for shielding from electromagnetic wave
CN1085588A (en) * 1992-10-10 1994-04-20 朱瓒 Far-infrared radiation material and compound method thereof
EP1283287A2 (en) * 2001-08-03 2003-02-12 Hitachi Chemical Company, Ltd. Hollow carbon fiber and production method
CN101914821A (en) * 2010-05-14 2010-12-15 江苏大学 Ni-Zn ferrite/SiO2 composite nano-fiber and preparation method thereof
CN102154732A (en) * 2011-03-28 2011-08-17 际华三五零六纺织服装有限公司 Electromagnetic wave shielding fibre for garments
CN104562261A (en) * 2015-02-03 2015-04-29 湖州新创丝织品有限公司 Novel far infrared fiber spinning solution and preparation method thereof
KR20170089138A (en) * 2016-01-26 2017-08-03 (주) 국일신소재연구소 Method of preparing of functional fiber containing mixed mineral powder
CN108409151A (en) * 2018-06-01 2018-08-17 魏浩峰 A kind of no boron high-performance glass fiber and preparation method thereof
CN110157152A (en) * 2018-02-11 2019-08-23 青岛澜盟实业有限公司 A kind of carbon/glass dimension composite material vehicle cover preparation method

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04243932A (en) * 1991-01-29 1992-09-01 Nitto Boseki Co Ltd Inorganic fiber for shielding from electromagnetic wave
CN1085588A (en) * 1992-10-10 1994-04-20 朱瓒 Far-infrared radiation material and compound method thereof
EP1283287A2 (en) * 2001-08-03 2003-02-12 Hitachi Chemical Company, Ltd. Hollow carbon fiber and production method
CN101914821A (en) * 2010-05-14 2010-12-15 江苏大学 Ni-Zn ferrite/SiO2 composite nano-fiber and preparation method thereof
CN102154732A (en) * 2011-03-28 2011-08-17 际华三五零六纺织服装有限公司 Electromagnetic wave shielding fibre for garments
CN104562261A (en) * 2015-02-03 2015-04-29 湖州新创丝织品有限公司 Novel far infrared fiber spinning solution and preparation method thereof
KR20170089138A (en) * 2016-01-26 2017-08-03 (주) 국일신소재연구소 Method of preparing of functional fiber containing mixed mineral powder
CN110157152A (en) * 2018-02-11 2019-08-23 青岛澜盟实业有限公司 A kind of carbon/glass dimension composite material vehicle cover preparation method
CN108409151A (en) * 2018-06-01 2018-08-17 魏浩峰 A kind of no boron high-performance glass fiber and preparation method thereof

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Application publication date: 20200424