CN110916185A - Natural compound antioxidant composition, application and preparation method - Google Patents
Natural compound antioxidant composition, application and preparation method Download PDFInfo
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- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 47
- 239000000203 mixture Substances 0.000 title claims abstract description 46
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 41
- 229930014626 natural product Natural products 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 239000000843 powder Substances 0.000 claims description 20
- 239000000284 extract Substances 0.000 claims description 19
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 claims description 11
- 235000011430 Malus pumila Nutrition 0.000 claims description 9
- 235000015103 Malus silvestris Nutrition 0.000 claims description 9
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 9
- 235000013824 polyphenols Nutrition 0.000 claims description 9
- 239000000654 additive Substances 0.000 claims description 8
- 230000000996 additive effect Effects 0.000 claims description 8
- 235000013361 beverage Nutrition 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- JEVVKJMRZMXFBT-XWDZUXABSA-N Lycophyll Natural products OC/C(=C/CC/C(=C\C=C\C(=C/C=C/C(=C\C=C\C=C(/C=C/C=C(\C=C\C=C(/CC/C=C(/CO)\C)\C)/C)\C)/C)\C)/C)/C JEVVKJMRZMXFBT-XWDZUXABSA-N 0.000 claims description 6
- 235000012661 lycopene Nutrition 0.000 claims description 6
- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 claims description 6
- 239000001751 lycopene Substances 0.000 claims description 6
- 229960004999 lycopene Drugs 0.000 claims description 6
- ZCIHMQAPACOQHT-ZGMPDRQDSA-N trans-isorenieratene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/c1c(C)ccc(C)c1C)C=CC=C(/C)C=Cc2c(C)ccc(C)c2C ZCIHMQAPACOQHT-ZGMPDRQDSA-N 0.000 claims description 6
- 150000001746 carotenes Chemical class 0.000 claims description 5
- 235000005473 carotenes Nutrition 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 claims description 5
- 235000013305 food Nutrition 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 244000144725 Amygdalus communis Species 0.000 claims description 3
- 235000011437 Amygdalus communis Nutrition 0.000 claims description 3
- 241000167854 Bourreria succulenta Species 0.000 claims description 3
- 235000004415 Burchellia bubalina Nutrition 0.000 claims description 3
- 240000008537 Burchellia bubalina Species 0.000 claims description 3
- 241001264174 Cordyceps militaris Species 0.000 claims description 3
- 244000000626 Daucus carota Species 0.000 claims description 3
- 235000002767 Daucus carota Nutrition 0.000 claims description 3
- 241000222336 Ganoderma Species 0.000 claims description 3
- 239000009429 Ginkgo biloba extract Substances 0.000 claims description 3
- 241000168517 Haematococcus lacustris Species 0.000 claims description 3
- 240000000950 Hippophae rhamnoides Species 0.000 claims description 3
- 235000003145 Hippophae rhamnoides Nutrition 0.000 claims description 3
- 241000209140 Triticum Species 0.000 claims description 3
- 235000021307 Triticum Nutrition 0.000 claims description 3
- 235000020224 almond Nutrition 0.000 claims description 3
- 235000019693 cherries Nutrition 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 229940087603 grape seed extract Drugs 0.000 claims description 3
- 235000002532 grape seed extract Nutrition 0.000 claims description 3
- 235000020717 hawthorn extract Nutrition 0.000 claims description 3
- 229940106587 pine bark extract Drugs 0.000 claims description 3
- 235000020741 pine bark extract Nutrition 0.000 claims description 3
- 229940109529 pomegranate extract Drugs 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 239000001717 vitis vinifera seed extract Substances 0.000 claims description 3
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- 235000007425 Aronia melanocarpa Nutrition 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000008176 lyophilized powder Substances 0.000 claims description 2
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- 239000003973 paint Substances 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 238000001291 vacuum drying Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 abstract description 7
- 238000002474 experimental method Methods 0.000 abstract description 5
- 230000000052 comparative effect Effects 0.000 abstract description 4
- 235000013376 functional food Nutrition 0.000 abstract description 4
- 239000002778 food additive Substances 0.000 abstract description 3
- 235000006708 antioxidants Nutrition 0.000 description 29
- 241000220225 Malus Species 0.000 description 10
- 239000004615 ingredient Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 3
- 235000012055 fruits and vegetables Nutrition 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 235000021452 apple slice Nutrition 0.000 description 2
- 235000021016 apples Nutrition 0.000 description 2
- OENHQHLEOONYIE-UKMVMLAPSA-N beta-Carotene Chemical compound CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241001092391 Sorbus Species 0.000 description 1
- 235000014459 Sorbus Nutrition 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 235000013734 beta-carotene Nutrition 0.000 description 1
- 239000011648 beta-carotene Substances 0.000 description 1
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 description 1
- 229960002747 betacarotene Drugs 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000020510 functional beverage Nutrition 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/135—Bacteria or derivatives thereof, e.g. probiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
A natural compound antioxidant composition, an application and a preparation method belong to the field of functional food additives, and the composition mainly comprises the following components in percentage by weight:
Description
Technical Field
The invention relates to a functional food additive, in particular to a natural compound antioxidant composition, belonging to the field of functional food additives.
Background
In the field of functional food and beverage manufacture, it is often desirable to use antioxidant ingredients. Common antioxidant ingredients are various naturally occurring vitamins or other synthetic chemicals.
The antioxidant ingredients are often added separately, and other substances are added for matching in order to achieve the effects of economy, formula stability and compatibility, and the result is that large-space ingredients and a large stack of chemical substance names appear in ingredients of the product.
At present, the situation can affect the sale of products when people adopt the natural green life concept: some consumers dislike these complex chemical names. For this reason, it is necessary to develop natural green antioxidant compositions.
Disclosure of Invention
Experiments prove that the composition meets the requirements and is composed of natural fruit and vegetable components.
Therefore, the invention provides the following technical scheme:
scheme one
The invention provides a natural compound antioxidant composition which is characterized by mainly comprising the following components in percentage by weight:
wherein, the variation range of the content of more than or equal to 10 percent by weight is +/-2 percent, the variation range of the content of more than or equal to 5 percent by weight is +/-1 percent, and the variation range of the content of more than or equal to 5 percent by weight is +/-0.3 percent.
Further, the natural compound antioxidant composition is characterized in that:
the paint mainly comprises the following components in percentage by weight:
further, the natural compound antioxidant composition is characterized in that:
the composition is in the form of powder particles, and the particle size is 500 mesh.
Scheme two
The natural compound antioxidant composition is used as an additive for preparing beverages, and the using amount of the natural compound antioxidant composition is 0.5-6% of the total mass.
The natural compound antioxidant composition is used as an additive for preparing solid beverage powder, and the using amount of the natural compound antioxidant composition is 2-10% of the total mass.
Use of a naturally formulated antioxidant composition as an additive for the preparation of cold-worked solid or semi-solid food in an amount of 0.5-6% of the total mass.
Scheme three
The preparation method of the natural compound antioxidant composition is characterized by comprising the following steps:
adding 5-10% of ethanol in the total mass of the formula raw materials into cherry extract, almond extract, grape seed extract embedded powder, pine bark extract embedded powder, haematococcus pluvialis, cordyceps militaris extract, aronia melanocarpa powder, wild sea buckthorn extract, wild pomegranate extract, wild hawthorn extract, wild ganoderma extract and ginkgo leaf extract in the formula amount, wetting, heating to 45-60 ℃, and mixing and stirring under the conditions of heat preservation and sealing;
cooling, adding wheat germ powder and carrot lyophilized powder according to the formula ratio, and stirring for moistening;
extruding the mixture into sheets by using a screw extruder, extruding for many times, and respectively adding β ethanol solutions of carotene, lycopene and apple polyphenol into the sheets in a spraying mode for many times when the ethanol content is reduced to be within 3 mass percent;
pulverizing the wetted sheet materials, mixing, vacuum drying at 35-40 deg.C, and sieving with 500 mesh sieve.
Action and Effect of the invention
The natural compound antioxidant composition is mainly composed of natural fruit and vegetable extracts, the components are green and natural, and the antioxidant effect of the natural compound antioxidant composition is equivalent to that of a synthetic chemical antioxidant proved by a comparative experiment. Because the natural green food does not contain a synthetic antioxidant and is obtained by compounding a plurality of natural ingredients, the natural green formula is more easily accepted by most consumers at the moment of advocating the natural green life concept, and the applicable population of the product is wider.
Detailed Description
In order to make the technical means, creation characteristics, achievement purposes and effects of the invention easy to understand, the following examples specifically describe the natural compound antioxidant composition, the solid beverage mixture, the beverage and the preparation method of the invention.
The preparation method of the natural compound antioxidant composition is characterized by comprising the following steps:
step one, cherry extract, almond extract, grape seed extract embedded powder, pine bark extract embedded powder, haematococcus pluvialis, cordyceps militaris extract, sorbus nigra powder, wild sea buckthorn extract, wild pomegranate extract, wild hawthorn extract, wild ganoderma extract and ginkgo leaf extract in a formula amount are wetted by ethanol which accounts for 5-10% of the total mass of the formula raw materials, heated to 45-60 ℃, and mixed and stirred under the conditions of heat preservation and sealing.
The components by weight percentage are as follows:
wherein, the variation range of the content of more than or equal to 10 percent by weight is +/-2 percent, the variation range of the content of more than or equal to 5 percent by weight is +/-1 percent, and the variation range of the content of more than or equal to 5 percent by weight is +/-0.3 percent.
This example requires 88g of the composition to be formulated as follows:
and step two, naturally cooling, adding the wheat germ powder and the carrot freeze-dried powder according to the formula amount, and stirring and wetting.
And step three, extruding the mixture into a sheet shape by using a screw extruder, extruding for multiple times, and respectively adding β ethanol solutions of carotene, lycopene and apple polyphenol into the sheet shape in a spraying mode for multiple times when the ethanol content is reduced to be within 3 mass percent.
The operation of multiple extrusion is that after each extrusion, the ethanol content in the extruded matter is tested, and the extrusion is stopped when the ethanol content is reduced to be within 3 percent by mass.
β the mass of ethanol in the ethanol solution of carotene, lycopene and apple polyphenol is 5-10 times of the total mass of β of carotene, lycopene and apple polyphenol.
And step four, crushing and mixing the wetted flaky powder, drying in vacuum at 35-40 ℃, and sieving by a 500-mesh sieve to obtain the powder.
And (4) testing the in vitro antioxidant activity.
The browning and discoloration test of apple slices was used to test the ratio of antioxidant activity of the compositions of the present invention to β carotene, lycopene, and apple polyphenol solutions at different concentrations.
Preparing three groups of concentrated solutions of 1.1%, 0.6% and 2.2% of apple polyphenol respectively, and storing at low temperature and under nitrogen.
The prepared composition is dissolved by using 1 time, 2 times, 5 times, 10 times and 20 times of distilled water, then the clear solution is obtained by filtration, and the clear solution is rapidly stored at low temperature in nitrogen.
Red crisp apples (Shaanxi red Fuji apples, produced in 9 months of Shaanxi) having a fruit diameter of about 8cm were selected, cut into thin pieces of about 2mm in thickness, and placed on white tiles, respectively.
The above composition extract and apple polyphenol solution with different concentrations were dipped in cotton cloth with a length and width of 2cm, and then rubbed on the appropriate position of the apple slices.
And (5) standing and observing.
The results are shown in the following table.
Comparative experiments prove that the antioxidant effect of 100 times of the water extract (1.0% concentration) of the composition is equivalent to the effect of apple polyphenol with 2.2% concentration.
Use of
The natural compound antioxidant composition is used as an additive for preparing beverages, and the using amount of the natural compound antioxidant composition is 0.5-6% of the total mass.
The natural compound antioxidant composition is used as an additive for preparing solid beverage powder, and the using amount of the natural compound antioxidant composition is 2-10% of the total mass.
Effects and effects of the embodiments
The natural compound antioxidant composition provided by the embodiment mainly comprises natural fruit and vegetable extracts, the components are green and natural, and the antioxidant effect of the natural compound antioxidant composition is equivalent to that of a synthetic chemical antioxidant proved by a comparative experiment. Because the natural green food does not contain a synthetic antioxidant and is obtained by compounding a plurality of natural ingredients, the natural green formula is more easily accepted by most consumers at the moment of advocating the natural green life concept, and the applicable population of the product is wider.
The above embodiments are preferred examples of the present invention, and are not intended to limit the scope of the present invention.
Claims (7)
1. A natural compound antioxidant composition is characterized by mainly comprising the following components in percentage by weight:
wherein, the variation range of the content of more than or equal to 10 percent by weight is +/-2 percent, the variation range of the content of more than or equal to 5 percent by weight is +/-1 percent, and the variation range of the content of more than or equal to 5 percent by weight is +/-0.3 percent.
3. the naturally compounded antioxidant composition of claim 1 or 2, characterized in that:
the composition is in the form of powder particles, and the particle size is 500 mesh.
4. The natural compound antioxidant composition is used as an additive for preparing beverages, and the using amount of the natural compound antioxidant composition is 0.5-6% of the total mass.
5. The natural compound antioxidant composition is used as an additive for preparing solid beverage powder, and the using amount of the natural compound antioxidant composition is 2-10% of the total mass.
6. Use of a naturally formulated antioxidant composition as an additive for the preparation of cold-worked solid or semi-solid food in an amount of 0.5-6% of the total mass.
7. The preparation method of the natural compound antioxidant composition is characterized by comprising the following steps:
adding 5-10% of ethanol in the total mass of the formula raw materials into cherry extract, almond extract, grape seed extract embedded powder, pine bark extract embedded powder, haematococcus pluvialis, cordyceps militaris extract, aronia melanocarpa powder, wild sea buckthorn extract, wild pomegranate extract, wild hawthorn extract, wild ganoderma extract and ginkgo leaf extract in the formula amount, wetting, heating to 45-60 ℃, and mixing and stirring under the conditions of heat preservation and sealing;
cooling, adding wheat germ powder and carrot lyophilized powder according to the formula ratio, and stirring for moistening;
extruding the mixture into sheets by using a screw extruder, extruding for many times, and respectively adding β ethanol solutions of carotene, lycopene and apple polyphenol into the sheets in a spraying mode for many times when the ethanol content is reduced to be within 3 mass percent;
pulverizing the wetted sheet materials, mixing, vacuum drying at 35-40 deg.C, and sieving with 500 mesh sieve.
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2019
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