CN110840495A - Blood-staining-preventing self-cleaning surgical instrument and preparation method thereof - Google Patents

Blood-staining-preventing self-cleaning surgical instrument and preparation method thereof Download PDF

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Publication number
CN110840495A
CN110840495A CN201910981914.3A CN201910981914A CN110840495A CN 110840495 A CN110840495 A CN 110840495A CN 201910981914 A CN201910981914 A CN 201910981914A CN 110840495 A CN110840495 A CN 110840495A
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China
Prior art keywords
surgical instrument
coating
blood
cleaning
staining
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CN201910981914.3A
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Chinese (zh)
Inventor
刘新
王德伦
秦文跃
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DALIAN SHUNDA MINIMALLY INVASIVE SCIENCE & TECHNOLOGY Co Ltd
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DALIAN SHUNDA MINIMALLY INVASIVE SCIENCE & TECHNOLOGY Co Ltd
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Priority to CN201910981914.3A priority Critical patent/CN110840495A/en
Publication of CN110840495A publication Critical patent/CN110840495A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B2017/00526Methods of manufacturing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B2017/00831Material properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B2017/00831Material properties
    • A61B2017/0096Material properties self cleaning, e.g. having lotus effect

Abstract

The invention relates to the technical field of medical instruments, and particularly discloses a blood-sticking-preventing self-cleaning surgical instrument and a preparation method thereof. The invention has self-cleaning and anti-sticking properties to human blood and tissue fluid, can repel blood stain, dust and other foreign matters, can effectively reduce the disinfection and cleaning time in the operation process, thereby shortening the operation time, relieving the pain of patients, avoiding surgical instruments from indirectly infecting other parts of the body due to the adhesion of the blood and the tissue of the patients in the operation, and reducing the possibility of complications of the patients.

Description

Blood-staining-preventing self-cleaning surgical instrument and preparation method thereof
Technical Field
The invention relates to the technical field of medical instruments, in particular to a blood-staining-resistant self-cleaning surgical instrument and a preparation method thereof.
Background
With the continuous development of science and technology and the improvement of living standard of people, the requirements of the public on medical treatment are gradually improved, the requirements on treatment quality and life quality are obviously improved, the treatment result is concerned, and the cleanness, damage degree, safety, comfort and minimal invasion in the treatment process are more concerned. In the medical field, surgery is a main treatment method of surgery, and a scalpel is a medical instrument commonly used in surgery and used for cutting an affected part of a patient during a surgery to maintain the health of the patient.
The phenomenon that blood and tissue fluid are stained with the scalpel often occurs in the operation process, the scalpel can be polluted, the scalpel is very easy to adhere to the hands of a doctor to cause the situations of sliding of a scalpel handle and the like, and then the doctor or the patient is accidentally injured, and even other surgical instruments or other parts of the patient can be stained with the scalpel, so that postoperative infection or cross propagation of infectious diseases of the doctor and the patient can be caused. Meanwhile, too long cleaning and disinfecting time for the scalpel in the operation process can increase operation risk and is not beneficial to postoperative recovery of a patient.
Patent publication No. CN107736920A proposes a surgical instrument, wherein a plurality of arc-shaped blocks are arranged on the main body of the surgical instrument in the circumferential direction, so that the friction between the main body and the hand of the surgical instrument can be effectively increased through the arc-shaped blocks, and the probability of slipping is reduced, but human tissues and blood can still adhere to the surgical instrument, so that various risks caused by slipping of the surgical instrument inevitably exist.
The patent with publication number CN203263575U provides a splash-proof scalpel, a splash-proof cover which is concave spherical and has the diameter and the length about 1/2-2/3 of the scalpel handle is arranged between the scalpel handle and the scalpel blade, the top surface of the sphere faces the scalpel handle, the splash-proof scalpel has certain splash-proof performance, but the view of a doctor is easily shielded in the operation process, the time consumed by cleaning and disinfecting the scalpel is prolonged to a certain extent, and the splash-proof scalpel cannot be widely applied to the actual operation environment.
The patent with publication number CN108836438A provides a minimally invasive scalpel for general surgery, the inside of the scalpel blade is provided with an empty groove, the middle part of the inner cavity of a handle is provided with a connecting groove which is communicated with the empty groove, the left end of the handle is provided with a micropump, the inlet end of the micropump is communicated with the connecting groove, and the outlet end of the micropump is connected with a liquid discharge pipe.
In conclusion, the above methods cannot fundamentally solve the problem that the surgical instrument indirectly infects other parts of the body due to the super-hydrophilicity of the surgical instrument to blood and tissue fluid, and meanwhile, the hidden trouble that the knife slides off from the hand due to the blood staining of the surgical instrument still exists for doctors.
Disclosure of Invention
The invention aims to provide a blood-staining-preventing self-cleaning surgical instrument and a preparation method thereof, so as to solve the problems that the surgical instrument in the prior art is easy to stain blood and human tissue fluid.
In order to solve the technical problem, the invention provides a preparation method of a blood-staining-resistant self-cleaning surgical instrument, which comprises the following steps:
s1, performing oil removal, polishing and cleaning treatment on a to-be-treated part of a surgical instrument;
s2, filtering the coating containing the nano ceramic particles by using a filter screen, and then uniformly mixing the coating with a lubricant;
s3, coating the mixed coating on the part to be treated of the surgical instrument;
and S4, taking out the surgical instrument from the mixed coating, and ceramizing the coating of the to-be-treated part of the surgical instrument.
Preferably, in step S1, the metal substrate of the to-be-treated portion of the surgical instrument is made of one of stainless steel, titanium alloy, ceramic, polymer material and plastic, the to-be-treated portion of the surgical instrument is first cleaned and degreased with absolute ethanol, and then is mechanically polished to remove an oxide layer after being dried, and then is cleaned with deionized water and ultrasonic waves, and is dried again.
Preferably, the mechanical polishing is performed by using an abrasive material or sand paper with the size of more than 800#, and the ultrasonic cleaning time is 4-6 min.
Preferably, in step S2, the diameter of the nano ceramic particles is 10 to 100nm, the nano ceramic is one or a mixture of several of alumina ceramic, silicon nitride ceramic and silicon carbide ceramic, the specification of the filter screen is greater than or equal to 400 meshes, the lubricant is one or a mixture of several of perfluoropolyether oil, dupont krytox, perfluorotripentylamine and silicone oil, and the mass ratio of the coating containing the nano ceramic particles to the lubricant is greater than or equal to 1: 1.
Preferably, in the step S3, the coating mode is one of spraying, brushing, rolling and dipping, and the coating is coated once.
Preferably, in step S3, the part to be treated of the surgical instrument is soaked in the mixed paint and coated, and then the mixture is sufficiently soaked and then placed obliquely, so that a uniform coating layer is formed on the surface of the part to be treated of the surgical instrument.
Preferably, the inclination angle is 15-50 degrees, and the inclination standing time is 20-40 min.
Preferably, in step S4, the surgical instrument is taken out of the mixed paint, and then naturally dried or quickly surface-dried, and then left at room temperature to ceramize the coating of the portion to be treated of the surgical instrument.
Preferably, the standing time at normal temperature is 1-2 h.
The invention also provides a blood-staining-preventing self-cleaning surgical instrument which is prepared by the preparation method of the blood-staining-preventing self-cleaning surgical instrument.
The blood-staining-preventing self-cleaning surgical instrument has self-cleaning property and anti-staining property on human blood and tissue fluid, can repel foreign matters such as blood stains, dust and the like, can effectively reduce the disinfection and cleaning time in the surgical process, thereby shortening the surgical time, relieving the pain of patients, avoiding the surgical instrument from indirectly infecting other parts of the body due to the adhesion of the blood and the tissue of the surgical patients, and reducing the possibility of complications of the patients. The process is simple and convenient, the anti-blood-staining self-cleaning surgical instrument can be prepared in a short time, the cost is low, the self-cleaning surface is formed after the hydrophobic self-cleaning ceramic coating and the lubricant are wetted, the rolling angle is small, foreign matters such as human blood, tissue fluid, air dust and the like can be repelled, the original structure of the surgical instrument is not changed, the use is convenient, the applicability is good, the anti-blood-staining self-cleaning surgical instrument can be widely applied to surgery, is nontoxic and harmless to the human body, does not change the sharpness performance of the surgical instrument, does not influence the service performance of the surgical instrument, can reduce the probability of slipping the surgical instrument from the hand in the surgery process of a patient, reduces the occurrence of accidental situations, reduces the work difficulty of.
Detailed Description
The following examples further describe embodiments of the present invention in detail. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
The preparation method of the blood-staining-preventing self-cleaning surgical instrument comprises the following steps of:
s1, performing oil removal, polishing and cleaning treatment on a to-be-treated part of a surgical instrument;
the metal substrate material of the part to be treated of the surgical instrument is one of stainless steel, titanium alloy, ceramic, high molecular material and plastics, the surface of the part to be treated of the surgical instrument is cleaned by absolute ethyl alcohol to remove oil, an oxide layer is removed by mechanical polishing after blow-drying, then the part is cleaned by deionized water and ultrasonic waves and blow-dried again, the mechanical polishing is carried out by grinding materials or abrasive paper more than 800#, and the ultrasonic cleaning time is 4-6 min.
S2, filtering the coating containing the nano ceramic particles by using a filter screen, and then uniformly mixing the coating with a lubricant;
the diameter of the nano ceramic particles is 10-100 nm, the nano ceramic is one or a mixture of more of alumina ceramic, silicon nitride ceramic and silicon carbide ceramic, the specification of the filter screen is greater than or equal to 400 meshes, the lubricant is one or a mixture of more of perfluoropolyether oil, Dupont krytox, perfluoro tripentylamine and silicone oil, and the mass ratio of the coating containing the nano ceramic particles to the lubricant is greater than or equal to 1: 1.
S3, coating the mixed coating on the part to be treated of the surgical instrument;
the coating mode is one of spraying, brushing, roller coating and dip coating, the coating can be coated once, otherwise, the coating of the subsequent coating is not adhered to the first time or has poor adhesive force, and the coating modes are as follows: spraying, namely spraying by a common spray gun, wherein the spraying can be carried out once; brushing, namely uniformly coating a brush with medium hardness, wherein the brush can be brushed once; roller coating is performed, wherein uniform roller coating is performed, and the roller coating can be performed once; dip-coating, namely dip-coating once;
soaking the part to be treated of the surgical instrument in the mixed coating for coating, fully soaking, and then obliquely standing to form a uniform coating on the surface of the part to be treated of the surgical instrument, wherein the inclination angle is 15-50 degrees, and the oblique standing time is 20-40 min;
the environment is kept clean in the coating construction process, so that dust or impurities are prevented from reducing the hydrophobic self-cleaning property of the coating; the coating tool needs to be clean and dry and not be stained with water or other substances, and the coating tool is cleaned: and after the cleaning by absolute ethyl alcohol, cleaning by clear water, drying by compressed air and storing.
S4, taking out the surgical instrument from the mixed coating to ceramic the coating of the to-be-treated part of the surgical instrument;
and taking the surgical instrument out of the mixed coating, and naturally drying or quickly drying the surgical instrument, wherein the naturally drying refers to keeping the coating at 25 ℃ for 12-24 hours, the quickly drying refers to drying the coating at 100 ℃ for 30-50 minutes, and then placing at normal temperature to ceramic the coating of the part to be processed of the surgical instrument, and the time of placing at normal temperature is 1-2 hours.
Example 1
S1, cleaning and degreasing a metal stainless steel plate to-be-treated part of a surgical instrument with the size of 20mm multiplied by 2mm by absolute ethyl alcohol, polishing the metal stainless steel plate to remove a surface oxide layer by using 800# abrasive paper and 1500# abrasive paper after blow-drying, cleaning the polished stainless steel plate by using a large amount of deionized water, cleaning for 5min by using ultrasonic waves, and blow-drying by using a blower.
S2, filtering the silicon carbide ceramic coating liquid with the diameter of 100nm by using a 400-mesh filter screen, mixing the silicon carbide ceramic coating liquid with dimethyl silicon oil with the kinematic viscosity of 10cs according to the mass ratio of 1:1, and uniformly stirring.
S3, immersing the to-be-treated part of the pretreated surgical instrument into the coating, fully soaking, then obliquely standing to form a layer of uniform coating on the surface, standing to 30min at an inclination angle of 20 degrees, and inclining at 20 degrees to enable the redundant coating to flow out of the surface to obtain a stable coating.
And S4, taking out the part to be treated of the surgical instrument after the pre-soaking treatment, drying for 40min at 100 ℃, standing for 1 hour at normal temperature after the coating is dried and cooled, and completing ceramic coating, thus obtaining the self-cleaning blood-staining-resistant surgical instrument.
Example 2
S1, cleaning and deoiling a metal titanium alloy plate at a to-be-treated part of a surgical instrument with the size of 20mm multiplied by 10mm multiplied by 2mm by absolute ethyl alcohol, polishing the metal titanium alloy plate by using 800# abrasive paper and 1500# abrasive paper respectively after blow-drying to remove a surface oxide layer, cleaning the polished titanium alloy plate by using a large amount of deionized water, cleaning for 5min by using ultrasonic waves, and blow-drying by using a blower.
S2, filtering the alumina ceramic coating liquid with the diameter of 50nm by using a 400-mesh filter screen, mixing the alumina ceramic coating liquid with the perfluoropolyether oil according to the mass ratio of 1:1, and uniformly stirring.
S3, immersing the to-be-treated part of the pretreated surgical instrument into the coating, fully soaking, then obliquely standing to form a layer of uniform coating on the surface, standing to 30min at an inclination angle of 20 degrees, and inclining at 20 degrees to enable the redundant coating to flow out of the surface to obtain a stable coating.
And S4, taking out the part to be treated of the surgical instrument after the pre-soaking treatment, drying for 40min at 100 ℃, standing for 1 hour at normal temperature after the coating is dried and cooled, and completing ceramic coating, thus obtaining the self-cleaning blood-staining-resistant surgical instrument.
Example 3
S1, cleaning and deoiling a metal aluminum alloy plate at a to-be-treated part of a surgical instrument with the size of 20mm multiplied by 2mm by absolute ethyl alcohol, polishing the metal aluminum alloy plate by using 800# abrasive paper and 1500# abrasive paper respectively after drying, removing a surface oxide layer, cleaning the polished aluminum alloy plate by using a large amount of deionized water, cleaning for 5min by using ultrasonic waves, and drying by using a blower.
S2, filtering the alumina ceramic coating liquid with the diameter of 50nm by using a 400-mesh filter screen, mixing the alumina ceramic coating liquid with perfluorotripentylamine according to the mass ratio of 1:1, and uniformly stirring.
S3, immersing the to-be-treated part of the pretreated surgical instrument into the coating, fully soaking, then obliquely standing to form a layer of uniform coating on the surface, standing to 30min at an inclination angle of 20 degrees, and inclining at 20 degrees to enable the redundant coating to flow out of the surface to obtain a stable coating.
And S4, taking out the substrate of the part to be treated of the surgical instrument after the pre-soaking treatment, drying for 40min at the temperature of 100 ℃, standing for 1 hour at normal temperature after the coating is dried and cooled, and completing ceramic coating, thus obtaining the self-cleaning blood-staining-resistant surgical instrument.
The invention also provides a blood-staining-preventing self-cleaning surgical instrument which is prepared by the preparation method of the blood-staining-preventing self-cleaning surgical instrument.
The surgical instrument may be: medical scalpels, curved vessel forceps, straight vessel forceps, right-angle forceps, tissue scissors, thread scissors, surgical forceps, needle holders, suture needles, tissue forceps, cocklebur forceps, tissue forceps, appendix forceps and the like.
The blood-staining-preventing self-cleaning surgical instrument has self-cleaning property and anti-staining property on human blood and tissue fluid, can repel foreign matters such as blood stains, dust and the like, can effectively reduce the disinfection and cleaning time in the surgical process, thereby shortening the surgical time, relieving the pain of patients, avoiding the surgical instrument from indirectly infecting other parts of the body due to the adhesion of the blood and the tissue of the surgical patients, and reducing the possibility of complications of the patients. The process is simple and convenient, the anti-blood-staining self-cleaning surgical instrument can be prepared in a short time, the cost is low, the self-cleaning surface is formed after the hydrophobic self-cleaning ceramic coating and the lubricant are wetted, the rolling angle is small, foreign matters such as human blood, tissue fluid, air dust and the like can be repelled, the original structure of the surgical instrument is not changed, the use is convenient, the applicability is good, the anti-blood-staining self-cleaning surgical instrument can be widely applied to surgery, is nontoxic and harmless to the human body, does not change the sharpness performance of the surgical instrument, does not influence the service performance of the surgical instrument, can reduce the probability of slipping the surgical instrument from the hand in the surgery process of a patient, reduces the occurrence of accidental situations, reduces the work difficulty of.
The embodiments of the present invention have been presented for purposes of illustration and description, and are not intended to be exhaustive or limited to the invention in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiment was chosen and described in order to best explain the principles of the invention and the practical application, and to enable others of ordinary skill in the art to understand the invention for various embodiments with various modifications as are suited to the particular use contemplated.

Claims (10)

1. A preparation method of a blood-staining-preventing self-cleaning surgical instrument is characterized by comprising the following steps:
s1, performing oil removal, polishing and cleaning treatment on a to-be-treated part of a surgical instrument;
s2, filtering the coating containing the nano ceramic particles by using a filter screen, and then uniformly mixing the coating with a lubricant;
s3, coating the mixed coating on the part to be treated of the surgical instrument;
and S4, taking out the surgical instrument from the mixed coating, and ceramizing the coating of the to-be-treated part of the surgical instrument.
2. The method for preparing a blood-staining prevention self-cleaning surgical instrument as claimed in claim 1, wherein in the step S1, the metal substrate of the portion to be treated of the surgical instrument is made of one of stainless steel, titanium alloy, ceramic, polymer material and plastic, the surface of the portion to be treated of the surgical instrument is first cleaned and degreased with absolute ethanol, and then dried, mechanically polished to remove an oxide layer, and then cleaned with deionized water and ultrasonic waves, and dried again.
3. The method for preparing a blood-staining-resistant self-cleaning surgical instrument as claimed in claim 2, wherein the mechanical polishing is performed by polishing with an abrasive material or sand paper of 800# or more, and the ultrasonic cleaning time is 4-6 min.
4. The method for preparing the blood-staining-resistant self-cleaning surgical instrument as claimed in claim 1, wherein in step S2, the diameter of the nano ceramic particles is 10-100 nm, the nano ceramic is one or more of alumina ceramic, silicon nitride ceramic and silicon carbide ceramic, the filter screen is 400 meshes or larger, the lubricant is one or more of perfluoropolyether oil, dupont krytox, perfluorotripentylamine and silicone oil, and the mass ratio of the coating containing the nano ceramic particles to the lubricant is 1:1 or larger.
5. The method of claim 1, wherein in step S3, the coating is performed by one of spraying, brushing, rolling and dipping, and the coating is applied once.
6. The method of claim 1, wherein in step S3, the portion of the surgical instrument to be treated is dipped in the mixed coating and then coated, and the mixture is dipped sufficiently and then allowed to stand at an angle to form a uniform coating on the surface of the portion of the surgical instrument to be treated.
7. The method for preparing a blood-staining-preventing self-cleaning surgical instrument as claimed in claim 6, wherein the inclination angle is 15-50 °, and the inclined standing time is 20-40 min.
8. The method of claim 1, wherein in step S4, the surgical instrument is taken out of the mixed paint, and then naturally dried or quickly surface-dried, and then placed at room temperature to ceramize the paint on the portion of the surgical instrument to be treated.
9. The method for preparing a blood-staining-preventing self-cleaning surgical instrument as claimed in claim 8, wherein the time for standing at room temperature is 1-2 hours.
10. A blood-staining-preventing self-cleaning surgical instrument, which is prepared by the preparation method of the blood-staining-preventing self-cleaning surgical instrument as claimed in any one of claims 1 to 9.
CN201910981914.3A 2019-10-16 2019-10-16 Blood-staining-preventing self-cleaning surgical instrument and preparation method thereof Pending CN110840495A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115721785A (en) * 2021-08-30 2023-03-03 大连理工大学 Preparation method of medical anti-adhesion conductive coating

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CN106581783A (en) * 2016-12-30 2017-04-26 马爱进 Ceramic coating scalpel
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CN108836438A (en) * 2018-07-20 2018-11-20 丛硕 A kind of general surgery's minimally-invasive scalpel
CN208926521U (en) * 2018-05-02 2019-06-04 比尔安达(上海)润滑材料有限公司 The medical operation of coating lubricant coating is cut
CN109881192A (en) * 2019-01-25 2019-06-14 华南理工大学 A kind of bionical adherent surfaces and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030109865A1 (en) * 2001-12-12 2003-06-12 Megadyne Medical Products, Inc. Utilization of a multi-character material in a surface coating of an electrosurgical instrument
US20050055021A1 (en) * 2003-09-08 2005-03-10 Clement Thomas P. Method and material for coating electro-cautery probes and lubricating surgical instruments
CN203263575U (en) * 2013-05-08 2013-11-06 余华 Splash-proof scalpel for veterinarians
CN204072309U (en) * 2014-06-06 2015-01-07 江苏凝克医疗器械科技有限公司 A kind of surgical instrument
CN106581783A (en) * 2016-12-30 2017-04-26 马爱进 Ceramic coating scalpel
CN107736920A (en) * 2017-09-13 2018-02-27 常州优复瑞医疗器械有限公司 A kind of scalpel
CN208926521U (en) * 2018-05-02 2019-06-04 比尔安达(上海)润滑材料有限公司 The medical operation of coating lubricant coating is cut
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CN109881192A (en) * 2019-01-25 2019-06-14 华南理工大学 A kind of bionical adherent surfaces and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115721785A (en) * 2021-08-30 2023-03-03 大连理工大学 Preparation method of medical anti-adhesion conductive coating

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Application publication date: 20200228