CN110833806A - But circulative cooling formula reation kettle - Google Patents

But circulative cooling formula reation kettle Download PDF

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Publication number
CN110833806A
CN110833806A CN201810933613.9A CN201810933613A CN110833806A CN 110833806 A CN110833806 A CN 110833806A CN 201810933613 A CN201810933613 A CN 201810933613A CN 110833806 A CN110833806 A CN 110833806A
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China
Prior art keywords
kettle body
reaction kettle
cooling
stirring
liquid supply
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Pending
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CN201810933613.9A
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Chinese (zh)
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王宜宝
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Individual
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Priority to CN201810933613.9A priority Critical patent/CN110833806A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • B01J2219/00063Temperature measurement of the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a circulative cooling type reaction kettle, which comprises a reaction kettle body, a stirring unit, a temperature measuring unit, a pressure measuring unit, a cooling circulation device and heating equipment, wherein the bottom end of a stirring shaft is fixedly sleeved with a stirring paddle, the bending angle of a blade of the stirring paddle is 110 plus materials, 125 degrees, the rotating coverage surface of the blade of the stirring paddle can be increased, the stirring uniformity is increased, and the stirring effect is excellent; the cooling liquid flows into the liquid supply box through the liquid supply equipment, the needle valve can effectively control the cooling liquid entering the cooling cavity groove at the inner edge of the reaction kettle body through the conveying pipeline, the cooling liquid can effectively cool materials, the suction pump can suck the cooling liquid in the cooling cavity groove at the inner edge of the reaction kettle body into the conveying pipeline with acceleration, the warmed cooling liquid flows into the cooler through the output pipeline with acceleration through the liquid suction pump and is cooled, the cooling liquid flows into the liquid supply box again after being cooled to form a circulation, the use amount of the cooling liquid can be greatly reduced, the cost is greatly saved, and the cyclic continuous utilization of resources is realized.

Description

But circulative cooling formula reation kettle
Technical Field
The invention relates to the technical field of experimental equipment, in particular to a circulative cooling type reaction kettle device.
Background
The broad understanding of the reaction vessel is that there is a physical or chemical reaction vessel, through the structural design and parameter configuration of the vessel, the heating, evaporation, cooling and low-speed mixing functions of the process requirements are realized, the reaction vessel is widely applied to petroleum, chemical engineering, rubber, pesticides, dyes, medicines, foods, and pressure vessels for completing the processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation, etc., such as reactors, reaction pots, decomposing pots, polymerization vessels, etc.; the material is generally carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy, Monel, Inconel) alloy and other composite materials. The existing reaction kettle is unreasonable in structural design, the rotating coverage of the stirring paddle blades is not wide enough in the stirring process of stirring equipment, so that materials are easily stirred unevenly, and the stirring effect is not good; and after the heating furnace is cooled by using the cooling liquid, the discharged liquid can not be reused, the cooling liquid needs to be continuously provided by the liquid supply equipment for cooling, the usage amount of the cooling liquid is extremely large, the cost is extremely high, and the development view of the cyclic continuous utilization of real resources is seriously not met.
Disclosure of Invention
The invention aims to solve the problem of providing a stirring shaft with a stirring paddle fixed at the bottom end, wherein the bending angle of a blade of the stirring paddle is 110-125 degrees, the rotating coverage of the blade of the stirring paddle can be increased, the stirring uniformity is increased, and the stirring effect is excellent; the cooling liquid flows into the liquid supply box through the liquid supply equipment, the needle valve can effectively control the cooling liquid entering the cooling cavity groove at the inner edge of the reaction kettle body through the conveying pipeline, the cooling liquid can effectively cool materials, the suction pump can suck the cooling liquid in the cooling cavity groove at the inner edge of the reaction kettle body into the conveying pipeline with acceleration, the warmed cooling liquid flows into the cooler through the output pipeline with acceleration through the liquid suction pump to be cooled, the cooling liquid flows into the liquid supply box again to form a circulation, the use amount of the cooling liquid can be greatly reduced, the cost is greatly saved, and the circulating cooling type reaction kettle device capable of continuously utilizing the resources in a circulating mode is realized.
In order to solve the problems, the invention provides a circulative cooling type reaction kettle, which comprises a reaction kettle body, a stirring unit, a temperature measuring unit, a pressure measuring unit, a cooling circulating device and heating equipment, wherein the stirring unit is arranged at the upper end of the reaction kettle body and extends downwards to the inner end of the reaction kettle body, the temperature measuring unit is arranged at the side end of the reaction kettle body and extends to the inner end of the reaction kettle body, the pressure measuring unit is arranged at the top end of the reaction kettle body and extends downwards to the inner end of the reaction kettle body, the cooling circulating device is communicated with a cavity groove at the inner end of the reaction kettle body, the reaction kettle body is sleeved in the heating equipment, the stirring unit comprises a driving motor, a magnetic driving system, a stirring shaft and a stirring paddle, the lower end of the driving motor is provided with the magnetic driving system and is in transmission connection with the driving system, the bottom end of the magnetic driving system is, the bottom end of the stirring shaft is fixedly sleeved with a stirring paddle, the bending angle of the stirring paddle blade is 110-125 degrees, the cooling circulation device comprises a liquid supply device, a liquid supply box, a needle valve, a suction pump and a cooler, one end of the liquid supply device is connected with the liquid supply box, one end of the liquid supply box is communicated with a conveying pipeline, the conveying pipeline penetrates through the reaction kettle body and extends into the cooling cavity groove at the inner edge of the reaction kettle body, the needle valve is arranged on the conveying pipeline, an output pipeline is arranged at the other end in the cooling cavity groove at the inner edge of the reaction kettle body, the output pipeline penetrates through the cooling cavity groove at the inner edge of the reaction kettle body and extends upwards to be communicated with the suction pump, the cooler is arranged at one side of the suction pump and is communicated with the suction pump, and the cooler is communicated with the liquid supply.
As a further improvement of the invention, the reaction kettle body comprises a kettle body, a kettle cover and a strengthening and reinforcing sealing element, wherein the kettle cover is arranged on the kettle body, the strengthening and reinforcing sealing element is symmetrically arranged at the side end of the kettle cover, and the kettle cover and the strengthening and reinforcing sealing element are fixedly connected through a fastening bolt.
As a further improvement of the invention, the temperature measuring unit comprises a temperature measuring sensor, a single chip microcomputer and a display, the model of the temperature sensor is DS18B20, the model of the single chip microcomputer is P87LPC764, the temperature sensor is arranged in a cavity groove at the inner end of the reaction kettle body, one end of the temperature sensor is electrically connected with the single chip microcomputer through a lead, the lead is hermetically arranged in the temperature measuring sleeve, and one end of the single chip microcomputer is electrically connected with the display.
As a further improvement of the invention, the pressure measuring unit comprises a pressure measuring probe, an MCU processor and a pressure gauge, the pressure measuring probe penetrates through the kettle cover and is arranged in the cavity groove of the kettle body, the pressure measuring probe of the pressure measuring probe is electrically connected with the MCU processor through a lead, and the MCU processor is electrically connected with the pressure gauge through a lead.
As a further improvement of the invention, the heating device is a heating furnace, and one side of the heating device is provided with a heating power supply binding post.
Adopt above-mentioned structure, its beneficial effect lies in:
the invention has simple and reasonable structural design, the stirring shaft penetrates through the reaction kettle body and is arranged in the cavity groove of the reaction kettle body, the bottom end of the stirring shaft is fixedly sleeved with the stirring paddle, the bending angle of the blade of the stirring paddle is 110-125 degrees, the rotating coverage surface of the blade of the stirring paddle can be increased, the stirring uniformity is increased, the stirring effect is excellent, the cooling circulation device comprises a liquid supply device, a liquid supply box, a needle valve, a suction pump and a cooler, one end of the liquid supply device is connected with the liquid supply box, one end of the liquid supply box is communicated with a conveying pipeline, the conveying pipeline penetrates through the reaction kettle body and extends into the cooling cavity groove at the inner edge of the reaction kettle body, the conveying pipeline is provided with the needle valve, the cooling liquid flowing into the liquid supply box through the liquid supply device can be effectively controlled by the needle valve, the cooling liquid can effectively cool the material, the other end in the cooling cavity groove at the inner edge of the reaction kettle body is, the output pipeline penetrates through the inner edge cooling cavity groove of the reaction kettle body and extends upwards to be communicated with the suction pump, a cooler is arranged on one side of the suction pump and is communicated with the suction pump, the suction pump can suck cooling liquid in the inner edge cooling cavity groove of the reaction kettle body into the conveying pipeline in an accelerating mode, the liquid suction pump then accelerates the flow of the heated cooling liquid into the cooler from the output pipeline to be cooled, the cooling liquid flows into the liquid supply box again to form a circulation after the cooling is completed, the use amount of the cooling liquid can be greatly reduced, the cost is greatly saved, and the cyclic continuous utilization of resources is realized.
Drawings
FIG. 1 is a schematic structural diagram of a circulatively cooled reactor apparatus according to the present invention.
In the figure: 1-a reaction kettle body, 101-a kettle body, 102-a kettle cover, 103-a reinforced sealing piece, 104-a fastening bolt, 105-a cooling cavity groove, 2-a stirring unit, 201-a driving motor, 202-a magnetic driving system, 203-a stirring shaft, 204-a stirring paddle, 3-a temperature measuring unit, 301-a temperature sensor, 302-a single chip microcomputer, 303-a display, 4-a pressure measuring unit, 401-a pressure measuring probe, 402-an MCU processor, 403-a pressure gauge, 5-a cooling circulating device, 501-a liquid supply device, 502-a liquid supply box, 503-a needle valve, 504-a suction pump, 505-a cooler, 506-a conveying pipeline, 507-an output pipeline, 6-a heating device and 601-a heating power supply terminal.
Detailed Description
The invention is further explained below with reference to the figures and examples.
The first embodiment is as follows: the utility model provides a but circulative cooling formula reation kettle, includes reation kettle body 1, stirring unit 2, temperature measuring unit 3, pressure measuring unit 4, cooling cycle device 5 and heating equipment 6, stirring unit 2 is located reation kettle body 1 upper end and downwardly extending to its inner, temperature measuring unit 3 is installed in reation kettle body 1 side and is extended to its inner, pressure measuring unit 4 is located reation kettle body 1 top and downwardly extending to its inner, cooling cycle device 5 is put through with reation kettle body 1 inner end cavity groove mutually, reation kettle body 1 cover is located in heating equipment 6.
Example two: the reaction kettle body 1 comprises a kettle body 101, a kettle cover 102 and a reinforcing and reinforcing sealing element 103, wherein the kettle body 101 is provided with the kettle cover 102, the reinforcing and reinforcing sealing element 103 is symmetrically arranged at the side end of the kettle cover 102, the kettle cover 102 and the reinforcing and reinforcing sealing element 103 are fixedly connected through a fastening bolt 104, and other technical schemes are the same as those of the first embodiment.
Example three; the stirring unit 2 comprises a driving motor 201, a magnetic drive system 202, a stirring shaft 203 and a stirring paddle 204, wherein the magnetic drive system 202 is arranged at the lower end of the driving motor 201 and is in transmission connection with the driving motor, the stirring shaft 203 is arranged at the bottom end of the magnetic drive system 202 and is in transmission connection with the magnetic drive system, the stirring shaft 203 penetrates through the reaction kettle body 1 and is arranged in a cavity groove of the reaction kettle body, the stirring paddle 204 is fixedly sleeved at the bottom end of the stirring shaft 203, the blade bending angle of the stirring paddle 204 is 110 and 125 degrees, and other technical schemes are the same as those in the first to second embodiments.
Example four: temperature measurement unit 3 includes temperature sensor 301, singlechip 302 and display 303, temperature sensor 301 model is DS18B20, singlechip 302 model is P87LPC764, temperature sensor 301 locates the inner end chamber groove of reation kettle body 1, temperature sensor 301 one end passes through wire electric connection with singlechip 302, the wire is sealed to be located in the temperature measurement sleeve, singlechip 302 one end and display 303 electric connection, and other technical scheme are the same with embodiment one to three.
Example five: the pressure measuring unit 4 comprises a pressure measuring probe 401, an MCU processor 402 and a pressure gauge 403, the pressure measuring probe 401 penetrates through the kettle cover 102 and is arranged in a cavity groove of the kettle body 101, the pressure measuring probe 401 is electrically connected with the MCU processor 402 through a conducting wire, the MCU processor 402 is electrically connected with the pressure gauge 403 through a conducting wire, and other technical schemes are the same as those of the first to the fourth embodiments.
Example six: the cooling circulation device 5 comprises a liquid supply device 501, a liquid supply box 502, a needle valve 503, a suction pump 504 and a cooler 505, wherein one end of the liquid supply device 501 is connected with the liquid supply box 502, one end of the liquid supply box 502 is communicated with a conveying pipeline 506, the conveying pipeline 506 penetrates through the reaction kettle body 1 and extends into the cooling cavity groove 105 on the inner edge of the reaction kettle body, the needle valve 503 is arranged on the conveying pipeline 506, the other end of the cooling cavity groove on the inner edge of the reaction kettle body 1 is provided with an output pipeline 507, the output pipeline 507 penetrates through the cooling cavity groove 105 on the inner edge of the reaction kettle body 1 and extends upwards to be communicated with the suction pump 504, one side of the suction pump 504 is provided with the cooler 504 and is communicated with the suction pump, the cooler 504 is communicated with the liquid supply box 502 to form a circulation, and other technical schemes are the same as the first to the fifth.
Example seven: the heating device 6 is a heating furnace, a heating power supply binding post 601 is arranged on one side of the heating device 6, and the other technical schemes are the same as the first to sixth embodiments.
In order to facilitate understanding of the above-described embodiments of the present invention, the following detailed description will be given of the above-described embodiments of the present invention in a specific manner of use.
The specific working process is as follows: firstly, materials are added into a cavity groove of a reaction kettle body 1, then a kettle cover 102 is closed and fixed with a strengthening and reinforcing sealing piece 103 through a fastening bolt 104, a temperature sensor 301 of a temperature measuring unit 3 can display the temperature in the cavity groove of the reaction kettle body 1 on a display 303 through a singlechip 302, when the temperature in the cavity groove of the reaction kettle body 1 needs to be raised and the materials need to be heated, a heating device 6 is started to heat the reaction kettle body 1, when the temperature on the display 303 reaches a specified temperature, the heating is stopped, a pressure measuring probe 401 of a pressure measuring unit 4 can transmit the pressure value in the reaction kettle body 1 to a pressure gauge 403 for displaying through an MCU processor 402, when the temperature in the cavity groove needs to be cooled and the materials need to be cooled, a liquid supply device 501 of a cooling circulation device 5 is opened, cooling liquid flows into a conveying pipeline 506 from a liquid supply tank 502, a needle valve 503 is opened, the coolant liquid flows to cooling chamber 105 of reation kettle body 1 by pipeline 506 in, the coolant liquid cools off reation kettle body 1 chamber and material, rethread suction pump 504 is with higher speed with the coolant liquid flow into cooler 505 in by output pipeline 507 and cools off, flow into again after the cooling is accomplished and supply liquid case 202 and form a circulation, when the temperature on the display 303 reaches the assigned temperature, close cooling circulation device 5, when needs stir the material, start driving motor 201 of stirring unit 2, driving motor 201 drives magnetism and drives system 202 and operates, magnetism drives system 202 and drives stirring shaft 203 thereby drive stirring rake 204 and stir.
The foregoing is illustrative and explanatory of the invention and is not intended to limit the advantages attainable thereby, and it is within the scope of the present application for any one or more of the advantages to be realized, whether simple changes in structure are possible in the practice of the invention, and/or in some embodiments.

Claims (5)

1. A circulative cooling formula reation kettle which characterized in that: the reaction kettle comprises a reaction kettle body (1), a stirring unit (2), a temperature measuring unit (3), a pressure measuring unit (4), a cooling circulating device (5) and heating equipment (6), wherein the stirring unit (2) is arranged at the upper end of the reaction kettle body (1) and extends downwards to the inner end of the reaction kettle body, the temperature measuring unit (3) is arranged at the side end of the reaction kettle body (1) and extends to the inner end of the reaction kettle body, the pressure measuring unit (4) is arranged at the top end of the reaction kettle body (1) and extends downwards to the inner end of the reaction kettle body, the cooling circulating device (5) is communicated with a cavity groove at the inner end of the reaction kettle body (1), the reaction kettle body (1) is sleeved in the heating equipment (6), the stirring unit (2) comprises a driving motor (201), a magnetic driving system (202), a stirring shaft (203) and a stirring paddle (204), the lower end of the driving motor (201) is provided with the, the bottom end of the magnetic drive system (202) is provided with a stirring shaft (203) and is in transmission connection with the stirring shaft, the stirring shaft (203) penetrates through the reaction kettle body (1) and is arranged in a cavity groove of the reaction kettle body, the bottom end of the stirring shaft (203) is fixedly sleeved with a stirring paddle (204), the bending angle of a blade of the stirring paddle (204) is 110-125 degrees, the cooling circulating device (5) comprises a liquid supply device (501), a liquid supply box (502), a needle valve (503), a suction pump (504) and a cooler (505), one end of the liquid supply device (501) is connected with the liquid supply box (502), one end of the liquid supply box (502) is communicated with a conveying pipeline (506), the conveying pipeline (506) penetrates through the reaction kettle body (1) and extends into an inner edge cooling cavity groove (105) of the reaction kettle body, the needle valve (503) is arranged on the conveying pipeline (506), and an output pipeline (507) is arranged at the other end in the inner edge cooling cavity groove of the reaction kettle, the output pipeline (507) penetrates through the cooling cavity groove (105) on the inner edge of the reaction kettle body (1) and extends upwards to be communicated with the suction pump (504), a cooler (504) is arranged on one side of the suction pump (504) and communicated with the suction pump, and the cooler (504) is communicated with the liquid supply tank (502) to form a cycle.
2. A circulatively cooled reactor according to claim 1, wherein: the reaction kettle body (1) comprises a kettle body (101), a kettle cover (102) and a reinforcing and reinforcing sealing piece (103), wherein the kettle cover (102) is arranged on the kettle body (101), the reinforcing and reinforcing sealing piece (103) is symmetrically arranged at the side end of the kettle cover (102), and the kettle cover (102) and the reinforcing and reinforcing sealing piece (103) are fixedly connected through a fastening bolt (104).
3. A circulatively cooled reactor according to claim 1, wherein: temperature measurement unit (3) are including temperature sensor (301), singlechip (302) and display (303), temperature sensor (301) model is DS18B20, singlechip (302) model is P87LPC764, the inner end chamber groove of reation kettle body (1) is located in temperature sensor (301), temperature sensor (301) one end and singlechip (302) pass through wire electric connection, the wire is sealed to be located in the temperature measurement cover pipe, singlechip (302) one end and display (303) electric connection.
4. A circulatively cooled reactor according to claim 2, wherein: the pressure measuring unit (4) comprises a pressure measuring probe (401), an MCU (microprogrammed control unit) processor (402) and a pressure gauge (403), wherein the pressure measuring probe (401) penetrates through the kettle cover (102) to be arranged in a cavity groove of the kettle body (101), the pressure measuring probe (401) is electrically connected with the MCU processor (402) through a wire, and the MCU processor (402) is electrically connected with the pressure gauge (403) through a wire.
5. A circulatively cooled reactor according to claim 1, wherein: the heating device (6) is a heating furnace, and a heating power supply binding post (601) is arranged on one side of the heating device (6).
CN201810933613.9A 2018-08-16 2018-08-16 But circulative cooling formula reation kettle Pending CN110833806A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810933613.9A CN110833806A (en) 2018-08-16 2018-08-16 But circulative cooling formula reation kettle

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Application Number Priority Date Filing Date Title
CN201810933613.9A CN110833806A (en) 2018-08-16 2018-08-16 But circulative cooling formula reation kettle

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CN110833806A true CN110833806A (en) 2020-02-25

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115231579A (en) * 2022-08-18 2022-10-25 浙江科磊新材料有限公司 Preparation process and preparation device for synthesizing lithium magnesium silicate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115231579A (en) * 2022-08-18 2022-10-25 浙江科磊新材料有限公司 Preparation process and preparation device for synthesizing lithium magnesium silicate
CN115231579B (en) * 2022-08-18 2023-12-26 浙江科磊新材料有限公司 Preparation process and preparation device for synthesizing lithium magnesium silicate

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Application publication date: 20200225

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