CN110801043A - Microcapsule for improving immunity of chronic disease patient and preparation method thereof - Google Patents

Microcapsule for improving immunity of chronic disease patient and preparation method thereof Download PDF

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Publication number
CN110801043A
CN110801043A CN201911178753.0A CN201911178753A CN110801043A CN 110801043 A CN110801043 A CN 110801043A CN 201911178753 A CN201911178753 A CN 201911178753A CN 110801043 A CN110801043 A CN 110801043A
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China
Prior art keywords
microcapsule
chia seed
core material
immunity
preparation
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CN201911178753.0A
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Chinese (zh)
Inventor
徐同成
岳昊
邱斌
贾敏
刘丽娜
刘玮
宗爱珍
杜方岭
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Institute of Agro Food Science and Technology of Shandong Academy of Agricultural Sciences
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Institute of Agro Food Science and Technology of Shandong Academy of Agricultural Sciences
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/30—Encapsulation of particles, e.g. foodstuff additives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
    • A23L25/30—Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/10—Foods or foodstuffs containing additives; Preparation or treatment thereof containing emulsifiers
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115—Fatty acids or derivatives thereof; Fats or oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Mycology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention particularly relates to a microcapsule for improving the immunity of a chronic patient and a preparation method thereof, belonging to the field of food processing. The microcapsule consists of a solid and water, wherein the solid comprises the following components in parts by weight: 30-45% of core material; 53-68% of wall material; and 2% of an emulsifier. The core material is chia seed oil and chia seed powder; the wall material is one or a mixture of more of high amylose corn starch, sodium caseinate, fructo-oligosaccharide, sorghum starch and maltodextrin. The prepared microcapsule has good stability, high solubility and good grease embedding effect; it is another object of the present invention to provide a process for producing microcapsules which is simple and feasible and whose process is easy to control. The microcapsule of the invention is suitable for various chronic patients to take.

Description

Microcapsule for improving immunity of chronic disease patient and preparation method thereof
Technical Field
The invention particularly relates to a microcapsule for improving the immunity of a chronic patient and a preparation method thereof, belonging to the field of food processing.
Background
The microcapsule is widely applied in different fields of food, biotechnology, chemical industry, medicine and the like, and has unique advantages compared with other technologies. Microencapsulation physically encapsulates the sensitive components in a coating to protect these components or the "core material" from adverse reactions (e.g., light, oxygen, temperature, humidity); optimizing the physical properties (such as odor, appearance, solubility) of the core material itself; the stability of the core material is improved; isolating immiscible or interactive substances.
Chronic diseases, a generalized collective term for diseases whose etiology is complex and some of which have not been completely identified. Common chronic diseases mainly include cardiovascular and cerebrovascular diseases, cancer, diabetes and chronic respiratory diseases, wherein the cardiovascular and cerebrovascular diseases comprise hypertension, stroke and coronary heart disease. The chronic diseases mainly cause the damage of important organs such as brain, heart, kidney and the like, are easy to cause disability, influence the labor capacity and the life quality, are extremely expensive in medical cost, and increase the economic burden of society and families.
Chia seed is rich in nutrition, fat, high-quality protein, dietary fiber and various minerals. The ratio of essential amino acids to total amino acids in chia seed protein is superior to common peanut protein, linseed protein and walnut protein, and is similar to soybean protein. The amino acid composition in chia seed protein is close to the ideal mode recommended by FAO/WHO, has higher edible value and is a high-quality vegetable protein source. In addition, chia seed is rich in vitamin E, carotenoid, polyphenol compounds and other antioxidant active substances, and has high physiological activity and application value.
Compared with other vegetable oils, the α -linolenic acid (ALA) content of chia seed oil is far ahead (50.6 percent of linseed), rape (8.1 percent), soybean (7.6 percent) and sunflower (1.8 percent)).
Disclosure of Invention
According to the characteristics of chia seed oil and chronic diseases, the invention provides the microcapsule for improving the immunity of chronic patients, and the prepared microcapsule has good stability, high solubility and good grease embedding effect by adopting chia seed powder and chia seed oil; another object of the invention is to provide a simple and feasible production method of chia seed oil microcapsules, wherein the process is easy to control.
A microcapsule for improving the immunity of patients with chronic diseases consists of a solid and water, wherein the solid comprises the following components in parts by weight:
30-45% of core material;
53-68% of wall material;
and 2% of an emulsifier.
The core material is chia seed oil and chia seed powder;
the wall material is one or a mixture of more of high amylose corn starch, sodium caseinate, fructo-oligosaccharide, sorghum starch and maltodextrin.
The emulsifier is one or more of chia seed gum, monoglyceride, sucrose ester, polyoxyethylene sorbitan fatty acid ester, and acacia.
The ratio of the solid to the water is 1: 3.
The preparation method of the chia seed oil microcapsule comprises the following steps:
(1) preparation of a core material: adding chia seed powder into chia seed oil, and fully mixing; preparing emulsion, namely the core material;
(2) dissolving: heating water to 65-70 deg.C; adding wall materials and an emulsifier into water in sequence according to the weight proportion, and fully stirring;
(3) homogenizing: after the core material is added, high-speed shearing is carried out for 5-10min, the shearing rotating speed is 10000-;
(4) spray drying: the inlet temperature is 175-.
The prepared microcapsule for improving the immunity of patients with chronic diseases is applied to the preparation of medicines for treating chronic diseases.
The invention has the advantages that:
1. high nutritive value
The chia seed oil is rich in unsaturated fatty acid, wherein the content of α -linolenic acid is over 60 percent, and the chia seed oil can meet the special nutritional requirements of various chronic patients and can be used as an oil component suitable for the chronic patients to eat.
2. Good oxidation resistance
The microcapsule product prepared by the invention has the characteristics of less loss of effective components, uniform particle size, good stability, easy dissolution, strong oxidation resistance and the like. The microcapsule shows ideal antioxidant effect, and the results of accelerated oxidation tests show that the oxidation stability of the chia seed oil microcapsule is far higher than that of non-embedded chia seed oil. On the 7 th day of the accelerated oxidation experiment, the peroxide value of the microcapsule product is far lower than that of the uninsulated chia seed oil, the oxidation stability is good, and the shelf life of the functional oil can be prolonged.
3. Wide application
Can be widely applied to the field of food, including the processing production of special medical food.
Detailed Description
Example 1
The preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 20g of sorghum starch, 18g of high amylose corn starch, 31.15g of maltodextrin, 1.5g of monoglyceride and 0.5g of chia seed gum, and fully stirring and dissolving at 65 ℃ to 500 mL; then 28.85g of core material is added, and the mixture is sheared for 5 minutes at high speed under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Example 2
Preparation of a core material: the preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 10g of sorghum starch, 10g of high amylose corn starch, 48g of maltodextrin, 1.55g of monoglyceride and 0.45g of chia seed gum, and fully stirring and dissolving the mixture to 500mL at the temperature of 65 ℃; then 30g of core material is added, and the mixture is sheared for 5 minutes at a high speed under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Example 3
The preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 10g of sorghum starch, 30g of high amylose corn starch, 18g of maltodextrin, 1g of monoglyceride and 1g of chia seed gum, and fully stirring and dissolving at 65 ℃ to 500 mL; then adding 40g of core material, and shearing at high speed for 5 minutes under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Comparative example 1
The preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, adding 1.55g of monoglyceride and 0.45g of flaxseed gum, fully stirring, and then adding chia seed powder. Making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 10g of sorghum starch, 10g of high amylose corn starch and 48g of maltodextrin, and fully stirring and dissolving the sorghum starch, the high amylose corn starch and the maltodextrin to 500mL at the temperature of 65 ℃; then 30g of core material is added, and the mixture is sheared for 5 minutes at a high speed under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Comparative example 2
Preparation of a core material: the preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 10g of sorghum starch, 15.95g of high amylose corn starch, 44.7g of maltodextrin and 0.5g of chia seed gum, and fully stirring and dissolving at 65 ℃ to 500 mL; then 28.85g of core material is added, and the mixture is sheared for 5 minutes at high speed under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Comparative example 3
Preparation of a core material: the preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 20g of sorghum starch, 60g of high amylose corn starch, 58.5g of maltodextrin, 1.8g of monoglyceride and 1.2g of chia seed gum, and fully stirring and dissolving the mixture to 500mL at the temperature of 65 ℃; then adding 40g of core material, and shearing at high speed for 5 minutes under the condition of 10000 revolutions per minute; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Comparative example 4
Preparation of a core material: the preparation process of the core material comprises the following steps: firstly, adding chia seed oil into a container, then adding chia seed powder, and fully mixing; making into emulsion, packaging, and storing at appropriate temperature.
A preparation process of a microcapsule for improving the immunity of patients with chronic diseases comprises the following steps: weighing 10g of sorghum starch, 5g of high amylose corn starch, 50g of maltodextrin, 1.2g of monoglyceride and 0.8g of chia seed gum, adding 20g of core material, and fully stirring and dissolving at 65 ℃ to 500 mL; shearing at high speed for 5 minutes under the condition of 10000 r/min; homogenizing the emulsion with a high-pressure homogenizer under 30MPa for 3 times; finally, the inlet temperature of spray drying is 175-.
Examples of the effects of the invention
Effect example 1
The experiments on the functional oils and fats in different proportions, which contribute to the improvement of diabetes, were as follows:
selecting healthy mice with the same variety and age, and constructing a hyperlipidemia model;
control group: feeding common feed
Example set: feeding common feed and chia seed oil microcapsules in examples 1-3 and comparative examples 1-4;
wherein the feed feeding amount of each group is identical; and (4) measuring blood fat after feeding for 3 months.
And (3) determining the blood fat of the mouse: after the mice fasted overnight for 12 hours without water prohibition, the heart was bled and the blood lipid level was measured using a full-automatic biochemical analyzer.
Blood lipid measurement of mouse (unit mmol/L)
Effect example two
The experiments on the functional oils and fats in different proportions, which contribute to the improvement of diabetes, were as follows:
selecting healthy mice with the same variety and age, and constructing a diabetes model;
control group: feeding common feed
Example set: feeding common feed and chia seed oil microcapsules in examples 1-3 and comparative examples 1-4;
wherein the feed feeding amount of each group is identical, and blood glucose is measured after feeding for 3 months.
Blood glucose measurement results (unit mg/dL)
Figure DEST_PATH_IMAGE004
Effect example III
The embedding rates of the functional oil and fat microcapsules prepared in examples 1 to 3 and comparative examples 2 to 4 were measured, and the results were as follows:
Figure DEST_PATH_IMAGE006
effect example four
The stability of the functional oil microcapsules prepared by the invention is evaluated: the method comprises the following steps: and (3) dissolving the functional oil microcapsules by using water at the temperature of 80 ℃ to obtain a 10% functional oil microcapsule solution, uniformly stirring the solution by using a glass rod, standing for 1h after the solution is uniformly stirred, and observing the stability of the emulsion and whether floating oil appears on the surface. The test results were as follows:
Figure DEST_PATH_IMAGE008
effect example five
The solubility of the chia seed oil microcapsules prepared by the invention is evaluated: the method comprises the following steps: accurately weighing 5g chia seed oil microcapsule sample, uniformly pouring into a 50mL beaker, dissolving the microcapsule with 38mL of distilled water at 25-30 ℃, transferring into a 50mL centrifuge tube, screwing a bottle stopper, placing in a centrifuge, centrifuging for 10min at 4000 r min-1, and pouring out the supernatant. Adding 38mL of distilled water at 25-30 ℃, fully shaking to dissolve the precipitate again, centrifuging for 10min at 4000 r min-1, pouring out the supernatant, washing the precipitate with a small amount of distilled water into an evaporation dish which is dried to constant weight, and placing the evaporation dish into an oven at 105 ℃ to be dried to constant weight. The solubility is calculated as:
solubility =1- [ (W)2-W1）×100%][（1-A）×W0]-1
Wherein, W0Is the microcapsule sample mass, W1For evaporating dish mass, W2The mass of the evaporating dish plus the mass of insoluble matter, and A is the water content of the microcapsule.
Figure DEST_PATH_IMAGE010
Therefore, the chia seed oil microcapsule provided by the invention has good solubility.
Effect example six
And simultaneously putting the chia seed oil and the chia seed oil microcapsule into an oven at 63 +/-2 ℃ to perform an accelerated oxidation experiment, and sampling every 24 hours to determine the change of the peroxide value. The peroxide number was determined according to GB 5009.227-2016.
Peroxide number measurement (unit mmol/Kg)
Group of Day 0 3 days 7 days
Crude oil 2.085 8.281 21.245
Microcapsules 2.467 3.427 5.641
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are within the scope of the invention.

Claims (6)

1. The microcapsule for improving the immunity of chronic patients is characterized by comprising a solid and water, wherein the solid comprises the following components in parts by weight:
30-45% of core material;
53-68% of wall material;
and 2% of an emulsifier.
2. The core material is chia seed oil and chia seed powder;
the wall material is one or a mixture of more of high amylose corn starch, sodium caseinate, fructo-oligosaccharide, sorghum starch and maltodextrin.
3. The microcapsule according to claim 1, wherein the emulsifier is chia seed gum and one or more of monoglyceride, sucrose ester, polyoxyethylene sorbitan fatty acid ester, and acacia.
4. The microcapsule according to claim 1, wherein the ratio of the solid to the water is 1: 3.
5. The method for preparing microcapsules for enhancing immunity of patients with chronic diseases according to claim 1, comprising the steps of:
(1) preparation of a core material: adding chia seed powder into chia seed oil, and fully mixing; preparing emulsion, namely the core material;
(2) dissolving: heating water to 65-70 deg.C; adding wall materials and an emulsifier into water in sequence according to the weight proportion, and fully stirring;
(3) homogenizing: after the core material is added, high-speed shearing is carried out for 5-10min, the shearing rotating speed is 10000-;
(4) spray drying: the inlet temperature is 175-.
6. Use of microcapsules for enhancing the immunity of patients suffering from chronic diseases, prepared according to claim 4, for the preparation of a medicament for the treatment of chronic diseases.
CN201911178753.0A 2019-11-27 2019-11-27 Microcapsule for improving immunity of chronic disease patient and preparation method thereof Pending CN110801043A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116458646A (en) * 2023-04-23 2023-07-21 山东康乐医疗管理有限公司 Production method of compound nutrient

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104323282A (en) * 2014-11-05 2015-02-04 潘炳阳 Soft capsule with chia seed oil and preparation method thereof
CN105996040A (en) * 2016-05-20 2016-10-12 福建师范大学 Microcapsule powder and preparation method thereof
CN109452378A (en) * 2018-12-29 2019-03-12 武汉轻工大学 It is a kind of to handle the method for being rich in the grease of alpha-linolenic acid and grease and its application
CN110063500A (en) * 2019-05-24 2019-07-30 山东省立医院 A kind of low GI value biodiesel microcapsules and preparation method thereof
CN110169578A (en) * 2019-05-24 2019-08-27 山东省农业科学院农产品研究所 A kind of biodiesel microcapsules and preparation method thereof containing odd sub- seed glue

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104323282A (en) * 2014-11-05 2015-02-04 潘炳阳 Soft capsule with chia seed oil and preparation method thereof
CN105996040A (en) * 2016-05-20 2016-10-12 福建师范大学 Microcapsule powder and preparation method thereof
CN109452378A (en) * 2018-12-29 2019-03-12 武汉轻工大学 It is a kind of to handle the method for being rich in the grease of alpha-linolenic acid and grease and its application
CN110063500A (en) * 2019-05-24 2019-07-30 山东省立医院 A kind of low GI value biodiesel microcapsules and preparation method thereof
CN110169578A (en) * 2019-05-24 2019-08-27 山东省农业科学院农产品研究所 A kind of biodiesel microcapsules and preparation method thereof containing odd sub- seed glue

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116458646A (en) * 2023-04-23 2023-07-21 山东康乐医疗管理有限公司 Production method of compound nutrient

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Application publication date: 20200218