CN1107881A - Fluoride sealant for thread - Google Patents

Fluoride sealant for thread Download PDF

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Publication number
CN1107881A
CN1107881A CN 94101903 CN94101903A CN1107881A CN 1107881 A CN1107881 A CN 1107881A CN 94101903 CN94101903 CN 94101903 CN 94101903 A CN94101903 A CN 94101903A CN 1107881 A CN1107881 A CN 1107881A
Authority
CN
China
Prior art keywords
thread
acetone
sealant
fluoride
dioxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 94101903
Other languages
Chinese (zh)
Other versions
CN1045106C (en
Inventor
李生田
马惠敏
潘成林
刘利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Changchun Institute of Applied Chemistry of CAS
Original Assignee
Changchun Institute of Applied Chemistry of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Changchun Institute of Applied Chemistry of CAS filed Critical Changchun Institute of Applied Chemistry of CAS
Priority to CN94101903A priority Critical patent/CN1045106C/en
Publication of CN1107881A publication Critical patent/CN1107881A/en
Application granted granted Critical
Publication of CN1045106C publication Critical patent/CN1045106C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The oil-resistant sealant for screw sealing of mechanical parts is prepared with butadiene nitrile rubber, teflon, SiO2, phenolic resin, acetone as solvent, isocyanate as viscosity increaser and ethylene diamine or 5% ammonia water as infiltrant, and features better adhesion and thermal stability.

Description

Fluoride sealant for thread
The invention belongs to the mechanical whorl oil-resistant seal material.
Screw and oily medium contact in various machineries and the gear reducer, and the other end is exposed to the external world, and bolt and screw make whole tool machine seepage oil because the tolerance that processing brings causes the thread seal degradation, cause environmental pollution and quality product to descend.Therefore, people's sealing material that begins one's study remedies the deficiency that mechanical workout is brought, and solves the problem of screw thread seepage oil.
Dalian second Organic Chemical Plant, Beijing Ailanthus altissima rubber item two factories, biochemical research institute in Xiangfan is with anaerobic glue, nylon, urethane etc. are the feedstock production thread locking adhesive.Because anaerobic glue and ester class price are more expensive, end properties is undesirable, therefore is difficult to wide popularization and application.
The purpose of this invention is to provide a kind ofly with paracril, tetrafluoroethylene is a main raw, adds aerosil, resol, is the thread locking adhesive of solvent with acetone.
Preparation technology of the present invention be with paracril and phenolic resin in mill, melting temperature is below 70 ℃, glue and the resin even lower roll that is mixed, become the 1-1.5mm sheet material, put into reactor after sheet material is pulverized and add acetone, be dissolved into glue, add silicon-dioxide and tetrafluoroethylene powder again, after the normal temperature and pressure stirring (3-4 hour) evenly, going out still is finished product.
Material mixture ratio (calculating) with weight ratio:
Paracril (100)+fluorinated ethylene propylene (25-65)+silicon-dioxide (10-65)+sugar (3-5)+phenolic resin (5-15)+treating compound (0.5-3)+anti-aging agent (0.5-1)+acetone (400-500)
The employing tackifier are isocyanic ester, and treating compound is the ammoniacal liquor of quadrol or 5%.
The various performances of thread locking adhesive of the present invention's preparation are:
(1) alternating temperature-changing-40-140 ℃
(2) anti-machine oil (95-100 ℃ of 24hr)≤2.4
(3) the maximum gap≤0.3mm that fills
(4) 10 kilograms/cm of tensile strength 2(1mpa)
(5) room temperature is stored throughout the year
The thread locking adhesive of the present invention's preparation has good sticking power, suitable ductility, elasticity, creep properties, guarantee that bolt load is constant, has good winter hardiness simultaneously, high thermal resistance, oil-proofness, therefore, sealing glue use temperature is wide, and can be widely used in the thread seal of mechanical combiner.
Embodiment provided by the invention is as follows:
Embodiment 1:
Butadiene-acrylonitrile rubber (100)+polytetrafluoroethylene (25)+silicon-dioxide (25)+sugar (3)+anti-aging agent (1)+5% ammoniacal liquor (2)+acetone (400)
Embodiment 2:
Paracril (100)+polytetrafluoroethylene (50)+silicon-dioxide (50)+anti-aging agent (1)+sugar (3)+5% ammoniacal liquor (2)+isocyanic ester (10)+acetone (500)
Embodiment 3:
Butadiene-acrylonitrile rubber (100)+polytetrafluoroethylene (60)+silicon-dioxide (10)+anti-aging agent (1)+5% ammoniacal liquor (3)+acetone (400)
Embodiment 4:
Butadiene-acrylonitrile rubber (100)+polytetrafluoroethylene (42.6)+silicon-dioxide (10)+anti-aging agent (1)+quadrol (3)+isocyanic ester (5)+acetone (500)

Claims (2)

1, a kind of fluoride sealant for thread is characterized in that the prescription of sealing glue is as follows:
(calculating) paracril (100)+tetrafluoroethylene (25-65)+silicon-dioxide (10-65)+sugar (3-5)+resol (5-15)+treating compound (0.5-3)+anti-aging agent (0.5-1) composition+acetone (400-500) with weight ratio;
2, seal gum as claimed in claim 1 is characterized in that used tackifier are isocyanic ester, and treating compound is the ammoniacal liquor of quadrol or 5%.
CN94101903A 1994-03-03 1994-03-03 Fluoride sealant for thread Expired - Fee Related CN1045106C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN94101903A CN1045106C (en) 1994-03-03 1994-03-03 Fluoride sealant for thread

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN94101903A CN1045106C (en) 1994-03-03 1994-03-03 Fluoride sealant for thread

Publications (2)

Publication Number Publication Date
CN1107881A true CN1107881A (en) 1995-09-06
CN1045106C CN1045106C (en) 1999-09-15

Family

ID=5030428

Family Applications (1)

Application Number Title Priority Date Filing Date
CN94101903A Expired - Fee Related CN1045106C (en) 1994-03-03 1994-03-03 Fluoride sealant for thread

Country Status (1)

Country Link
CN (1) CN1045106C (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100453799C (en) * 2001-11-10 2009-01-21 罗伯特-博希股份公司 Valve for the control of fluids
CN103481513A (en) * 2013-09-23 2014-01-01 苏州市涵信塑业有限公司 Method for processing PTFE-coated rubber sealing gasket
CN109504497A (en) * 2018-12-17 2019-03-22 内蒙古三业科技开发有限公司 A kind of high-temperature anticorrosion renovation agent and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1007159B (en) * 1987-08-07 1990-03-14 湖南省长沙化工机械厂 Prepn. of general metal cutting fluid

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100453799C (en) * 2001-11-10 2009-01-21 罗伯特-博希股份公司 Valve for the control of fluids
CN103481513A (en) * 2013-09-23 2014-01-01 苏州市涵信塑业有限公司 Method for processing PTFE-coated rubber sealing gasket
CN109504497A (en) * 2018-12-17 2019-03-22 内蒙古三业科技开发有限公司 A kind of high-temperature anticorrosion renovation agent and preparation method thereof
CN109504497B (en) * 2018-12-17 2021-07-06 内蒙古三业科技开发有限公司 High-temperature anticorrosion repairing agent and preparation method thereof

Also Published As

Publication number Publication date
CN1045106C (en) 1999-09-15

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