CN110774649A - Composite desulfurizer equipment and preparation method thereof - Google Patents
Composite desulfurizer equipment and preparation method thereof Download PDFInfo
- Publication number
- CN110774649A CN110774649A CN201911028701.5A CN201911028701A CN110774649A CN 110774649 A CN110774649 A CN 110774649A CN 201911028701 A CN201911028701 A CN 201911028701A CN 110774649 A CN110774649 A CN 110774649A
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- Prior art keywords
- stirring
- rod
- fixedly connected
- desulfurizing agent
- extruding
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B11/00—Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
- B30B11/22—Extrusion presses; Dies therefor
- B30B11/24—Extrusion presses; Dies therefor using screws or worms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C7/00—Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
- C21C7/04—Removing impurities by adding a treating agent
- C21C7/064—Dephosphorising; Desulfurising
- C21C7/0645—Agents used for dephosphorising or desulfurising
Abstract
The invention discloses a composite desulfurizer device and a preparation method thereof, the composite desulfurizer device comprises a stirring box, a cover plate is fixedly arranged on the upper surface of the stirring box, a support cylinder is fixedly connected at the center of the upper surface of the cover plate, a stirring motor is fixedly arranged on the upper surface of the support cylinder, a stirring shaft is fixedly connected with the lower surface of the stirring motor, the outer surface of the stirring shaft is rotatably connected at the inner center of the stirring box, a hollow rod is fixedly connected with the outer surface of the stirring shaft, a through hole is arranged on the outer surface of the hollow rod, short rods are fixedly connected with the outer surface of the hollow rod, the through hole and the short rods are distributed at intervals on the outer surface of the hollow rod, a vertical rod is fixedly connected at the other side of the hollow rod, an inclined rod is fixedly connected with the lower surface of the vertical rod, and the vertical rod and the inclined, the production and use cost is reduced.
Description
Technical Field
The invention relates to the field of a desulfurizer, and particularly relates to a composite desulfurizer equipment and a preparation method thereof.
Background
With the increasing emphasis on environmental protection, the requirements for filtering and discharging the flue gas, especially the requirement for filtering sulfur, are becoming stricter, and because of the characteristics of sulfides, desulfurization is generally performed by using a desulfurizing agent through chemical adsorption.
However, the existing desulfurizer mostly passes through a complex chemical reaction process flow during production and processing, so that the raw material cost is high, the production is inconvenient to control, the use condition of the desulfurizer at the processing position is harsh, the desulfurizer is not easy to use, the cost of filtering and discharging is greatly reduced, and a new desulfurizer and a preparation method are to be provided.
Disclosure of Invention
Aiming at the problems in the prior art, the invention aims to provide a composite desulfurizer device and a preparation method thereof, multiple raw materials can be mixed and stirred through a stirring shaft and a vertical rod in a stirring box, the raw materials are mixed and produced in a physical mode, the control is convenient, the cost is low, an extrusion cylinder is used for extrusion molding to prepare a desulfurizer bar, the desulfurizer bar can be directly installed and positioned for use, and then flue gas is adsorbed for chemical filtration, the stability and the efficiency are high, so that the production and processing efficiency can be greatly improved, and the production and use cost is reduced.
In order to solve the above problems, the present invention adopts the following technical solutions.
The utility model provides a compound desulfurizer equipment and preparation method thereof, includes the agitator tank, the last fixed surface of agitator tank installs the apron, the upper surface center fixedly connected with support cylinder of apron, the last fixed surface of support cylinder installs agitator motor, agitator motor's lower fixed surface is connected with the (mixing) shaft, the surface rotation of (mixing) shaft is connected in the inside center department of agitator tank, the outer fixed surface of (mixing) shaft is connected with hollow rod, hollow rod's surface is equipped with the through-hole, hollow rod's outer fixed surface is connected with the quarter butt, through-hole and quarter butt interval distribution are in hollow rod's surface, hollow rod's opposite side fixedly connected with montant, the lower fixed surface of montant is connected with the slope pole, montant and slope pole all rotate the internal surface who connects in the agitator tank.
Further, the inside of (mixing) shaft is equipped with the cavity, the surface upper end of cavity is equipped with the intercommunication groove, the intercommunication groove is located the inside of a support section of thick bamboo, can lead to water through the intercommunication groove, and then inside getting into the material from the cavity, guarantees the homogeneity of adding water and mixing, does benefit to the use.
Further, the lower surface of agitator tank is equipped with the toper and fights, the lower fixed surface that the toper was fought installs the butterfly valve, and the below through fighting at the toper is installed the butterfly valve, does benefit to the control ejection of compact, guarantees to mix the requirement.
Further, the lower fixed surface of butterfly valve installs the extrusion cylinder, the rear side surface of extrusion cylinder is equipped with the design pipe, and the desulfurizer bar can be made through the design pipe of extrusion cylinder rear side installation, and convenient production does benefit to control.
Further, the front end fixed surface of extruding a section of thick bamboo is connected with extrusion motor, extrusion motor's rear side surface is equipped with the hob, the surface of hob rotates to be connected in the inboard surface of extruding a section of thick bamboo, drives the hob through extrusion motor, can screw extrusion, makes things convenient for the ejection of compact to stereotype, and is high-efficient stable.
Furthermore, the desulfurizer is a bar material, comprises 40-60% of quicklime, 10-15% of magnesium oxide, 5-10% of charcoal, 15-20% of clay and 8-15% of water, is produced by mixing common raw materials, is low in cost and is beneficial to control and processing.
Further, the preparation method of the desulfurizing agent comprises the following steps:
s1, weighing the solid raw materials according to the mass percentage for later use;
s2, crushing the weighed solid raw materials by a crusher, and filtering by a screen to ensure that the fineness is 75-100 micrometers to obtain crushed raw materials;
s3, adding the crushed raw materials into a stirring box, starting a stirring motor to drive a stirring shaft 14 to rotate, and uniformly stirring for 30 to 50 minutes at the speed of 30 to 45 revolutions per minute to obtain a mixed raw material;
s4, adding water into the supporting cylinder, uniformly stirring for 15 to 20 minutes at a speed of 15 to 20 revolutions per minute, and allowing water flow to enter the mixed raw material through the cavity, the hollow rod and the through hole to obtain a viscous raw material;
s5, opening a butterfly valve during continuous stirring, and dropping the viscous raw materials into the extrusion cylinder;
s6, turning on an extrusion motor to drive a screw rod to rotate, extruding the viscous raw material into a sizing pipe, and cutting to obtain a bar stock;
and S7, airing the rod material to obtain the desulfurizer rod material.
Further, the drying condition of the step S7 is natural drying in the shade at room temperature.
Compared with the prior art, the invention has the advantages that:
(1) this scheme is through inside (mixing) shaft and the montant of agitator tank, can mix the stirring with multiple raw materials, adopts the physical mode to mix production, convenient control, and is with low costs.
(2) Can lead to water through the intercommunication groove, and then get into the material from the cavity inside, guarantee to add the homogeneity that water mixes, do benefit to the use.
(3) A butterfly valve is arranged below the conical hopper, so that the discharging control is facilitated, and the mixing requirement is ensured.
(4) The shaping pipe is arranged at the rear side of the extrusion cylinder, so that a desulfurizer bar can be manufactured, the production is convenient, and the control is facilitated.
(5) The screw rod is driven by the extrusion motor, so that the extrusion can be carried out spirally, the discharge shaping is convenient, and the extrusion die is efficient and stable.
(6) Common raw materials are adopted for mixing production, the cost is low, and the control processing is facilitated.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a partial schematic view of a stir shaft connection of the present invention;
fig. 3 is a schematic view of a partial connection structure of the vertical rod of the present invention.
The reference numbers in the figures illustrate:
1 stirring box, 11 cover plates, 12 supporting cylinders, 13 stirring motors, 14 stirring shafts, 15 hollow rods, 16 through holes, 17 short rods, 18 vertical rods, 19 inclined rods, 2 cavities, 21 communicating grooves, 22 conical hoppers, 23 butterfly valves, 24 extruding cylinders, 25 shaping pipes, 26 extruding motors and 27 spiral rods.
Detailed Description
The technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention; it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments, and all other embodiments obtained by those skilled in the art without any inventive work are within the scope of the present invention.
Referring to fig. 1-3, a composite desulfurizer device and a preparation method thereof, comprising a stirring box 1, referring to fig. 1 and 3, wherein a cover plate 11 is fixedly installed on the upper surface of the stirring box 1, a charging opening is arranged at the upper end of the stirring box, a support cylinder 12 is fixedly connected to the center of the upper surface of the cover plate 11, a stirring motor 13 with the model number of YEJ-M15 is fixedly installed on the upper surface of the support cylinder 12, and is connected to a control switch and a working power supply in series through a circuit, the stirring motor 14 can be driven to rotate to stir, a stirring shaft 14 is fixedly connected to the lower surface of the stirring motor 13, the outer surface of the stirring shaft 14 is rotatably connected to the center of the inside of the stirring box 1, a hollow rod 15 is fixedly connected to the outer surface of the stirring shaft 14, a through hole 16 is formed in the outer surface of the hollow rod 15, a short rod, hollow rod 15's opposite side fixedly connected with montant 18, montant 18's lower fixed surface is connected with slope pole 19, montant 18 and slope pole 19 all rotate to be connected in the inside surface of agitator tank 1, take hollow rod 15 to rotate through (mixing) shaft 14, just also can take montant 18 and slope pole 19 to rotate, and then stir and mix, improve the homogeneity of raw materials, guarantee the adsorption reaction effect.
Referring to fig. 1 and 2, a cavity 2 is arranged inside a stirring shaft 14, a communication groove 21 is arranged at the upper end of the outer surface of the cavity 2, the communication groove 21 is positioned inside a support cylinder 12, water can be added into the support cylinder 12, and thus the water can enter the cavity 2 through the communication groove 21 and can enter the hollow rod 15, and then the water flows out along a through hole 16 and uniformly enters the mixed material when rotating and stirring, so that the mixing uniformity is ensured, the bar adsorption effect is improved, a conical hopper 22 is arranged on the lower surface of the stirring box 1, a butterfly valve 23 is fixedly arranged on the lower surface of the conical hopper 22 and can be controlled to open and close to facilitate discharging, an extrusion cylinder 24 is fixedly arranged on the lower surface of the butterfly valve 23, a sizing pipe 25 is arranged on the rear side surface of the extrusion cylinder 24, an extrusion motor 26 is fixedly connected to the front end surface of the extrusion cylinder 24, the type is YEJ-M10, can take hob 27 to rotate, and then carry the material after will mixing backward, enter into the sizing pipe 25 inside, can the stroke cylinder bar, can cut off suitable length in the exit, do benefit to production and processing, make things convenient for the later stage installation to use, extrusion motor 26's rear side surface is equipped with hob 27, and hob 27's surface rotates to be connected in the interior side surface of extruding a section of thick bamboo 24.
The preparation method of the desulfurizing agent comprises the following steps:
s1, weighing the solid raw materials according to the mass percentage for later use;
s2, crushing the weighed solid raw materials by a crusher, and filtering by a screen to ensure that the fineness is 75-100 micrometers to obtain crushed raw materials;
s3, adding the crushed raw materials into a stirring box, starting a stirring motor to drive a stirring shaft 14 to rotate, and uniformly stirring for 30 to 50 minutes at the speed of 30 to 45 revolutions per minute to obtain a mixed raw material;
s4, adding water into the supporting cylinder, uniformly stirring for 15 to 20 minutes at a speed of 15 to 20 revolutions per minute, and allowing water flow to enter the mixed raw material through the cavity, the hollow rod and the through hole to obtain a viscous raw material;
s5, opening a butterfly valve during continuous stirring, and dropping the viscous raw materials into the extrusion cylinder;
s6, turning on an extrusion motor to drive a screw rod to rotate, extruding the viscous raw material into a sizing pipe, and cutting to obtain a bar stock;
and S7, airing the rod material to obtain the desulfurizer rod material.
Example 1
The desulfurizer is a bar material, comprises 60% of quicklime, 10% of magnesium oxide, 5% of charcoal, 12% of clay and 13% of water, has large content of quicklime and long adsorption service time, increases material gaps through the clay and the charcoal, increases the contact area of flue gas, and is beneficial to improving the adsorption efficiency.
Example 2
The desulfurizer is a bar material, comprises 50% of quicklime, 10% of magnesium oxide, 10% of charcoal, 20% of clay and 10% of water, has high content of clay and charcoal, can increase the bonding strength of the bar material, is not easy to crack, and ensures the use stability.
Example 3
The desulfurizer is a bar material, comprises 50% of quicklime, 12% of magnesium oxide, 8% of charcoal, 15% of clay and 15% of water, is uniform in raw materials, facilitates uniform mixing, shortens processing time and reduces cost.
The foregoing is only a preferred embodiment of the present invention; the scope of the invention is not limited thereto. Any person skilled in the art should be able to cover the technical scope of the present invention by equivalent or modified solutions and modifications within the technical scope of the present invention.
Claims (8)
1. The utility model provides a compound desulfurizer equipment, includes agitator tank (1), its characterized in that: the stirring device is characterized in that the upper surface of the stirring box (1) is fixedly provided with a cover plate (11), the upper surface center of the cover plate (11) is fixedly connected with a supporting cylinder (12), the upper surface of the supporting cylinder (12) is fixedly provided with a stirring motor (13), the lower surface of the stirring motor (13) is fixedly connected with a stirring shaft (14), the outer surface of the stirring shaft (14) is rotatably connected with the inner center of the stirring box (1), the outer surface of the stirring shaft (14) is fixedly connected with a hollow rod (15), the outer surface of the hollow rod (15) is provided with a through hole (16), the outer surface of the hollow rod (15) is fixedly connected with a short rod (17), the through hole (16) and the short rod (17) are distributed on the outer surface of the hollow rod (15) at intervals, the other side of the hollow rod (15) is fixedly connected with a vertical rod (18), the lower surface, the vertical rod (18) and the inclined rod (19) are both rotatably connected to the inner surface of the stirring box (1).
2. The compound desulfurizing agent apparatus according to claim 1, wherein: the stirring shaft (14) is internally provided with a cavity (2), the upper end of the outer surface of the cavity (2) is provided with a communicating groove (21), and the communicating groove (21) is positioned in the supporting cylinder (12).
3. The compound desulfurizing agent apparatus according to claim 1, wherein: the lower surface of agitator tank (1) is equipped with toper fill (22), the lower surface fixed mounting of toper fill (22) has butterfly valve (23).
4. A composite desulfurizing agent apparatus according to claim 3, wherein: the lower fixed surface of butterfly valve (23) installs and extrudes a section of thick bamboo (24), the rear side surface of extruding a section of thick bamboo (24) is equipped with sizing pipe (25).
5. The compound desulfurizing agent apparatus according to claim 4, wherein: the extruding device is characterized in that an extruding motor (26) is fixedly connected to the surface of the front end of the extruding cylinder (24), a screw rod (27) is arranged on the surface of the rear side of the extruding motor (26), and the outer surface of the screw rod (27) is rotatably connected to the surface of the inner side of the extruding cylinder (24).
6. The preparation method of the compound desulfurizing agent according to claim 1, characterized in that: the desulfurizer is a bar material and comprises 40-60% of quicklime, 10-15% of magnesium oxide, 5-10% of charcoal, 15-20% of clay and 8-15% of water.
7. The compound desulfurizing agent device and the preparation method thereof according to claim 1, characterized in that: the preparation method of the desulfurizing agent comprises the following steps:
s1, weighing the solid raw materials according to the mass percentage for later use;
s2, crushing the weighed solid raw materials by a crusher, and filtering by a screen to ensure that the fineness is 75-100 micrometers to obtain crushed raw materials;
s3, adding the crushed raw materials into a stirring box, starting a stirring motor to drive a stirring shaft 14 to rotate, and uniformly stirring for 30 to 50 minutes at the speed of 30 to 45 revolutions per minute to obtain a mixed raw material;
s4, adding water into the supporting cylinder, uniformly stirring for 15 to 20 minutes at a speed of 15 to 20 revolutions per minute, and allowing water flow to enter the mixed raw material through the cavity, the hollow rod and the through hole to obtain a viscous raw material;
s5, opening a butterfly valve during continuous stirring, and dropping the viscous raw materials into the extrusion cylinder;
s6, turning on an extrusion motor to drive a screw rod to rotate, extruding the viscous raw material into a sizing pipe, and cutting to obtain a bar stock;
and S7, airing the rod material to obtain the desulfurizer rod material.
8. The compound desulfurizing agent device and the preparation method thereof according to claim 7, characterized in that: and the step S7 is carried out under the airing condition of natural shade drying at room temperature.
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CN201911028701.5A CN110774649A (en) | 2019-10-28 | 2019-10-28 | Composite desulfurizer equipment and preparation method thereof |
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CN201911028701.5A CN110774649A (en) | 2019-10-28 | 2019-10-28 | Composite desulfurizer equipment and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112807954A (en) * | 2021-02-01 | 2021-05-18 | 大连亚泰科技新材料股份有限公司 | Preparation process of magnesium-based composite desulfurizer |
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Application publication date: 20200211 |