CN110760864A - Concentrated sulfuric acid deoiling slagging-off circulation recovery unit - Google Patents
Concentrated sulfuric acid deoiling slagging-off circulation recovery unit Download PDFInfo
- Publication number
- CN110760864A CN110760864A CN201911202108.8A CN201911202108A CN110760864A CN 110760864 A CN110760864 A CN 110760864A CN 201911202108 A CN201911202108 A CN 201911202108A CN 110760864 A CN110760864 A CN 110760864A
- Authority
- CN
- China
- Prior art keywords
- tank
- acid
- concentrated sulfuric
- sulfuric acid
- chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims abstract description 54
- 238000011084 recovery Methods 0.000 title claims abstract description 12
- 239000002253 acid Substances 0.000 claims abstract description 43
- 238000005192 partition Methods 0.000 claims abstract description 14
- 238000004064 recycling Methods 0.000 claims abstract description 14
- 239000002893 slag Substances 0.000 claims abstract description 8
- 239000007788 liquid Substances 0.000 claims description 7
- 238000007667 floating Methods 0.000 claims description 6
- 230000005484 gravity Effects 0.000 claims 1
- 238000005554 pickling Methods 0.000 abstract description 8
- 125000004122 cyclic group Chemical group 0.000 abstract description 3
- 239000003921 oil Substances 0.000 description 17
- 210000005056 cell body Anatomy 0.000 description 13
- 238000000034 method Methods 0.000 description 7
- 238000003860 storage Methods 0.000 description 6
- 235000011149 sulphuric acid Nutrition 0.000 description 5
- 239000001117 sulphuric acid Substances 0.000 description 5
- 238000005238 degreasing Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000009713 electroplating Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000004065 wastewater treatment Methods 0.000 description 2
- 239000002033 PVDF binder Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 1
- 230000008707 rearrangement Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/36—Regeneration of waste pickling liquors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/003—Filters in combination with devices for the removal of liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Filtration Of Liquid (AREA)
Abstract
The invention discloses a concentrated sulfuric acid deoiling and deslagging cyclic recovery device which comprises a deoiling tank, a filter, a relay tank and a receiving barrel, wherein the filter is used for communicating the deoiling tank with the relay tank through a pipeline, the relay tank is connected with the receiving barrel through a pipeline, the deoiling tank comprises a tank body, an acid inlet chamber, an intermediate chamber and an acid outlet chamber are formed in the tank body in a dividing mode through a first partition plate and a second partition plate, a filter bag is arranged at the top of the acid inlet chamber, the top of the first partition plate is fixed in the tank body, a communication port used for communicating the acid inlet chamber with the intermediate chamber is formed between the bottom of the first partition plate and the bottom of the tank, the bottom of the second partition plate is fixed at the bottom of the tank, and a communication port used. The oil and slag removal circulation recovery device for concentrated sulfuric acid is used for removing oil, removing slag and purifying concentrated sulfuric acid which is used for multiple times, and then sending the purified concentrated sulfuric acid into the pickling tank for recycling. The resources are recycled, unnecessary consumption is avoided, pollution is reduced, and a large amount of pollution treatment cost is saved.
Description
Technical Field
The invention belongs to a concentrated sulfuric acid pickling technology, and particularly relates to a circulating recovery device for removing oil and slag of concentrated sulfuric acid.
Background
The concentrated sulfuric acid pickling is an important process in the electroplating pretreatment process of hardware or ornaments, and the concentration of sulfuric acid used in the process is sometimes as high as 98%. In the existing practical electroplating operation, the procedure is generally as follows: workers put the workpiece into a concentrated sulfuric acid storage barrel and then put out after the pickling is finished. Thus, after the sulfuric acid in the storage barrel is used for a plurality of times, the sulfuric acid is polluted due to oils carried into the workpiece and oxide layers such as rust peeled from the workpiece, and the pickling effect is further influenced. At this point, the barrel of sulfuric acid can only be scrapped, and a new barrel of sulfuric acid is usually replaced to meet the process requirements. The waste sulfuric acid can only be used as pollution waste and flows into the waste water treatment, and a large amount of waste water treatment cost is consumed.
Disclosure of Invention
The invention aims to provide a circulating recovery device for removing oil and slag of concentrated sulfuric acid, which is used for solving the problem that the concentrated sulfuric acid used for multiple times cannot be recycled in the acid pickling process of the concentrated sulfuric acid in the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme:
a concentrated sulfuric acid deoiling slagging-off circulation recovery unit, it includes except that oil tank, filter, relay groove and receiving bucket, except that the acid outlet of oil tank is connected with the feed liquor end of filter through the pipeline, the play liquid end of filter is connected with relay groove through the pipeline, relay groove is connected with receiving bucket through the pipeline, except that the oil tank includes the cell body, cut apart through first baffle and second baffle in the cell body and form into acid inlet chamber, intermediate chamber and acid outlet chamber, the top of entering the acid inlet chamber is provided with the filter bag, the below of filter bag is provided with the filter bag shelf, a plurality of shelf hole has been seted up on the filter bag shelf, the height of first baffle and second baffle is less than the interior degree of depth of cell body, the top of first baffle is fixed in the cell body, form the intercommunication mouth that is used for entering acid chamber and intermediate chamber intercommunication between its bottom and the tank bottom of cell body, the bottom of the second partition plate is fixed in the groove bottom of the groove body, a communicating port for communicating the middle chamber with the acid outlet chamber is formed in the top of the second partition plate, and the acid outlet of the oil removing groove is formed in the bottom of the acid outlet chamber.
Particularly, a horizontally arranged strip-shaped overflow port is formed in one side wall of the acid inlet chamber above the filter bag shelf, and a floating oil collecting hopper is arranged on the outer wall of the acid inlet chamber corresponding to the overflow port.
Particularly, the bottom of the relay tank is arranged on a high-level platform, the receiving barrel is positioned at the low level of the relay tank, and the concentrated sulfuric acid which is filtered and purified in the relay tank flows into the receiving barrel through self weight.
In particular, the bottom of the receiving tub is provided with a tray.
Particularly, a shelf support is fixed in the acid inlet chamber, and the filter bag shelf is placed on the shelf support.
Particularly, the opening end of the filter bag is fixedly connected with the top notch of the groove body through binding.
In particular, the space of the acid inlet chamber is larger than the space of the intermediate chamber and the acid outlet chamber.
Compared with the prior art, the concentrated sulfuric acid oil-removing and deslagging cyclic recovery device has the advantages that the concentrated sulfuric acid oil-removing and deslagging cyclic recovery device can be used for removing oil, deslagging and purifying repeatedly used concentrated sulfuric acid, and then the purified concentrated sulfuric acid is sent into a pickling tank for recycling. The method realizes the recycling of resources, reduces the production cost, avoids unnecessary consumption, reduces the pollution and further saves a large amount of pollution treatment cost.
Drawings
Fig. 1 is a schematic perspective view of a concentrated sulfuric acid oil-removing and slag-removing recycling device according to an embodiment of the present invention;
FIG. 2 is a top view of a concentrated sulfuric acid oil-removing and deslagging recycling device provided in the embodiment of the invention;
fig. 3 is a schematic diagram of an internal structure of a degreasing tank of a concentrated sulfuric acid degreasing and deslagging recycling device according to an embodiment of the present invention;
FIG. 4 is a plan view of the pipeline connection of the concentrated sulfuric acid oil degreasing and deslagging recycling device provided by the embodiment of the invention;
fig. 5 is a schematic structural diagram of a filter bag shelf of the concentrated sulfuric acid oil-removing and deslagging recycling device according to the embodiment of the present invention.
Detailed Description
The technical scheme of the invention is further explained by the specific implementation mode in combination with the attached drawings.
To facilitate an understanding of the invention, the invention will now be described more fully with reference to the accompanying drawings. Preferred embodiments of the present invention are shown in the drawings. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete. It will be understood that when an element is referred to as being "secured to" another element, it can be directly on the other element or intervening elements may also be present. When an element is referred to as being "connected" to another element, it can be directly connected to the other element or intervening elements may also be present. The terms "vertical," "horizontal," "left," "right," and the like as used herein are for illustrative purposes only and do not represent the only embodiments. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
Referring to fig. 1 to 5, in the embodiment, a concentrated sulfuric acid deoiling and deslagging recycling device includes a deoiling tank 1, a filter 2, a relay tank 3 and a receiving barrel 4, an acid outlet 5 of the deoiling tank 1 is connected with a liquid inlet end of the filter 2 through a pipeline, a liquid outlet end of the filter 2 is connected with the relay tank 3 through a pipeline, the relay tank 3 is disposed on a high platform 6, so that the relay tank 3 is located at a high position of the deoiling tank 1 and the receiving barrel 4, the relay tank 3 is connected with the receiving barrel 4 through a pipeline, the filtered and purified concentrated sulfuric acid in the relay tank 3 flows into the receiving barrel 4 through self weight, and a tray 7 is disposed at the bottom of the receiving barrel 4. The material and the filter element of the filter are specially customized and are used for filtering concentrated acid and removing oil, sediment and other impurities in the acid liquor.
Except that oil groove 1 includes the cell body, the cell body adopts the outer groove lining PVDF inner bag of PP way, be provided with first baffle 8 and second baffle 9 along its length direction interval in the cell body, first baffle 8 and second baffle 9 divide the inner space of cell body apart to form into sour room 10, intermediate chamber 11 and play sour room 12, it compares with intermediate chamber 11 and play sour room 12 to enter sour room 10, and the volume space is bigger, can make things convenient for the workman to directly carry out the pickling operation in this indoor, saves former sulphuric acid storage bucket. Or waste acid in the storage barrel is received and enters the chamber for subsequent oil removal treatment under the condition of keeping the original sulfuric acid storage barrel. The top of the acid inlet chamber 10 is provided with a filter bag 13, the filter bag is made of a polytetrafluoroethylene filter screen, the open end of the filter bag 13 is fixedly connected to the top notch of the groove body through binding, a filter bag shelf 14 is arranged below the filter bag 13, a plurality of shelf holes 15 are formed in the filter bag shelf 14, a shelf support 16 is fixed in the acid inlet chamber 10, and the filter bag shelf 14 is placed on the shelf support 16.
The interior degree of depth that highly is less than the cell body of first baffle 8 and second baffle 9, the top welded fastening of first baffle 8 is in the cell body, form the intercommunication mouth that is used for entering the bottom and the 11 intercommunications of intermediate chamber of sour room 10 between the tank bottom of its bottom and cell body, the bottom of second baffle 9 is fixed in the tank bottom of cell body, its top forms the intercommunication mouth that is used for the top and the play sour room 10 intercommunication of intermediate chamber 11, except that the play sour mouth 5 of oil groove 1 sets up in the bottom of a sour room 12, the flow direction of the liquid in the room 10 of advancing does: the acid inlet chamber 10 enters from the top → flows out from the bottom to enter the middle chamber 11 → flows out from the top of the middle chamber 11 to enter the acid outlet chamber 12 → flows out from the bottom of the acid outlet chamber 12.
A side wall of the acid inlet chamber 10 above the filter bag shelf 14 is provided with a horizontally arranged strip-shaped overflow port 17, and a floating oil collecting hopper 18 is arranged on the outer wall of the acid inlet chamber 10 corresponding to the overflow port 17, so that floating oil or floating slag in the acid liquid flows into the floating oil collecting hopper 18 through the overflow port 17 and is discharged through a pipeline.
Concentrated sulfuric acid deoiling slagging-off circulation recovery unit adopts a deoiling groove 1 of taking the deoiling function in order to replace original sulphuric acid storage bucket for the first step sulphuric acid deoiling, again with an external slagging-off filter 2 of this deoiling groove 1, to the internal sulphuric acid loop filter, clean sulphuric acid after filtering the slagging-off stores and can be beaten back the descaling bath reuse through a relay groove 3.
It is to be noted that the foregoing is only illustrative of the preferred embodiments of the present invention and the technical principles employed. It will be understood by those skilled in the art that the present invention is not limited to the particular embodiments described herein, but is capable of various obvious changes, rearrangements and substitutions as will now become apparent to those skilled in the art without departing from the scope of the invention. Therefore, although the present invention has been described in greater detail by the above embodiments, the present invention is not limited to the above embodiments, and may include other equivalent embodiments without departing from the spirit of the present invention, and the scope of the present invention is determined by the scope of the appended claims.
Claims (7)
1. The concentrated sulfuric acid deoiling and deslagging recycling device is characterized by comprising a deoiling tank, a filter, a relay tank and a receiving barrel, wherein an acid outlet of the deoiling tank is connected with a liquid inlet end of the filter through a pipeline, a liquid outlet end of the filter is connected with the relay tank through a pipeline, the relay tank is connected with the receiving barrel through a pipeline, the deoiling tank comprises a tank body, an acid inlet chamber, a middle chamber and an acid outlet chamber are formed in the tank body by being divided through a first partition plate and a second partition plate, a filter bag is arranged at the top of the acid inlet chamber, a filter bag shelf is arranged below the filter bag, a plurality of shelf holes are formed in the filter bag shelf, the height of the first partition plate and the height of the second partition plate are smaller than the inner depth of the tank body, the top of the first partition plate is fixed in the tank body, and a communication port for communicating the acid inlet chamber with the middle chamber is formed between the bottom of the, the bottom of the second partition plate is fixed in the groove bottom of the groove body, a communicating port for communicating the middle chamber with the acid outlet chamber is formed in the top of the second partition plate, and the acid outlet of the oil removing groove is formed in the bottom of the acid outlet chamber.
2. The concentrated sulfuric acid oil-removing and slag-removing circulation recovery device as claimed in claim 1, wherein a horizontally arranged strip-shaped overflow port is formed in one side wall of the acid inlet chamber above the filter bag shelf, and a floating oil collecting hopper is arranged on the outer wall of the acid inlet chamber corresponding to the overflow port.
3. The oil and slag removal recycling apparatus for concentrated sulfuric acid as claimed in claim 1, wherein the bottom of the relay tank is disposed on a high platform, the receiving barrel is located at a low position of the relay tank, and the filtered and purified concentrated sulfuric acid in the relay tank flows into the receiving barrel by gravity.
4. The oil and slag removal recycling apparatus of concentrated sulfuric acid according to claim 3, wherein a tray is disposed at the bottom of the receiving barrel.
5. The concentrated sulfuric acid oil-removing and slag-removing recycling device of claim 1, wherein a shelf support is fixed in the acid inlet chamber, and the filter bag shelf is placed on the shelf support.
6. The concentrated sulfuric acid oil-removing and slag-removing circulation recovery device as claimed in claim 1, wherein the open end of the filter bag is fixedly connected to the top notch of the tank body by binding.
7. The oil and slag removal recycling apparatus of concentrated sulfuric acid according to claim 1, wherein the space of the acid inlet chamber is larger than the space of the intermediate chamber and the acid outlet chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911202108.8A CN110760864A (en) | 2019-11-29 | 2019-11-29 | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911202108.8A CN110760864A (en) | 2019-11-29 | 2019-11-29 | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110760864A true CN110760864A (en) | 2020-02-07 |
Family
ID=69340253
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911202108.8A Pending CN110760864A (en) | 2019-11-29 | 2019-11-29 | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110760864A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112939632A (en) * | 2021-01-19 | 2021-06-11 | 宁夏润安微肥科技有限公司 | Calcium ammonium nitrate production system |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201735212U (en) * | 2010-07-05 | 2011-02-09 | 无锡出新环保设备有限公司 | Gravity oil-water separator |
| CN202009027U (en) * | 2011-04-07 | 2011-10-12 | 晶澳太阳能有限公司 | Filtering device of pickling tank |
| CN202945327U (en) * | 2012-10-19 | 2013-05-22 | 天津市七星精密机械有限公司 | Pickling circulation system |
| CN204661830U (en) * | 2015-05-06 | 2015-09-23 | 广西柳州市龙发金属表面处理技术有限公司 | Spent acid online recycling recycling device |
| CN204982057U (en) * | 2015-09-23 | 2016-01-20 | 河北钢铁股份有限公司邯郸分公司 | Pickling line pickling medium circulation system |
| CN106676558A (en) * | 2017-01-05 | 2017-05-17 | 宝钢工程技术集团有限公司 | Circulatory solution filtering device and method |
| CN108486590A (en) * | 2018-04-08 | 2018-09-04 | 珠海市玛斯特五金塑胶制品有限公司 | Oil removing and sour reutilization system and method is electroplated |
| CN211471558U (en) * | 2019-11-29 | 2020-09-11 | 无锡星亿智能环保装备股份有限公司 | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit |
-
2019
- 2019-11-29 CN CN201911202108.8A patent/CN110760864A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201735212U (en) * | 2010-07-05 | 2011-02-09 | 无锡出新环保设备有限公司 | Gravity oil-water separator |
| CN202009027U (en) * | 2011-04-07 | 2011-10-12 | 晶澳太阳能有限公司 | Filtering device of pickling tank |
| CN202945327U (en) * | 2012-10-19 | 2013-05-22 | 天津市七星精密机械有限公司 | Pickling circulation system |
| CN204661830U (en) * | 2015-05-06 | 2015-09-23 | 广西柳州市龙发金属表面处理技术有限公司 | Spent acid online recycling recycling device |
| CN204982057U (en) * | 2015-09-23 | 2016-01-20 | 河北钢铁股份有限公司邯郸分公司 | Pickling line pickling medium circulation system |
| CN106676558A (en) * | 2017-01-05 | 2017-05-17 | 宝钢工程技术集团有限公司 | Circulatory solution filtering device and method |
| CN108486590A (en) * | 2018-04-08 | 2018-09-04 | 珠海市玛斯特五金塑胶制品有限公司 | Oil removing and sour reutilization system and method is electroplated |
| CN211471558U (en) * | 2019-11-29 | 2020-09-11 | 无锡星亿智能环保装备股份有限公司 | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112939632A (en) * | 2021-01-19 | 2021-06-11 | 宁夏润安微肥科技有限公司 | Calcium ammonium nitrate production system |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN205765228U (en) | A kind of component of machine processing scrap devil liquor recovery workbench | |
| CN206045590U (en) | A kind of oil water separator for food and drink kitchen | |
| CN108145522A (en) | A kind of machine chip liquid processing device and its processing method | |
| CN211471558U (en) | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit | |
| CN201942752U (en) | Recovered acid liquor filtering device for pipeline acid washing | |
| CN201735212U (en) | Gravity oil-water separator | |
| CN110760864A (en) | Concentrated sulfuric acid deoiling slagging-off circulation recovery unit | |
| CN206881242U (en) | High efficiency oil-water separate tank | |
| CN203829789U (en) | De-slagging device of degreasing tank | |
| CN101973648A (en) | Gravity oil and water separator | |
| CN201990549U (en) | Circulating water self-cleaning system | |
| CN108479192A (en) | Industrial wastewater treatment device | |
| CN205294995U (en) | Oil field waste liquid sand setting deoiling device | |
| CN208865293U (en) | Industrial wastewater treatment device | |
| CN220664928U (en) | Secondary filtering device for electroplating wastewater | |
| CN217127593U (en) | Battery steel casing deoiling device | |
| CN215232422U (en) | Novel sludge filtering equipment | |
| CN204637772U (en) | A kind of sewage physical processing apparatus | |
| CN219783946U (en) | Production electrolyte waste liquid recovery device | |
| CN211339094U (en) | High efficiency washing sewage retrieval and utilization equipment | |
| CN216259587U (en) | Copper strip cleaning water circulating device | |
| CN213924111U (en) | High-temperature high-pressure advection microbubble air-flotation oil receiving tank | |
| CN209940682U (en) | Copper extractant industrial waste water deoiling device | |
| CN208632237U (en) | Waste water pretreatment system | |
| CN220393958U (en) | Electroplating solution bag |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |