CN110713875A - Multi-grain strong-flavor liquor ethyl acetate control method - Google Patents

Multi-grain strong-flavor liquor ethyl acetate control method Download PDF

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Publication number
CN110713875A
CN110713875A CN201911185297.2A CN201911185297A CN110713875A CN 110713875 A CN110713875 A CN 110713875A CN 201911185297 A CN201911185297 A CN 201911185297A CN 110713875 A CN110713875 A CN 110713875A
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cellar
grain
ethyl acetate
grains
steps
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李刚
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Sichuan Yibin Changxing Liquor Industry Co Ltd
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Sichuan Yibin Changxing Liquor Industry Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • C12G3/021Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • C12G3/021Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn
    • C12G3/022Preparation of other alcoholic beverages by fermentation of botanical family Poaceae, e.g. wheat, millet, sorghum, barley, rye, or corn of botanical genus Oryza, e.g. rice

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
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  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
  • Alcoholic Beverages (AREA)

Abstract

The invention relates to a biological fermentation technology, in particular to a method for controlling ethyl acetate of multi-grain strong aromatic Chinese spirits. Controlling in a wine making process flow, wherein the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out of a steamer, adding water, spreading and airing, stirring yeast, putting into a cellar for fermentation, and taking out of the cellar to obtain a mother lees; in the step of adding the mother lees for batching, grains, cooked bran and mother lees are added for batching, and the batching is carried out according to the amount of starch in the mother lees, so that the starch content in the cellar is 18-20% in the step of cellar entry fermentation. By adopting the control method, the content ratio of the four major esters of the prepared liquor is well controlled, and the typical multi-grain strong aromatic liquor flavor is obtained.

Description

Multi-grain strong-flavor liquor ethyl acetate control method
Technical Field
The invention relates to a biological fermentation technology, in particular to a method for controlling ethyl acetate of multi-grain strong aromatic Chinese spirits.
Background
Ethyl caproate, ethyl lactate, ethyl acetate and ethyl butyrate are used as 'four major esters' of the strong aromatic white spirit, the four major esters are main aroma components of the strong aromatic white spirit, the quantity ratio relationship of the four major esters plays an important role in the typical flavor presentation of the multi-grain strong aromatic white spirit, and the ratio (ethyl hexyl ratio) of the high-quality strong aromatic raw wine ethyl acetate to the ethyl caproate is (0.5-0.6): 1, but the phenomenon that the ethyl acetate is higher or the ethyl hexyl ratio is close to 1 or exceeds 1 occurs in the multi-grain aroma brewing process, which becomes a problem for restricting the improvement of the quality of the multi-grain aroma white wine. Therefore, how to control in the production process to adjust the content ratio of the tetrads in the produced white spirit needs to be solved.
Disclosure of Invention
The invention aims to provide a method for controlling ethyl acetate of multi-grain strong aromatic Chinese spirits, and solves the problem of how to control in a production process to adjust the content ratio of four major esters in the produced Chinese spirits.
In order to solve the technical problems, the invention adopts the following technical scheme:
the multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out of a steamer, adding water, spreading and airing, stirring yeast, putting into a cellar for fermentation, and taking out of the cellar to obtain a mother lees; in the step of adding the mother lees for batching, grains, cooked bran and mother lees are added for batching, and the batching is carried out according to the amount of starch in the mother lees, so that the starch content in the cellar is 18-20% in the step of cellar entry fermentation. Starch is the source of the final product obtained in the production process and is the main material condition for providing the metabolism and circulation of microorganisms. The starch can adjust the acidity and moisture of the starch entering the pool, can adjust the fermentation temperature, and can also provide sufficient nutrition for the growth of microorganisms. The starch content is high, the early-stage heating too-violent acid production amplitude is promoted to be too large, the starch concentration is low, the early-stage heating is too slow or not heated, and therefore the starch content entering the cellar is controlled to be 18-20%.
Preferably, in the step of adding the ingredients of the spent grains, the ratio of the cooked bran to the grains is 25-27% by weight. The cooked bran as a filler can adjust the fermentation interface and the starch content, and the reasonable bran-grain ratio is a necessary condition for ensuring the fermentation.
Preferably, in the grain crushing step, the grains comprise sorghum, rice, glutinous rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent. The crushing is too coarse, the boiling gelatinization is not easy to be thorough, and the wine yield is influenced; the fermented grains are easy to become greasy or pimple after being crushed too fine, steam is easy to press during distillation, the amount of the filler is increased, and the quality of the wine is affected.
Preferably, in the step of distilling and picking the wine, the thickness of the grain lees is 5-10 cm, the steam is kept to be started when the grain lees are put into a steamer, the steam can penetrate out of the grain lees, the steam is closed for 3-5 min after a steamer cover is covered, then the steam is opened, and the time from the covering of a dish to the taking out of the steamer is more than or equal to 60 min. When the thickness of the grains is matched with the adjustment of steam and the distillation time, the aroma components in the wine can be fully extracted.
Preferably, the time from the cover plate to the retort discharge is 65-70 min.
Preferably, in the step of pumping water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 52-55%. The wine with excessive water consumption has thin flavor and insufficient water consumption, which causes poor fermentation
Preferably, in the step of mixing the yeast, the ratio of the yeast to the grain is 20-22% by weight. The yeast is used as a saccharification leaven, the temperature is quickly raised when the dosage is large, the saccharification fermenting capacity is reduced when the dosage is small, and the starch utilization rate is reduced.
Preferably, in the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 19-22 ℃. The temperature can provide a growth, reproduction and metabolism environment for various microorganisms, the fermentation grains can be burnt when the temperature of the fermentation grains entering the cellar is too high, the temperature of the fermentation grains entering the cellar is too low, the early-stage temperature rise is too slow or not, and the growth of the microorganisms is hindered under the conditions.
Preferably, in the cellar opening and discharging step, when the yellow water exists after the vinasse is started, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 65-75 hours, 1 time of yellow water is scooped within 2 hours, and the depth of the yellow water in the yellow water pit is less than or equal to 20 cm. The water content and the acidity in the mother lees are reduced, the method is beneficial to the drainage of the wine and the lower drainage of fermentation, and the yellow water depth is more than 20 cm, so that the method is not beneficial to the drainage of the acidity of the mother lees.
Compared with the prior art, the invention has the beneficial effects that: the control method provided by the invention is adopted to control the four major ester content ratio of the prepared liquor well, so that the flavor of typical multi-grain strong aromatic white liquor is obtained.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1:
the multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out from a steamer, adding water, spreading and airing, stirring yeast, entering a cellar for fermentation, taking out from the cellar to obtain a mother lees, and using the obtained mother lees in the step of adding the mother lees ingredient.
In the grain crushing step, the grains comprise sorghum, rice, sticky rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent.
In the step of adding the mother lees for burdening, grains, cooked bran and mother lees are added for burdening, and burdening is carried out according to the starch content in the mother lees, so that the starch content in the cellar is 20 percent when the cellar is put into the fermentation step. The proportion of the cooked bran to the grain is 27 percent by weight.
In the step of distilling and picking wine, the thickness of the grain dreg is 10 cm, steam is kept to be started when the grain dreg is fed into a steamer, the steam can penetrate out of the grain dreg, the steam is closed for 3min after a steamer cover is covered, then the steam is opened, and the time from the tray covering to the steamer discharging is 65 min.
In the step of measuring water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 55 percent.
In the step of mixing the yeast, the yeast-grain ratio is 22 percent by weight.
In the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 19 ℃.
In the cellar opening and discharging step, when the vinasse is started to have yellow water, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 75 hours, 1 time of yellow water is ladled out within 2 hours, and the depth of the yellow water in the yellow water pit is guaranteed to be less than or equal to 20 cm.
Example 2:
the multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out from a steamer, adding water, spreading and airing, stirring yeast, entering a cellar for fermentation, taking out from the cellar to obtain a mother lees, and using the obtained mother lees in the step of adding the mother lees ingredient.
In the grain crushing step, the grains comprise sorghum, rice, sticky rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent.
In the step of adding the mother lees for burdening, grains, cooked bran and mother lees are added for burdening, and burdening is carried out according to the starch content in the mother lees, so that the starch content in the cellar is 18 percent when the cellar is put into the fermentation step. The ratio of the cooked bran to the grain is 25 percent by weight.
In the step of distilling and picking wine, the thickness of the grain dreg is 10 cm, steam is kept to be started when the grain dreg is fed into a steamer, the steam can penetrate out of the grain dreg, the steam is closed for 5min after a steamer cover is covered, then the steam is opened, and the time from the tray covering to the steamer discharging is 60 min.
In the step of measuring water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 52 percent.
In the step of mixing the yeast, the ratio of the yeast to the grain is 20 percent by weight.
In the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 22 ℃.
In the cellar opening and discharging step, when the vinasse is started to have yellow water, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 65 hours, 1 time of yellow water is ladled out within 2 hours, and the depth of the yellow water in the yellow water pit is guaranteed to be less than or equal to 20 cm.
Example 3:
the multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out from a steamer, adding water, spreading and airing, stirring yeast, entering a cellar for fermentation, taking out from the cellar to obtain a mother lees, and using the obtained mother lees in the step of adding the mother lees ingredient.
In the grain crushing step, the grains comprise sorghum, rice, sticky rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent.
In the step of adding the mother lees for burdening, grains, cooked bran and mother lees are added for burdening, and burdening is carried out according to the starch content in the mother lees, so that the starch content in the cellar is 19 percent when the cellar is put into the fermentation step. The ratio of the cooked bran to the grain is 25-27% by weight.
In the step of distilling and picking wine, the thickness of the grain dreg is 10 cm, steam is kept to be started when the grain dreg is fed into a steamer, the steam can penetrate out of the grain dreg, the steam is closed for 3min after a steamer cover is covered, then the steam is opened, and the time from the tray covering to the steamer discharging is 65 min.
In the step of measuring water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 55 percent.
In the step of mixing the yeast, the yeast-grain ratio is 22 percent by weight.
In the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 20 ℃.
In the cellar opening and discharging step, when the vinasse is started to have yellow water, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 72 hours, 1 time of yellow water is ladled out within 2 hours, and the depth of the yellow water in the yellow water pit is guaranteed to be less than or equal to 20 cm.
The most preferred embodiment is as follows:
the multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out from a steamer, adding water, spreading and airing, stirring yeast, entering a cellar for fermentation, taking out from the cellar to obtain a mother lees, and using the obtained mother lees in the step of adding the mother lees ingredient.
In the grain crushing step, the grains comprise sorghum, rice, sticky rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent.
In the step of adding the mother lees for burdening, grains, cooked bran and mother lees are added for burdening, and burdening is carried out according to the starch content in the mother lees, so that the starch content in the cellar is 19 percent when the cellar is put into the fermentation step. The ratio of the cooked bran to the grain is 25 percent by weight.
In the step of distilling and picking wine, the thickness of the grain dreg is 7 cm, steam is kept to be started when the grain dreg is fed into a steamer, the steam can penetrate out of the grain dreg, the steam is closed for 4min after a steamer cover is covered, then the steam is opened, and the time from the tray covering to the steamer discharging is 65 min.
In the step of measuring water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 53 percent.
In the step of mixing the yeast, the yeast-grain ratio is 22 percent by weight.
In the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 20 ℃.
In the cellar opening and discharging step, when the vinasse is started to have yellow water, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 72 hours, 1 time of yellow water is ladled out within 2 hours, and the depth of the yellow water in the yellow water pit is guaranteed to be less than or equal to 20 cm.
The table for detecting the physical and chemical indexes of the white spirit after production by adopting the method of the embodiment is as follows:
raw wine batches Hexanoic acid ethyl ester (mg/100 ml) Ethyl lactate (mg/100 ml) Ethyl acetate (mg/100 ml) Butyric acid ethyl ester (mg/100 ml) Hex of ethyl
1 359 185 231 34 0.52/1
2 321 163 230 34 0.51/1
3 342 182 228 35 0.53/1
Therefore, the multi-grain strong-flavor liquor produced by the embodiment has the typical flavor of the multi-grain strong-flavor liquor.
Reference throughout this specification to multiple illustrative embodiments means that a particular method described in connection with the embodiments is included in at least one embodiment described generally throughout this application. The appearances of the same phrase in various places in the specification are not necessarily all referring to the same embodiment. Further, while a method is described in connection with any one embodiment, it is to be understood that it is within the scope of the invention to implement such a method in connection with other embodiments.

Claims (9)

1. The multi-grain strong aromatic white spirit ethyl acetate control method is controlled in a wine making process flow, and the wine making process flow comprises the following steps: crushing grains, adding a mother lees ingredient, distilling and picking wine, taking out of a steamer, adding water, spreading and airing, stirring yeast, putting into a cellar for fermentation, and taking out of the cellar to obtain a mother lees; the method is characterized in that: in the step of adding the mother lees for batching, grains, cooked bran and mother lees are added for batching, and the batching is carried out according to the amount of starch in the mother lees, so that the starch content in the cellar is 18-20% in the step of cellar entry fermentation.
2. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the step of adding the mother lees for preparing the ingredients, the ratio of the cooked bran to the grains is 25-27% by weight.
3. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the grain crushing step, the grains comprise sorghum, rice, sticky rice, wheat and corn, and after five grains are crushed and mixed, the weight of fine powder which can pass through a 20-mesh sieve is less than or equal to 20 percent.
4. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the step of distilling and picking wine, the thickness of the grain residue is 5-10 cm, steam is kept to be started when the grain residue is fed into a steamer, the steam can penetrate out of the grain residue, the steam is closed for 3-5 min after a steamer cover is covered, then the steam is opened, and the time from the disc covering to the steamer discharging is not less than 60 min.
5. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 4, characterized by comprising the following steps: and the time from the cover plate to the retort discharge is 65-70 min.
6. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the step of measuring water, the using amount of water is determined according to the water content of the fermented grains, and finally the water content in the cellar is controlled to be 52-55%.
7. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the step of mixing the yeast, the ratio of the yeast to the grain is 20-22% by weight.
8. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the cellar entry fermentation step, the temperature of the fermented grains entering the cellar is controlled to be 19-22 ℃.
9. The method for controlling ethyl acetate in multi-grain Luzhou-flavor liquor according to claim 1, characterized by comprising the following steps: in the cellar opening and discharging step, when the vinasse is started to have yellow water, the vinasse is stopped, a yellow water pit is dug for dropping the cellar, the cellar dropping time is 65-75 hours, 1 time of yellow water is scooped up within 2 hours, and the depth of the yellow water in the yellow water pit is guaranteed to be less than or equal to 20 cm.
CN201911185297.2A 2019-11-27 2019-11-27 Multi-grain strong-flavor liquor ethyl acetate control method Pending CN110713875A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111304032A (en) * 2020-03-16 2020-06-19 宜宾五粮液股份有限公司 Method for producing low fusel oil base wine by solid state fermentation
CN111763588A (en) * 2020-07-01 2020-10-13 山东景芝酒业股份有限公司 Method for reducing ethyl acetate content in strong aromatic wine under mechanical production conditions
CN115058304A (en) * 2022-07-15 2022-09-16 中国食品发酵工业研究院有限公司 Brewing method for reducing ethyl acetate content of Luzhou-flavor liquor

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108929829A (en) * 2018-08-30 2018-12-04 河北凤来仪酒业有限公司 A kind of brewing method of Strong-flavor spirit base

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108929829A (en) * 2018-08-30 2018-12-04 河北凤来仪酒业有限公司 A kind of brewing method of Strong-flavor spirit base

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111304032A (en) * 2020-03-16 2020-06-19 宜宾五粮液股份有限公司 Method for producing low fusel oil base wine by solid state fermentation
CN111763588A (en) * 2020-07-01 2020-10-13 山东景芝酒业股份有限公司 Method for reducing ethyl acetate content in strong aromatic wine under mechanical production conditions
CN115058304A (en) * 2022-07-15 2022-09-16 中国食品发酵工业研究院有限公司 Brewing method for reducing ethyl acetate content of Luzhou-flavor liquor
CN115058304B (en) * 2022-07-15 2023-08-29 中国食品发酵工业研究院有限公司 Brewing method for reducing ethyl acetate content of Luzhou-flavor liquor

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