CN110668587A - Separation device for immiscible liquids - Google Patents
Separation device for immiscible liquids Download PDFInfo
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/00—Treatment of water, waste water, or sewage
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Abstract
本发明提供了一种不相溶液体的分离装置,包括封闭的容器,所述容器具有第一进口、第二进口、第一出口和第二出口;风机连接切换单元;切换单元具有第一端口、第二端口、第三端口和第四端口;浮力件在容器内上升时封堵所述第二进口,下降时打开所述第二进口;浮力件随着所述容器内液面变化而沿着导轨上下运动;阀控制所述第一进口的开启和关闭。本发明具有分离效率高等优点。
The invention provides a separation device for immiscible liquid, comprising a closed container, the container has a first inlet, a second inlet, a first outlet and a second outlet; a fan is connected to a switching unit; the switching unit has a first port , the second port, the third port and the fourth port; the buoyant member blocks the second inlet when it rises in the container, and opens the second inlet when it falls; The guide rail moves up and down; the valve controls the opening and closing of the first inlet. The present invention has the advantages of high separation efficiency.
Description
技术领域technical field
本发明涉及液体分离,特别涉及不相溶液体的分离装置。The present invention relates to liquid separation, in particular to a separation device for immiscible liquids.
背景技术Background technique
切削液是金属在切、削、磨等加工过程中,用来冷却和润滑的金属加工液。其种类繁多、成分复杂,通常包含基础油、乳化剂、防锈剂等。切削液(主要针对水基切削液)在使用中经常出现杂油、颗粒等问题。这些杂油主要由工件带入或者机床液压油、导轨油泄露造成。传统的机床都自带油水分离操作,利用钢带除油机将使用过的切削液中的油分离出来,但是处理速度慢而且效果有限,致使厚厚的油层悬浮于液体表面,时间久了滋生微生物影响切削液性能。Cutting fluid is a metal working fluid used to cool and lubricate in the process of cutting, grinding and grinding. There are many kinds and complex components, usually including base oil, emulsifier, rust inhibitor, etc. Cutting fluids (mainly for water-based cutting fluids) often have problems such as miscellaneous oils and particles during use. These miscellaneous oils are mainly caused by the introduction of workpieces or the leakage of hydraulic oil and guide rail oil of machine tools. Traditional machine tools have their own oil-water separation operation. The steel belt degreaser is used to separate the oil in the used cutting fluid, but the processing speed is slow and the effect is limited, resulting in a thick oil layer suspended on the surface of the liquid, which breeds for a long time. Microorganisms affect cutting fluid performance.
脱模剂是压铸生产中必不可少的辅助材料,在压铸生产过程中,为提高模具型腔的使用寿命,并使压铸件顺利脱模,保证压铸件表面光洁、轮廓清晰完整,必须“脱模剂”,在压铸生产中,大量的脱模剂会被喷到模具上,部分脱模剂在高温下蒸发,部分吸附在模具上使用消耗,而大部分则一次性使用后直接流入模具下方,成为含油废液,一般通过压铸机下方地沟收集再进行后续处理。Release agent is an indispensable auxiliary material in die-casting production. In the process of die-casting production, in order to improve the service life of the mold cavity, make the die-casting part demold smoothly, and ensure the surface of the die-casting part is smooth and clean, the contour is clear and complete, it must be "released". "Molding agent", in the production of die casting, a large amount of release agent will be sprayed on the mold, some of the release agent will evaporate at high temperature, some will be absorbed on the mold for consumption, and most will flow directly under the mold after one-time use , which becomes oily waste liquid, which is generally collected through the ditch below the die-casting machine for subsequent treatment.
脱脂工序是汽车涂装前处理工艺的一个基本工序,白车身经过焊接之后,车身内外表面和内腔都有很多污油,包括冷却油、抗拉伸油和防锈油等。脱脂工艺出现问题,会影响电泳漆的质量,进而影响漆膜的附着力和耐腐蚀性。随着生产线上过车量日益增多,脱脂液含油量也增多,污油处理不干净电泳槽会被污染,甚至导致涂装车间停产整顿,所以要将脱脂槽液取出进行油水分离操作。The degreasing process is a basic process in the pre-treatment process of automobile painting. After the body-in-white is welded, there are many dirty oils on the inner and outer surfaces and inner cavities of the body, including cooling oil, anti-stretching oil and anti-rust oil. Problems in the degreasing process will affect the quality of the electrophoretic paint, which in turn affects the adhesion and corrosion resistance of the paint film. With the increasing number of vehicles passing on the production line, the oil content of the degreasing solution also increases. If the dirty oil is not cleanly treated, the electrophoresis tank will be polluted, and even lead to the shutdown of the painting workshop for rectification. Therefore, the degreasing tank solution should be taken out for oil-water separation operation.
切削液、脱模剂和脱脂剂净化回用处理一方面可以节约生产加工成本,另一方面可以减少危险废物的排放量,实现绿色清洁生产。净化回用处理的主要目的是把混入其中的杂油分离出来,常见的油水分离方法有物理分离法和化学分离法,物理法是通过油和水的密度差或吸附、过滤的方式,将水中混入的油除去,主要方法有加热分离法、过滤分离法、气浮分离法、超滤膜分离法、反渗透分离法、聚结分离法和离心分离法等;化学分离主法要是通过破乳剂实现破乳,由于会添加药剂会影响待处理液成分,增加分离难度,一般不采用。The purification and reuse of cutting fluid, mold release agent and degreasing agent can save production and processing costs on the one hand, and reduce the discharge of hazardous wastes on the other hand to achieve green and clean production. The main purpose of purification and reuse treatment is to separate the miscellaneous oil mixed into it. Common oil-water separation methods include physical separation method and chemical separation method. The main methods for removing the mixed oil are heating separation method, filtration separation method, air flotation separation method, ultrafiltration membrane separation method, reverse osmosis separation method, coalescence separation method and centrifugal separation method; the main method of chemical separation is through demulsifier To achieve demulsification, it is generally not used because the addition of chemicals will affect the composition of the liquid to be treated and increase the difficulty of separation.
以下为目前常见的分离方法:The following are the most common separation methods:
上述各种分离方法的不足在于:The shortcomings of the above-mentioned separation methods are:
1.加热分离法采用蒸汽或加热装置进行破乳,设备简单、投资少,但是除油效果差、能耗大;1. The heating separation method adopts steam or heating device for demulsification, the equipment is simple and the investment is low, but the oil removal effect is poor and the energy consumption is large;
2.重力或气浮分离根据油水密度或浮力不同,方法简单,除油效果稳定,但是所需时间长;2. Gravity or air flotation separation is based on the density or buoyancy of oil and water, the method is simple, and the oil removal effect is stable, but it takes a long time;
3.聚结分离通过粗粒化材料,使分散于水中的油分聚集增大,直至浮力大于黏附力而上浮,设备简单,投资少,聚并材料使用周期较长,但是需要根据不同的含油废液选择不用的聚结填料,大大降低了方法的适应性;3. Coalescing and separation Through the coarse-grained material, the oil content dispersed in the water increases, until the buoyancy is greater than the adhesion force and floats up. The equipment is simple, the investment is low, and the use period of the coalescing material is long, but it needs to be based on different oily wastes. The use of coalescing fillers that are not used in the liquid selection greatly reduces the adaptability of the method;
4.利用中空纤维膜的选择透过性原理,油水分离效果好,但是会同时去除部分有效成分、成本高、投资大、设备复杂操作难;4. Using the selective permeability principle of hollow fiber membrane, the oil-water separation effect is good, but it will remove some active ingredients at the same time, high cost, large investment, and complicated equipment operation is difficult;
5.过滤分离一般采用亲油性材料吸附溶液中的油分,出液水质好,设备小型化且操作简单,但是设备投资高,滤料滤袋再生困难;5. Filtration and separation generally use lipophilic materials to absorb the oil in the solution, the effluent water quality is good, the equipment is miniaturized and the operation is simple, but the equipment investment is high, and the regeneration of the filter material and filter bag is difficult;
6.离心分离法利用快速旋转产生的离心力,使密度大的水沿环状路径流向外侧,密度小的油抛向内圈,并聚形成大的油珠而上浮分离,但日常维护困难,有可能破坏待处理液有效成分。6. Centrifugal separation method uses centrifugal force generated by rapid rotation to make water with high density flow to the outside along the annular path, while oil with low density is thrown to the inner ring, and aggregates to form large oil droplets and floats up and separates, but daily maintenance is difficult and there are May destroy the active ingredients of the liquid to be treated.
发明内容SUMMARY OF THE INVENTION
为解决上述现有技术方案中的不足,本发明提供了一种分离效果好、自动化、分离准确、多功能的不相溶液体的分离装置。In order to solve the deficiencies in the above-mentioned prior art solutions, the present invention provides a separation device for immiscible liquid with good separation effect, automation, accurate separation and multi-function.
本发明的目的是通过以下技术方案实现的:The purpose of this invention is to realize through the following technical solutions:
不相溶液体的分离装置,所述不相溶液体的分离装置包括封闭的容器,所述容器具有第一进口、第二进口、第一出口和第二出口,自上而下地,所述第二进口、第一出口和第二出口依次排列;Separation device for immiscible liquid, the separation device for immiscible liquid includes a closed container, the container has a first inlet, a second inlet, a first outlet and a second outlet, from top to bottom, the first The second inlet, the first outlet and the second outlet are arranged in sequence;
所述不相溶液体的分离装置还包括:The device for separating the immiscible liquid also includes:
风机,所述风机连接切换单元;a fan, the fan is connected to the switching unit;
切换单元,所述切换单元具有第一端口、第二端口、第三端口和第四端口;所述第一端口选择性地连通第二端口和第四端口,所述第三端口选择性地连通第二端口和第四端口;所述风机的输入端连通所述第四端口,输出端连通第二端口;所述第一端口连通外界,第三端口连通所述第二进口;a switching unit, the switching unit has a first port, a second port, a third port and a fourth port; the first port selectively communicates with the second port and the fourth port, and the third port selectively communicates The second port and the fourth port; the input end of the fan communicates with the fourth port, and the output end communicates with the second port; the first port communicates with the outside world, and the third port communicates with the second inlet;
浮力件,所述浮力件在容器内上升时封堵所述第二进口,下降时打开所述第二进口;a buoyancy piece, the buoyancy piece blocks the second inlet when it rises in the container, and opens the second inlet when it falls;
导轨,所述浮力件随着所述容器内液面变化而沿着所述导轨上下运动;a guide rail, the buoyant member moves up and down along the guide rail as the liquid level in the container changes;
阀,所述阀控制所述第一进口的开启和关闭:当所述第一端口和第四端口连通,及第二端口和第三端口连通时,第一进口关闭;当所述第一端口和第二端口连通,及第三端口和第四端口连通时,第一进口开启。a valve that controls the opening and closing of the first inlet: when the first port is in communication with the fourth port, and the second port is in communication with the third port, the first inlet is closed; when the first port is in communication When communicating with the second port, and when the third port is communicating with the fourth port, the first inlet is opened.
与现有技术相比,本发明具有的有益效果为:Compared with the prior art, the present invention has the following beneficial effects:
1.分离快速、效果好;1. The separation is fast and the effect is good;
创造性地利用了风机和切换单元的组合,使得封闭的容器内根据需要地调整压力:The combination of the fan and the switching unit is creatively used, so that the pressure in the closed container can be adjusted as needed:
当切换单元的第一端口连通第二端口,以及第三端口连通第四端口时,第二进口为开启状态,阀自动打开,废液通过第一进口进入封闭的容器内,废液中不相溶的液体快速分离,密度较小的液体上浮到上层,密度较大的液体下沉到下层,不相溶液体分离快速,且分离效果好;When the first port of the switching unit is connected to the second port, and the third port is connected to the fourth port, the second inlet is in an open state, the valve is automatically opened, and the waste liquid enters the closed container through the first inlet, and the waste liquid is not in phase. The dissolved liquid is quickly separated, the liquid with lower density floats to the upper layer, and the liquid with higher density sinks to the lower layer, the separation of immiscible liquid is fast, and the separation effect is good;
2.自动化;2. Automation;
创造性地利用了浮力件和第二进口的组合,使得当切换单元的第一端口连通第二端口,以及第三端口连通第四端口时,阀自动开启第一进口,容器内液面上升,而随着封闭容器内液面上升的浮力件自动地封堵了第二进口,无需人工关闭第二进口,实现了自动化控制;The combination of the buoyancy member and the second inlet is creatively used, so that when the first port of the switching unit is connected to the second port and the third port is connected to the fourth port, the valve automatically opens the first inlet, the liquid level in the container rises, and the With the rising liquid level in the closed container, the buoyancy element automatically blocks the second inlet, and there is no need to manually close the second inlet, and automatic control is realized;
另,当切换单元的第一端口连通第四端口,以及第三端口连通第二端口时,浮力件脱离第二进口,阀自动关闭第一进口,容器内液面下降,从而排出容器内的下层密度较大的液体,且可以排到较高的位置(位置高于液面的位置),无需人工开启第二进口,实现了自动化控制;In addition, when the first port of the switching unit is connected to the fourth port, and the third port is connected to the second port, the buoyant member is separated from the second inlet, the valve automatically closes the first inlet, and the liquid level in the container drops, thereby discharging the lower layer in the container The liquid with higher density can be discharged to a higher position (a position higher than the liquid level), without the need to manually open the second inlet, and realize automatic control;
3.分离准确;3. Accurate separation;
利用观察窗,实时观察容器内液面的上升以及液体的分层效果,当液面不再上升,且不相溶液体的分离完成后,第一出口基本处于上下层液体的分界处,利用第一出口排出容器内第一出口上方的上层液体;Use the observation window to observe the rise of the liquid level in the container and the stratification effect of the liquid in real time. When the liquid level no longer rises and the separation of the incompatible liquid is completed, the first outlet is basically at the boundary between the upper and lower liquids. An outlet discharges the upper layer liquid above the first outlet in the container;
之后,切换单元的第一端口连通第四端口,以及第三端口连通第二端口,浮力件脱离第二进口,下层液体通过第二出口排出;Afterwards, the first port of the switching unit communicates with the fourth port, and the third port communicates with the second port, the buoyant member is separated from the second inlet, and the lower layer liquid is discharged through the second outlet;
4.多功能;4. Multifunctional;
利用滚轮,实现了容器的可移动;利用过滤单元,实现了对废液的过滤,截留了颗粒物,保证了分离后液体的洁净度。The use of rollers realizes the movement of the container; the use of filter units realizes the filtration of waste liquid, retains particulate matter, and ensures the cleanliness of the liquid after separation.
附图说明Description of drawings
参照附图,本发明的公开内容将变得更易理解。本领域技术人员容易理解的是:这些附图仅仅用于举例说明本发明的技术方案,而并非意在对本发明的保护范围构成限制。图中:The disclosure of the present invention will become more easily understood with reference to the accompanying drawings. Those skilled in the art can easily understand that these drawings are only used to illustrate the technical solutions of the present invention, and are not intended to limit the protection scope of the present invention. In the picture:
图1是根据本发明实施例的不相溶液体的分离装置的结构简图。FIG. 1 is a schematic structural diagram of a separation device for immiscible liquids according to an embodiment of the present invention.
具体实施方式Detailed ways
图1和以下说明描述了本发明的可选实施方式以教导本领域技术人员如何实施和再现本发明。为了教导本发明技术方案,已简化或省略了一些常规方面。本领域技术人员应该理解源自这些实施方式的变型或替换将在本发明的范围内。本领域技术人员应该理解下述特征能够以各种方式组合以形成本发明的多个变型。由此,本发明并不局限于下述可选实施方式,而仅由权利要求和它们的等同物限定。Figure 1 and the following description describe alternative embodiments of the invention to teach those skilled in the art how to implement and reproduce the invention. In order to teach the technical solutions of the present invention, some conventional aspects have been simplified or omitted. Those skilled in the art will appreciate that variations or substitutions from these embodiments will fall within the scope of the present invention. Those skilled in the art will appreciate that the following features can be combined in various ways to form various variations of the invention. Thus, the present invention is not limited to the alternative embodiments described below, but only by the claims and their equivalents.
实施例1:Example 1:
图1示意性地给出了本发明实施例的不相溶液体的分离装置的结构简图,如图1所示,所述不相溶液体的分离装置包括:Fig. 1 schematically shows the structure diagram of the separation device for immiscible liquid according to the embodiment of the present invention. As shown in Fig. 1 , the separation device for immiscible liquid includes:
封闭的容器11,所述容器具有第一进口21、第二进口22、第一出口和第二出口,自上而下地,所述第二进口、第一出口和第二出口依次排列;第一进口21和第二进口22可设置在所述容器的顶壁;The
风机31,所述风机31连接切换单元32;A
切换单元32,所述切换单元32具有第一端口、第二端口、第三端口和第四端口;所述第一端口选择性地连通第二端口和第四端口,所述第三端口选择性地连通第二端口和第四端口;所述风机的输入端连通所述第四端口,输出端连通第二端口;所述第一端口连通外界,第三端口连通所述第二进口;a
浮力件51,如浮球,所述浮力件51在容器内上升时封堵所述第二进口22,下降时打开所述第二进口22;The
导轨52,所述浮力件51随着所述容器11内液面变化而沿着所述导轨52上下运动;a
阀41,所述阀41控制所述第一进口21的开启和关闭:当所述第一端口和第四端口连通,及第二端口和第三端口连通时,第一进口21关闭;当所述第一端口和第二端口连通,及第三端口和第四端口连通时,第一进口21开启。
为了实现第一进口的自动开启和自动关闭,进一步地,所述第一阀包括:In order to realize automatic opening and automatic closing of the first inlet, further, the first valve includes:
封板,所述封板用于封堵所述第一进口,设置在所述容器内,且所述封板的一端与所述容器连接。A sealing plate, which is used to block the first inlet, is arranged in the container, and one end of the sealing plate is connected to the container.
为了提高了封板和第一进口间的密封程度,进一步地,所述封板的与所述第一进口接触的部分采用柔性材料。In order to improve the sealing degree between the sealing plate and the first inlet, further, the part of the sealing plate that is in contact with the first inlet is made of flexible material.
为了控制容器内分离后的上层液体和下层液体的排放,进一步地,所述不相溶液体的分离装置还包括:In order to control the discharge of the separated upper layer liquid and lower layer liquid in the container, further, the separation device for the immiscible liquid also includes:
另设的阀42-43,所述另设的阀分别连通所述第一出口和第二出口。Separately provided valves 42-43 communicate with the first outlet and the second outlet respectively.
为了截留废液中的颗粒物,进一步地,所述不相溶液体的分离装置还包括:In order to retain the particulate matter in the waste liquid, further, the separation device for the immiscible liquid also includes:
过滤单元81,所述过滤单元81的进口适于连通废液,出口连通所述第一进口21。The
为了约束浮力件的上下移动及左右移动,进一步地,自上而下地,所述导轨51围出区域的内径R不变或逐渐变大,且R≥R0,R0为所述浮力件51的外径。In order to constrain the up-and-down movement and the left-right movement of the buoyant member, further, from top to bottom, the inner diameter R of the area enclosed by the
为了提高分离装置的移动便利性,进一步地,所述不相溶液体的分离装置还包括:In order to improve the moving convenience of the separation device, further, the separation device for the immiscible liquid further includes:
滚轮71,所述滚轮71设置在所述容器11的底部。A
为了实时观察不相溶液体的分离效果,进一步地,所述不相溶液体的分离装置还包括:In order to observe the separation effect of the immiscible liquid in real time, further, the separation device of the immiscible liquid also includes:
观察窗61,所述观察窗61采用透过可见光的材料,并设置在所述容器11的侧壁。The
实施例2:Example 2:
根据本发明实施例的不相溶液体的分离装置的应用例,如切削液、脱模剂、脱脂槽液处理中的油水分离。The application examples of the separation device for immiscible liquids according to the embodiments of the present invention are the separation of oil and water in the treatment of cutting fluids, mold release agents, and degreasing bath fluids.
在本应用例中,如图1所示,过滤单元81设置在容器11的上部,采用不锈钢过滤网,滤径不小于0.1μm;废液依次经过过滤网和第一进口21,之后进入容器11内分离;阀41设置在所述容器11的内部,且处于第一进口21的下侧;封板的外缘套有柔性的密封材料,封板的一侧连接容器内壁,在自由状态下,封板和第一进口间的夹角为锐角,如30度、45度、60度,优选小于45度的锐角;导轨52采用具有通孔的筒形结构,保证筒形内外连通,内径R不变或逐渐变大,且R≥R0,如R=1.1R0,R0为所述浮力件的外径,R0≥R1,R1为所述第二进口的内径;第一出口和第二出口处分别连通阀门42-43,滚轮71安装在容器的底部;在容器的临着常规的容器内上层液体和下层液体分界处附近的侧壁设有透明的观察窗61;浮力件51采用浮球。In this application example, as shown in FIG. 1 , the
本实施例的不相溶液体的分离装置的工作方式为:The working mode of the separation device of the immiscible liquid of the present embodiment is:
进液步骤:Inlet steps:
切换单元32的第一端口连通第二端口,以及第三端口连通第四端口,风机31工作,第二进口为开启状态;同时,封板下降,与第一进口间的夹角变大,阀41自动开启第一进口21,容器11内的压力小于容器外的压力;The first port of the switching
废液经过过滤单元81,之后通过第一进口21进入封闭的容器11内,废液中不相溶的液体快速分离,密度较小的液体上浮到上层,密度较大的液体下沉到下层,不相溶液体分离快速,且分离效果好;The waste liquid passes through the
随着容器内液面的上升,在导轨52围成区域内上升的浮球封堵了第二进口22;As the liquid level in the container rises, the floating ball rising in the area enclosed by the
排液步骤:Draining steps:
利用观察窗61实时查看容器11内的液体分离情况和液面上升情况,当分离完成后;打开阀门42,容器内第一出口上方的上层液体通过第一出口排出;鉴于每次进液量基本一致,决定了容器内液面位置的确定性,也即上层液体和下层液体分界处的确定性,第一出口设置在所述分界处;Use the
待上层液体排完后,切换单元32的第一端口连通第四端口,以及第三端口连通第二端口,风机31工作,浮力件51脱离第二进口22,封板上移,与第一进口间的夹角逐渐变小,阀自动关闭第一进口,容器内的压力大于容器外的压力;After the upper layer liquid is discharged, the first port of the switching
阀门43打开,第二出口与外界连通;容器11内液面下降,从而排出容器内的下层密度较大的液体,且可以排到较高的位置(位置高于液面的位置);The
利用滚轮71实现了分离装置的移动;The movement of the separation device is realized by using the
当需要维护时,打开过滤单元81,清理集聚在过滤网一侧的颗粒物。When maintenance is required, open the
根据本发明应用例达到的益处在于:利用风机和切换单元、第一进口及第二进口的组合,容器内的压力小于外界压力,提高了容器内不相溶液体的分离速度以及分离效果;并实现了第一进口和第二进口的自动开启和自动关闭;第一进口的位置基于处于容器内上层液体和下层液体的分界处,准确地排出容器内分离出的上层液体。The benefits achieved according to the application example of the present invention are: using the combination of the fan, the switching unit, the first inlet and the second inlet, the pressure in the container is lower than the external pressure, which improves the separation speed and separation effect of the immiscible liquid in the container; and The automatic opening and closing of the first inlet and the second inlet are realized; the position of the first inlet is based on the boundary between the upper liquid and the lower liquid in the container, and the upper liquid separated in the container is accurately discharged.
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| CN111825233A (en) * | 2020-08-24 | 2020-10-27 | 兰州交通大学 | A centrifugal water purification device |
| CN119186204A (en) * | 2024-11-14 | 2024-12-27 | 中国华能集团清洁能源技术研究院有限公司 | Carbon dioxide trapping device and carbon dioxide trapping system with same |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111825233A (en) * | 2020-08-24 | 2020-10-27 | 兰州交通大学 | A centrifugal water purification device |
| CN119186204A (en) * | 2024-11-14 | 2024-12-27 | 中国华能集团清洁能源技术研究院有限公司 | Carbon dioxide trapping device and carbon dioxide trapping system with same |
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