CN110658125A - Core holder for slurry dynamic pollution experiment - Google Patents

Core holder for slurry dynamic pollution experiment Download PDF

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Publication number
CN110658125A
CN110658125A CN201911106072.3A CN201911106072A CN110658125A CN 110658125 A CN110658125 A CN 110658125A CN 201911106072 A CN201911106072 A CN 201911106072A CN 110658125 A CN110658125 A CN 110658125A
Authority
CN
China
Prior art keywords
sleeve
diaphragm
plug
core holder
pollution experiment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911106072.3A
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Chinese (zh)
Inventor
米中荣
何冰
袁浩
周长江
韩炜
岑玉达
符奇
徐兵
杨鸿�
黄凯
万传治
张春琳
刘家材
张小平
杜新龙
李辰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu North Petroleum Exploration & Development Technology Ltd
Original Assignee
Chengdu North Petroleum Exploration & Development Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chengdu North Petroleum Exploration & Development Technology Ltd filed Critical Chengdu North Petroleum Exploration & Development Technology Ltd
Priority to CN201911106072.3A priority Critical patent/CN110658125A/en
Publication of CN110658125A publication Critical patent/CN110658125A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/0806Details, e.g. sample holders, mounting samples for testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample

Abstract

The invention discloses a rock core holder for a mud dynamic pollution experiment, which comprises a sleeve, a first plug and a second plug, wherein the first plug and the second plug are detachably connected to two ends of the sleeve, a diaphragm is arranged in the sleeve and surrounds a cylindrical structure coaxial with the sleeve, a hollow area formed by the diaphragm in a surrounding mode is a rock core holding area, a confining pressure area is arranged between the outer wall of the diaphragm and the inner wall of the sleeve, and a pressurizing opening communicated with the confining pressure area is arranged on the surface of the sleeve. The invention aims to provide a rock core holder for a dynamic slurry pollution experiment, which aims to solve the problems of large error and limited accuracy in the simulation of the dynamic slurry pollution experiment in the prior art, and achieves the purposes of providing a special rock core holder for the dynamic slurry pollution experiment and improving the accuracy of objective parameters in the simulation experiment process.

Description

Core holder for slurry dynamic pollution experiment
Technical Field
The invention relates to the field of stratum evaluation of oil and gas fields, in particular to a core holder for a mud dynamic pollution experiment.
Background
The core holder is an appliance used for holding and protecting a rock sample and sealing a cylindrical surface or an end surface (generally an end surface with a reserved fluid inlet and outlet) when the seepage characteristics of the rock sample are measured in a laboratory or a displacement test is carried out, and is an indispensable important auxiliary component in the development of experimental instrument devices. According to the conventional rock core holder, confining pressure is simulated through a rigid shell, and stratum confining pressure can be simulated for conventional measurement of physical parameters such as rock core permeability and porosity, so that the requirement is met. However, with the continuous deepening of the knowledge of the stratum and the continuous refinement of the development and planning of the oil and gas field, the pollution and damage of the drilling fluid (mud) to the stratum around the wellbore have become a main research subject for increasing the yield of the oil and gas field. Wherein, the traditional skin coefficient is calculated by a formula; the existing mud pollution experiment applies rigid confining pressure and static wellbore pressure to a full-diameter core for simulation. Comprehensively, the difficulty of the research on the mechanism of the full-diameter core slurry pollution injury in the prior art is that the size of a core holder is large, and the simulation difficulty of sealing and slurry dynamic circulation is large, so that the simulation accuracy is limited.
Disclosure of Invention
The invention aims to provide a rock core holder for a dynamic slurry pollution experiment, which aims to solve the problems of large error and limited accuracy in the simulation of the dynamic slurry pollution experiment in the prior art, and achieves the purposes of providing a special rock core holder for the dynamic slurry pollution experiment and improving the accuracy of objective parameters in the simulation experiment process.
The invention is realized by the following technical scheme:
a rock core holder for mud dynamic pollution experiment, including the sleeve, can dismantle first end cap, the second end cap of connection at sleeve both ends, set up the diaphragm in the sleeve, the diaphragm encloses into the tubular structure coaxial with the sleeve, and the diaphragm is the rock core clamping area around the hollow region who forms, is confining pressure district between diaphragm outer wall and the sleeve inner wall, sleeve surface set up with the pressure port of confining pressure district intercommunication.
Aiming at the problems of large error and limited accuracy in the simulation of a dynamic slurry pollution experiment in the prior art, the invention provides the core holder for the dynamic slurry pollution experiment. In the prior art, a core holder provides a simulated confining pressure for a core through a rigid sleeve or a shell, the simulation mode is substantially to see a reservoir surrounding rock as a fully compact lithology approaching a pure rigid body, however, in a mud dynamic pollution experiment, dynamic mud is required to act on the surface of the core to test the pollution rate and degree of the core, in the process, the actual size of the confining pressure influences the permeation rate of the mud in the core, and the prior art ignores the point. For this reason, this application sets up the diaphragm in the sleeve, and the diaphragm encloses into the tubular structure coaxial with the sleeve, is the confined pressure district between diaphragm outer wall and the sleeve inner wall. This application is when using, pack into the core in the sleeve and make the core be located the diaphragm inside, pressurize in to the confined pressure district through the pressurization mouth for pressure in the confined pressure district reaches actual reservoir confined pressure, and the confined pressure is pressed the diaphragm on surveyed core surface, thereby realizes the purpose of more accurate simulation reservoir actual conditions, makes the accuracy of mud dynamic pollution experiment greatly improve. The diaphragm in this application has the ductility, consequently can ensure under the confining pressure effect of artifical application, with the inseparable effect of pasting on the rock core surface of diaphragm, realizes transmitting the confining pressure to being surveyed the rock core through the diaphragm on. Preferably, the diaphragm is a non-porous and waterproof rubber sheet or a silica gel sheet. Preferably, the diaphragm in this application surrounds the inner diameter of the cylindrical structure formed, corresponding to the coring inner diameter of the coring barrel used.
Further, sleeve both ends all set up the convex annular boss of orientation sleeve inside direction, the diaphragm is fixed on annular boss. This scheme is passed through the annular boss that the sleeve both ends inwards stretched out, for the diaphragm provides the installation station, ensures the relatively fixed between diaphragm and the sleeve. Simultaneously, through the annular bosses at the two ends, a more stable installation station is provided for the first plug and the second plug, and mutual interference between the plugs and the diaphragm is avoided.
Furthermore, the diaphragm is fixedly connected with the surface of one side, which is radially outward, of the annular boss. The diaphragm is connected at the radial lateral surface outwards of annular boss promptly to make confined pressure district pressurization back, the confined pressure can be with the inseparable pressure of diaphragm on the annular boss at both ends, realize the self-sealing effect through the cooperation of confined pressure and diaphragm, and then solved prior art, in the full diameter rock core mud dynamic pollution experimentation, the problem of the sealed difficulty of rock core holder. In this scheme, the confined pressure that applys is big more, and sealed effect is better.
Further, the diaphragm comprises a cylindrical main body part, and two ends of the main body part are sealing parts; the outer diameters of the main body part and the sealing part are equal, and the inner diameter of the main body part is smaller than that of the sealing part; the two ends of the main body part are respectively abutted against the annular bosses at the two ends, and the inner wall of the sealing part is attached to the surface of one side, facing outwards in the radial direction, of the annular boss. That is to the diaphragm, the main part is thicker, and the sealing is thinner, and the annular boss that leans on both ends respectively at the both ends of main part ensures sealedly, and the sealing pastes at the radial outside lateral surface of annular boss to make fully to wrap up between the tip of diaphragm and annular boss, no matter be the terminal surface of annular boss, or its lateral surface, all can fully contact with the diaphragm, thereby eliminate the gap, further improve the sealing performance of this application.
Further, the sealing part is bonded with the annular boss or/and connected with the annular boss through a bolt. The best mode is that firstly, the whole body is bonded between the two curved surfaces, and then, the bolt is used for further fastening. The bonding mode can further eliminate the gap and improve the sealing capability, and the bolt connection mode can ensure relative fixation.
Furthermore, one end, facing the inside of the sleeve, of the first plug is provided with a circle of annular gap, and one end of the main body part is abutted to the inside of the annular gap. In order to avoid sealing failure between first end cap and the sleeve, this scheme sets up round annular breach towards the inside one end of sleeve at first end cap, and the one end of the main part of diaphragm is supported and is held together in the annular breach, and the one end of diaphragm main part fills completely promptly in the annular breach, comes the gap on the terminal surface including first end cap of shutoff and sleeve through the terminal surface of main part, and under the confining pressure effect, can also be in with the main part pressure on the annular breach, all realize sealedly in the follow each side, show to improve and realize the effect of self sealedly through the diaphragm. In the scheme, one end of the first plug in the direction is used as the outlet end of the rock core holder.
Furthermore, after the first plug and the end part of the sleeve are connected in place, the outer end of the first plug along the axis direction is flush with the end part of the sleeve, and the outer end of the annular gap along the axis direction is flush with the corresponding annular boss. After first end cap installation is accomplished promptly, satisfy first end cap and flush along the outer end and the sleeve tip of axis direction, annular breach and annular boss also flush to make the tip of diaphragm main part can be supported and close up on the stable plane that annular breach and annular boss formed, avoid the diaphragm main part to support and close up the problem that the position is uneven leads to sealed inefficacy.
Furthermore, one end face, facing the interior of the sleeve, of the second plug is in contact with one end of the main body part along the axis direction. Similarly, the end face gap of the second plug is plugged through the end part of the main body part, and the sealing effect of one end of the second plug is improved. Preferably, one end of the main body part close to the second plug is partially in contact with the second plug and partially in contact with the annular boss on the side, so that the gap between the second plug and the annular boss is plugged through the main body part.
Furthermore, a liquid outlet channel is arranged on the first plug, and two circulating channels are arranged on the second plug. According to the scheme, one end where the second plug is located is used as a first end close to the shaft, and one end where the first plug is located is used as an end far away from the shaft; in order to match with a mud dynamic pollution experiment, two circulating channels are arranged on the second plug, so that the drilling fluid can be conveniently circulated to simulate a dynamic pollution process. The first plug is provided with a liquid outlet channel which is convenient for containing and measuring the filtered drilling fluid.
Further, the second end cap sets up the anti-compression ring towards the inside one end of sleeve, anti-compression ring and diaphragm interference fit, two circulation channel all communicate to the anti-compression ring around in the region that forms. Two circulation passage all communicate to the resistance to compression ring around the regional in that forms, therefore the dynamic simulation of mud is accomplished in resistance to compression ring is inside, in order to avoid artifical confined pressure of exerting in this application to disturb the mud flow state, influence mud dynamic simulation process, this scheme sets up the resistance to compression ring, resistance to compression ring and diaphragm interference fit to keep apart with the diaphragm through the mud of resistance to compression ring in with the experimentation, avoid confined pressure to act on dynamic mud. Preferably, this scheme is when using, and the one end of putting into the rock core is supported and is held up on the compression ring terminal surface, can improve the stability of rock core in the experimentation through the compression ring.
Compared with the prior art, the invention has the following advantages and beneficial effects:
1. the core holder for the mud dynamic pollution experiment is characterized in that a core is arranged in a sleeve, the core is positioned in a diaphragm, a pressure is applied to a confining pressure area through a pressure application port, the pressure in the confining pressure area reaches the actual reservoir confining pressure, the diaphragm is pressed on the surface of the measured core through the confining pressure, and therefore the purpose of accurately simulating the actual condition of the reservoir is achieved, and the accuracy of the mud dynamic pollution experiment is greatly improved.
2. According to the core holder for the mud dynamic pollution experiment, after the confining pressure area is pressurized, the confining pressure can tightly press the diaphragm on the annular bosses at two ends, and the automatic sealing effect is realized through the cooperation of the confining pressure and the diaphragm, so that the problem that the core holder is difficult to seal in the full-diameter core mud dynamic pollution experiment process in the prior art is solved.
3. According to the core holder for the mud dynamic pollution experiment, two ends of the main body part of the diaphragm respectively abut against the annular bosses at two ends to ensure sealing, and the sealing part is attached to the surface of the radially outward side of the annular boss, so that the diaphragm and the end part of the annular boss are fully wrapped, the end surface of the annular boss or the outer side surface of the annular boss can be fully contacted with the diaphragm, gaps are eliminated, and the sealing performance of the core holder is further improved.
4. The core holder for the mud dynamic pollution experiment is characterized in that an anti-compression ring is specially arranged to avoid the interference of manually applied confining pressure on the mud flow state and the influence on the mud dynamic simulation process, and the anti-compression ring is in interference fit with a diaphragm, so that the mud and the diaphragm in the experiment process are isolated through the anti-compression ring, and the confining pressure is prevented from acting on the dynamic mud.
Drawings
The accompanying drawings, which are included to provide a further understanding of the embodiments of the invention and are incorporated in and constitute a part of this application, illustrate embodiment(s) of the invention and together with the description serve to explain the principles of the invention. In the drawings:
FIG. 1 is a cross-sectional view of an embodiment of the present invention;
FIG. 2 is a schematic view of a diaphragm in an embodiment of the present invention.
Reference numbers and corresponding part names in the drawings:
1-sleeve, 2-first plug, 201-annular gap, 3-second plug, 4-diaphragm, 401-main body part, 402-sealing part, 5-core holding area, 6-confining area, 7-pressurizing port, 8-liquid outlet channel, 9-circulating channel, 10-annular boss, 11-bolt and 12-compression-resistant ring.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail below with reference to examples and accompanying drawings, and the exemplary embodiments and descriptions thereof are only used for explaining the present invention and are not meant to limit the present invention.
Example 1:
the core holder for the mud dynamic pollution experiment as shown in fig. 1 and 2 comprises a sleeve 1, a first plug 2 and a second plug 3 which are detachably connected to two ends of the sleeve 1, wherein a diaphragm 4 is arranged in the sleeve 1, the diaphragm 4 surrounds a cylindrical structure coaxial with the sleeve 1, a hollow area formed by the diaphragm 4 in a surrounding mode is a core holding area 5, a confining pressure area 6 is arranged between the outer wall of the diaphragm 4 and the inner wall of the sleeve 1, and a pressurizing opening 7 communicated with the confining pressure area 6 is arranged on the surface of the sleeve 1.
In this embodiment, the diaphragm 4 is made of an elastic silica gel sheet, and the pressure gauge for monitoring the pressure in the pressure surrounding area 6 is arranged on the pressure port 7, and the pressure port can be closed.
Example 2:
as shown in fig. 1 and 2, in the core holder for the dynamic slurry contamination experiment, on the basis of embodiment 1, annular bosses 10 protruding toward the inner direction of the sleeve 1 are respectively disposed at two ends of the sleeve 1, and the membrane 4 is fixed on the annular bosses 10. The diaphragm 4 is fixedly connected with one side surface of the annular boss 10 which is radially outward. The diaphragm 4 includes a cylindrical main body 401, and both ends of the main body 401 are sealed portions 402; the outer diameters of the main body part 401 and the sealing part 402 are equal, and the inner diameter of the main body part 401 is smaller than that of the sealing part 402; the two ends of the main body part 401 respectively abut against the annular bosses 10 at the two ends, and the inner wall of the sealing part 402 is attached to the surface of one side of the annular boss 10 facing outwards in the radial direction. The sealing part 402 is bonded to the annular boss 10 or/and connected by bolts 11. One end of the first plug 2 facing the inside of the sleeve 1 is provided with a circle of annular gap 201, and one end of the main body part 401 is abutted to the annular gap 201. After the end part of the sleeve 1 is connected with the first plug 2 in place, the outer end of the first plug 2 in the axis direction is flush with the end part of the sleeve 1, and the outer end of the annular gap 201 in the axis direction is flush with the corresponding annular boss 10. One end surface of the second plug 3 facing the inside of the sleeve 1 is in contact with one end of the main body 401 in the axial direction.
Preferably, the first plug 2 is provided with a liquid outlet channel 8, and the second plug 3 is provided with two circulation channels 9. One end of the second plug 3 facing the interior of the sleeve 1 is provided with an anti-compression ring 12, the anti-compression ring 12 is in interference fit with the diaphragm, and the two circulation channels 9 are communicated to the area formed by the anti-compression ring 12 in a surrounding mode.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are merely exemplary embodiments of the present invention, and are not intended to limit the scope of the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.

Claims (10)

1. A rock core holder for mud dynamic pollution experiment, including sleeve (1), can dismantle first end cap (2), second end cap (3) of connection at sleeve (1) both ends, its characterized in that, set up diaphragm (4) in sleeve (1), diaphragm (4) enclose into the tubular structure coaxial with sleeve (1), and diaphragm (4) are rock core clamping area (5) around the hollow region who forms, are confined pressure district (6) between diaphragm (4) outer wall and sleeve (1) inner wall, sleeve (1) surface set up with pressure port (7) of confined pressure district (6) intercommunication.
2. The core holder for the mud dynamic pollution experiment is characterized in that two ends of the sleeve (1) are respectively provided with an annular boss (10) protruding towards the inner direction of the sleeve (1), and the diaphragm (4) is fixed on the annular bosses (10).
3. The core holder for the mud dynamic pollution experiment is characterized in that the diaphragm (4) is fixedly connected with one side surface of the annular boss (10) which is outward in the radial direction.
4. The core holder for the mud dynamic pollution experiment is characterized in that the diaphragm (4) comprises a cylindrical main body part (401), and sealing parts (402) are arranged at two ends of the main body part (401); the outer diameters of the main body part (401) and the sealing part (402) are equal, and the inner diameter of the main body part (401) is smaller than that of the sealing part (402); the two ends of the main body part (401) are respectively abutted to the annular bosses (10) at the two ends, and the inner wall of the sealing part (402) is attached to the radial outward side surface of the annular boss (10).
5. The core holder for the mud dynamic pollution experiment is characterized in that the sealing part (402) is bonded with the annular boss (10) or/and connected with the annular boss through a bolt (11).
6. The core holder for the mud dynamic pollution experiment is characterized in that one end, facing the interior of the sleeve (1), of the first plug (2) is provided with a ring of annular gaps (201), and one end of the main body part (401) is abutted in the annular gaps (201).
7. The core holder for the mud dynamic pollution experiment is characterized in that after the first plug (2) and the end of the sleeve (1) are connected in place, the outer end of the first plug (2) in the axial direction is flush with the end of the sleeve (1), and the outer end of the annular gap (201) in the axial direction is flush with the corresponding annular boss (10).
8. The core holder for the mud dynamic pollution experiment is characterized in that one end face, facing the interior of the sleeve (1), of the second plug (3) is in contact with one end of the main body part (401) in the axial direction.
9. The core holder for the mud dynamic pollution experiment according to any one of claims 1 to 8, characterized in that a liquid outlet channel (8) is arranged on the first plug (2), and two circulation channels (9) are arranged on the second plug (3).
10. The core holder for the mud dynamic pollution experiment is characterized in that an anti-compression ring (12) is arranged at one end, facing the interior of the sleeve (1), of the second plug (3), the anti-compression ring (12) is in interference fit with the diaphragm, and the two circulation channels (9) are communicated to an area formed by the anti-compression ring (12).
CN201911106072.3A 2019-11-13 2019-11-13 Core holder for slurry dynamic pollution experiment Pending CN110658125A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911106072.3A CN110658125A (en) 2019-11-13 2019-11-13 Core holder for slurry dynamic pollution experiment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911106072.3A CN110658125A (en) 2019-11-13 2019-11-13 Core holder for slurry dynamic pollution experiment

Publications (1)

Publication Number Publication Date
CN110658125A true CN110658125A (en) 2020-01-07

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113484223A (en) * 2021-08-26 2021-10-08 中国石油大学(北京) Full-diameter core holder
CN113624608A (en) * 2020-05-07 2021-11-09 中国石油天然气股份有限公司 Device and method for testing fracture initiation pressure of reservoir rock
CN116297112A (en) * 2023-05-25 2023-06-23 上海联风气体有限公司 Gas permeability detection equipment and detection method for polymer film

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113624608A (en) * 2020-05-07 2021-11-09 中国石油天然气股份有限公司 Device and method for testing fracture initiation pressure of reservoir rock
CN113624608B (en) * 2020-05-07 2023-09-26 中国石油天然气股份有限公司 Reservoir rock fracture pressure testing device and method
CN113484223A (en) * 2021-08-26 2021-10-08 中国石油大学(北京) Full-diameter core holder
CN113484223B (en) * 2021-08-26 2023-02-03 中国石油大学(北京) Full-diameter core holder
CN116297112A (en) * 2023-05-25 2023-06-23 上海联风气体有限公司 Gas permeability detection equipment and detection method for polymer film
CN116297112B (en) * 2023-05-25 2023-09-15 上海联风气体有限公司 Gas permeability detection equipment and detection method for polymer film

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