CN110655382A - Preparation method of health-care ball with high far infrared radiance - Google Patents

Preparation method of health-care ball with high far infrared radiance Download PDF

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Publication number
CN110655382A
CN110655382A CN201910711369.6A CN201910711369A CN110655382A CN 110655382 A CN110655382 A CN 110655382A CN 201910711369 A CN201910711369 A CN 201910711369A CN 110655382 A CN110655382 A CN 110655382A
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health
ball
mud
far infrared
care
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Inventor
李萍
邵光明
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Jingdezhen Yulu Ceramics Co.,Ltd.
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Jingdezhen Yuteng Porcelain Co Ltd
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Priority to CN201910711369.6A priority Critical patent/CN110655382A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/30Treatment of water, waste water, or sewage by irradiation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3436Alkaline earth metal silicates, e.g. barium silicate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/606Drying
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Organic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Hydrology & Water Resources (AREA)
  • Water Supply & Treatment (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Toxicology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Radiation-Therapy Devices (AREA)

Abstract

The invention belongs to the field of material science and engineering, and particularly relates to a preparation method of a health-care ball with high far infrared radiance. A preparation method of a health care ball with high far infrared radiance comprises the following steps: (1) preparing pug; (2) preparing materials; (3) ageing the material obtained in the step (2) for more than 12 hours for later use; (4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips; (5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks; (6) drying; (7) and firing the dried green health-care ball at 1050-1100 ℃ for 5-7 hours, and cooling to normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.

Description

Preparation method of health-care ball with high far infrared radiance
Technical Field
The invention belongs to the field of material science and engineering, and particularly relates to a preparation method of a health-care ball with high far infrared radiance.
Background
With the continuous improvement of the living standard of people in China, the quality requirement of people on drinking water is higher and higher, and tap water provided for residents in China still has more or less defects at present. The main problems include: 1. with the long-time use of the pipeline, the interior of the pipeline is aged continuously, so that harmful bacteria are easy to breed; 2. the water molecules in tap water have low activity and are not easy to be absorbed by human bodies.
Disclosure of Invention
The purpose of the invention is as follows: the invention makes improvement aiming at the problems in the prior art, namely the invention discloses a preparation method of a health care ball with high far infrared radiance, which can be used for efficiently and environmentally treating and purifying tap water without any side effect; but also can be used for mineral hydration of barreled purified water, and solves the unhealthy problem of drinking water caused by long-term drinking of purified water which is easy to be ignored by people.
The technical scheme is as follows: a preparation method of a health care ball with high far infrared radiance comprises the following steps:
(1) preparation of pug
(11) Placing the purple sand ore in a staling bin, and staling for at least 15 days to obtain well-staled purple sand ore;
(12) pouring the purple sand ore obtained in the step (11), kaolin, auxiliary materials and water into a ball milling tank with added ball stones, and then carrying out ball milling for 7-9 hours at a rotating speed of 500-700 rpm to obtain slurry, wherein:
purple sand ore: kaolin: the mass ratio of the auxiliary materials is (60-70): (20-30): (15-25);
water: material preparation: the ball stone is 1: 1: 2;
(13) sieving the slurry obtained in the step (12) by a screen of 160-250 meshes, filtering out screen residue, and conveying the filtered slurry into a mud press for pressing to obtain mud;
(2) ingredients
Pouring 50-80 parts by mass of the pug obtained in the step (1), 20-30 parts by mass of medical stone, 10-20 parts by mass of borocalcite, 30-50 parts by mass of water and 1-3 parts by mass of humic material into a stirrer, and stirring for 5-6 hours at the rotating speed of 500-700 rpm to obtain a well-mixed material;
(3) ageing the material obtained in the step (2) for more than 12 hours for later use;
(4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips;
(5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks;
(6) drying
Drying the green health-care ball obtained in the step (5) at 90-120 ℃ for 12-15 hours for later use;
(7) firing into
And firing the dried green health-care ball at 1050-1100 ℃ for 5-7 hours, and cooling to normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.
Further, the auxiliary material in the step (12) is sodium humate.
Further, the auxiliary material in the step (2) is electrolyte or CMC.
Further, the water content of the mud strips in the step (4) is 18-22 wt%.
Further, the water content of the green health care ball dried in the step (6) is less than 3 wt%.
Has the advantages that: the preparation method of the health-care ball with the high far infrared radiance disclosed by the invention has the following beneficial effects:
(1) the health-care ball disclosed by the invention has far infrared radiance of 0.86-0.87, can convert a macromolecular structure of water into a small molecular chain structure, and is beneficial to absorption of a human body;
(2) due to the obvious antibacterial action, the health-care ball disclosed by the invention completely does not need to introduce metal or organic antibacterial materials when treating water and containing tap water and barreled water, and ensures that the drinking purified water is pure natural and has important attributes of environmental protection.
The specific implementation mode is as follows:
the following describes in detail specific embodiments of the present invention.
Detailed description of the preferred embodiment 1
A preparation method of a health care ball with high far infrared radiance comprises the following steps:
(1) preparation of pug
(11) Placing the purple sand ore in a staling bin, and staling for 15 days to obtain well-staled purple sand ore;
(12) pouring the purple sand ore obtained in the step (11), kaolin, auxiliary materials and water into a ball milling tank with added ball stones, and then carrying out ball milling for 9 hours at the rotating speed of 500rpm to obtain slurry, wherein:
purple sand ore: kaolin: the mass ratio of the auxiliary materials is 60: 20: 15;
water: the materials (comprising purple sand ore, kaolin and auxiliary materials) are as follows: the ball stone is 1: 1: 2;
(13) sieving the slurry obtained in the step (12) by a 160-mesh sieve, filtering out screen residue, and conveying the filtered slurry into a mud press for pressing to obtain mud;
(2) ingredients
Pouring 50 parts of pug obtained in the step (1), 20 parts of medical stone, 10 parts of borocalcite, 30 parts of water and 1 part of humus into a stirrer by mass, and stirring for 6 hours at the rotating speed of 500rpm to obtain a mixed material;
(3) ageing the material obtained in the step (2) for 12 hours for later use;
(4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips;
(5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks;
(6) drying
Drying the green health-care ball obtained in the step (5) at 90 ℃ for 15 hours for later use;
(7) firing into
And firing the dried green health-care ball for 7 hours at 1050 ℃, and cooling to the normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.
Further, the auxiliary material in the step (12) is sodium humate.
Further, the auxiliary material in the step (2) is CMC.
Further, the water content of the mud strips in the step (4) is 18 wt%.
Further, the water content of the green health care ball dried in the step (6) is less than 3 wt%.
Specific example 2
A preparation method of a health care ball with high far infrared radiance comprises the following steps:
(1) preparation of pug
(11) Placing the purple sand ore in a staling bin, and staling for 30 days to obtain well-staled purple sand ore;
(12) pouring the purple sand ore obtained in the step (11), kaolin, auxiliary materials and water into a ball milling tank with added ball stones, and then carrying out ball milling for 7 hours at the rotating speed of 700rpm to obtain slurry, wherein:
purple sand ore: kaolin: the mass ratio of the auxiliary materials is 70: 30: 25;
water: material preparation: the ball stone is 1: 1: 2;
(13) screening the slurry obtained in the step (12) by a 250-mesh screen, filtering out screen residue, and conveying the filtered slurry into a mud press for pressing to obtain mud;
(2) ingredients
Pouring 80 parts of pug obtained in the step (1), 30 parts of medical stone, 20 parts of borocalcite, 50 parts of water and 3 parts of humus into a stirrer by mass, and stirring for 5 hours at the rotating speed of 700rpm to obtain a well-mixed material;
(3) ageing the material obtained in the step (2) for 24 hours for later use;
(4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips;
(5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks;
(6) drying
Drying the green health-care ball obtained in the step (5) at 120 ℃ for 12 hours for later use;
(7) firing into
And firing the dried green health-care ball for 5 hours at 1100 ℃, and cooling to the normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.
Further, the auxiliary material in the step (12) is sodium humate.
Further, the auxiliary material in the step (2) is electrolyte.
Further, the water content of the mud strips in the step (4) is 22 wt%.
Further, the water content of the green health care ball dried in the step (6) is less than 3 wt%.
Specific example 3
A preparation method of a health care ball with high far infrared radiance comprises the following steps:
(1) preparation of pug
(11) Placing the purple sand ore in a staling bin, and staling for 45 days to obtain well-staled purple sand ore;
(12) pouring the purple sand ore obtained in the step (11), kaolin, auxiliary materials and water into a ball milling tank with added ball stones, and then carrying out ball milling for 8 hours at the rotating speed of 600rpm to obtain slurry, wherein:
purple sand ore: kaolin: the mass ratio of the auxiliary materials is 65: 25: 20;
water: material preparation: the ball stone is 1: 1: 2;
(13) sieving the slurry obtained in the step (12) by a 200-mesh sieve, filtering out screen residue, and conveying the filtered slurry into a mud press for pressing to obtain mud;
(2) ingredients
Pouring 60 parts of pug obtained in the step (1), 25 parts of medical stone, 15 parts of borocalcite, 40 parts of water and 2 parts of humus into a stirrer by mass, and stirring for 5.5 hours at the rotating speed of 600rpm to obtain a well-mixed material;
(3) ageing the material obtained in the step (2) for 18 hours for later use;
(4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips;
(5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks;
(6) drying
Drying the green health-care ball obtained in the step (5) at 110 ℃ for 14 hours for later use;
(7) firing into
And firing the dried green health-care ball at 1080 ℃ for 6 hours, and cooling to the normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.
Further, the auxiliary material in the step (12) is sodium humate.
Further, the auxiliary material in the step (2) is CMC.
Further, the water content of the mud strips in the step (4) is 20 wt%.
Further, the water content of the green health care ball dried in the step (6) is less than 3 wt%.
The embodiments of the present invention have been described in detail. However, the present invention is not limited to the above-described embodiments, and various changes can be made within the knowledge of those skilled in the art without departing from the spirit of the present invention.

Claims (5)

1. A preparation method of a health care ball with high far infrared radiance is characterized by comprising the following steps:
(1) preparation of pug
(11) Placing the purple sand ore in a staling bin, and staling for at least 15 days to obtain well-staled purple sand ore;
(12) pouring the purple sand ore obtained in the step (11), kaolin, auxiliary materials and water into a ball milling tank with added ball stones, and then carrying out ball milling for 7-9 hours at a rotating speed of 500-700 rpm to obtain slurry, wherein:
purple sand ore: kaolin: the mass ratio of the auxiliary materials is (60-70): (20-30): (15-25);
water: material preparation: the ball stone is 1: 1: 2;
(13) sieving the slurry obtained in the step (12) by a screen of 160-250 meshes, filtering out screen residue, and conveying the filtered slurry into a mud press for pressing to obtain mud;
(2) ingredients
Pouring 50-80 parts by mass of the pug obtained in the step (1), 20-30 parts by mass of medical stone, 10-20 parts by mass of borocalcite, 30-50 parts by mass of water and 1-3 parts by mass of humic material into a stirrer, and stirring for 5-6 hours at the rotating speed of 500-700 rpm to obtain a well-mixed material;
(3) ageing the material obtained in the step (2) for more than 12 hours for later use;
(4) putting the material obtained in the step (3) into a mud press to press mud cakes, and putting the mud cakes into a vacuum pug mill to mill mud strips;
(5) putting the mud strips obtained in the step (4) into a granulating machine, and extruding green health-care ball blanks;
(6) drying
Drying the green health-care ball obtained in the step (5) at 90-120 ℃ for 12-15 hours for later use;
(7) firing into
And firing the dried green health-care ball at 1050-1100 ℃ for 5-7 hours, and cooling to normal temperature along with the furnace to obtain the health-care ball with the high far infrared radiance.
2. The method for preparing health-care balls with high far infrared radiance of claim 1, wherein the auxiliary material in step (12) is sodium humate.
3. The method for preparing a health-care ball with high far infrared radiance of claim 1, wherein the auxiliary material in step (2) is electrolyte or CMC.
4. The preparation method of the health-care ball with the high far infrared radiance as claimed in claim 1, wherein the water content of the mud strips in the step (4) is 18-22 wt%.
5. The method for preparing a health-care ball with high far infrared radiance of claim 1 wherein the moisture content of the green health-care ball dried in step (6) is less than 3 wt%.
CN201910711369.6A 2019-08-02 2019-08-02 Preparation method of health-care ball with high far infrared radiance Pending CN110655382A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112552017A (en) * 2020-12-18 2021-03-26 占智宽 Forming process of far infrared purple sand bead net
CN113248236A (en) * 2021-06-23 2021-08-13 淄博和润马科托矿业技术有限公司 Infrared alumina ceramic fitness ball and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112552017A (en) * 2020-12-18 2021-03-26 占智宽 Forming process of far infrared purple sand bead net
CN113248236A (en) * 2021-06-23 2021-08-13 淄博和润马科托矿业技术有限公司 Infrared alumina ceramic fitness ball and preparation method thereof

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