CN110605083A - Reactor capable of high-temperature reaction - Google Patents

Reactor capable of high-temperature reaction Download PDF

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Publication number
CN110605083A
CN110605083A CN201810618742.9A CN201810618742A CN110605083A CN 110605083 A CN110605083 A CN 110605083A CN 201810618742 A CN201810618742 A CN 201810618742A CN 110605083 A CN110605083 A CN 110605083A
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CN
China
Prior art keywords
tube
reaction container
reaction
pipeline
vent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810618742.9A
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Chinese (zh)
Inventor
伍广
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Individual
Original Assignee
Individual
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Filing date
Publication date
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Priority to CN201810618742.9A priority Critical patent/CN110605083A/en
Publication of CN110605083A publication Critical patent/CN110605083A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a reactor capable of high-temperature reaction, which solves the problem that an enamel reaction device capable of ventilating can not continuously provide higher-temperature environment for the reaction in the enamel reaction device. Including the reaction vessel lid, the reaction vessel body, and be provided with the breather pipe of inlet and venthole of ventilating, the reaction vessel lid is provided with the pipeline connecting device who is connected with the breather pipe, the venthole passes through pipeline connecting device and stretches into the reaction vessel body internally, the inlet setting of ventilating is outside the reaction vessel lid, reaction vessel body inboard is provided with the glass lining inlayer, glass lining inlayer outside is provided with presss from both sides the jacket layer, it is provided with the pipeline to press from both sides the jacket layer top outside, it is provided with the lower pipeline to press from both sides the jacket layer bottom outside, be provided with steam input tube and hot water output tube on the upper tube, be provided with steam output tube and hot water input tube on the lower pipeline, steam is gone into the jacket layer by the steam input tube through the upper tube, discharge by the steam output tube through the lower pipeline, hot water is gone into the jacket layer by.

Description

Reactor capable of high-temperature reaction
Technical Field
The invention relates to the field of reaction equipment, in particular to a reactor capable of reacting at high temperature.
Background
The enamel reactor is made up by lining the glass containing high-silicon dioxide on the inner surface of steel container, and burning at high temp. to firmly adhere it to the metal surface. Therefore, it has the dual advantages of glass stability and metal strength, and is an excellent corrosion-resistant device. Is widely applied to the industries of chemical industry, petroleum, medicine, pesticide, food and the like.
In some processes, it is desirable to have a gas participate in the reaction, and different reactions require different amounts of gas to be added to the reaction vessel. Some are added before the reaction, some are added in the middle of the reaction, and some are added for a period of time and then are stopped. This requires the reaction vessel to be provided with gas passages for feeding gas into the body of the reaction vessel and for satisfying different gas feeding requirements. However, the existing enamel reaction vessel does not have corresponding gas channels and cannot be used for reactions needing gas participation.
Furthermore, in some production processes, the reactants in the reaction vessel need to be reacted in a relatively high temperature environment, or the reaction speed can be fastest, which is obviously not considered in the prior art.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: provides a reactor capable of high-temperature reaction, which solves the problem that the ventilating enamel reaction device can not continuously provide higher temperature environment for the reaction in the reactor.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a reactor capable of high-temperature reaction comprises a reaction container cover, a reaction container body and a vent pipe provided with a vent inlet and a vent hole, wherein the vent pipe is a glass lining pipeline, the vent hole is formed at the lower end of the vent pipe, the reaction container cover is provided with a pipeline connecting device connected with the vent pipe, the vent hole extends into the reaction container body through the pipeline connecting device, the vent pipe is movably connected with the pipeline connecting device, the vent pipe can vertically move up and down relative to the pipeline connecting device, the vent inlet is formed outside the reaction container cover, and the top of the reaction container cover is provided with a glass lining pipe orifice; the pressure device is connected with the vent pipe sequentially through the pressure rod and the pressure table, the pressure device is used for controlling the vent pipe to move vertically, and the vent inlet is formed in one side of the pressure table; the reaction container cover is provided with a thermometer sleeve fixing device, and the thermometer sleeve extends into the reaction container body through the thermometer sleeve fixing device; the reaction vessel body inboard is provided with the glass-lined inlayer, is provided with the jacket layer outside the glass-lined inlayer, the jacket layer top outside is provided with the pipeline, the jacket layer bottom outside is provided with the lower pipeline, be provided with steam input tube and hot water output tube on the upper pipeline, be provided with steam output tube and hot water input tube on the lower pipeline, steam gets into the jacket layer through the upper pipeline by the steam input tube, and the steam output tube discharges through the lower pipeline, and hot water gets into the jacket layer through the lower pipeline by the hot water input tube, discharges through the hot water output tube through the upper pipeline.
Preferably, the bottom of the reaction vessel body is provided with a glass lining discharging pipe, and the glass lining discharging pipe is provided with a glass lining discharging valve.
Preferably, the top of the reaction container cover is also provided with a manhole.
Preferably, a stirrer is further provided in the reaction vessel body.
Preferably, a clip with suspension protection is arranged between the reaction container cover and the reaction container body, and a sealing sheet is arranged at the front end of the clip.
Compared with the prior art, the invention has the following beneficial effects:
(1) the reaction vessel body is provided with the jacket layer, and the jacket layer can input steam or hot water according to actual needs to provide required ambient temperature for reactants in the reaction vessel body, so that the reaction vessel can be suitable for the reactants with certain requirements on temperature to react in the reaction vessel, and the application range of the reaction device is greatly increased; or steam or hot water is input in the reaction process, so that the reaction speed of reactants in the reaction container body is accelerated, and the reaction time is greatly shortened.
(2) The interlayer body adopts a mode of one pipe for multiple purposes, and simultaneously conveys steam and hot water, thereby effectively reducing the number of pipelines and saving materials.
(3) The invention is provided with the vent pipe with the vent inlet and the vent hole, can add gas into the enamel reaction vessel body, meets the requirements of adding different gases, solves the problem that the enamel reaction vessel cannot be used for the reaction needing the gas to participate, and enlarges the application range of the enamel reaction vessel.
(4) The vent pipe is movably connected with the pipeline connecting device, and the vent pipe can vertically move relative to the pipeline connecting device, so that the influence on stirring and mixing of materials in the reaction container body when gas does not need to be introduced can be effectively avoided.
(5) The invention adopts the pressure device to control the vent pipe to move vertically, is convenient to operate and effectively reduces the labor intensity of workers.
Drawings
FIG. 1 is a schematic view of the structure of the present invention
Description of the drawings: 1 is the reaction vessel lid, 2 is the reaction vessel body, 3 is the jacket layer, 4 is the glass-lined inlayer, 5 is the glass-lined baiting valve, 6 is the checkpost, 7 is the gasket, 8 is the upper pipeline, 9 is the thermowell fixing device, 10 is the steam input tube, 11 is the hot water output tube, 12 is the steam output tube, 13 is the hot water input tube, 14 is the thermowell, 15 is the glass-lined mouth of pipe, 16 is the agitator, 17 is the access hole, 18 is the pipe connection device, 19 is the breather pipe, 20 is the venthole, 21 is pressure device, 22 is the depression bar, 23 is the pressure platform, 24 is the entry of ventilating, 25 is the lower pipeline.
Detailed Description
As shown in fig. 1: a reactor capable of high-temperature reaction comprises a reaction container cover 1, a reaction container body 2 and a vent pipe 19 provided with a vent inlet 24 and a vent hole 20, wherein the vent pipe 19 is a glass lining pipeline, the vent hole 20 is arranged at the lower end of the vent pipe 19, the reaction container cover 1 is provided with a pipeline connecting device 18 connected with the vent pipe 19, the vent hole 20 extends into the reaction container body 2 through the pipeline connecting device 18, the vent pipe 19 is movably connected with the pipeline connecting device 18, the vent pipe 19 can vertically move up and down relative to the pipeline connecting device 18, the vent inlet 24 is arranged outside the reaction container cover 1, and the top of the reaction container cover 1 is provided with a glass lining pipe orifice 15; the device is characterized by further comprising a pressure device 21, a pressure rod 22 and a pressure platform 23, wherein the pressure device 21 is connected with the vent pipe 19 sequentially through the pressure rod 22 and the pressure platform 23, the pressure device 21 is used for controlling the vent pipe 19 to move vertically, and the vent inlet 24 is arranged on one side of the pressure platform 23; the reaction container further comprises a thermo-well tube 14, wherein a thermo-well tube fixing device 9 is arranged on the reaction container cover 1, and the thermo-well tube 14 extends into the reaction container body 2 through the thermo-well tube fixing device 9; the inner side of the reaction vessel body 2 is provided with a glass lining inner layer 4, and the outer side of the glass lining inner layer 4 is provided with
There is jacket layer 3, jacket layer 3 top outside is provided with upper pipe 8, jacket layer 3 bottom outside is provided with lower pipeline 25, be provided with steam input tube 10 and hot water output tube 11 on the upper pipe 8, be provided with steam output tube 12 and hot water input tube 13 on the lower pipeline 25, steam gets into jacket layer 3 through upper pipe 8 by steam input tube 10, is discharged by steam output tube 12 through lower pipeline 25, and hot water gets into jacket layer 3 through lower pipeline 25 by hot water input tube 13, is discharged by hot water output tube 11 through upper pipe 8.
Preferably, the bottom of the reaction vessel body 2 is provided with a glass lining discharging pipe, and the glass lining discharging pipe is provided with a glass lining discharging valve 5.
Preferably, the top of the reaction container cover 1 is further provided with a manhole 17.
Preferably, a stirrer 16 is further provided in the reaction vessel body 2.
Preferably, a clip 6 with suspension protection is arranged between the reaction vessel cover 1 and the reaction vessel body 2, and a sealing sheet 7 is arranged at the front end of the clip 6.

Claims (5)

1. A reactor capable of high temperature reaction, characterized in that: the reaction container comprises a reaction container cover (1), a reaction container body (2) and a vent pipe (19) provided with a vent inlet (24) and a vent hole (20), wherein the vent pipe (19) is a glass lining pipeline, the vent hole (20) is arranged at the lower end of the vent pipe (19), the reaction container cover (1) is provided with a pipeline connecting device (18) connected with the vent pipe (19), the vent hole (20) extends into the reaction container body (2) through the pipeline connecting device (18), the vent pipe (19) is movably connected with the pipeline connecting device (18), the vent pipe (19) can vertically move relative to the pipeline connecting device (18), the vent inlet (24) is arranged outside the reaction container cover (1), and the top of the reaction container cover (1) is provided with a glass lining pipe (15); the device is characterized by further comprising a pressure device (21), a pressure rod (22) and a pressure platform (23), wherein the pressure device (21) is connected with the vent pipe (19) sequentially through the pressure rod (22) and the pressure platform (23), the pressure device (21) is used for controlling the vent pipe (19) to move vertically, and the vent inlet (24) is formed in one side of the pressure platform (23); the reaction container is characterized by further comprising a thermo-well tube (14), wherein a thermo-well tube fixing device (9) is arranged on the reaction container cover (1), and the thermo-well tube (14) extends into the reaction container body (2) through the thermo-well tube fixing device (9); reaction vessel body (2) inboard is provided with glass-lined inner layer (4), and glass-lined inner layer (4) outside is provided with jacket layer (3), jacket layer (3) top outside is provided with upper tube (8), jacket layer (3) bottom outside is provided with lower pipeline (25), be provided with steam input tube (10) and hot water output tube (11) on upper tube (8), be provided with steam output tube (12) and hot water input tube (13) on lower pipeline (25), steam gets into jacket layer (3) through upper tube (8) by steam input tube (10), and is discharged by steam output tube (12) through lower pipeline (25), and hot water gets into jacket layer (3) through lower pipeline (25) by hot water input tube (13), is discharged by hot water output tube (11) through upper tube (8).
2. A high temperature reactive reactor as defined in claim 1, wherein: the bottom of the reaction vessel body (2) is provided with a glass lining discharging pipe, and the glass lining discharging pipe is provided with a glass lining discharging valve (5).
3. A high temperature reactive reactor as defined in claim 1, wherein: the top of the reaction container cover (1) is also provided with a manhole (17).
4. A high temperature reactive reactor as defined in claim 1, wherein: a stirrer (16) is also arranged in the reaction vessel body (2).
5. A high temperature reactive reactor as defined in claim 1, wherein: a clip (6) with suspension protection is arranged between the reaction container cover (1) and the reaction container body (2), and a sealing sheet (7) is arranged at the front end of the clip (6).
CN201810618742.9A 2018-06-15 2018-06-15 Reactor capable of high-temperature reaction Pending CN110605083A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810618742.9A CN110605083A (en) 2018-06-15 2018-06-15 Reactor capable of high-temperature reaction

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810618742.9A CN110605083A (en) 2018-06-15 2018-06-15 Reactor capable of high-temperature reaction

Publications (1)

Publication Number Publication Date
CN110605083A true CN110605083A (en) 2019-12-24

Family

ID=68888112

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810618742.9A Pending CN110605083A (en) 2018-06-15 2018-06-15 Reactor capable of high-temperature reaction

Country Status (1)

Country Link
CN (1) CN110605083A (en)

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WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20191224