CN1105771C - 合成液体燃料 - Google Patents

合成液体燃料 Download PDF

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CN1105771C
CN1105771C CN00100669A CN00100669A CN1105771C CN 1105771 C CN1105771 C CN 1105771C CN 00100669 A CN00100669 A CN 00100669A CN 00100669 A CN00100669 A CN 00100669A CN 1105771 C CN1105771 C CN 1105771C
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fuel
liquid fuel
add
parts
stir
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CN1262310A (zh
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鲁希诺
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Beijing Qingyan Lihua Petroleum Chemical Technology Co., Ltd.
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鲁希诺
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Abstract

本发明涉及燃料，具体地说是一种合成液体燃料，现有的燃料是天然石油裂解的废料，本发明是人工合成液体燃料，由甲醇、二茂铁CHF、高铬酸钾、二甲苯和石油醚五种化学原料组成，制备方法详见说明书，本发明优点是原料来源丰富，成本低、合成不复杂，使用方便，增加燃料品种，弥补天然产品的供应紧缺，该燃料适用于工业和民用。

Description

合成液体燃料
本发明涉及燃料类，更确切地说是涉及一种新型液体燃料。
燃料品种有气态、液态和固态三种，其中液态燃料均为天然石油裂解的付产品，成分复杂、价格高，到目前为止，市场上仍没有由人工合成的液体燃料。
本发明目的是提供成分简单、价格低的一种人工合成液体燃料。
本发明的技术方案是：甲醇100000份中，含由下述重量比的原料所组成：
CHF           20份
高铬酸钾      25份
二甲苯        60份
石油醚        60份
本发明的制备方法包括以下步骤：
(1)把主料甲醇加入反应容器，开始搅拌，同时加入CHF，继续搅拌2分钟；
(2)加入高铬酸钾，搅拌2分钟后静止3分钟；
(3)加入二甲苯，同时开始搅拌，1分钟后，加入石油醚，即可罐装入瓶。
本发明的原料及作用：
1、甲醇，又名工业酒精 分子式CH3OH，有毒，罐封保存，该该物质充分燃烧时是兰色火焰，热值较高，挥发性强。
2、CHF 分子式(C5H5)2Fe、米黄色粉状，用棕色玻璃容器盛装，易溶于醚类，一种火箭用添加剂，在整个反应中，主要起消烟、助燃提高热值的作用。
3、高铬酸钾 分子式KCrO4，强氧化剂。
4、二甲苯 分子式C8H16，为对二甲苯和邻二甲苯，可以提高添加剂与添加剂之间的反应速度，缩短反应时间。
5、石油醚，极易挥发，与人体接触，使人体产生凉感，主要用于溶解二茂铁，增加反应速度。
本发明的优点是人工合成时不复杂，原料来源丰富，成本低，使用方便，增加燃料品种，以弥补天然燃料供应紧缺。
下面就一个实施例，对本发明作详细说明：
实施例1
在反应釜中，加入甲醇100公斤，开始搅拌，同时加入CHF20克，继续搅拌2分钟，加入高铬酸钾25克，搅拌2分钟后，静止3分钟，加入二甲苯60克，同时开始搅拌，1分钟后加入石油醚60克，即可罐装入钢瓶，该钢瓶必须能够承受3个大气压。
合成液体燃料符合表1规定的指标：
表1
    项目  质量指标  试验方法
密度(15℃)，kg/m3  SH/T 02211)
蒸气压(37.8℃)，KPa        不大于   1380  GB/T 66022)
C5及C5以上组分含量，％(V/V)不大于   3.0  SH/T 0230
残留物  SY/T 7509
蒸发残留物，ML/100mL  不大于油渍观察   0.05通过3)
铜片腐蚀，级          不大于   1  SH/T 0232
总硫含量，mg/m3      不大于   343  SH/T 0222
游离水   无  目测4)
1)密度也可用GB/T 12576方法计算，但仲裁按SH/T 0221测定。2)蒸气压也可用GB/T 12576方法计算，但仲裁按GB/T 6602测定。3)按SY/T 7509方法所述，每次以0.1ml的增量将0.3ml溶剂残留物混合物滴到滤纸上，2min后在日光下观察，无持久不退的油环为通过。4)在测定密度的同时用目测法测定试样是否存在游离水。
为确保合成液体燃料，要求具有特殊臭味，必要时加入硫醇、硫醚等硫化物配制的加臭剂，加入量不得超过0.001％(m/m)。
该合成液体燃料适用于工业和民用。

Claims (2)

1、一种合成液体燃料，其特征在于：甲醇100000份中，含由下述重量比的原料所组成：
CHF             20份
高铬酸钾         25份
二甲苯           60份
石油醚           60份
2、一种权利要求1所述的合成液体燃料的制备方法，其特征在于包括以下步骤：
(1)把主料甲醇加入反应容器，开始搅拌，同时加入CHF，继续搅拌2分钟；
(2)加入高铬酸钾，搅拌2分钟后静止3分钟；
(3)加入二甲苯，同时开始搅拌，1分钟后，加入石油醚，即可罐装入瓶。
CN00100669A 2000-01-27 2000-01-27 合成液体燃料 Expired - Fee Related CN1105771C (zh)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN00100669A CN1105771C (zh) 2000-01-27 2000-01-27 合成液体燃料

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CN1105771C true CN1105771C (zh) 2003-04-16

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100365107C (zh) * 2004-07-28 2008-01-30 怀化市桥兴环保液体燃料有限责任公司 易点稳燃高热值合成液体燃料及其制备方法
CN103525478A (zh) * 2013-10-15 2014-01-22 常州市梧桐树环保科技有限公司 用于工业喷雾扩散燃烧的水性液体燃料及其合成方法
CN110283634A (zh) * 2019-07-12 2019-09-27 石鑫 一种生物质汽柴醇及加工工艺

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054262A (zh) * 1991-01-17 1991-09-04 林业田 合成汽油
CN1099406A (zh) * 1994-02-02 1995-03-01 张殿清 无污染高效安全燃料及其工艺方法和灶具

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054262A (zh) * 1991-01-17 1991-09-04 林业田 合成汽油
CN1099406A (zh) * 1994-02-02 1995-03-01 张殿清 无污染高效安全燃料及其工艺方法和灶具

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