CN110559974A - Solid-liquid separation mechanism of reaction kettle - Google Patents

Solid-liquid separation mechanism of reaction kettle Download PDF

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Publication number
CN110559974A
CN110559974A CN201910967034.0A CN201910967034A CN110559974A CN 110559974 A CN110559974 A CN 110559974A CN 201910967034 A CN201910967034 A CN 201910967034A CN 110559974 A CN110559974 A CN 110559974A
Authority
CN
China
Prior art keywords
reaction kettle
kettle body
filter screen
solid
liquid separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910967034.0A
Other languages
Chinese (zh)
Inventor
刘铎
刘驭东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Yuzhi Equipment Technology Co Ltd
Original Assignee
Shenzhen Yuzhi Equipment Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Yuzhi Equipment Technology Co Ltd filed Critical Shenzhen Yuzhi Equipment Technology Co Ltd
Priority to CN201910967034.0A priority Critical patent/CN110559974A/en
Publication of CN110559974A publication Critical patent/CN110559974A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/03Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/05Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements supported
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/56Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/88Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices
    • B01D29/90Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices for feeding
    • B01D29/906Special treatment of the feed stream before contacting the filtering element, e.g. cutting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/88Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices
    • B01D29/94Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices for discharging the filter cake, e.g. chutes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses a solid-liquid separation mechanism of a reaction kettle, which comprises a reaction kettle body and a stirrer, wherein the reaction kettle body is provided with a reaction kettle cover; the top of the reaction kettle body is provided with an air outlet, the side surface of the reaction kettle body is provided with a feed inlet, and the bottom of the reaction kettle body is provided with a liquid outlet; the stirrer comprises a stirring shaft and a driving motor fixed on the top of the stirring shaft; the lower end of the stirring shaft is positioned in the reaction kettle body, and the upper end of the stirring shaft penetrates through the reaction kettle body and is connected with the output end of the driving motor; the outer surface of the stirring shaft is provided with stirring blades; a clapboard which can be transversely pulled is arranged in the reaction kettle body; a plurality of blocking blocks are also arranged in the reaction kettle body and are positioned above the partition plate; still be equipped with first filter screen in the reation kettle body, first filter screen is located the below of baffle, and first filter screen is equipped with the waste material push rod between the baffle, is equipped with first waste residue discharge port on the lateral wall of the reation kettle body of one of them one end of first filter screen. The invention can fully carry out solid-liquid separation and prolong the service life of the reaction kettle.

Description

Solid-liquid separation mechanism of reaction kettle
Technical Field
The invention relates to a reaction kettle, in particular to a solid-liquid separation mechanism of the reaction kettle.
Background
The reaction kettle is a common container for physical or chemical reaction, is widely used in the industries of chemical industry, petroleum, pesticide, medical treatment and the like, and is used for completing the technological processes of synthesis, condensation, vulcanization and the like. In the operation process of the reaction kettle, after the chemical reaction of the materials in the reaction kettle is finished, the solid-liquid mixture after the reaction needs to be separated to obtain liquid and solid.
In the prior art, solid-liquid mixture in a reaction kettle needs to be discharged to the outside, and then the solid-liquid mixture is separated in a filtering mode of a centrifugal machine or a plate-and-frame filter press, so that the process is complex and the energy consumption is high. Therefore, the solid-liquid mixture in the reaction kettle is discharged to the outside for solid-liquid separation, and the requirements of industrial operation cannot be met. And a few reaction kettles can be used for solid-liquid separation in the reaction kettles, but the structure is unreasonable, so that solid-liquid separation cannot be sufficiently carried out, and the separation efficiency is low.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a solid-liquid separation mechanism of a reaction kettle.
In order to achieve the purpose, the invention adopts the following technical scheme: a solid-liquid separation mechanism of a reaction kettle comprises a reaction kettle body and a stirrer; the top of the reaction kettle body is provided with an air outlet, the side surface of the reaction kettle body is provided with a feed inlet, and the bottom of the reaction kettle body is provided with a liquid outlet; the stirrer comprises a stirring shaft and a driving motor fixed at the top of the stirring shaft; the lower end of the stirring shaft is positioned in the reaction kettle body, and the upper end of the stirring shaft penetrates through the reaction kettle body and is connected with the output end of the driving motor; the outer surface of the stirring shaft is provided with stirring blades; a partition plate capable of being pulled transversely is arranged in the reaction kettle body; a plurality of blocking blocks are also arranged in the reaction kettle body and are positioned above the partition plate; still be equipped with first filter screen in the reation kettle body, first filter screen is located the below of baffle, first filter screen in be equipped with the waste material push rod between the baffle, be equipped with first waste residue discharge port on the lateral wall of the reation kettle body of one of them one end of first filter screen.
The further technical scheme is as follows: the stop block is in an upward convex arch shape.
The further technical scheme is as follows: the reaction kettle is characterized in that a second filter screen is obliquely arranged in the reaction kettle body and is positioned below the first filter screen, and a second waste residue discharge port is formed in the side wall of the reaction kettle body at the lower end of the second filter screen.
The further technical scheme is as follows: the first filter screen is provided with a plurality of round or triangular meshes.
The further technical scheme is as follows: the first filter screen is made of ceramic or glass.
The further technical scheme is as follows: the inclination angle of the second filter screen is 15-25 degrees.
The further technical scheme is as follows: still be equipped with the washing shower in the reation kettle body, the washing shower is located stirring vane's top, the washing sprays to go up the interval and is provided with a plurality of shower heads.
The further technical scheme is as follows: the one end that the baffle stretches out in reation kettle is provided with the handle, the baffle with the junction of reation kettle body is equipped with the sealing washer.
Compared with the prior art, the invention has the beneficial effects that: according to the solid-liquid separation mechanism of the reaction kettle, provided by the invention, solid-liquid separation can be fully carried out by arranging the two layers of filter screens in the reaction kettle body. In addition, the blocking block arranged on the reaction kettle can reduce the impact force of the materials above the partition plate on the first filter screen when the partition plate is opened, so that the service life of the first filter screen is prolonged.
The foregoing description is only an overview of the technical solutions of the present invention, and in order to make the technical means of the present invention more clearly understood, the present invention may be implemented according to the content of the description, and in order to make the above and other objects, features, and advantages of the present invention more apparent, the following detailed description will be given of preferred embodiments.
Drawings
FIG. 1 is a schematic structural diagram of a specific embodiment of a solid-liquid separation mechanism of a reaction kettle according to the present invention;
FIG. 2 is a schematic structural view of a second filter screen in an embodiment of a solid-liquid separation mechanism of a reaction vessel according to the present invention;
FIG. 3 is a schematic structural diagram of a first filter screen in an embodiment of a solid-liquid separation mechanism of a reaction kettle according to the present invention.
Reference numerals
1. A reaction kettle body; 11. an air outlet; 12. a feed inlet; 13. a first slag discharge port; 14. a second slag discharge port; 15. a blocking block; 16. a partition plate; 161. a handle; 17. a waste push rod; 18. a first filter screen; 181. a circular hole; 19. a second filter screen; 2. a stirring shaft; 21. a stirring blade; 22. a drive motor; 3. a shower pipe; 31. and a spray header.
Detailed Description
In order to more fully understand the technical content of the present invention, the technical solution of the present invention will be further described and illustrated with reference to the following specific embodiments, but not limited thereto.
It is to be understood that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity/action/object from another entity/action/object without necessarily requiring or implying any actual such relationship or order between such entities/actions/objects.
It should be further understood that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or system that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or system. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other like elements in a process, method, article, or system that comprises the element.
referring to fig. 1-3, the present embodiment provides a solid-liquid separation mechanism for a reaction kettle, which includes a reaction kettle body 1 and a stirrer; the top of the reaction kettle body 1 is provided with an air outlet 11, the side surface is provided with a feed inlet 12, and the bottom is provided with a liquid outlet; the stirrer comprises a stirring shaft 2 and a driving motor 22 fixed on the top of the stirring shaft 2; the lower end of the stirring shaft 2 is positioned in the reaction kettle body 1, and the upper end of the stirring shaft 2 penetrates through the reaction kettle body 1 and is connected with the output end of the driving motor 22; the outer surface of the stirring shaft 2 is provided with stirring blades 21; a clapboard 16 which can be pulled transversely is arranged in the reaction kettle body 1; a plurality of blocking blocks 15 are also arranged in the reaction kettle body 1, and the blocking blocks 15 are positioned above the partition plate 16; still be equipped with first filter screen 18 in the reation kettle body 1, first filter screen 18 is located the below of baffle 16, and first filter screen 18 is equipped with waste material push rod 17 between baffle 16, is equipped with first waste residue discharge port 13 on the lateral wall of reation kettle body 1 of one end wherein of first filter screen 18. Preferably, the first filter 18 is provided with a plurality of circular holes 181, and the first filter 18 is made of ceramic material.
specifically, the waste pushing rod 17 is connected to a motor (not shown in the figure), and the motor is fixed to the outer side of the reaction kettle body 1. When solid waste is accumulated on the first filter 18, the waste push rod 17 is driven by the motor to move so as to push the solid waste on the first filter 18 to move towards the first waste outlet 13. In addition, be fixed with the stopper 15 above baffle 16, when baffle 16 opened, the material of baffle 16 top can reach first filter screen 18 under the effect of gravity on, consequently, set up baffle 16 and can effectually reduce the impact force of material to first filter screen 18 to the life of extension first filter screen 18. Preferably, the blocking block 15 is in an upwardly convex arch shape, and the arch shape can effectively reduce the residue of the material on the blocking block 15.
Further, still incline in the reation kettle body 1 and be provided with second filter screen 19, second filter screen 19 is located the below of first filter screen 18, is equipped with second waste residue discharge port 14 on the lateral wall of the reation kettle body 1 of the lower one end in second filter screen 19 position. Specifically, the second filter 19 may be made of cloth material. Preferably, the angle of inclination of the second filter 19 is 20 °.
Further, still be equipped with in the reation kettle body 1 and wash shower 3, wash shower 3 and be located stirring vane 21's top, wash and spray and go up the interval and be provided with a plurality of shower heads 31. The arranged spray header 31 can clean the interior of the reaction kettle body 1.
Further, a handle 161 is arranged at one end of the partition 16 extending out of the reaction kettle, and a sealing ring is arranged at the joint of the partition 16 and the reaction kettle body 1. The handle 161 is provided for pulling the partition 16, and the sealing ring is provided for improving the sealing performance of the connection between the partition 16 and the reaction kettle body 1.
During operation, the material gets into reation kettle body 1 from feed inlet 12 in, after the reaction is accomplished, opens baffle 16 (through pulling baffle 16 left), and the material pours to first filter screen 18 on (block that piece 15 can play certain buffer memory effect to the material this moment), and the material filters through first filter screen 18, and the solid waste who stays first filter screen 18 top is discharged from first waste discharge port 13 under the promotion of waste material push rod 17. The second filter screen 19 filters the material after first filter screen 18 filters again for the second time, and remaining waste residue on the second filter screen 19 discharges through second waste residue discharge port 14 (because second filter screen 19 sets up that inclines, therefore the waste residue on the second filter screen 19 can get into second waste residue discharge port 14 automatically), and the waste material is through twice after filtering, and the waste water that remains at last passes through the leakage fluid dram and discharges.
In other embodiments, the outer surface of the reaction kettle body is provided with the control box and the servo motor for controlling the partition plate to move, the control box is internally provided with the microcontroller, the microcontroller is electrically connected with the servo motor, and when the microcontroller receives a control instruction, the servo motor is controlled to drive the partition plate to move, so that the intelligent degree is improved.
The scheme does not need to discharge solid-liquid mixed materials in the reaction kettle to the outside, and then separates the solid-liquid mixture in a filtering mode of a centrifugal machine or a plate-and-frame filter press, so that the energy conservation is facilitated.
The technical contents of the present invention are further illustrated by the examples only for the convenience of the reader, but the embodiments of the present invention are not limited thereto, and any technical extension or re-creation based on the present invention is protected by the present invention. The protection scope of the invention is subject to the claims.

Claims (8)

1. A solid-liquid separation mechanism of a reaction kettle comprises a reaction kettle body and a stirrer; the reaction kettle is characterized in that the top of the reaction kettle body is provided with an air outlet, the side surface is provided with a feed inlet, and the bottom is provided with a liquid outlet; the stirrer comprises a stirring shaft and a driving motor fixed at the top of the stirring shaft; the lower end of the stirring shaft is positioned in the reaction kettle body, and the upper end of the stirring shaft penetrates through the reaction kettle body and is connected with the output end of the driving motor; the outer surface of the stirring shaft is provided with stirring blades; a partition plate capable of being pulled transversely is arranged in the reaction kettle body; a plurality of blocking blocks are also arranged in the reaction kettle body and are positioned above the partition plate; still be equipped with first filter screen in the reation kettle body, first filter screen is located the below of baffle, first filter screen in be equipped with the waste material push rod between the baffle, be equipped with first waste residue discharge port on the lateral wall of the reation kettle body of one of them one end of first filter screen.
2. The solid-liquid separating mechanism of reactor according to claim 1, wherein the barrier is in the shape of an arch protruding upward.
3. The solid-liquid separation mechanism of a reaction kettle according to claim 1, characterized in that a second filter screen is obliquely arranged in the reaction kettle body, the second filter screen is positioned below the first filter screen, and a second waste residue discharge port is arranged on the side wall of the reaction kettle body at the lower end of the second filter screen.
4. The solid-liquid separation mechanism of the reaction kettle according to claim 3, wherein the first filter screen is provided with a plurality of round or triangular meshes.
5. The solid-liquid separation mechanism of the reaction kettle according to claim 3, wherein the first filter screen is made of ceramic or glass.
6. The solid-liquid separation mechanism of a reaction kettle according to claim 1, wherein the inclination angle of the second filter screen is 15 ° to 25 °.
7. The solid-liquid separation mechanism of the reaction kettle according to claim 1, wherein a cleaning spray pipe is further arranged in the reaction kettle body, the cleaning spray pipe is positioned above the stirring blade, and a plurality of spray heads are arranged on the cleaning spray pipe at intervals.
8. The solid-liquid separation mechanism of the reaction kettle according to claim 1, wherein a handle is arranged at one end of the partition plate extending out of the reaction kettle, and a sealing ring is arranged at the joint of the partition plate and the reaction kettle body.
CN201910967034.0A 2019-10-12 2019-10-12 Solid-liquid separation mechanism of reaction kettle Pending CN110559974A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910967034.0A CN110559974A (en) 2019-10-12 2019-10-12 Solid-liquid separation mechanism of reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910967034.0A CN110559974A (en) 2019-10-12 2019-10-12 Solid-liquid separation mechanism of reaction kettle

Publications (1)

Publication Number Publication Date
CN110559974A true CN110559974A (en) 2019-12-13

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Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113731336A (en) * 2021-09-26 2021-12-03 渤海宏铄(连云港)清洁技术有限公司 Industrial waste salt treatment device capable of quickly decomposing waste salt and use method thereof
CN115518441A (en) * 2022-11-03 2022-12-27 安徽睿弘环保科技有限公司 Desulfurization waste liquid acidification pretreatment filtration equipment

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20120084460A (en) * 2011-01-20 2012-07-30 이엔비나노텍(주) Manufacturing device of nanoporous silica using filter media
CN204768713U (en) * 2015-07-03 2015-11-18 宁波大学 Make things convenient for solid -liquid separation's reation kettle
CN207153705U (en) * 2017-08-28 2018-03-30 新能能源有限公司 A kind of reactor with solid-liquid separation function
CN208244627U (en) * 2018-04-03 2018-12-18 天津金隅宝辉砂浆有限公司 Agitating auger is used in a kind of production of additive
CN209302758U (en) * 2018-12-18 2019-08-27 丹东康复制药有限公司 A kind of reaction kettle convenient for separation of solid and liquid
CN211051493U (en) * 2019-10-12 2020-07-21 深圳市驭智装备技术有限公司 Solid-liquid separation mechanism of reaction kettle

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20120084460A (en) * 2011-01-20 2012-07-30 이엔비나노텍(주) Manufacturing device of nanoporous silica using filter media
CN204768713U (en) * 2015-07-03 2015-11-18 宁波大学 Make things convenient for solid -liquid separation's reation kettle
CN207153705U (en) * 2017-08-28 2018-03-30 新能能源有限公司 A kind of reactor with solid-liquid separation function
CN208244627U (en) * 2018-04-03 2018-12-18 天津金隅宝辉砂浆有限公司 Agitating auger is used in a kind of production of additive
CN209302758U (en) * 2018-12-18 2019-08-27 丹东康复制药有限公司 A kind of reaction kettle convenient for separation of solid and liquid
CN211051493U (en) * 2019-10-12 2020-07-21 深圳市驭智装备技术有限公司 Solid-liquid separation mechanism of reaction kettle

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113731336A (en) * 2021-09-26 2021-12-03 渤海宏铄(连云港)清洁技术有限公司 Industrial waste salt treatment device capable of quickly decomposing waste salt and use method thereof
CN115518441A (en) * 2022-11-03 2022-12-27 安徽睿弘环保科技有限公司 Desulfurization waste liquid acidification pretreatment filtration equipment
CN115518441B (en) * 2022-11-03 2024-09-13 安徽睿弘环保科技有限公司 Desulfurization waste liquid system sour pretreatment filtration equipment

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