CN110511007A - A kind of core-type induction furnace furnace lining material and preparation method thereof - Google Patents

A kind of core-type induction furnace furnace lining material and preparation method thereof Download PDF

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Publication number
CN110511007A
CN110511007A CN201910832484.9A CN201910832484A CN110511007A CN 110511007 A CN110511007 A CN 110511007A CN 201910832484 A CN201910832484 A CN 201910832484A CN 110511007 A CN110511007 A CN 110511007A
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granularity
glass sand
mesh
sand
furnace lining
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赵方玉
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Gaoyou Ruiyi Furnace Lining Material Co Ltd
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Gaoyou Ruiyi Furnace Lining Material Co Ltd
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    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/66Monolithic refractories or refractory mortars, including those whether or not containing clay
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    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206Magnesium oxides or oxide-forming salts thereof
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    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3409Boron oxide, borates, boric acids, or oxide forming salts thereof, e.g. borax
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
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    • C04B2235/5463Particle size distributions
    • C04B2235/5472Bimodal, multi-modal or multi-fraction

Abstract

The present invention relates to furnace lining technical fields, and disclose a kind of core-type induction furnace furnace lining material, raw material including following parts by weight: 100 parts of glass sand, 5~7 parts of magnesia powder, 0.08 part of zirconium oxide, 0.8~1.2 part of boric acid, the glass sand includes the glass sand of following granularity by weight percentage: the glass sand 15~25% that granularity is the glass sand 15~25% of 5~10 mesh, granularity is 15~30 mesh, the glass sand 15~25% that granularity is 35~40 mesh.The core-type induction furnace furnace lining material and preparation method thereof, by using glass sand, and the granularity that rational proportion is different, the intermediate frequency furnace lining porosity is small, and compactness is high, agglutinating property is good and resistance to chilling and shock heating is good, furnace lining material refractoriness of the present invention is higher than 1720 DEG C, and softening temperature is higher than 1700 DEG C, has good hot stability, chemical stability and mechanical performance, good insulating, construction can well and sintering character is good.

Description

A kind of core-type induction furnace furnace lining material and preparation method thereof
Technical field
The present invention relates to furnace lining technical field, specially a kind of core-type induction furnace furnace lining material and preparation method thereof.
Background technique
The intermediate frequency furnace that stove namely our written words are said is worthy of careful study about intermediate frequency furnace lining with refractory material very much, He not only involves furnace life, it is necessary to which guaranteeing experienced steel grade, these all have to be understood that clear, furnace lining when introducing to client It is divided into ruining for acid refractory, neutral refractory, basic refractory and stove fire proof material of furnace lining with refractory material Mechanism is damaged, not in addition being in the mood for induction melting furnace refractory material there are also intermediate frequency or intermediate frequency should have the characteristics that this is as one Qualified cupola drop work must it is to be understood that common sense.
Notification number: a kind of medium-frequency induction furnace furnace lining material and preparation method thereof is proposed in CN104446547A and is used Method, matrix of this application by adjusting magnesian ramming mass in different parts are formed, so that slag line is close with converter life, are reduced Intermediate frequency furnace ramming mass use cost, but the invention material coarseness sand grains is excessive, knotting density contrast, what is contacted with metal Surface is difficult to be formed firm and complete sinter layer, and makes to expand when lining sintering larger, easily causes breakout, porosity Increase, influences lining durability so proposing that a kind of core-type induction furnace is solved to mention among the above with furnace lining material and preparation method thereof Out the problem of.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of core-type induction furnace furnace lining material and its preparation sides Method has good hot stability, chemical stability and mechanical performance, and good insulating, construction energy is good, sintering character is good, builds Furnace and it is easy to maintenance the advantages that, solve that material coarseness sand grains is excessive, and knotting density contrast is difficult on the surface contacted with metal Firm and complete sinter layer is formed, and makes to expand when lining sintering larger, easily causes breakout, porosity increases, shadow The problem of ringing lining durability.
(2) technical solution
To realize above-mentioned good hot stability, chemical stability and mechanical performance, good insulating, construction can good, burning Tie performance is good, brickwork and it is easy to maintenance the purpose of, the invention provides the following technical scheme:
A kind of core-type induction furnace furnace lining material, which is characterized in that the raw material including following parts by weight: high-purity quartz 100 parts of sand, 5~7 parts of magnesia powder, 0.08 part of zirconium oxide, 0.8~1.2 part of boric acid, the glass sand is by weight percentage Glass sand including following granularity: granularity is the glass sand 15~25% of 5~10 mesh, granularity is 15~30 mesh Glass sand 15~25%, the glass sand 15~25% that granularity is 35~40 mesh, granularity be 45~50 purposes Glass sand 10~20% and granularity be 60~70 mesh glass sand 5~8% and granularity 200 mesh 8~ 10% glass sand.
Preferably, the glass sand of the furnace lining raw material includes the high-purity quartz of following granularity by weight percentage Sand: granularity is the glass sand 18~22% of 5~8 mesh, granularity is 20~25 mesh glass sand 18~22%, grain Degree is that glass sand 18~22%, the glass sand 16~18% that granularity is 48~50 mesh and the granularity of 38 mesh are 8~10% glass sands of the glass sands 6~8% of 63~66 mesh and granularity in 200 mesh.
Preferably, the glass sand of the furnace lining raw material includes the high-purity quartz of following granularity by weight percentage Sand: granularity is the glass sand 22% of 7 mesh, granularity is 28 mesh glass sand 24%, granularity are that 38 purposes are high-purity Degree quartz sand 20%, the glass sand 20% that granularity is 46 mesh and granularity are the glass sand 6% and grain of 68 mesh Spend 8% glass sand in 200 mesh.
Preferably, the glass sand of the furnace lining raw material includes the high-purity quartz of following granularity by weight percentage Sand: granularity is the glass sand 18% of 6 mesh, granularity is 25 mesh glass sand 22%, granularity are that 36 purposes are high-purity Degree quartz sand 25%, the glass sand 18% that granularity is 45 mesh and granularity are the glass sand 8% and grain of 68 mesh Spend 9% glass sand in 200 mesh.
Preferably, the glass sand includes the chemical component of following weight percent: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%.
Another technical problem to be solved by the present invention is that a kind of preparation method of core-type induction furnace furnace lining material is provided, The following steps are included:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
(3) beneficial effect
Compared with prior art, the present invention provides a kind of core-type induction furnace furnace lining material and preparation method thereof, tools It is standby following the utility model has the advantages that
The core-type induction furnace furnace lining material and preparation method thereof, by using glass sand, and rational proportion Different granularities, the intermediate frequency furnace lining porosity is small, and compactness is high, and agglutinating property is good and resistance to chilling and shock heating is good;In furnace lining material Magnesia powder is added, furnace lining material is effectively prevent to generate glass phase and soften at high temperature, boric acid, which is added, can reduce furnace lining material Sintering temperature promotes the formation of spinelle;Furnace lining material refractoriness of the present invention is higher than 1720 DEG C, and softening temperature is higher than 1700 DEG C, With good hot stability, chemical stability and mechanical performance, good insulating, construction can it is good, sintering character is good, brickwork and It is easy to maintenance.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution in the embodiment of the present invention is clearly and completely retouched It states, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts Example, shall fall within the protection scope of the present invention.
A kind of embodiment one: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of core-type induction furnace furnace lining material, the raw material including following parts by weight: 100 parts of glass sand, magnesium 6 parts of emery dust, 0.08 part of zirconium oxide, 1.0 parts of boric acid;The glass sand includes the chemical component of following weight percent: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is by weight Percentage includes the glass sand of following granularity: granularity is the glass sand 22% of 7 mesh, granularity is that 28 purposes are high-purity Spend quartz sand 24%, the glass sand 20% that granularity is 38 mesh, the glass sand 20% and grain that granularity is 46 mesh Degree be 68 mesh glass sand 6% and granularity 200 mesh 8% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
A kind of embodiment two: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of durable type intermediate frequency furnace acid liner material, the raw material including following parts by weight: 100 parts of glass sand, 5 parts of magnesia powder, 0.08 part of zirconium oxide, 0.8 part of boric acid;The glass sand include following weight percent chemistry at Point: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is pressed Weight percent includes the glass sand of following granularity: granularity is the glass sand 18% of 6 mesh, granularity is 25 purposes The glass sand 18% that glass sand 22%, granularity are the glass sand 25% of 36 mesh, granularity is 45 mesh with And granularity be 68 mesh glass sand 8% and granularity 200 mesh 9% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
A kind of embodiment three: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of durable type intermediate frequency furnace acid liner material, the raw material including following parts by weight: 100 parts of glass sand, 7 parts of magnesia powder, 0.08 part of zirconium oxide, 1.2 parts of boric acid;The glass sand include following weight percent chemistry at Point: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is pressed Weight percent includes the glass sand of following granularity: granularity is the glass sand 15% of 5 mesh, granularity is 15 purposes The glass sand 20% that glass sand 25%, granularity are the glass sand 25% of 35 mesh, granularity is 45 mesh with And granularity be 60 mesh glass sand 5% and granularity 200 mesh 10% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
A kind of example IV: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of durable type intermediate frequency furnace acid liner material, the raw material including following parts by weight: 100 parts of glass sand, 5.5 parts of magnesia powder, 0.08 part of zirconium oxide, 0.9 part of boric acid;The glass sand include following weight percent chemistry at Point: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is pressed Weight percent includes the glass sand of following granularity: granularity is the glass sand 25% of 10 mesh, granularity is 30 mesh Glass sand 25%, the glass sand 15% that granularity is 40 mesh, the glass sand 19% that granularity is 50 mesh And granularity be 70 mesh glass sand 8% and granularity 200 mesh 8% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
A kind of embodiment five: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of durable type intermediate frequency furnace acid liner material, the raw material including following parts by weight: 100 parts of glass sand, 5.5 parts of magnesia powder, 0.08 part of zirconium oxide, 0.4 part of boric acid;The glass sand include following weight percent chemistry at Point: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is pressed Weight percent includes the glass sand of following granularity: granularity is the glass sand 25% of 10 mesh, granularity is 30 mesh Glass sand 25%, the glass sand 15% that granularity is 40 mesh, the glass sand 19% that granularity is 50 mesh And granularity be 70 mesh glass sand 6% and granularity 200 mesh 7% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
A kind of embodiment six: core-type induction furnace furnace lining material and preparation method thereof, comprising the following steps:
A kind of durable type intermediate frequency furnace acid liner material, the raw material including following parts by weight: 100 parts of glass sand, 4.5 parts of magnesia powder, 0.08 part of zirconium oxide, 0.3 part of boric acid;The glass sand include following weight percent chemistry at Point: SiO299.5%, Al2O30.3%, Fe2O30.04%, ZrO20.06%, impurity 0.1%;The glass sand is pressed Weight percent includes the glass sand of following granularity: granularity is the glass sand 25% of 10 mesh, granularity is 30 mesh Glass sand 25%, the glass sand 15% that granularity is 40 mesh, the glass sand 19% that granularity is 50 mesh And granularity be 70 mesh glass sand 10% and granularity 200 mesh 11% glass sand.
A kind of preparation method of core-type induction furnace furnace lining material comprises the following sequential steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, in revolving speed 400-600r/ 30-40min is stirred under min and obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) green compact will be formed at green compact by mud cake prepared by step 3) being sent to molding machine compression moulding at 80-100MPa It is sent into the saturated vapor curing kilns that temperature is 120-150 DEG C and continues to conserve 17-20h, then natural cooling, dries in the shade, glazing, then Sintering.
The beneficial effects of the present invention are: using glass sand, and the granularity that rational proportion is different, intermediate frequency furnace lining gas Porosity is small, and compactness is high, and agglutinating property is good and resistance to chilling and shock heating is good;Magnesia powder is added in furnace lining material, at high temperature effectively Prevent furnace lining material from generating glass phase and softening, boric acid, which is added, can reduce the sintering temperature of furnace lining material, promote the shape of spinelle At;Furnace lining material refractoriness of the present invention is higher than 1720 DEG C, and softening temperature is higher than 1700 DEG C, has good hot stability, change Learn stability and mechanical performance, good insulating, construction can it is good, sintering character is good, brickwork and easy to maintenance.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of core-type induction furnace furnace lining material, which is characterized in that the raw material including following parts by weight: glass sand 100 parts, 5~7 parts of magnesia powder, 0.08 part of zirconium oxide, 0.8~1.2 part of boric acid, the glass sand wraps by weight percentage Include the glass sand of following granularity: granularity is the glass sand 15~25% of 5~10 mesh, granularity is 15~30 purposes The height that glass sand 15~25%, granularity are the glass sand 15~25% of 35~40 mesh, granularity is 45~50 mesh Purity quartz sand 10~20% and granularity be 60~70 mesh glass sand 5~8% and granularity 200 mesh 8~ 10% glass sand.
2. a kind of core-type induction furnace furnace lining material according to claim 1 and preparation method thereof, which is characterized in that institute The glass sand for stating furnace lining raw material includes the glass sand of following granularity by weight percentage: granularity is 5~8 purposes The high-purity that glass sand 18~22%, granularity are the glass sand 18~22% of 20~25 mesh, granularity is 38 mesh Quartz sand 18~22%, granularity be 48~50 mesh glass sand 16~18% and granularity be 63~66 mesh high-purity 8~10% glass sands of quartz sand 6~8% and granularity in 200 mesh.
3. a kind of core-type induction furnace furnace lining material according to claim 1 and preparation method thereof, which is characterized in that institute The glass sand for stating furnace lining raw material includes the glass sand of following granularity by weight percentage: granularity is the height of 7 mesh Purity quartz sand 22%, granularity are the glass sand 24% of 28 mesh, granularity is 38 mesh glass sand 20%, granularity The glass sand 6% and granularity that glass sand 20% and granularity for 46 mesh are 68 mesh are in the 8% high-purity of 200 mesh Spend quartz sand.
4. a kind of core-type induction furnace furnace lining material according to claim 1 and preparation method thereof, which is characterized in that institute The glass sand for stating furnace lining raw material includes the glass sand of following granularity by weight percentage: granularity is the height of 6 mesh Purity quartz sand 18%, granularity are the glass sand 22% of 25 mesh, granularity is 36 mesh glass sand 25%, granularity The glass sand 8% and granularity that glass sand 18% and granularity for 45 mesh are 68 mesh are in the 9% high-purity of 200 mesh Spend quartz sand.
5. a kind of core-type induction furnace furnace lining material according to claim 1 and preparation method thereof, which is characterized in that institute The chemical component that glass sand includes following weight percent: SiO299.5%, Al 2O30.3% is stated, Fe2O30.04%, ZrO20.06%, impurity 0.1%.
6. a kind of preparation method of core-type induction furnace furnace lining material, which comprises the following steps:
1) each raw material is weighed according to parts by weight;
2) glass sand and magnesia powder is dry-mixed uniformly mixed, obtain mixture;
3) mixture prepared by step 2) is mixed with zirconium oxide and boric acid and is placed in blender, at revolving speed 400-600r/min Stirring 30-40min obtains slurry, and slurry is sent into wet ball mill after ball milling 4-5h and carries out press filt, obtains mud cake;
4) mud cake prepared by step 3) molding machine compression moulding at 80-100MPa is sent to be sent into molding green compact at green compact Continue to conserve 17-20h in the saturated vapor curing kilns that temperature is 120-150 DEG C, then natural cooling, dries in the shade, and glazing is reburned Knot.
CN201910832484.9A 2019-09-04 2019-09-04 A kind of core-type induction furnace furnace lining material and preparation method thereof Pending CN110511007A (en)

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Application publication date: 20191129