CN110510651A - The method and device thereof of atrament in a kind of abjection ardealite - Google Patents
The method and device thereof of atrament in a kind of abjection ardealite Download PDFInfo
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- CN110510651A CN110510651A CN201910743720.XA CN201910743720A CN110510651A CN 110510651 A CN110510651 A CN 110510651A CN 201910743720 A CN201910743720 A CN 201910743720A CN 110510651 A CN110510651 A CN 110510651A
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- Prior art keywords
- ardealite
- atrament
- thickener
- cream
- clear liquid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/02—Settling tanks with single outlets for the separated liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/26—Separation of sediment aided by centrifugal force or centripetal force
- B01D21/267—Separation of sediment aided by centrifugal force or centripetal force by using a cyclone
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/46—Sulfates
- C01F11/468—Purification of calcium sulfates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B11/00—Calcium sulfate cements
- C04B11/26—Calcium sulfate cements strating from chemical gypsum; starting from phosphogypsum or from waste, e.g. purification products of smoke
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Degasification And Air Bubble Elimination (AREA)
Abstract
The method and device thereof of atrament, after ardealite is starched again, are classified to obtain the ardealite containing a large amount of atraments by two stages of hydrocyclones in a kind of abjection ardealite;Pump is delivered to the central tube of pre- thickener, layering is settled in pre- thickener, it is discharged compared with rubble cream from pre- thickener bottom, relatively fine gypsum and part atrament are discharged from pre- thickener middle and upper part overflow port, the relatively fine gypsum and part atrament gone out from overflow port overflow enters microlith cream concentrator central tube by chute, the further sedimentation layering in microlith cream concentrator, concentrator setting gear foam circle, black foam draws chute by black foam and enters black foam outlet discharge system, clear liquid is discharged from clear liquid overflow port and flows into liquid tank by chute, bottom discharge system of the microlith cream from concentrator, the present invention realizes the purpose of atrament in abjection ardealite using the sinking speed difference of different-grain diameter ardealite, process flow is simple, the application range of ardealite is expanded while improving ardealite grade.
Description
Technical field
The invention belongs to phosphorous chemical industry field and ardealite comprehensive utilization techniques, and in particular to black in a kind of abjection ardealite
The method and device thereof structure technology of substance.
Background technique
Phosphogypsum dihydrate is the industrial solid castoff excluded in dihydrate wet-process phosphoric acid production process, and main component is two
H 2 O calcium sulphate (CaSO4·2H2O), in addition to this also containing a small amount of soluble P2O5, F, the harmful substances such as black organic matter.Phosphorus
Organic matter in gypsum both increased building gypsum normal consistency water requirement, and the combination that can also weaken between dihydrate gypsum crystal makes firmly
Change body porosity to improve, but intensity reduces, compression strength can be made to reduce about 15% 0.1% low content organic matter,
Porosity increases by 9% (organic matter, eutectic phosphorus in the ardealite such as Peng Jiahui and its influence [J] construction material to performance
Report, 2003 (3): 221-226).
By ardealite resource utilization, in addition to solubility P in ardealite to be eliminated2O5, F to the influence of ardealite outside, also
Need to remove the atrament (organic matter) in ardealite.The method that major part technique is all made of flotation at present removes in ardealite
Atrament (organic matter), it is possible to bring new impurity into, and floating agent price general charged is expensive, is unfavorable for industrialization and pushes away
Extensively.Chinese patent CN105000585A is disclosed in a kind of ardealite and purification process technique, and this patent reports a kind of organic
Trash eliminator, but the device separates organic matter by aeration mode, and treating capacity is small, and the ardealite upper layer after separation is also contained
Partial organic matter, the organic matter isolated also contain a large amount of gypsum, are unfavorable for the resource utilization of ardealite.
Summary of the invention
The purpose of the present invention is to provide a kind of high degree of automation, process flow is simple, low energy consumption, gypsum utilization rate is high
Removal ardealite in atrament method.
Experiment shows: the partial size of ardealite is different, and contained impurity and sinking speed is different.Partial size is in+400 purposes
Ardealite, sinking speed are 2~5cm/min, and dihydrate gypsum content is greater than 85% in ardealite;Partial size is in -400 mesh~+600 mesh
Ardealite, sinking speed is 0.5~1cm/min, and dihydrate gypsum content is greater than 80% in ardealite;Phosphorus of the partial size in -600 mesh
Gypsum sinking speed is less than 0.3cm/min, and main component is the atrament containing organic matter in ardealite, and dihydrate gypsum content is small
In 50%.It can be easily by the same of the atrament abjection in ardealite using the sinking speed difference of different-grain diameter ardealite
When, ardealite is classified.
To achieve the above object, the present invention is achieved by following steps:
A kind of method of atrament in abjection ardealite, the invention is characterised in that, it is achieved by following steps:
A, it after ardealite is starched again, is classified to obtain the ardealite containing a large amount of atraments by two stages of hydrocyclones;
B, the ardealite containing a large amount of atraments is delivered to the central tube of pre- thickener by pump, sinks in pre- thickener
Drop layering, is discharged compared with rubble cream from pre- thickener bottom;Relatively fine gypsum and part atrament are arranged from pre- thickener middle and upper part
Out;Black foam is discharged from pre- thickener top;Tentatively achieve the purpose that remove atrament in ardealite;
C, it is dense that the relatively fine gypsum and part atrament gone out from pre- thickener overflow by chute enters microlith cream
Machine, the further sedimentation layering in microlith cream concentrator, black foam is by black foam outlet discharge system, and clear liquid is from clear liquid overflow port
It is discharged and flows into liquid tank;Compared with microlith cream from the bottom discharge system of microlith cream concentrator, reach black object in removal ardealite
The purpose of matter.
Ardealite partial size 90%-400 mesh of the present invention.
Device used by the method for atrament in a kind of abjection ardealite, including pre- thickener and microlith cream it is dense
Machine;Wherein:
Pre- thickener by outer cylinder, central tube, black foam outlet, overflow port, the outlet of rubble cream, speed reducer, scrape rake and form;Outside
It is circular cylinder body lower part is cone that barrel structure, which is top, and central tube is located at outer cylinder central upper portion position, in the top side of outer cylinder
Face is equipped with black foam outlet, is equipped with overflow port in the upper side of outer cylinder, and black foam outlet is 150mm~600mm higher than overflow port,
The outlet of rubble cream is equipped with for being discharged compared with rubble cream in the bottom sides of outer cylinder;Speed reducer is provided above central tube and passes through
Shaft is connected with the rake of scraping for being located at lower part in outer cylinder;
Microlith cream concentrator by black foam outlet, black foam draw chute, gear foam circle, clear liquid overflow baffle, clear liquid overflow port,
Central tube, decelerating motor, scrapes rake composition at bottom discharging mouth;Microlith cream concentrator is circular tube structure, and bottom is cone knot
Structure;Central tube is located at microlith cream concentrator internal upper part center, and decelerating motor is located above central tube, and speed motor passes through shaft
It connect with central tube and is connected with the rake of scraping for being located at bottom in cone;Pass through respectively from the inside to the outside on microlith cream concentrator top
Dowel weldering is connected with gear foam circle and clear liquid overflow launder baffle, wherein gear foam circle it is 100mm higher than clear liquid overflow launder baffle~
500mm;It is 100mm~1000mm smaller than clear liquid overflow launder baffle diameter to keep off foam loop diameter, keep off foam circle and clear liquid overflow launder baffle it
Between be equipped with black foam and draw chute, black foam draws chute and is connected with black foam outlet, and black foam draws chute and black foam outlet along keeping off
Equivalent arrangements have 6~24 groups between foam circle and clear liquid overflow launder baffle;Black foam draws chute by black foam and enters black foam outlet
Discharge system, clear liquid from the discharge of clear liquid overflow port by chute inflow liquid tank, compared with microlith cream from the bottom of microlith cream concentrator
Discharge gate discharge system achievees the purpose that remove atrament in ardealite.
The beneficial effects of the present invention are:
1, whole process is physical process, and it is low not introduce new chemical agent operating cost;
2, after ardealite sequentially settles in pre- thickener and microlith cream concentrator, the atrament in ardealite is substantially
Deviate from;
3, after ardealite sequentially settles in pre- thickener and microlith cream concentrator, the grade of ardealite is improved;
4, the clear liquid overflowed from microlith cream concentrator is substantially free of atrament, can shorten subsequent processing work
Sequence saves subsequent processing cost.
Detailed description of the invention
Fig. 1 is process flow diagram of the embodiment of the present invention;
Fig. 2 is the thickener elevation in the embodiment of the present invention;
Fig. 3 is the microlith cream concentrator elevation in the embodiment of the present invention;
Fig. 4 is the microlith cream concentrator top view in the embodiment of the present invention.
Specific embodiment
Technical solution in order to enable those skilled in the art to better understand the present invention, below with reference to embodiment to of the invention
Essential characteristics and advantage are described further, only a specific embodiment of the invention, but protection of the invention as described below
Range is not limited to this, and anyone skilled in the art in the technical scope disclosed by the present invention, can think easily
Change or replacement are obtained, should be covered by the protection scope of the present invention.
Embodiment 1
For the atrament in abjection ardealite, the present invention is achieved by following steps: see Fig. 1,
1, it after ardealite is starched again, is classified to obtain the ardealite containing a large amount of atraments by two stages of hydrocyclones, containing black
Color substance;
2, the ardealite containing a large amount of atraments is delivered to the central tube A11 of pre- thickener 1 by pump, in pre- thickener
Middle sedimentation layering, compared with rubble cream from 14 discharge of pre- thickener bottom rubble cream outlet, relatively fine gypsum and part atrament from
Pre- thickener middle and upper part overflow port 13 is discharged, and black foam is discharged from the black foam outlet 12 in pre- thickener top, tentatively reaches dephosphorization
The purpose of atrament in gypsum;
3, the relatively fine gypsum and part atrament gone out from pre- 13 overflow of thickener overflow port is entered thin by chute
Gypsum concentrator central tube B26, the further sedimentation layering in microlith cream concentrator 2, microlith cream concentrator setting gear foam circle are black
Foam draws chute 22 by black foam and enters black foam outlet B21 discharge system, and clear liquid passes through chute from the discharge of clear liquid overflow port 25
Liquid tank is flowed into, compared with microlith cream from 27 discharge system of bottom discharging mouth of concentrator 2, reaches atrament in removal ardealite
Purpose.
As shown in Figure 2: pre- thickener 1 exports 14 by central tube A11, black foam outlet A12, overflow port 13, rubble cream, subtracts
Fast machine A15, rake A16 composition is scraped, the top of pre- thickener 1 is equipped with black foam outlet 12, and the middle and upper part of pre- thickener 1 is equipped with overflow
Mouth 13, black foam outlet A12 is 150mm higher than overflow port 13, and speed reducer A15 is connected with rake A16 is scraped.
As shown in Figure 3, Figure 4: microlith cream concentrator 2 draws chute 22 by black foam outlet B21, black foam, keeps off foam circle 23, clear
Liquid overflow baffle 24, central tube B26, bottom discharging mouth 27, decelerating motor B28, scrapes rake B29 composition microlith at clear liquid overflow port 25
Cream concentrator 2 is sequentially equipped with gear foam circle 23, clear liquid overflow launder baffle 24 from the inside to the outside, keeps off foam circle 23 than clear liquid overflow launder baffle 24
High 300mm, gear foam loop diameter is 600mm smaller than clear liquid overflow launder baffle diameter, keeps off between foam circle 23 and clear liquid overflow launder baffle 24
Chute 22 is drawn equipped with black foam, black foam draws chute 22 and is connected with black foam outlet B21, and speed reducer B28 is connected with rake B29 is scraped,
Black foam draws chute and black foam outlet 12 groups of equivalent arrangements between gear foam circle and clear liquid baffle.
Embodiment 2
Deviate from the self-produced phosphogypsum dihydrate of company using method described in embodiment 1, abjection front and back ardealite physical and chemical indexes are such as
Shown in following table:
Embodiment 3
Deviate from the self-produced phosphogypsum dihydrate of company using method described in embodiment 1, abjection front and back ardealite physical and chemical indexes are such as
Shown in following table:
Embodiment 4
Deviate from the self-produced phosphogypsum dihydrate of company using method described in embodiment 1, abjection front and back ardealite physical and chemical indexes are such as
Shown in following table:
Claims (3)
1. a kind of method of atrament in abjection ardealite, which is characterized in that be achieved by following steps:
A, it after ardealite is starched again, is classified to obtain the ardealite containing a large amount of atraments by two stages of hydrocyclones;
B, the ardealite containing a large amount of atraments is delivered to the central tube of pre- thickener by pump, the sedimentation point in pre- thickener
Layer, is discharged compared with rubble cream from pre- thickener bottom;Relatively fine gypsum and part atrament are discharged from pre- thickener middle and upper part;It is black
Foam is discharged from pre- thickener top;Tentatively achieve the purpose that remove atrament in ardealite;
C, the relatively fine gypsum and part atrament gone out from pre- thickener overflow enters microlith cream concentrator, In by chute
Further sedimentation layering in microlith cream concentrator, black foam are discharged by black foam outlet discharge system, clear liquid from clear liquid overflow port
And flow into liquid tank;Compared with microlith cream from the bottom discharge system of microlith cream concentrator, reach atrament in removal ardealite
Purpose.
2. the method for atrament in a kind of abjection ardealite according to claim 1, which is characterized in that ardealite partial size
90%-400 mesh.
3. device used by the method for atrament, feature exist in a kind of abjection ardealite according to claim 1
In, including pre- thickener (1) and microlith cream concentrator (2);Wherein:
Pre- thickener (1) is exported by outer cylinder (17), central tube A (11), black foam outlet A (12), overflow port (13), rubble cream
(14), speed reducer A (15), scrape rake A (16) composition;It is circular cylinder body lower part is cone, center that outer cylinder (17) structure, which is top,
Cylinder A (11) is located at outer cylinder (17) central upper portion position, is equipped with black foam outlet A (12) in the top-side of outer cylinder (17), outside
The upper side of cylinder (17) is equipped with overflow port (13), and black foam outlet A (12) is 150mm~600mm higher than overflow port (13), outside
The bottom sides of cylinder (17) are equipped with rubble cream outlet (14) for being discharged compared with rubble cream;Speed reducer A (15) is provided at central tube A
(11) rake A (16) of scraping above and by shaft A (18) and positioned at outer cylinder (17) interior lower part is connected;
Microlith cream concentrator (2) You Heimo outlet B (21), black foam draw chute (22), gear foam circle (23), clear liquid overflow baffle
(24), clear liquid overflow port (25), central tube B (26), bottom discharging mouth (27), decelerating motor B (28), scrape rake B (29) composition;Carefully
Gypsum concentrator (2) is circular tube structure, and bottom is cone structure;Central tube B (26) is located in microlith cream concentrator (2)
Central upper portion position, decelerating motor B (28) are located above central tube B (26), and speed motor B (28) passes through shaft and central tube B
(26) it connects and is connect with rake B (29) of scraping for being located at bottom in cone;Distinguish from the inside to the outside on microlith cream concentrator (2) top
It is connected with gear foam circle (23) and clear liquid overflow launder baffle (24) by dowel weldering, wherein gear foam circle (23) is kept off than clear liquid overflow launder
Plate (24) high 100mm~500mm;It is 100mm~1000mm smaller than clear liquid overflow launder baffle (24) diameter to keep off foam circle (23) diameter, gear
It is equipped with black foam between foam circle (23) and clear liquid overflow launder baffle (24) and draws chute (22), black foam is drawn chute (22) He Heimo and drawn
It exports B (21) to be connected, black foam draws chute (22) He Heimo outlet B (21) along gear foam circle (23) and clear liquid overflow launder baffle
(24) equivalent arrangements have 6~24 groups between;Black foam draws chute (22) by black foam and enters black foam outlet B (21) discharge system
System, clear liquid from clear liquid overflow port (25) discharge by chute inflow liquid tank, compared with microlith cream from the bottom of microlith cream concentrator (2)
Discharge gate (27) discharge system achievees the purpose that remove atrament in ardealite.
Priority Applications (1)
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113511829A (en) * | 2021-04-23 | 2021-10-19 | 四川省生态环境科学研究院 | Method for preparing building gypsum powder from phosphogypsum |
CN115215365A (en) * | 2022-08-24 | 2022-10-21 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for generating and separating gypsum from titanium extraction tailings |
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Cited By (3)
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CN113511829A (en) * | 2021-04-23 | 2021-10-19 | 四川省生态环境科学研究院 | Method for preparing building gypsum powder from phosphogypsum |
CN115215365A (en) * | 2022-08-24 | 2022-10-21 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for generating and separating gypsum from titanium extraction tailings |
CN115215365B (en) * | 2022-08-24 | 2023-11-07 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for generating and separating gypsum from titanium extraction tailings |
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Application publication date: 20191129 |