CN110497546A - The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips - Google Patents

The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips Download PDF

Info

Publication number
CN110497546A
CN110497546A CN201910790559.1A CN201910790559A CN110497546A CN 110497546 A CN110497546 A CN 110497546A CN 201910790559 A CN201910790559 A CN 201910790559A CN 110497546 A CN110497546 A CN 110497546A
Authority
CN
China
Prior art keywords
abrasive
free
silicon
wire
cutting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910790559.1A
Other languages
Chinese (zh)
Inventor
冯砚博
陈博
高博文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Harbin University of Commerce
Original Assignee
Harbin University of Commerce
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Harbin University of Commerce filed Critical Harbin University of Commerce
Priority to CN201910790559.1A priority Critical patent/CN110497546A/en
Publication of CN110497546A publication Critical patent/CN110497546A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B27/00Other grinding machines or devices
    • B24B27/0076Other grinding machines or devices grinding machines comprising two or more grinding tools
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B27/00Other grinding machines or devices
    • B24B27/06Grinders for cutting-off
    • B24B27/0633Grinders for cutting-off using a cutting wire
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B57/00Devices for feeding, applying, grading or recovering grinding, polishing or lapping agents
    • B24B57/04Devices for feeding, applying, grading or recovering grinding, polishing or lapping agents for feeding of solid grinding, polishing or lapping agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28DWORKING STONE OR STONE-LIKE MATERIALS
    • B28D5/00Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
    • B28D5/0058Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material
    • B28D5/007Use, recovery or regeneration of abrasive mediums
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28DWORKING STONE OR STONE-LIKE MATERIALS
    • B28D5/00Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
    • B28D5/04Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor by tools other than rotary type, e.g. reciprocating tools
    • B28D5/045Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor by tools other than rotary type, e.g. reciprocating tools by cutting with wires or closed-loop blades

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Mechanical Treatment Of Semiconductor (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)

Abstract

The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips, belong to semiconductor material processing technique field, solve the problems, such as that silicon crystal slice exists, the method of free-consolidation abrasive compound multiline cut silicon chips includes to carry out sawing to silicon ingot using the method for concretion abrasive multi-wire saw, while the lapping liquid containing suspension diamond abrasive grain is sprayed onto cutting region;In the joint-cutting that the wire of surface consolidated diamond abrasive grain brings the lapping liquid containing suspension diamond abrasive grain into silicon ingot during wire, form free abrasive grain and fixed grain collective effect, sawing is carried out to silicon ingot jointly, silicon ingot is cut into several pieces during time processing;The equipment of free-consolidation abrasive compound multiline cut silicon chips includes free abrasive multi-wire saw equipment, in whole wire surface consolidated diamond abrasive grains of free abrasive multi-wire saw equipment;The present invention is for cutting silicon wafer.

Description

The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips
Technical field
The invention belongs to semiconductor material processing technique fields, and in particular to free-consolidation abrasive compound multi-wire saw silicon The method and apparatus of piece.
Background technique
Semiconductor processing technology based on silicon materials is the new and high technologies such as integrated circuit, electronic information and photovoltaic The key technology condition of industry development.Silicon crystal slice is the front end process of semiconductor processing industry chain, and working ability is direct Determine the performance quality of follow-up process and end product.In order to which the performance and economic benefit of end product is continuously improved, it is desirable that silicon Crystal cut processing technology develops to major diameter, small thickness, high quality, high production capacity, high efficiency and low consumed direction.It is processing On diameter of silicon crystal 300mm or more, and 120 μm of joint-cutting of slice and magnitude below, current extensive use free abrasive is multi-thread Cutting technique and diamond concretion abrasive multi-wire cutting technology.
Free abrasive multi-wire cutting technology is to apply sawing power using multiple tracks parallel wire, is suspended in lapping liquid Abrasive grain as cutting tools, slice processing is carried out to silicon ingot.
Diamond concretion abrasive multi-wire cutting technology is to utilize the parallel of multiple tracks surface consolidated diamond or silicon carbide abrasive particles Wire directly carries out sawing to silicon ingot, while cooling using coolant liquid.
It for free abrasive multi-wire cutting technology, is suspended in lapping liquid because abrasive grain is free, effectively cutting contact interface Very little causes clipping time long, and cutting efficiency is relatively low;By the saw size of silk diameter, tensile force size, lapping liquid density and The silicon chip surface roughness of the influence of the factors such as viscosity, free abrasive cutting is big;Use 120 μm of diameter thinner saw silk cuttings Die size deviation is often higher than the saw silk using 140 μm of diameter;Free abrasive cuts silicon ingot with brittle mode, processing Silicon crystal slice surface is isotropic pattern;And is made joint-cutting entrance, centre by the bullet stream effects of lapping liquid and cut Seam outlet grinding degree is irregular, causes silicon crystal slice different location quality different, angularity, curvature and the TTV of silicon wafer Equal face shape errors change greatly;These problems limit the application and development of free abrasive wire saw cutting.
For concretion abrasive multi-wire cutting technology, abrasive grain and the direct rigid contact of silicon ingot, although cutting efficiency increases, and And with the increase of saw silk abrasion, better plastic removal effect is shown, face crack is less, but face crack is deeper, The average fracture strength of chip is lower, and saws the lost of life of silk;In addition, concretion abrasive cutting silicon wafer is crisp-plasticity mixing Easily there is obvious cut mark parallel, the depth is irregular in mode cutting, silicon crystal slice surface;Concretion abrasive sawing silicon wafers elasticity modulus It is stronger in the direction for being parallel to stria, it is weaker perpendicular to the direction of stria;The silicon wafer of diamond concretion abrasive multi-wire saw sawing The silicon wafer of specific ionization abrasive material cutting has unacceptable high breakage rate;Concretion abrasive cuts silicon crystal slice along vertical cutting line side To Critical fracture performance be free abrasive cutting silicon crystal be sliced 57%, cause concretion abrasive cutting silicon wafer extreme fragile Concrete reason is now also indefinite;Due to these essential drawbacks, concretion abrasive multi-wire cutting technology can not replace trip completely From w ire s aws h cutting processing.
On the whole, for Multi-wire wafer cutting technique always to workpieces processing size is increased, slice is thin, improves Si wafer quality Direction is developed.Main target to silicon wafer industry is by reducing total thickness variations and surface defect, to improve the table of silicon wafer Face quality, and productivity is improved by reducing wafer thickness.Silicon ingot is bigger, and grooving is thinner, and that saws silk and silicon ingot fritters seam It lengthens and deepens, lapping liquid is more uneven or even stops, and will seriously affect giving full play to for lapping liquid effect.Semi-conductor silicon chip The growth requirement of industry more brings bigger difficulty to manufacturing technology, and the diameter of silicon wafer is gradually increased, and thickness constantly reduces, at present Processing method be not able to satisfy the demand for development of silicon wafer.
Summary of the invention
The purpose of the present invention is to solve silicon crystal to be sliced the existing above problem, and it is multiple to provide a kind of free-consolidation The method and apparatus of abrasive material multiline cut silicon chips is closed, its technical solution is as follows:
The method of free-consolidation abrasive compound multiline cut silicon chips, it includes the method using concretion abrasive multi-wire saw to silicon Crystal ingot carries out sawing, while the lapping liquid containing suspension diamond abrasive grain is sprayed onto cutting region;Surface consolidated diamond mill In the joint-cutting that the wire of grain brings the lapping liquid containing suspension diamond abrasive grain into silicon ingot during wire, formed free Abrasive grain and fixed grain collective effect carry out sawing to silicon ingot jointly, silicon ingot are cut into number during time processing Piece.
The equipment of free-consolidation abrasive compound multiline cut silicon chips, it includes free abrasive multi-wire saw equipment, free Whole wire surface consolidated diamond abrasive grains of abrasive material multi-wire saw equipment.
The invention has the benefit that the present invention merges the advantages of free-two kinds of abrasive grain grindings of consolidation, mutually make up Respective deficiency;Under the influence of lapping liquid flowing pressure field, velocity field, substantially the free abrasive grain of disordered motion presents certain The characteristics of motion;The enbrittle property of material, free abrasive grain and fixed grain of silicon ingot carries out double rub coupling to silicon ingot Grinding is closed, the contact area of diamond abrasive grain and silicon ingot, the effective cutting performance of enhancing macroscopic view are increased;In process, dissociate With consolidation diamond abrasive grain to the difference of the contact form of silicon ingot, it is caused to hit the difference of mode and number with silicon ingot. Reducing cutting depth is that fragile material improves ductile regime machining, reduces the processing of brittleness domain, to submit fragile material processing quality Key method.Internal energy storage and release summation and the period be diamond abrasive grain grinding silicon wafer material cutting depth at Cause.Fixed grain to the uniform force of silicon ingot and direction it is single, the utilization rate of grinding is higher, the fluid property of sticky lapping liquid Reducing fixed grain enhances microplasticity cutting performance to the parallel cutting crackle of silicon ingot, and increases breaking protection, thus more It is easy effectively to be cut;The coupling shear action of two kinds of abrasive grains is complementary, and more evenly, saw silk removes material to abrasive grain distribution density Rate increases, and improves cutting power.It reduces free abrasive grain to cut silicon ingot brittleness, increases fixed grain to the plasticity of silicon ingot Cutting reduces wafer surface crackle, and machining accuracy significantly improves, and surface quality is more preferable, and the breakage rate of silicon wafer reduces;
The present invention is opposite, and the advantage with existing processing method is: being distributed than the abrasive grain of traditional free abrasive silicon slice processing more equal Even, it is big to be effectively reduced grooving inlet abrasive grain density, and friction is serious, and silicon sheet material each position processes non-uniform situation;Than passing The contact area that binding material between silk and workpiece and abrasive material is sawed in concretion abrasive silicon slice processing of uniting increases.Since viscosity is ground The effect of grinding fluid can make to saw the decline of silk contact pressure, anti-to stop loss disconnected, the service life of increase saw silk;Since machining accuracy significantly improves, It, can silicon wafer with cutting diameter 300mm or more, within 120 μm of thickness so working ability increases;Pass through the matching of grinding parameter With setting, the controllability of diced system is obtained, even more silicon wafer diced system stablizes the basic guarantee processed.
Specifically, the free abrasive grain in the slurry and abrasive grain that consolidates is jointly right respectively and under coupling on saw silk The effects of silicon wafer impact, breakage, indentation, rolling cut.The track of free abrasive grain more order increases effective cutting force, improves material Cut effect.From there through the effect of lapping liquid, mixes in cutting, increase with plasticity in the brittleness that fixed grain carries out silicon crystal The microcosmic processing ingredient of big plastic region.
Crack of silicon chip damage is closely related with surface quality in crystal silicon material slice processing, joint-cutting bottom and joint-cutting side The difference of sub-surface crackle form and distribution, silicon wafer surface degree of injury is variant at two.Cut the sub-surface damage of trench bottom Hurt that crack distribution is intensive, and the sub-surface crack distribution for cutting seam side is seldom.Diamond abrasive grain on scroll saw to silicon crystal into Row squeezes and swiping, and crystal is got rid of in a brittle manner.In actually cutting, joint-cutting bottom bottom position material removes thickness most The removal thickness of height, joint-cutting boundary material is minimum, and the removal of this position brittleness domain material can be changed into the removal of plastic region material.It cuts Seam bottom is the crackle generated by the brittle removal of material, and cutting seam side material is largely plastic material removing method. The big crackle of some lateral length is remained in cutting seam side, and micro-vibration inside diced system, causes crystalline substance in addition The secondary removal of body side surface forms new crackle on joint-cutting surface, and original crack is extended, and reduces joint-cutting side plastic region The ratio of material removal.Slurry fluid behavior makes the miniature edge of silicon chip surface caused by fixed grain perpendicular to the cutting of cut direction Line is reduced.In the cutting of concretion abrasive silicon wafer, the abrasive grain of saw silk side makes crystalline silicon form parallel strip and the deep mixed period Distribution cutting line, this is mainly that there are tension and pressure for concretion abrasive cutting silicon chip surface stress, so that its breaking strength is low. Lapping liquid slurry forms protective effect to this phenomenon and reduces the crackle of silicon chip surface by the substitution effect of free abrasive.
Silicon wafer is free-and consolidation abrasive compound multi-wire saw processing technology belongs to Compound Machining, macroscopical cutting can be effectively reduced Power reduces broaching load.The stria of silicon chip surface, peeling and damaging layer and residual stress make moderate progress in this method.Pass through Cutting fluid ingredient is improved, the effect of tool carrier in cutting process is improved.Technological parameter is advanced optimized, raising silicon wafer is obtained and adds The best effort range of working medium amount improves working ability and product quality, reduces cost.
Detailed description of the invention:
Fig. 1 is the principle of the present invention schematic diagram.
Specific embodiment:
Referring to Fig.1, the method for free-consolidation abrasive compound multiline cut silicon chips, it includes using concretion abrasive multi-wire saw Method carries out sawing to silicon ingot 3, while the lapping liquid 2 containing suspension diamond abrasive grain is sprayed onto cutting region;Surface is solid The wire 1 of knot diamond abrasive grain brings the lapping liquid 2 containing suspension diamond abrasive grain into silicon ingot 3 cut during wire In seam, free abrasive grain and fixed grain collective effect are formed, sawing is carried out to silicon ingot 3 jointly, it will during time processing Silicon ingot 3 is cut into several pieces.
The equipment of free-consolidation abrasive compound multiline cut silicon chips, it includes free abrasive multi-wire saw equipment, free The 1 surface consolidated diamond abrasive grain of whole wires of abrasive material multi-wire saw equipment.
The method of free-consolidation abrasive compound multiline cut silicon chips, used steel wire diameter is between 50 to 250 μm; The average grain diameter for being fixedly arranged at the diamond abrasive grain on steel wire is between 5 to 30 μm;It is fixedly arranged between the diamond abrasive grain on steel wire Away from one times or so for its average grain diameter, adjusted by the parameter plated or welded;Be limited to slice surface material removing speed with And the influence of cutting output caused by abrasive grain size itself, the wire travelling speed for sawing silk is 20m/s or so;It is used to contain the gold that suspends The lapping liquid 2 of hard rock abrasive grain, be by average grain diameter be 5 to 30 μm diamond abrasive grain and polyethylene glycol liquid according to quality Concentration proportioning mixing than 20% to 30%, stirring environment temperature is greater than 20 DEG C, less than 40 DEG C, stirs 1 to 2 hour, stirring stops 5 Slurry does not have lamination in minute, forms homogeneous mixed liquor, is the diamond abrasive grain suspension of sticky polyethylene glycol.

Claims (3)

1. the method for free-consolidation abrasive compound multiline cut silicon chips, it is characterised in that it includes to use concretion abrasive multi-wire cutting The method cut carries out sawing to silicon ingot (3), while the lapping liquid (2) containing suspension diamond abrasive grain is sprayed onto cutting area Domain.
2. the method for free-consolidation abrasive compound multiline cut silicon chips as described in claim 1, it is characterised in that used Steel wire diameter is between 50 to 250 μm;The average grain diameter for being fixedly arranged at the diamond abrasive grain on steel wire is between 5 to 30 μm;Consolidation The spacing of diamond abrasive grain on steel wire is one times of its average grain diameter;The wire travelling speed for sawing silk is 20m/s;It is used to contain There is the lapping liquid (2) of suspension diamond abrasive grain, is the diamond abrasive grain and polyethylene glycol liquid for being 5 to 30 μm by average grain diameter Body is mixed according to the concentration proportioning of mass ratio 20% to 30%, and stirring environment temperature is greater than 20 DEG C, less than 40 DEG C, is stirred 1 to 2 hour It is made.
3. the equipment of free-consolidation abrasive compound multiline cut silicon chips, it includes free abrasive multi-wire saw equipment, and feature exists In whole wires (1) surface consolidated diamond abrasive grain in free abrasive multi-wire saw equipment.
CN201910790559.1A 2019-08-26 2019-08-26 The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips Pending CN110497546A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910790559.1A CN110497546A (en) 2019-08-26 2019-08-26 The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910790559.1A CN110497546A (en) 2019-08-26 2019-08-26 The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips

Publications (1)

Publication Number Publication Date
CN110497546A true CN110497546A (en) 2019-11-26

Family

ID=68589488

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910790559.1A Pending CN110497546A (en) 2019-08-26 2019-08-26 The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips

Country Status (1)

Country Link
CN (1) CN110497546A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111976043A (en) * 2020-08-26 2020-11-24 西安奕斯伟硅片技术有限公司 Crystal bar cutting device and crystal bar cutting method
CN112372862A (en) * 2020-11-12 2021-02-19 上海新昇半导体科技有限公司 Crystal bar workpiece plate and crystal bar cutting method
CN114670350A (en) * 2022-04-08 2022-06-28 浙江工业大学 Semiconductor monocrystalline silicon diamond wire saw cutting method based on phase change microcapsule suspension

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100126488A1 (en) * 2008-11-25 2010-05-27 Abhaya Kumar Bakshi Method and apparatus for cutting wafers by wire sawing
CN103025486A (en) * 2010-08-03 2013-04-03 尤希路化学工业有限公司 Aqueous processing solution for fixed abresive grain wire saw
CN103121245A (en) * 2011-11-17 2013-05-29 赵钧永 Consolidation grinding material wire-electrode cutting method and cutting fluid
CN103786274A (en) * 2014-01-23 2014-05-14 中国有色桂林矿产地质研究院有限公司 Diamond fretsaw device for polycrystalline silicon ingot squaring
CN206568356U (en) * 2016-10-21 2017-10-20 苏州伟益新材料科技有限公司 Three stranded diamond fretsaws
CN108437244A (en) * 2018-03-22 2018-08-24 山东大学 Free-fixed grain composite fret saw cutting method of photovoltaic polycrystalline silicon battery plate

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100126488A1 (en) * 2008-11-25 2010-05-27 Abhaya Kumar Bakshi Method and apparatus for cutting wafers by wire sawing
CN103025486A (en) * 2010-08-03 2013-04-03 尤希路化学工业有限公司 Aqueous processing solution for fixed abresive grain wire saw
CN103121245A (en) * 2011-11-17 2013-05-29 赵钧永 Consolidation grinding material wire-electrode cutting method and cutting fluid
CN103786274A (en) * 2014-01-23 2014-05-14 中国有色桂林矿产地质研究院有限公司 Diamond fretsaw device for polycrystalline silicon ingot squaring
CN206568356U (en) * 2016-10-21 2017-10-20 苏州伟益新材料科技有限公司 Three stranded diamond fretsaws
CN108437244A (en) * 2018-03-22 2018-08-24 山东大学 Free-fixed grain composite fret saw cutting method of photovoltaic polycrystalline silicon battery plate

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111976043A (en) * 2020-08-26 2020-11-24 西安奕斯伟硅片技术有限公司 Crystal bar cutting device and crystal bar cutting method
CN112372862A (en) * 2020-11-12 2021-02-19 上海新昇半导体科技有限公司 Crystal bar workpiece plate and crystal bar cutting method
CN114670350A (en) * 2022-04-08 2022-06-28 浙江工业大学 Semiconductor monocrystalline silicon diamond wire saw cutting method based on phase change microcapsule suspension

Similar Documents

Publication Publication Date Title
CN101979230B (en) Method for cutting silicon carbide crystal in sections by using multi-line cutter
CN110497546A (en) The method and apparatus of free-consolidation abrasive compound multiline cut silicon chips
KR101685329B1 (en) Method for simultaneously cutting a multiplicity of slices of particularly uniform thickness from a workpiece
US8075647B2 (en) Slurry for slicing silicon ingot and method for slicing silicon ingot using the same
EP2843688B1 (en) Dicing blade
JP5515593B2 (en) Method for cutting silicon ingot with wire saw and wire saw
Kim et al. Characterization of diamond wire-cutting performance for lifetime estimation and process optimization
JP2011031386A (en) Electro-deposition fixed abrasive grain wire and crystal slicing method using the same
TWI816414B (en) Method for simultaneously cutting a plurality of disks from a workpiece
JP2000218504A (en) Wire with fixed abrasive grains and cutting method for fixed abrasive grains wire saw
JP2003159642A (en) Work cutting method and multi-wire saw system
Maeda et al. High-speed slicing of SiC ingot by high-speed multi wire saw
CN207578758U (en) A kind of diamond wire for multi-wire saw
CN102264515A (en) Workpiece for frame gang saw, method for cutting the workpiece, and product cut by the method
US7086394B2 (en) Grindable self-cleaning singulation saw blade and method
JPS629864A (en) Machining method by multi-blade saw
JP2007273743A (en) Semiconductor substrate and dicing method thereof
JP2006059914A (en) Semiconductor device and manufacturing method thereof
CN220074422U (en) Diamond fine grinding wheel
US7115443B2 (en) Method and apparatus for manufacturing a packaged semiconductor device, packaged semiconductor device obtained with such a method and metal carrier suitable for use in such a method
TW201834050A (en) Method for manufacturing wafer
Chandra et al. Challenges in slicing large diameter silicon wafers using slurry wiresaw
Chung et al. Comparison of free abrasive machining processes in wafer manufacturing
CN118219447A (en) Crystal bar cutting mortar replacement method and mortar replacement device
CN114986727A (en) Semiconductor wafer double-film cutting method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20191126

RJ01 Rejection of invention patent application after publication