CN110470690A - Modified high molecular material thermal stability determination instrument - Google Patents

Modified high molecular material thermal stability determination instrument Download PDF

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Publication number
CN110470690A
CN110470690A CN201910821501.9A CN201910821501A CN110470690A CN 110470690 A CN110470690 A CN 110470690A CN 201910821501 A CN201910821501 A CN 201910821501A CN 110470690 A CN110470690 A CN 110470690A
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test tube
water
box
water bath
bath
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CN201910821501.9A
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CN110470690B (en
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耿建春
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Shanghai Lizhen Industrial Technology Co ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

The invention discloses modified high molecular material thermal stability determination instrument, including water bath box, water-bath chamber is offered in the water bath box, annular groove is offered on the water bath box, the annular groove annular is equidistantly fixedly installed with multiple telescopic rods.The present invention squeezes test tube fixing dish by pinch roller and makes test tube fixing dish that can make test tube in water-bath intracavitary arcuate oscillating motion under the action of telescopic rod and spring, heat in test tube is distributed not by sealing-plug, increase by thermal velocity, and it will not splash, heated test tube is set to be vented decompression by tracheae, it avoids rupturing, made in circular trough by dry bag in dry environment, by counterweight box motor output shaft will not be bent, and make pinch roller revolving speed uniform, make to be heated evenly and increases electrical machinery life, make each electronic equipment control connection by electric mortiser needle, and play installation locating effect, the intracavitary level condition of water-bath is accurately understood by glass liquid level pipe, increase the convenience of operation installation.

Description

Modified high molecular material thermal stability determination instrument
Technical field
The present invention relates to polymeric material field more particularly to a kind of modified high molecular material thermal stability determination instrument.
Background technique
Natural polymer is to be present in animal, plant and the intracorporal polymer substance of biology, can be divided into natural fiber, natural Resin, natural rubber, animal glue etc., synthesis high molecular material are primarily referred to as plastics, synthetic rubber and synthetic fibers three and synthesize greatly Material, additionally includes adhesive, coating and various functional high molecule materials, and synthesis high molecular material has natural polymer Sub- material is unexistent or more superior performance --- lesser density, higher mechanics, wearability, corrosion resistance, electricity are absolutely Edge etc. is applied in high molecular material at a certain field, is needed to carry out performance measurement to high molecular material, is judged whether to answer For this field, it is exactly to measure its thermal stability that it is most common, which to measure performance, for high molecular material, it is therefore desirable to dedicated thermostabilization Property measurement device measurement.
Existing high molecular material measurement device is general, and such as application No. is 201511024978.2 authorization patents of invention Described in " high molecular material thermal stability determination instrument ", it is mainly made of heater body, shake table and electric-control system, passes through Electric control system controls heating and shake table shake, and solution mobility is in increase test tube to increase heating speed, but deposits in this scheme It is also easy to produce resonance during test tube is in vibration, causes internal Polymer Solution easily to sputter and comes, influences measurement result, or even damage Bad device, and vibration can accelerate the heat of test tube inner macromolecule solution to distribute speed, so that Polymer Solution is heated more slowly.
Summary of the invention
The purpose of the present invention is to solve vibration existing in the prior art solution resonance in test tube may be made to splash, damage Bad experimental provision, influences experimental result, and shake that test tube can accelerate solution heat in test tube distributes speed, increases heating time The shortcomings that, and the modified high molecular material thermal stability determination instrument proposed.
To achieve the goals above, present invention employs following technical solutions:
Modified high molecular material thermal stability determination instrument, including water bath box offer water-bath chamber, institute in the water bath box It states and offers annular groove on water bath box, the annular groove annular is equidistantly fixedly installed with multiple telescopic rods, multiple described flexible The upper end of bar is fixedly installed with test tube fixing dish, and spring, and the upper and lower ends of spring point are arranged on each telescopic rod It is not fixed on the bottom surface of test tube fixing dish and the slot bottom of annular groove, the arbitrary region of test tube fixing dish can be by multiple flexible It is moved up and down under the action of bar and multiple springs;
Multiple test tube holes are offered on the test tube fixing dish, sliding is inserted with test tube in each test tube hole, often The nozzle of a test tube, which is filled in, is equipped with sealing-plug, tracheae is inserted on each sealing-plug, and tracheae is connected to test tube The internal outside with test tube, sealing-plug can block the nozzle of test tube, avoid invisible spectro solution from splashing, and enable to try When heated, internal solution heat dissipation reduces pipe, increases heating speed, reduces minute, the tracheae on sealing-plug can be avoided Test tube is completely plugged by sealing-plug, prevents test tube from leading to tube breaking because internal pressure increases during heating, increases and survey Surely the upper surface outside of the safety tested, the test tube fixing dish offers annular race;
The water-bath box cover is equipped with insulation cover, and the lower end of the insulation cover offers circular trough, the slot of the circular trough Motor is embedded in bottom wall, the groove bottom wall that the output shaft of the motor passes through circular trough is fixedly installed with bull stick, the bull stick One end is equipped with pinch roller, and pinch roller agrees with annular race, and the distance of pinch roller to annular race is greater than bull stick to test tube fixing dish Distance, i.e. pinch roller is pressed on test tube fixing dish so that side compressed spring and telescopic rod that test tube fixing dish is pushed down by pinch roller, Its test tube fixing dish is heeling condition, and when pinch roller rolls along annular race with the rotation of motor, pinch roller, which constantly changes, to be squeezed The position for pressing test tube fixing dish, i.e., so that test tube fixing dish annular moves up and down, then the test tube energy that is plugged on test tube fixing dish Enough to shake with test tube fixing dish in the intracavitary annular of water-bath, movement range is small, and shaking speed is uniform, so that invisible spectro solution is not Situations such as splashing can be generated;
The other end of the bull stick is fixedly installed with counterweight box, and counterweight box enables to motor not send out during rotation Life significantly shakes, and will not have an impact to the output shaft of motor in long-time use process, increases the use of device Service life.
Preferably, the fixed peace in the lower end of the insulation cover turns have multiple electric mortiser needles, and multiple electric mortiser needle slidings are plugged in On the upper surface of water bath box, control flow, the intracavitary bottom of the water-bath of the water bath box are fixedly installed on the upper surface of the insulation cover Wall, which is embedded in, is equipped with heating dish, and insulation cover is connect by multiple electric mortiser needles with water bath box, so that the heating dish of water bath box and guarantor Connection is controlled between the motor and control flow that temperature covers, convenient for adjusting the velocity of rotation and heating temperature of motor, and multiple electric mortisers Needle covers when on water bath box in insulation cover, can position insulation cover and water bath box, enables insulation cover quickly and accurate It covers on water bath box, so that operation is more convenient.
Preferably, it is placed with dry bag in the counterweight box, multiple dried holes, In are offered on the side wall of the counterweight box When test tube carries out heating water bath, the intracavitary liquid of water-bath can be evaporated into the circular trough of insulation cover, and dry bag is with counterweight box By bar rotation, the evaporation solution in circular trough is quickly collected, avoids evaporation solution from having an impact motor, the water bath box Side wall on insertion glass liquid level pipe is installed, the lower end of the glass liquid level pipe and the lower bottom wall of water-bath chamber pass through tubule company Logical, the upper surface of the water bath box offers water filling port, and water filling port is connected to water-bath chamber, i.e., from water filling port to the intracavitary injection of water-bath When bath solution, solution can be flowed into glass liquid level pipe by tubule, and in the intracavitary solution height of water-bath and glass liquid level pipe The height of solution is consistent, then user can be clearly understood that water-bath luminal solution position, fills solution convenient for user and adds Solubilization liquid.
The invention has the following advantages:
1, test tube fixing dish is squeezed by pinch roller, so that test tube fixing dish recycles everywhere under the action of telescopic rod and spring Decline rises, and the lower end for the test tube being plugged on test tube fixing dish is swung in the intracavitary arc circulation of water-bath, increases examination The flowing velocity of solution in managing, i.e., in increase test tube solution by thermal velocity, and arcuate oscillating motion will not generate solution in test tube Larger impact not will lead to solution splashing etc. in test tube, increase the safety of measurement experiment.
2, the risk that solution is splashed in test tube can be further decreased by setting sealing-plug in test tube top plug, and enables to try The heat of solution is more difficult in managing is dispersed on the outside of test tube from test tube mouth, can increase the heating speed of test tube, insert on sealing-plug Equipped with tracheae, internal gas is discharged from tracheae after enabling test tube heated, and avoiding test tube from being shut by sealing-plug leads to internal pressure Strong increase makes tube breaking, increases safety of the test tube in experiment.
3, counterweight box makes being equal in weight for bull stick both ends, can make motor rotation when will not be biased to certain side, Situations such as can make the output shaft of motor will not bend after prolonged use, increases the service life of device, and matches Weight box enables to pinch roller more at the uniform velocity, to guarantee the uniformity that test tube is swung with test tube fixing dish during rotation, increase it Heated uniformity increases measurement accuracy.
4, dry bag is placed in counterweight box, dry bag absorbs the intracavitary evaporation of water-bath by the dried hole on counterweight box side wall Increase the use of motor to the solution in insulation cover circular trough so that motor is at a comparatively dry environment Service life, and dry bag is rotated in circular trough with counterweight box by bull stick, circulatory motion can be dried, be increased in a ring groove Rate of drying.
5, the bottom surface of insulation cover installs multiple electric mortiser needles, and multiple electric mortiser needles are plugged on water bath box, i.e., multiple electric mortiser needles Heating dish in water bath box can be connected with motor by controller with the control flow on insulation cover, so that insulation cover and water-bath The control integration of box, is user-friendly for operating, and multiple electric mortiser needles cover in insulation cover and provide positioning when on water bath box Function, convenient for users to can quickly connect insulation cover with water bath box.
6, glass liquid level pipe is embedded on the side wall of water bath box, and user is passing through water filling port to the intracavitary filling water-bath of water-bath When solution, bath solution can be flowed into glass liquid level pipe, and glass liquid level pipe is equal with the intracavitary liquid level of water-bath, then makes User can be clearly understood that the intracavitary bath solution filling situation of water-bath, add convenient for users to filling bath solution or midway Add bath solution.
Make test tube fixing dish in the work of telescopic rod and spring in conclusion the present invention squeezes test tube fixing dish by pinch roller It can make test tube in the intracavitary arcuate oscillating motion of water-bath under, distribute heat in test tube not by sealing-plug, increase by thermal velocity, and It will not splash, so that heated test tube is vented decompression by tracheae, avoid rupturing, be made in circular trough by dry bag in drying Environment makes motor output shaft not bend, and makes pinch roller revolving speed uniform, make to be heated evenly and increase by counterweight box Electrical machinery life makes each electronic equipment control connection by electric mortiser needle, and plays installation locating effect, passes through glass liquid level pipe It is accurate to understand the intracavitary level condition of water-bath, increase the convenience of operation installation.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of modified high molecular material thermal stability determination instrument proposed by the present invention;
Fig. 2 is enlarged drawing at A in Fig. 1;
Fig. 3 is the test tube magnified partial view of modified high molecular material thermal stability determination instrument proposed by the present invention.
In figure: 1 water bath box, 2 electric mortiser needles, 3 insulation covers, 4 motors, 5 control flows, 6 pinch rollers, 7 sealing-plugs, 8 bull sticks, 9 dryings Bag, 10 counterweight boxes, 11 test tube fixing dishs, 12 test tube holes, 13 annular races, 14 test tubes, 15 water filling ports, 16 glass liquid level pipes, 17 Spring, 18 annular grooves, 19 telescopic rods, 20 tracheaes.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
In the description of the present invention, it is to be understood that, term " on ", "lower", "front", "rear", "left", "right", "top", The orientation or positional relationship of the instructions such as "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, merely to just In description the present invention and simplify description, rather than the device or element of indication or suggestion meaning must have a particular orientation, with Specific orientation construction and operation, therefore be not considered as limiting the invention.
Referring to Fig.1-3, modified high molecular material thermal stability determination instrument, including water bath box 1 offer in water bath box 1 Water-bath chamber offers annular groove 18 on water bath box 1, and 18 annular of annular groove is equidistantly fixedly installed with multiple telescopic rods 19, multiple The upper end of telescopic rod 19 is fixedly installed with test tube fixing dish 11, is arranged with spring 17 on each telescopic rod 19, and spring 17 Upper and lower ends are separately fixed at the bottom surface of test tube fixing dish 11 and the slot bottom of annular groove 18, the arbitrary region of test tube fixing dish 11 It can be by being moved up and down under the action of multiple telescopic rods 19 and multiple springs 17;
Multiple test tube holes 12 are offered on test tube fixing dish 11, sliding is inserted with test tube 14 in each test tube hole 12, often The nozzle of a test tube 14, which is filled in, is equipped with sealing-plug 7, tracheae 20 is inserted on each sealing-plug 7, and tracheae 20 is connected to test tube 14 Inside and test tube 14 outside, sealing-plug 7 can block the nozzle of test tube 14, avoid the solution in test tube 14 from splashing, and Enable to test tube 14 when heated, internal solution heat dissipation reduces, increase heating speed, reduction minute, on sealing-plug 7 It is completely plugged by sealing-plug 7 that tracheae 20 can be avoided test tube 14, prevents test tube 14 during heating due to internal pressure increases Cause test tube 14 to rupture, increases the safety of measurement experiment, offer annular race 13 on the outside of the upper surface of test tube fixing dish 11;
1 upper cover of water bath box is equipped with insulation cover 3, and the lower end of insulation cover 3 offers circular trough, is embedded in the groove bottom wall of circular trough There is motor 4, the groove bottom wall that the output shaft of motor 4 passes through circular trough is fixedly installed with bull stick 8, and one end of bull stick 8 is equipped with pinch roller 6, and pinch roller 6 agrees with annular race 13, the distance that pinch roller 6 arrives annular race 13 be greater than bull stick 8 to test tube fixing dish 11 away from From that is, pinch roller 6 is pressed on test tube fixing dish 11, so that test tube fixing dish 11 is by the side compressed spring 17 that pinch roller 6 is pushed down and stretches Contracting bar 19, test tube fixing dish 11 is heeling condition, when pinch roller 6 rolls along annular race 13 with the rotation of motor 4, pressure The position that wheel 6 constantly changes extruding test tube fixing dish 11 is then plugged in test tube that is, so that 11 annular of test tube fixing dish moves up and down Test tube 14 in fixed disk 11 can be as test tube fixing dish 11 be in the intracavitary annular shaking of water-bath, and movement range is small, shakes speed Uniformly, so that situations such as solution in test tube 14 will not generate splashing;
The other end of bull stick 8 is fixedly installed with counterweight box 10, and counterweight box 10 enables to motor 4 during rotation will not Generation significantly shakes, and will not have an impact to the output shaft of motor 4 in long-time use process, increases making for device Use the service life.
The fixed peace in the lower end of insulation cover 3 turns have multiple electric mortiser needles 2, and multiple electric mortiser needles 2 slide the upper end for being plugged in water bath box 1 On face, control flow 5 is fixedly installed on the upper surface of insulation cover 3, the intracavitary bottom wall of the water-bath of water bath box 1, which is embedded in, is equipped with heating Disk, insulation cover 3 is connect by multiple electric mortiser needles 2 with water bath box 1, so that the motor 4 in the heating dish of water bath box 1 and insulation cover 3 Connection is controlled between control flow 5, convenient for adjusting the velocity of rotation and heating temperature of motor 4, and multiple electric mortiser needles 2 are in insulation cover 3 cover when on water bath box 1, can position insulation cover 3 and water bath box 1, enable the quickly simultaneously accurate Gai Shui of insulation cover 3 It bathes on box 1, so that operation is more convenient.
It is placed with dry bag 9 in counterweight box 10, multiple dried holes are offered on the side wall of counterweight box 10, is carried out in test tube 14 When heating water bath, the intracavitary liquid of water-bath can be evaporated into the circular trough of insulation cover 3, and dry bag 9 passes through with counterweight box 10 Bull stick 8 rotates, and quickly collects the evaporation solution in circular trough, avoids evaporation solution from having an impact motor 4, the side of water bath box 1 Insertion is equipped with glass liquid level pipe 16 on wall, and the lower end of glass liquid level pipe 16 is connected to the lower bottom wall of water-bath chamber by tubule, water The upper surface of bath box 1 offers water filling port 15, and water filling port 15 is connected to water-bath chamber, i.e., from water filling port 15 to the intracavitary injection water of water-bath When bathing solution, solution can be flowed into glass liquid level pipe 16 by tubule, and the solution height and glass liquid level pipe 16 that water-bath is intracavitary The height of interior solution is consistent, then user can be clearly understood that water-bath luminal solution position, convenient for user fill solution and Add solution.
In the use of the present invention, multiple test tubes 14 are installed Polymer Solution, then with multiple sealings for being inserted with tracheae 20 Plug 7 stoppers multiple test tubes 14, and each test tube 14 is gently injected in the test tube hole 12 on test tube fixing dish 11, by water filling port 15 to The intracavitary injection bath solution of water-bath observes liquid level in glass liquid level pipe 16 and controls adding amount, then by the multiple of insulation cover 3 Electric mortiser needle 2 is directed at the slot connecting on water bath box 1 with electric mortiser needle 2, insulation cover 3 is put down after alignment, the lid of insulation cover 3 is made to be located at water It bathes on box 1, then connects power supply, measurement running parameter is set by the control flow 5 on insulation cover 3, start to work, heating Disk heats the intracavitary bath solution of water-bath, and the rotation of motor 4 rotates pinch roller 6 and counterweight box 10 in circular trough by bull stick 8, Pinch roller 6 squeezes test tube fixing dish 11, and test tube fixing dish 11 is extruded place's compressed spring 17 and telescopic rod 19, then has a down dip at extruding, It squeezes symmetrical region to rise, when constantly annular rolls pinch roller 6, former crush-zone is by the rebound of spring 17 so that test tube is fixed Disk 11 is gradually recovered and is gradually increasing, then the lower end for being plugged in multiple test tubes 14 on test tube fixing dish 11 is intracavitary constantly in water-bath Arcuate oscillating motion increases the flowing velocity of Polymer Solution, makes its heated quickening, and will not splash, and the drying in counterweight box 10 Bag 9 rotates in circular trough also with bull stick 8, is done the intracavitary bath solution being evaporated in circular trough of water-bath by dried hole It is dry, it avoids having an impact motor 4, when reaching the parameter set, motor 4 and heating dish are automatically powered off, and open insulation cover 3, it takes out test tube 14 and completes to be measured internal Polymer Solution.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (3)

1. modified high molecular material thermal stability determination instrument, including water bath box (1), which is characterized in that in the water bath box (1) Water-bath chamber is offered, is offered annular groove (18) on the water bath box (1), annular groove (18) annular is equidistantly fixedly mounted Have multiple telescopic rods (19), the upper end of multiple telescopic rods (19) is fixedly installed with test tube fixing dish (11), each described to stretch It is arranged on contracting bar (19) spring (17), and the upper and lower ends of spring (17) are separately fixed at the bottom of test tube fixing dish (11) The slot bottom in face and annular groove (18) is inserted with multiple test tubes (14), the test tube fixing dish on the test tube fixing dish (11) (11) annular race (13) are offered on the outside of upper surface;
Water bath box (1) upper cover is equipped with insulation cover (3), and the lower end of the insulation cover (3) offers circular trough, the circular trough Groove bottom wall in be embedded with motor (4), the groove bottom wall that the output shaft of the motor (4) passes through circular trough is fixedly installed with bull stick (8), one end of the bull stick (8) is equipped with pinch roller (6), and pinch roller (6) agrees with annular race (13), the bull stick (8) The other end is fixedly installed with counterweight box (10).
2. modified high molecular material thermal stability determination instrument according to claim 1, which is characterized in that the insulation cover (3) the fixed peace in lower end turns have multiple electric mortiser needles (2), and multiple electric mortiser needle (2) slidings are plugged in the upper surface of water bath box (1) On.
3. modified high molecular material thermal stability determination instrument according to claim 1, which is characterized in that the counterweight box (10) it is placed with dry bag (9) in, insertion is equipped with glass liquid level pipe (16) on the side wall of the water bath box (1).
CN201910821501.9A 2019-09-02 2019-09-02 Improved generation macromolecular material thermal stability apparatus Active CN110470690B (en)

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CN110470690B CN110470690B (en) 2021-09-03

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