CN110420571A - A kind of stirring means of cellulose - Google Patents

A kind of stirring means of cellulose Download PDF

Info

Publication number
CN110420571A
CN110420571A CN201910759604.7A CN201910759604A CN110420571A CN 110420571 A CN110420571 A CN 110420571A CN 201910759604 A CN201910759604 A CN 201910759604A CN 110420571 A CN110420571 A CN 110420571A
Authority
CN
China
Prior art keywords
cellulose
stirring
water
stirring means
agitator tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910759604.7A
Other languages
Chinese (zh)
Inventor
苏向东
杨宗伦
张宇
王彦
刘钊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guizhou Good Hundred Year Housing Industry Co Ltd
Guizhou Institute of Technology
Original Assignee
Guizhou Good Hundred Year Housing Industry Co Ltd
Guizhou Institute of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guizhou Good Hundred Year Housing Industry Co Ltd, Guizhou Institute of Technology filed Critical Guizhou Good Hundred Year Housing Industry Co Ltd
Priority to CN201910759604.7A priority Critical patent/CN110420571A/en
Publication of CN110420571A publication Critical patent/CN110420571A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00Dissolving
    • B01F21/02Methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00Dissolving
    • B01F21/10Dissolving using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/115Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/93Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary discs

Abstract

The present invention provides a kind of stirring means of cellulose.This method comprises: stirring at normal temperature in agitator tank is added in cellulose and water;The amount ratio of the cellulose and water is 1:(90-110);The revolving speed of the agitating shaft of the agitator tank is 1400-1600r/min, and the dispersion disk diameter of shaft bottom is 0.35-0.45m;The tank body internal diameter of the agitator tank is 1.4-1.6m, is highly 3-3.4m;The dispersion impeller is away from tank base 0.5-0.7m.The present invention can all dissolve cellulose in 5min, substantially increase the dissolved efficiency to cellulose;Obtained cellulose solution, uniform exquisitely carved, no white point, solute effect are fabulous;The finally solute effect to cellulose has directly been ensured by the restriction to motor, tank body, dispersion impeller;And the dissolution equipment structure used is simple;Low manufacture cost;Directly cellulose can be dissolved in the water of room temperature.

Description

A kind of stirring means of cellulose
Technical field
The invention belongs to celluloses to stir field, be related to a kind of stirring means of cellulose.
Background technique
Hollow extrusion molding cement plate, also referred to as ECP plate are that (paper pulp fiber, polypropylene are fine with portland cement, fiber Dimension etc.), siliceous material (silica flour etc.) be primary raw material, through vacuum high-pressure extrusion molding, by low-temperature steam maintenance operating it Afterwards, manufactured hollow profile board is conserved using high temperature and pressure.
The EPC plate of the current independent research of my company, is related to the processing to cellulose in process of production, specifically needs The room temperature aqueous solution of cellulose is obtained, and must be uniform by cellulose dissolution, can guarantee the intensity of EPC plate.And cellulose Be in room temperature it is insoluble, my company is in order to attempt to make cellulose be scattered in water using mixing plant by cellulose dissolution Yu Shuizhong In.Commercially available agitator tank used in my company's production old type tube product is first attempted to, as a result cellulose point occurs in this mode It dissipates not open, dissolves non-uniform problem, it is impossible to meet the production requirements of my company.Later my company arrange professional to I State coastal area, main mixing plant manufacturer find suitable mixing plant, my associate tested a lot of stir Mixing equipment, but the aqueous solution that these mixing plants obtain after continuously stirring 2 hours to cellulose, however it remains white point, naked eyes Visible white point is not scattered cellulose, or even the case where burn during the test there have been motor.To fiber The mixing time of element is too long and has the problem big, at high cost that consumes energy, and is not suitable for producing.So not having in existing technology Meet the mixing plant of my companies needs.For this purpose, my company is merely able to self-organization research and development, fortunately, by a large amount of real It tests and studies, my company finally realizes the product and method for meeting production requirement.
In conclusion existing at present can not all dissolve cellulose, there is, low efficiency poor to the dispersion effect of cellulose, Motor is easy the problem of burning when stirring cellulose.
Goal of the invention
The object of the present invention is to provide a kind of stirring means of cellulose.The present invention can by cellulose all dissolve, have pair The dissolved efficiency of cellulose is high, solute effect is good and motor is not easy the advantages of burning.
The present invention adopts the following technical scheme that realization goal of the invention:
A kind of stirring means of cellulose, which is characterized in that stirred this method comprises: room temperature in agitator tank is added in cellulose and water It mixes;The amount ratio of the cellulose and water is 1:(90-110);The revolving speed of the agitating shaft of the agitator tank is 1400-1600r/ Min, the dispersion disk diameter of shaft bottom are 0.35-0.45m;;The tank body internal diameter of the agitator tank is 1.4-1.6m, is highly 3-3.4m;The dispersion impeller is away from tank base 0.5-0.7m.
In the stirring means of cellulose above-mentioned, the amount ratio of the cellulose and water is 1:100.
In the stirring means of cellulose above-mentioned, the revolving speed of the agitating shaft of the agitator tank is 1480r/min.
In the stirring means of cellulose above-mentioned, the viscosity of the cellulose is 200,000 viscositys.
In the stirring means of cellulose above-mentioned, the additional amount of the water is 1.4-1.6t.
In the stirring means of cellulose above-mentioned, the agitator tank uses the variable-frequency motor of 37kW.
In the stirring means of cellulose above-mentioned, the time of the stirring is 4-6min.
In the stirring means of cellulose above-mentioned, it is highly 3.2m that the tank body internal diameter of the agitator tank, which is 1.5m,.
In the stirring means of cellulose above-mentioned, the dispersion impeller is away from tank base 0.6m.
In the stirring means of cellulose above-mentioned, the dispersion impeller is the tooth-like dispersion impeller in periphery, diameter 0.4m.
Compared with prior art, the invention has the following advantages:
1, dissolution can be stirred to the cellulose of 200,000 viscositys through the invention, and it is only necessary to 5min or so can be completed, And the cellulose of 15kg disposably can be about dissolved in 1.5 tons of water, stirring efficiency is high.
2, it is observed that the cellulose solution finally obtained by the method for the invention is uniformly exquisitely carved, no white point has dissolution effect The good advantage of fruit.And by after cellulose solution standing a few hours, solution is still transparent, and no white point occurs.
3, the present invention uses the variable-frequency motor of 37kW, and when to disperse disk rotating speed be 1400-1600r/min, it is ensured that final Stirring efficiency, have the function of automatic frequency-conversion, protection realized to motor itself, motor is not easy to burn, long service life;Through trying Test, if motor is non-frequency motor, since the viscosity of cellulose is very big, motor in driving mixing component in its dispersion process, Motor can be burnt because of excess load;Energy consumption can be improved if the power of motor is higher, leads to the raising of production cost.
4, it is tested, has and be only 1.4-1.6m in the tank body internal diameter of agitator tank given to this invention, be highly 3- 3.4m;The dispersion disk diameter of shaft bottom is 0.35-0.45m;Dispersion impeller is away from tank base 0.5-0.7m parameters range Interior, the dissolution of cellulose in water can be completed in 5min or so.Beyond or below tank body given to this invention and dispersion The parameter area of disk is all unable to get optimal working efficiency and effect.As: dispersion impeller is arranged in away from tank base 90cm Highly, cellulose can not all be dissolved continuous stirring in water cellulose 1 hour.
5, stirring jar structure defined by the present invention is simple, comprises only a motor and a dispersion impeller, is fabricated to This low advantage;Existing agitator tank some is also additionally arranged in stirring pot bottom to fiber including at least two dispersion impellers, some The crushing device of element, but in practical applications, these designs even can not all dissolve cellulose within 2 hours, For stirring cellulose, these devices are the costs of manufacture for increasing equipment in vain.
6, the present invention can be achieved by cellulose uniform dissolution in normal-temperature water, and required energy consumption is very small.It is set in of the invention Under the property room temperature for considering cellulose during meter, cellulose was not only not soluble in water, but also did not dissolved in general organic solvent, also not It is dissolved in dilute alkaline soln.Therefore paid high-temperature water on probation improves the dissolubility of cellulose, when water temperature is improved to 90 DEG C or so, nothing Need any stirring that can be directly dissolved in water with regard to cellulose, but water temperature needed for producing EPC plate cannot be excessively high, high temperature is molten The solution of cellulose is solved in water temperature drop, cellulose will appear the phenomenon that gelling is layered, and be unable to meet production requirement.And It improves water temperature and also results in greatly increasing for energy consumption, production is got up not cost-effective.Conversely, cellulose can be directly dissolved in by the present invention Design in normal-temperature water has the advantages that low energy consumption.
In summary: the present invention can all dissolve cellulose in 5min, substantially increase the dissolution effect to cellulose Rate;Obtained cellulose solution, uniform exquisitely carved, no white point, solute effect are fabulous;Pass through the restriction to motor, tank body, dispersion impeller The finally solute effect to cellulose is directly ensured;And the dissolution equipment structure used is simple;Low manufacture cost;Can directly by Cellulose is dissolved in the water of room temperature.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
The step of embodiment 1, the stirring means of cellulose, stirring, is: cellulose and normal-temperature water being added in agitator tank and stirred It mixes, takes out the stirring liquid of cellulose after stirring.
For the specific water that is added for 1.5t, the amount ratio of cellulose and water is 1:100, and the cellulose standard of addition is 200,000 glutinous Degree stirs 5min.
For the motor that agitator tank uses for the variable-frequency motor of 37kW, variable-frequency motor drives agitating shaft rotation to realize stirring, stirring Speed is 1480r/min;The bottom end of agitating shaft connects the tooth-like dispersion impeller in periphery, and the diameter of dispersion impeller is 0.4m, away from tank base 0.6m;The internal diameter of tank body is 1.5m, is highly 3.2m.
The step of embodiment 2, the stirring means of cellulose, stirring, is: cellulose and normal-temperature water being added in agitator tank and stirred It mixes, takes out the stirring liquid of cellulose after stirring.
For the specific water that is added for 1.4t, the amount ratio of cellulose and water is 1:90, and the cellulose standard of addition is 200,000 glutinous Degree stirs 4min.
For the motor that agitator tank uses for the variable-frequency motor of 37kW, variable-frequency motor drives agitating shaft rotation to realize stirring, stirring Speed is 1400r/min;The bottom end of agitating shaft connects the tooth-like dispersion impeller in periphery, and the diameter of dispersion impeller is 0.35m, away from tank base 0.5m;The internal diameter of tank body is 1.4m, is highly 3m.
The step of embodiment 3, the stirring means of cellulose, stirring, is: cellulose and normal-temperature water being added in agitator tank and stirred It mixes, takes out the stirring liquid of cellulose after stirring.
For the specific water that is added for 1.6t, the amount ratio of cellulose and water is 1:110, and the cellulose standard of addition is 200,000 glutinous Degree stirs 6min.
For the motor that agitator tank uses for the variable-frequency motor of 37kW, variable-frequency motor drives agitating shaft rotation to realize stirring, stirring Speed is 1600r/min;The bottom end of agitating shaft connects the tooth-like dispersion impeller in periphery, and the diameter of dispersion impeller is 0.45m, away from tank base 0.7m;The internal diameter of tank body is 1.5m, is highly 3.4m.

Claims (10)

1. a kind of stirring means of cellulose, which is characterized in that this method comprises: room temperature in agitator tank is added in cellulose and water Stirring;The amount ratio of the cellulose and water is 1:(90-110);The revolving speed of the agitating shaft of the agitator tank is 1400-1600r/ The tank body internal diameter of min, agitator tank are 1.4-1.6m, are highly 3-3.4m;The dispersion disk diameter of shaft bottom is 0.35- 0.45m;Dispersion impeller is away from tank base 0.5-0.7m.
2. the stirring means of cellulose according to claim 1, it is characterised in that: the amount ratio of the cellulose and water is 1:100.
3. the stirring means of cellulose according to claim 1, it is characterised in that: the revolving speed of the agitating shaft of the agitator tank For 1480r/min.
4. the stirring means of cellulose according to claim 1, it is characterised in that: the viscosity of the cellulose is 200,000 glutinous Degree.
5. the stirring means of cellulose according to claim 1, it is characterised in that: the additional amount of the water is 1.4- 1.6t。
6. the stirring means of cellulose according to claim 1, it is characterised in that: the agitator tank uses the frequency conversion of 37kW Motor.
7. the stirring means of cellulose according to claim 1, it is characterised in that: the time of the stirring is 4-6min.
8. the stirring means of cellulose according to claim 1, it is characterised in that: the tank body internal diameter of the agitator tank is 1.5m is highly 3.2m.
9. the stirring means of cellulose according to claim 8, it is characterised in that: the dispersion impeller is away from tank base 0.6m。
10. the stirring means of cellulose according to claim 1, it is characterised in that: the dispersion impeller is tooth-like point of periphery Dissipate disk, diameter 0.4m.
CN201910759604.7A 2019-08-16 2019-08-16 A kind of stirring means of cellulose Pending CN110420571A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910759604.7A CN110420571A (en) 2019-08-16 2019-08-16 A kind of stirring means of cellulose

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910759604.7A CN110420571A (en) 2019-08-16 2019-08-16 A kind of stirring means of cellulose

Publications (1)

Publication Number Publication Date
CN110420571A true CN110420571A (en) 2019-11-08

Family

ID=68415100

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910759604.7A Pending CN110420571A (en) 2019-08-16 2019-08-16 A kind of stirring means of cellulose

Country Status (1)

Country Link
CN (1) CN110420571A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007051430B3 (en) * 2007-10-25 2009-03-19 Ak System Gmbh dissolver
CN201969518U (en) * 2010-12-13 2011-09-14 安徽好思家涂料有限公司 Automatic cellulose ether dissolving material weighing and conveying device
CN206253023U (en) * 2016-11-30 2017-06-16 山东恒联新材料股份有限公司 A kind of cellulosics high viscosity viscose glue dissolver
CN107983222A (en) * 2017-12-29 2018-05-04 绍兴柯桥诚鑫精密铸造有限公司 A kind of mixing arrangement of spinning sizing agent
CN109605546A (en) * 2018-12-26 2019-04-12 贵州好百年住宅工业有限公司 A kind of extrusion forming fiber cement board extrusion line

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007051430B3 (en) * 2007-10-25 2009-03-19 Ak System Gmbh dissolver
CN201969518U (en) * 2010-12-13 2011-09-14 安徽好思家涂料有限公司 Automatic cellulose ether dissolving material weighing and conveying device
CN206253023U (en) * 2016-11-30 2017-06-16 山东恒联新材料股份有限公司 A kind of cellulosics high viscosity viscose glue dissolver
CN107983222A (en) * 2017-12-29 2018-05-04 绍兴柯桥诚鑫精密铸造有限公司 A kind of mixing arrangement of spinning sizing agent
CN109605546A (en) * 2018-12-26 2019-04-12 贵州好百年住宅工业有限公司 A kind of extrusion forming fiber cement board extrusion line

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陆振曦等: "《食品机械原理与设计》", 31 May 1995, 北京:中国轻工业出版社 *

Similar Documents

Publication Publication Date Title
CN104499079B (en) A kind of original liquid coloring is prepared the method for black polyester fiber
CN110078877A (en) A kind of methods and applications preparing dispersing agent using lignin degradation products
CN102660050A (en) Method for improving mechanical property of cellulose acetate
CN101413146B (en) Boiling method for preparing cotton linter dissolving pulp by using composite additive
CN102731754A (en) Polyester polymerizing black stock solution dying method
CN110420571A (en) A kind of stirring means of cellulose
CN101713157A (en) Dyeing process of olive-green insulating paperboard
CN103275229B (en) Aqueous fracturing fluid superelevation glues the preparation method of Xylo-Mucine
CN205199386U (en) A dispersator for adding lustre to membrane production
CN205109541U (en) Double -shaft coating dispersing machine
CN107828201A (en) LED light diffusing agents and preparation method thereof and the photodiffusion material containing the light diffusing agent
CN204398131U (en) The dismountable agitating device of a kind of mixer
CN204237904U (en) A kind of original liquid coloring prepares the process units of black polyester fiber
CN202983575U (en) Concrete mixing and stirring machine for coagulants
CN203507925U (en) Dye stirring paddle
CN103242540B (en) Lignin-based amphiphilic azo-polymer colloidal spheres as well as preparation method and application thereof
CN208449193U (en) A kind of high-speed mixer
CN103360650B (en) A kind of corrosion resistant cable jacket material
CN213479176U (en) Sealing device of premixing machine
CN202590803U (en) Stirring type alkali fusion reaction still for producing H-acid
CN1084816C (en) Producing process capable of lowering decline of cellulose mucus colour and lustre, and polymerization degree
CN207446218U (en) A kind of half water law phosphoric acid special agitating apparatus
CN2890051Y (en) Equipment for producing modified asphalt
CN203725074U (en) Raw material premixing and stirring device for producing organic fertilizer
CN203007184U (en) Reaction sub-system for producing carboxylic styrene butadiene latex

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20191108

RJ01 Rejection of invention patent application after publication