CN110409863A - Leakage of coil roofing maintenance process - Google Patents
Leakage of coil roofing maintenance process Download PDFInfo
- Publication number
- CN110409863A CN110409863A CN201910635456.8A CN201910635456A CN110409863A CN 110409863 A CN110409863 A CN 110409863A CN 201910635456 A CN201910635456 A CN 201910635456A CN 110409863 A CN110409863 A CN 110409863A
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- China
- Prior art keywords
- parts
- leakage
- maintenance process
- coil
- asphalt adhesive
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J195/00—Adhesives based on bituminous materials, e.g. asphalt, tar, pitch
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04G—SCAFFOLDING; FORMS; SHUTTERING; BUILDING IMPLEMENTS OR AIDS, OR THEIR USE; HANDLING BUILDING MATERIALS ON THE SITE; REPAIRING, BREAKING-UP OR OTHER WORK ON EXISTING BUILDINGS
- E04G23/00—Working measures on existing buildings
- E04G23/02—Repairing, e.g. filling cracks; Restoring; Altering; Enlarging
- E04G23/0281—Repairing or restoring roofing or roof covering
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The present invention provides a kind of leakage of coil roofing maintenance process, belong to building and repair field.Leakage of coil roofing maintenance process includes the following steps: that inspection judges leakage cause;It is taken and the matched maintenance process of leakage cause according to leakage cause;When coiled material and binder course are removed: cutting the coiled material of removing, expose laminating layer in laminating layer external coating binder and paste new waterproof roll;When coil waterproof layer cracks: then both sides screed-coat at excision coil waterproof layer crack pours into asphalt adhesive;When inlet for stom water and waterproof roll connector alice: alice being cleaned out, brushing asphalt adhesive recloses;When waterproof roll bulge: surface, brushwork adhesive, one layer of waterproof roll of paving are cleared up for extracting air, waterproof roll at another hole injection adhesive or excision bulge out in the drill two holes in bulge, a hole.There are good durability and anti-extreme weather ability using the roofing that this technique was repaired.
Description
Technical field
The invention belongs to buildings to repair field, especially a kind of leakage of coil roofing maintenance process.
Background technique
Roof leakage maintenance is very common phenomenon, and roof leakage easily occur in especially some houses long neglected and in disrepair,
However the reason of roof leakage be it is varied, cannot treat different things as the same.
Roof leakage is mainly the following reason:
One, the defect with design is reconnoitred
Soil exploration layouts unreasonable or is limited the exploration that cannot layout according to standard by place, and foundation is caused to set
There is relatively large deviation in timing, differential settlement occurs after leading to building use, and then makes roofing Local Cracking and leak.Design
Upper building roof flat shape bumps are more, easily form stress at bumps and concentrate, at the lower formation cracking that expands with heat and contract with cold throughout the year.
Two, the influence of sunshine
Prolonged illumination can eventually lead to and accelerate the aging and fracture of waterproof roll.
Three, the influence of temperature
High temperature can accelerate the oxidation and ageing process of asphalt material.The viscosity flow of material is very big at high operating temperatures, holds
It is also easy to produce plastic creep.Low temperature can be such that the brittleness of common water-proofing coiled material increases, and cold(ing)crack and deformation is caused to be broken.This
Sample, if ambient air temperature changes greatly or when temperature is lower, fracture or the probability of cracking, which will occur, for material to obviously increase.
Four, the influence of rainfall and snowfall
More frequent and long roof ponding can cause local damage to waterproof roll.Snowfall cooling and longer thawing
Process also will increase the brittleness of common waterproof material.
Five, the influence of construction technology
Basement process is not in place, and after building up load differential settlement occurs for residential building, leads to parapet even roofing cracking
Cause to leak.Roof construction layer quality is not checked on, prestressed cored slab rainy duct internal water accumulation during installing, by one section
The load action of time, prestressed cored slab occur deflection deformation, cause plate end crack, ponding exudation, cause bedroom cross wall with
Ceiling intersection leaks.Roofing screed-coat is with low quality, without sufficiently dry, dusting;Substrate surface is uneven etc.;Or
Person's waterproof roll itself it is off quality;Or since hot glue ramming material and self-adhering-type coiled material construction temperature are low, cause waterproof layer
It is bonded loosely with base and removes disengagement and form waterproof layer and binder course removing.Roof-base is uneven or base does not clean
Completely, to there is the dusts such as miscellaneous soil to be mixed into form separation layer;Screed-coat intensity is low, of poor quality;Roofing area is bigger, parting seam
It is arranged unreasonable;Adhesive bitument primer covers difference etc..Rolled roofing material overlapping mode is nonstandard, and inlet for stom water, coiled material are received at first-class thin portion
It manages not in place.
Six, the influence of roof construction design
In the biggish situation of the building roof ratio of slope, rainwater can be smoothly discharged out roofing, reduce rainwater and pitch is anti-
The time of contact of water coiled material, so as to extend the service life of waterproof material.
Seven, the influence of roof use process
In normal use, asphalt water-proof coiled material is caused to be destroyed due to maintenance roofing or in roofing setting other equipment.
In accessible roof maintenance, in the case where not paying attention to protection, pitch is easy to be trampled on.Other equipment are when being installed on roofing
Fixation may destroy common waterproof roll.Such as television antenna, solar water heater are installed.
Will receive various factors in prepared roofing use process, the influence including design, construction, material, environment etc. and send out
It is raw to destroy and leak.In the prior art, foot pain of usually treating the head when the head aches cures foot and takes an unnecessary way, without comprehensively dividing before maintenance
Analysis, the leakage for caused by different reasons are all made of single method to handle, and causing repeatedly to repair but not can solve at all
Problem.
Summary of the invention
Since above-mentioned deficiency exists in the prior art, the present invention provides a kind of leakage of coil roofing maintenance process.This hair
The bright different damaged situation for prepared roofing has pointedly used different renovation techniques.And developing one kind has
Also there is the asphalt adhesive of good anti-leakage effect under extreme weather conditions, suitable for the leakage of coil roofing maintenance in a variety of situations
Technique.
Specifically, the present invention is achieved through the following technical solutions:
Leakage of coil roofing maintenance process, includes the following steps:
Inspection judges leakage cause;
It is taken and the matched maintenance process of leakage cause according to leakage cause;
It is described to include: with the matched maintenance process of leakage cause
When coiled material and binder course are removed: cutting the coiled material of removing, expose laminating layer, laminating layer is toasted drying, is being pasted
Layer surface brushing binder is closed, new waterproof roll is pasted;
When coil waterproof layer cracks: the screed-coat of each 30-50mm wide in both sides, depth are vertical at excision coil waterproof layer crack
It is greater than 30mm downwards, then pours into asphalt adhesive, asphalt adhesive height is made to be higher by roofing 2-3mm;
When inlet for stom water and waterproof roll connector alice: alice is cleaned out, dust is removed, dry, brushing asphalt adhesive weight
New closing;
When waterproof roll bulge and bulge diameter is less than or equal to 80mm: the drill two holes in bulge, a hole syringe will rouse
Air extraction in packet, another hole syringe inject adhesive, and injection rate is the 85-100% of bulge volume;
When waterproof roll bulge and bulge diameter is greater than 80mm: waterproof roll at excision bulge clears up surface, brushes bonding
Agent, one layer of waterproof roll of paving, coiled material and cut edge lap width are more than or equal to 150mm.
Preferably, the waterproof roll is the SBS waterproof roll that thickness is more than or equal to 4mm.
Preferably, described adhesive is ethylene-propylene-diene monomer viscose binder or neoprene adhesive.
Preferably, the asphalt adhesive is prepared by matrix pitch, diluent, additive;
The additive includes at least one of surfactant, regenerative agent, antistripping agent.
Preferably, the additive further includes lignin or lignin derivative;
The lignin derivative preparation method is by 40-60 part lignin and 0.5-1.0 parts of zinc powders by weight
It is added in 200-300 parts of formic acid, is heated to 100-110 DEG C of holding 2-3 hours, be cooled to 60-70 DEG C, be added 200-300 parts
5-10wt% hydrogen peroxide and 0.2-0.5 parts of ferric sulfate are heated to 100-110 DEG C of holding 1-3 hours, centrifugation, take liquid to get.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part surfactant is prepared.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part antistripping agent is prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent is prepared.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part surfactant, 0.2-1.0 parts of antistripping agents are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of surfactants are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of antistripping agents are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of antistripping agents, 0.2-1.0 parts of surfactants are prepared.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part surfactant, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part antistripping agent, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive is by 90-120 part matrix pitch, 20-30 parts of diluents, 0.2-1.0 by weight
Part surfactant, 0.2-1.0 parts of antistripping agents, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of surfactants, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of antistripping agents, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the asphalt adhesive by by weight 90-120 part matrix pitch, 20-30 parts of diluents, 1-5 parts again
Raw agent, 0.2-1.0 parts of antistripping agents, 0.2-1.0 parts of surfactants, 0.5-1.5 parts of lignin or derivatives thereof are prepared.
Preferably, the diluent includes gasoline, diesel oil, paraxylene, turpentine oil, White Mineral Oil, cyclohexanone or oleic acid first
At least one of ester.
Preferably, the surfactant includes at least one of amide surfactants and/or organic acid table
At least one of face activating agent;
The amide surfactants structural formula is CnH2n+1COONH2, wherein n is more than or equal to 6 less than or equal to 20
Integer;
The organic acid surfactant structure formula is CnH2n+1COOH, wherein n is more than or equal to 6 less than or equal to 20
Integer.
It is highly preferred that the surfactant is selected from lauric acid, myristic acid, palmitinic acid, lauramide, myristoyl
Any one or more in amine, palmitamide.
It is highly preferred that the surfactant is lauric acid and myristamide mass ratio is (2-3): 1 mixture.
Preferably, the regenerative agent the preparation method is as follows:
(1) 0.5-1 part sodium alkyl sulfonate by weight is added in 100-120 parts of water, adds 5-10 parts of oil
Rouge stirring and emulsifying 60-120 minutes, obtains emulsion;
(2) by by weight 1-2 part melamine and 1.8-2.4 parts of urea be added in 10-20 parts of water, then be passed through
1.2-1.6 parts of formaldehyde adjust pH value to 8-9 with the sodium hydrate aqueous solution of 5-20wt%, are warming up to 70-80 DEG C, stir 60-90
Minute, it is back to room temperature naturally, obtains pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case of stirring, is heated to 65 with the rate of heat addition of 3-5 DEG C/min
DEG C, system pH is adjusted to 2-3 with 5-20wt% aqueous citric acid solution, is stirred 4-8 hour, filtering takes solid, dry to get
Regenerative agent.
Preferably, the grease is hydroxy stearic acid ester oils.
It is highly preferred that the hydroxy stearic acid ester oils are selected from hydroxyl Octacosanol hydroxy stearic acid ester, isooctadecanol hydroxyl
Stearate, glycerol dihydroxystearic acid ester, ethylene glycol hydroxy stearic acid ester, any one in propylene glycol hydroxy stearic acid ester
Or it is a variety of.
Preferably, the preparation method of the asphalt adhesive is to be uniformly mixed each raw material by weight ratio to obtain the final product.
The invention has the beneficial effects that: the present invention has pointedly used not for the different damaged situation of prepared roofing
Same renovation technique, takes many kinds of measures such as construction, technique, material, and multi-pronged, integrated treatment fundamentally solves leakage
Problem.And it develops a kind of with the asphalt adhesive for also having good anti-leakage effect under extreme weather conditions, is suitable for more
Leakage of coil roofing maintenance process in the case of kind, has used some substances voluntarily prepared, to it in the formula of asphalt adhesive
Performance has biggish promotion.
Specific embodiment
The present invention is further elaborated on With reference to embodiment, following embodiments are only used to explain
The present invention can not be considered as to further limitation of the invention.
Specifically, raw material sources used in following embodiments or No. CAS it is as follows:
Matrix pitch, AH-90 type pitch are purchased from Taizhou Wang Hai petrochemical industry Co., Ltd.
Ethylene-propylene-diene monomer viscose binder, for the ethylene-propylene-diene monomer viscose binder of the model CA40H of 3M company production.
Waterproof roll is thick for the waterproof roll of the polyvinyl chloride material of Hebei Jie Langte waterproof material Co., Ltd production
Degree is 4mm.
Antistripping agent, for the KBL-1 type antistripping agent of Shenyang Yi Dao Science and Technology Ltd. production.
No. 0 diesel oil is purchased from middle petrochemical industry.
Methyl oleate, No. CAS: 112-62-9.
Lauric acid, No. CAS: 143-07-7.
Myristamide, No. CAS: 638-58-4.
Dodecyl sodium sulfate, No. CAS: 2386-53-0.
Glycerol dihydroxystearic acid ester, No. CAS: 122546-20-7.
Ethylene glycol hydroxy stearic acid ester, No. CAS: 33907-46-9.
Propylene glycol hydroxy stearic acid ester, No. CAS: 33907-47-0.
Melamine, No. CAS: 108-78-1.
Urea, No. CAS: 57-13-6.
Formaldehyde, No. CAS: 50-00-0.
Citric acid, No. CAS: 77-92-9.
Lignin, No. CAS: 9005-53-2, the dealkalize lignin of Shanghai Lin En development in science and technology Co., Ltd production, fineness
(120 screen residue)≤1.0%.
Zinc powder, No. CAS: 7440-66-6,800 mesh.
Formic acid, No. CAS: 64-18-6.
Hydrogen peroxide, No. CAS: 7722-84-1.
Ferric sulfate, No. CAS: 10028-22-5.
Embodiment 1
Jiading district in Shanghai's cell is 6 layers of brick mix structure, and roofing is followed successively by from top to bottom using waterproof coiled material, roof structure
Coil waterproof layer, screed-coat, insulating layer and structure sheaf, in December, 2003 are delivered for use, and in September, 2017 starts localized seepage occur
Situation, in November, 2017 start to repair.
Upon examination it is found that there are problems that following four:
One, coiled material and screed-coat are removed;Two, coil waterproof layer cracks;Three, inlet for stom water and waterproof roll connector alice;Four,
There is the bulge that 6 diameters are respectively 30mm, 35mm, 45mm, 60mm, 70mm, 70mm.
Coiled material and waterproof layer are removed, the waterproof roll of removing is cut, exposes screed-coat, is heated to 60 using electric oven rifle
DEG C baking dry 5 minutes, brushing binder was brushed with a thickness of 5mm on screed-coat, pastes new waterproof roll;
Crack for coil waterproof layer: the screed-coat of each 30mm wide in both sides, depth are vertical at excision coil waterproof layer crack
Downward 35mm, then pours into asphalt adhesive, and asphalt adhesive height is made to be higher by roofing 3mm;
For inlet for stom water and waterproof roll connector alice: alice being cleaned out, dust is removed, is heated to using electric oven rifle
60 DEG C drying 5 minutes, brushing asphalt adhesive recloses, brush with a thickness of 3mm;
For waterproof roll bulge and bulge diameter is less than or equal to 80mm: the drill two holes in bulge, and a hole will with syringe
Air extraction in bulge, another hole syringe inject adhesive, and injection rate is the 100% of bulge volume;
Adhesive used in above-described embodiment is ethylene-propylene-diene monomer viscose binder;
Asphalt adhesive used in above-described embodiment is self-control asphalt adhesive, and the asphalt adhesive is by 100 parts of bases by weight
Matter pitch, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent, 0.5 part of surfactant and 1 part of lignin derivative system
It is standby to form;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The mixture that the surfactant is lauric acid and myristamide mass ratio is 2:1;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of glycerol dihydroxies
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The lignin derivative the preparation method is as follows:
The lignin derivative preparation method be by by weight 50 parts of lignin and 0.8 part of zinc powder be added to
In 250 parts of formic acid, it is heated to 100 DEG C and is kept for 2 hours, be cooled to 60 DEG C, 250 parts of 6wt% hydrogen peroxide and 0.5 part of sulfuric acid are added
Iron, be heated to 100 DEG C keep 1 hour, 10000rpm be centrifuged 10 minutes, take liquid to get.
The preparation method of above-mentioned asphalt adhesive is by 100 parts of matrix pitches by weight, 23 parts of diluents, 3 parts of regeneration
Agent, 0.5 part of antistripping agent, 0.5 part of surfactant and 1 part of lignin derivative are uniformly mixed to obtain the final product.
By maintenance, leakage phenomenon did not occurred again for the residential building in January, 2019, during which live through -5 DEG C low temperature,
The weather such as 40 DEG C of high temperature and typhoon, it was demonstrated that method for maintaining provided by the invention has a very high anti-extreme weather performance.
Embodiment 2
A kind of asphalt adhesive different from asphalt adhesive used in embodiment 1 is provided, the asphalt adhesive is by by weight
100 parts of matrix pitches, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent and the preparation of 0.5 part of surfactant of meter and
At;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The surfactant is myristamide;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of ethylene glycol hydroxyls
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The preparation method of above-mentioned asphalt adhesive be by by by weight 100 parts of matrix pitches, 23 parts of diluents, 3 parts again
Raw agent, 0.5 part of antistripping agent and 0.5 part of surfactant are uniformly mixed to obtain the final product.
Embodiment 3
A kind of asphalt adhesive different from asphalt adhesive used in embodiment 1 is provided, the asphalt adhesive is by by weight
100 parts of matrix pitches, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent and the preparation of 0.5 part of surfactant of meter and
At;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The surfactant is lauric acid;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of ethylene glycol hydroxyls
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The preparation method of above-mentioned asphalt adhesive be by by by weight 100 parts of matrix pitches, 23 parts of diluents, 3 parts again
Raw agent, 0.5 part of antistripping agent and 0.5 part of surfactant are uniformly mixed to obtain the final product.
Embodiment 4
A kind of asphalt adhesive different from asphalt adhesive used in embodiment 1 is provided, the asphalt adhesive is by by weight
100 parts of matrix pitches, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent and the preparation of 0.5 part of surfactant of meter and
At;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The mixture that the surfactant is lauric acid and myristamide mass ratio is 2:1;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of ethylene glycol hydroxyls
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The preparation method of above-mentioned asphalt adhesive be by by by weight 100 parts of matrix pitches, 23 parts of diluents, 3 parts again
Raw agent, 0.5 part of antistripping agent and 0.5 part of surfactant are uniformly mixed to obtain the final product.
Embodiment 5
A kind of asphalt adhesive different from asphalt adhesive used in embodiment 1 is provided, the asphalt adhesive is by by weight
100 parts of matrix pitches, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent and the preparation of 0.5 part of surfactant of meter and
At;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The mixture that the surfactant is lauric acid and myristamide mass ratio is 2:1;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of propylene glycol hydroxyls
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The preparation method of above-mentioned asphalt adhesive be by by by weight 100 parts of matrix pitches, 23 parts of diluents, 3 parts again
Raw agent, 0.5 part of antistripping agent and 0.5 part of surfactant are uniformly mixed to obtain the final product.
Embodiment 6
A kind of asphalt adhesive different from asphalt adhesive used in embodiment 1 is provided, the asphalt adhesive is by by weight
100 parts of matrix pitches, 23 parts of diluents, 3 portions of regenerative agents, 0.5 part of antistripping agent and the preparation of 0.5 part of surfactant of meter and
At;
The diluent is the mixture of No. 0 diesel oil and methyl oleate mass ratio 5:1;
The mixture that the surfactant is lauric acid and myristamide mass ratio is 2:1;
The regenerative agent the preparation method is as follows:
(1) 0.7 part of dodecyl sodium sulfate by weight is added in 100 parts of water, adds 7 parts of glycerol dihydroxies
Base stearate 500rpm stirring and emulsifying 60 minutes, obtains emulsion;
(2) by by weight 1 part of melamine and 2 parts of urea be added in 15 parts of water, then be passed through 1.5 parts of formaldehyde,
PH value is adjusted to 8 with the sodium hydrate aqueous solution of 8wt%, is warming up to 70 DEG C, 500rpm is stirred 80 minutes, it is back to room temperature naturally,
Obtain pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case where keeping the stirring of 300rpm, with the heating speed of 5 DEG C/min
Rate is heated to 65 DEG C, and system pH is adjusted to 3 with 10wt% aqueous citric acid solution, is stirred 4 hours, is crossed 200 meshes, take solid,
Constant weight is dried under vacuum under conditions of 50 DEG C/100Pa to get regenerative agent.
The preparation method of above-mentioned asphalt adhesive be by by by weight 100 parts of matrix pitches, 23 parts of diluents, 3 parts again
Raw agent, 0.5 part of antistripping agent and 0.5 part of surfactant are uniformly mixed to obtain the final product.
Test case 1
Shearing performance test
The asphalt adhesive that embodiment 1-6 is provided is used and carries out shear strength test, 100mm × 50mm waterproof roll is bonded
On cement mortar specimen, cutting for 7 days testing water-proof coiled materials and substrate is placed under conditions of -10 DEG C, 25 DEG C and 40 DEG C respectively
Shearing stress is tested using dynamic shear rheometer.
Test result is as shown in table 1.
1 shear strength of table
As seen from the above table, it is strong to all have very good shearing within the scope of larger temperature for asphalt adhesive provided by the invention
Degree, screens by plurality of raw materials, effectively improves the shear strength under its low temperature and high temperature.
Test case 2
Residual stability test
Residual stability test is carried out to the asphalt adhesive that embodiment 1-6 is provided, test method is referring to JTCF40-2004 standard
The test of asphalt adhesive residual stability is carried out, the residual stability is the ratio of inundation Marshall and standard Marshall stability.
Test result is as shown in table 2.
2 residual stability of table
Residual stability | |
Embodiment 1 | 102% |
Embodiment 2 | 66% |
Embodiment 3 | 70% |
Embodiment 4 | 85% |
Embodiment 5 | 84% |
Embodiment 6 | 93% |
As seen from the above table, residual stability of the invention is all larger than 65%, generally 70% or more, up to
102%, it was demonstrated that asphalt adhesive provided by the invention has good endurance quality.
Claims (10)
1. leakage of coil roofing maintenance process, which comprises the steps of:
Inspection judges leakage cause;
It is taken and the matched maintenance process of leakage cause according to leakage cause;
It is described to include: with the matched maintenance process of leakage cause
When coil waterproof layer cracks: the screed-coat of each 30-50mm wide in both sides at excision coil waterproof layer crack, depth is vertically downward
Greater than 30mm, asphalt adhesive is then poured into, asphalt adhesive height is made to be higher by roofing 2-3mm;
When inlet for stom water and waterproof roll connector alice: alice being cleaned out, dust is removed, dry, brushing asphalt adhesive seals again
It closes.
2. leakage of coil roofing maintenance process according to claim 1, which is characterized in that the asphalt adhesive is dripped by matrix
Blueness, diluent, additive are prepared;
The additive includes at least one of surfactant, regenerative agent, antistripping agent.
3. leakage of coil roofing maintenance process according to claim 2, which is characterized in that the asphalt adhesive is by by weight
90-120 part matrix pitch, 20-30 parts of diluents, 1-5 portions of regenerative agents, 0.2-1.0 parts of antistripping agents, the 0.2-1.0 parts of tables of meter
Face activating agent is prepared.
4. leakage of coil roofing maintenance process according to claim 2, which is characterized in that the additive further includes wooden
Element or lignin derivative;
The lignin derivative preparation method be by by weight 40-60 part lignin and the additions of 0.5-1.0 parts of zinc powders
Into 200-300 parts of formic acid, it is heated to 100-110 DEG C of holding 2-3 hours, is cooled to 60-70 DEG C, 200-300 parts of 5- are added
10wt% hydrogen peroxide and 0.2-0.5 parts of ferric sulfate are heated to 100-110 DEG C of holding 1-3 hours, centrifugation, take liquid to get.
5. leakage of coil roofing maintenance process according to claim 4, which is characterized in that the asphalt adhesive is by by weight
90-120 part matrix pitch, 20-30 parts of diluents, 1-5 portions of regenerative agents, 0.2-1.0 parts of antistripping agents, the 0.2-1.0 parts of tables of meter
Face activating agent, 0.5-1.5 part lignin or derivatives thereof is prepared.
6. the leakage of coil roofing maintenance process according to any one of claim 2-5, which is characterized in that the diluent
Including at least one of gasoline, diesel oil, paraxylene, turpentine oil, White Mineral Oil, cyclohexanone or methyl oleate.
7. the leakage of coil roofing maintenance process according to any one of claim 2-5, which is characterized in that the surface is living
Property agent includes at least one of amide surfactants and/or at least one of organic acid surfactant;
The amide surfactants structural formula is CnH2n+1COONH2, wherein n is the integer for being less than or equal to 20 more than or equal to 6;
The organic acid surfactant structure formula is CnH2n+1COOH, wherein n is the integer for being less than or equal to 20 more than or equal to 6.
8. the leakage of coil roofing maintenance process according to any one of claim 2-5, which is characterized in that the regenerative agent
The preparation method is as follows:
(1) 0.5-1 part sodium alkyl sulfonate by weight is added in 100-120 parts of water, adds 5-10 parts of greases, stirs
Emulsification 60-120 minutes is mixed, emulsion is obtained;
(2) by by weight 1-2 part melamine and 1.8-2.4 parts of urea be added in 10-20 parts of water, then be passed through 1.2-
1.6 parts of formaldehyde adjust pH value to 8-9 with the sodium hydrate aqueous solution of 5-20wt%, are warming up to 70-80 DEG C, 60-90 points of stirring
Clock is back to room temperature naturally, obtains pre-polymerization liquid;
(3) pre-polymerization liquid is added in emulsion in the case of stirring, is heated to 65 DEG C with the rate of heat addition of 3-5 DEG C/min,
System pH is adjusted to 2-3 with 5-20wt% aqueous citric acid solution, is stirred 4-8 hours, filtering, solid is taken, it is dry to get regeneration
Agent.
9. leakage of coil roofing maintenance process according to claim 8, which is characterized in that the grease is hydroxy stearic acid
Ester oils.
10. the leakage of coil roofing maintenance process according to any one of claim 2-5, which is characterized in that the pitch
The preparation method of glue is to be uniformly mixed each raw material by weight ratio to obtain the final product.
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Cited By (1)
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CN115341783A (en) * | 2022-07-21 | 2022-11-15 | 黄建洲 | Building surface waterproof SBS coiled material seepage repair car |
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