CN110403886A - A kind of cosmetic additive agent and preparation method thereof - Google Patents
A kind of cosmetic additive agent and preparation method thereof Download PDFInfo
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- CN110403886A CN110403886A CN201810386081.1A CN201810386081A CN110403886A CN 110403886 A CN110403886 A CN 110403886A CN 201810386081 A CN201810386081 A CN 201810386081A CN 110403886 A CN110403886 A CN 110403886A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
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Abstract
The invention discloses a kind of cosmetic additive agents, are made of the raw material of following parts by weight: 30-50 parts of jellyfish, 20-40 parts of centella, 20-40 parts of ivy, 15-25 parts of yellow chamomile, 3-5 parts of Coleus forskohlii, 4-6 parts of comfrey, 3-5 parts of multi-vitamins, 1-3 parts of apple polyphenol, 1-3 parts of ferulic acid, 2-4 parts of arbutin, 3-5 parts of astringent, 1-3 parts of calamine, 5-7 parts of Vitamin C Ethyl Ether, 3-5 parts of didextrose base gallate, 4-6 parts of zirconia ball, 20-40 parts of pearl powder, 3-5 parts of tributyl phosphate.The present invention can lock the moisture of skin with depth, even in the lower environment of relative humidity, also skin moisture can be kept for a long time, so that skin is not dried water shortage because of the influence of environment, to keep the moisture content of skin for a long time and moisten degree, and improves skin elasticity, the oxidation of tyrosinase and DOPA is directly binded to tyrosinase and blocked by itself, the decomposition and excretion for accelerating melanin, block the formation of melanin, to carry out white-skinned face function.
Description
Technical field
The present invention relates to cosmetic technical field, specifically a kind of cosmetic additive agent and preparation method thereof.
Background technique
Water, is Source of life, is also the source of skin beauty.Healthy and beautiful skin should be full and plentiful, Mei Gexi
Born of the same parents' moisture is sufficient, the colour of skin and gloss of health is presented, and dermatoglyph is orderly, physiological function is sound;And cell water shortage can be led
It causes the generation of dry line, or even becomes permanent wrinkle and the colour of skin is dark and gloomy, dermatoglyph is mixed and disorderly or even physiological function (example
Such as: metabolism, excretion) missing.Key factor whether influencing skin health is the water content of skin.Usual epidermis and corium contain
Water is about 75%;The water content of cuticula is the state that the skin of 10-20% can show health, is generally not less than
10%.The problem of if water content of cuticula is lower than 10%, will appear dry skin, such as wrinkle, decortication, dark and gloomy etc..
In addition, with the aggravation of people's life, the quickening of work rhythm and environmental pollution, the skin problem that people face
More and more, especially obscure, pigmentation of the colour of skin etc. has become common problem, therefore skin-lightening cosmetic is also opened as skin care item
One hot spot in hair field.It is increasingly mature with people's consumption idea, consumer to the focus of skin-lightening cosmetic not only
It is that its is both effectiveness, while also more focuses on its safety.
In recent years, as the transition of weather, the deterioration of environment, the drying of skin and its coarse obscure problem have become one greatly
Puzzlement.Numerous cosmetics consumers and cosmetics researcher are intended to be able to solve or alleviate the drying of skin and obscure
Problem.Currently, have the moisturizing whitening product of more moisturizing class on the market, but due to the obscure skin of drying be not only by
What moisturizing was able to solve, cause the effect of long-term moisturizing whitening barely satisfactory.
Summary of the invention
The purpose of the present invention is to provide a kind of cosmetics with excellent performance of keeping humidity and cell anti-inflammatory ability to add
Add agent and preparation method thereof, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 30-50 parts of jellyfish, 20-40 parts of centella, ivy
20-40 parts, 15-25 parts of yellow chamomile, 3-5 parts of Coleus forskohlii, 4-6 parts of comfrey, 3-5 parts of multi-vitamins, apple polyphenol 1-3
Part, 1-3 parts of ferulic acid, 2-4 parts of arbutin, 3-5 parts of astringent, 1-3 parts of calamine, 5-7 parts of Vitamin C Ethyl Ether, didextrose
3-5 parts of base gallate, 4-6 parts of zirconia ball, 20-40 parts of pearl powder, 3-5 parts of tributyl phosphate.
As a further solution of the present invention: the cosmetic additive agent is made of: jellyfish the raw material of following parts by weight
35-45 parts, 25-35 parts of centella, 25-35 parts of ivy, 18-22 parts of yellow chamomile, 3.5-4.5 parts of Coleus forskohlii, comfrey
4.5-5.5 parts, 3.5-4.5 parts of multi-vitamins, 1.5-2.5 parts of apple polyphenol, 1.5-2.5 parts of ferulic acid, arbutin 2.5-3.5
Part, 3.5-4.5 parts of astringent, 1.5-2.5 parts of calamine, 5.5-6.5 parts of Vitamin C Ethyl Ether, didextrose base gallate 3.5-4.5
Part, 4.5-5.5 parts of zirconia ball, 25-35 parts of pearl powder, 3.5-4.5 parts of tributyl phosphate.
As a further solution of the present invention: the cosmetic additive agent is made of the raw material of following parts by weight: jellyfish 40
Part, 30 parts of centella, 30 parts of ivy, 20 parts of yellow chamomile, 4 parts of Coleus forskohlii, 5 parts of comfrey, 4 parts of multi-vitamins, apple
2 parts of fruit polyphenol, 2 parts of ferulic acid, 3 parts of arbutin, 4 parts of astringent, 2 parts of calamine, 6 parts of Vitamin C Ethyl Ether, didextrose base Gallate
Sour 4 parts, 5 parts of zirconia ball, 30 parts of pearl powder, 4 parts of tributyl phosphate.
As a further solution of the present invention: the acidic hydrolysis agent is hydrochloric acid solution, sulfuric acid solution, nitric acid solution;Institute
Stating basic hydrolysis agent is potassium hydroxide solution, sodium hydroxide solution, calcium hydroxide suspension.
As further scheme of the invention: the concentration of the acidic hydrolysis agent and basic hydrolysis agent is 2-3mol/
L。
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) by after jellyfish desalting processing, place is hydrolyzed using 90-120 parts of acidic hydrolysis agent and 90-120 parts of basic hydrolysis agent
Reason Hydrolysis At Room Temperature 0.5-2 hours, obtains acid viscous fluid and alkaline viscous fluid under the pressure of 0.1-0.6MPa;By the acid
Property viscous fluid and the alkaline viscous fluid carry out separating treatment respectively, obtain acid clear liquid and alkaline clear liquid, will be described acid clear
Liquid and the alkaline clear liquid merge, and obtain mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, obtains jellyfish extract
It is spare;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and addition 15-25 volume is measured molten again thereto
Agent extracts at least 2 times, each 3-5h, and mixing extracts obtained extracting solution every time, obtains mixed extract;Obtained mixing is mentioned
It takes liquid to be concentrated, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1600-1800rpm, and feed pressure starts grinding after being 0.1-0.3KPa, and pearl powder and ethyl alcohol are pressed 1:15
Mass volume ratio mixing after be added after distilled water and tributyl phosphate carry out grinding 1-2h, pearl powder slurry is discharged, will be precious
It is ground in an oven using ceramic mortar, mistake after dried cake after being washed with deionized 2-3 times after the freeze-drying of pearl slurry material
It is spare that 120 meshes obtain Nano grade pearl powder;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 100-150 mesh, 7-9 times of quality of the two is added
45% ethyl alcohol, stir process 3-5h is sealed at 65-70 DEG C, then carries out microwave abstracting 30-50min, it is standby to filter to take extract liquor
With;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 20-40min is stirred at 30-50 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 70-80 DEG C, after ultrasonic vibration 1-3h, then is cooled to 50-60 DEG C, continues to stir 3-5h, be cooled to 30-40 DEG C,
At 1600-1800rpm after stirring 20-40min to obtain the final product.
Compared with prior art, the beneficial effects of the present invention are:
The present invention can lock the moisture of skin with depth, even can also keep for a long time in the lower environment of relative humidity
Skin moisture makes skin not dry water shortage because of the influence of environment, to keep the moisture content of skin for a long time and moisten
Degree, and improve skin elasticity, the oxidation of tyrosinase and DOPA is directly binded to tyrosinase and blocked by itself, is added
The decomposition and excretion of fast melanin, can effectively inhibit the activity of the tyrosinase in skin, block the formation of melanin, thus
Carry out white-skinned face function.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 30 parts of jellyfish, 20 parts of centella, 20 parts of ivy, spring
15 parts of yellow chrysanthemum, 3 parts of Coleus forskohlii, 4 parts of comfrey, 3 parts of multi-vitamins, 1 part of apple polyphenol, 1 part of ferulic acid, arbutin 2
Part, 3 parts of astringent, 1 part of calamine, 5 parts of Vitamin C Ethyl Ether, 3 parts of didextrose base gallate, 4 parts of zirconia ball, pearl powder 20
Part, 3 parts of tributyl phosphate.
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) it by after jellyfish desalting processing, is hydrolyzed using 90 parts of acidic hydrolysis agent and 90 parts of basic hydrolysis agent, In
Under the pressure of 0.1MPa, Hydrolysis At Room Temperature 0.5 hour, acid viscous fluid and alkaline viscous fluid are obtained;By the acid viscous fluid and
The alkalinity viscous fluid carries out separating treatment respectively, obtains acid clear liquid and alkaline clear liquid, by the acid clear liquid and the alkali
Property clear liquid merge, obtain mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, it is spare to obtain jellyfish extract;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and the solvent that 15 volumes are measured again is added thereto
Extraction at least 2 times, each 3h, mixing extract obtained extracting solution every time, obtain mixed extract;The mixed extract that will be obtained
Concentration, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1600rpm, and feed pressure starts grinding after being 0.1KPa, and pearl powder and ethyl alcohol are pressed to the quality volume of 1:15
After carrying out grinding 1h than addition distilled water after mixing and tributyl phosphate, pearl powder slurry is discharged, pearl powder slurry is freezed
It after dried cake in an oven is washed with deionized after 2 times after drying, is ground using ceramic mortar, crosses 120 meshes and received
The other pearl powder of meter level is spare;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, is sieved with 100 mesh sieve, 45% second of 7 times of quality of the two is added
Alcohol seals stir process 3h at 65 DEG C, then carries out microwave abstracting 30min, and it is spare to filter to take extract liquor;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 20min is stirred at 30 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 70 DEG C, after ultrasonic vibration 1h, then is cooled to 50 DEG C, continues to stir 3h, be cooled to 30 DEG C, stir at 1600 rpm
It mixes after 20min to obtain the final product.
Embodiment 2
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 35 parts of jellyfish, 25 parts of centella, 25 parts of ivy, spring
18 parts of yellow chrysanthemum, 3.5 parts of Coleus forskohlii, 4.5 parts of comfrey, 3.5 parts of multi-vitamins, 1.5 parts of apple polyphenol, ferulic acid 1.5
Part, 2.5 parts of arbutin, 3.5 parts of astringent, 1.5 parts of calamine, 5.5 parts of Vitamin C Ethyl Ether, 3.5 parts of didextrose base gallate,
4.5 parts of zirconia ball, 25 parts of pearl powder, 3.5 parts of tributyl phosphate.
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) it by after jellyfish desalting processing, is hydrolyzed using 100 parts of acidic hydrolysis agent and 100 parts of basic hydrolysis agent, In
Under the pressure of 0.2MPa, Hydrolysis At Room Temperature 1 hour, acid viscous fluid and alkaline viscous fluid are obtained;By the acid viscous fluid and institute
It states alkaline viscous fluid and carries out separating treatment respectively, obtain acid clear liquid and alkaline clear liquid, by the acid clear liquid and the alkalinity
Clear liquid merges, and obtains mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, it is spare to obtain jellyfish extract;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and the solvent that 18 volumes are measured again is added thereto
Extraction at least 2 times, each 3.5h, mixing extract obtained extracting solution every time, obtain mixed extract;Obtained mixing is extracted
Liquid concentration, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1650rpm, and feed pressure starts grinding after being 0.15KPa, and pearl powder and ethyl alcohol are pressed to the mass body of 1:15
After product carries out grinding 1.2h than addition distilled water after mixing and tributyl phosphate, pearl powder slurry is discharged, by pearl powder slurry
It after dried cake in an oven is washed with deionized after 2 times after freeze-drying, is ground using ceramic mortar, crosses 120 meshes and obtain
It is spare to Nano grade pearl powder;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 110 meshes, the 45% of 7.5 times of quality of the two is added
Ethyl alcohol seals stir process 3.5h at 66 DEG C, then carries out microwave abstracting 35min, and it is spare to filter to take extract liquor;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 25min is stirred at 35 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 72 DEG C, after ultrasonic vibration 1.5h, then is cooled to 52 DEG C, continues to stir 3.5h, 32 DEG C are cooled to, in 1650rpm
After lower stirring 25min to obtain the final product.
Embodiment 3
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 40 parts of jellyfish, 30 parts of centella, 30 parts of ivy, spring
20 parts of yellow chrysanthemum, 4 parts of Coleus forskohlii, 5 parts of comfrey, 4 parts of multi-vitamins, 2 parts of apple polyphenol, 2 parts of ferulic acid, arbutin 3
Part, 4 parts of astringent, 2 parts of calamine, 6 parts of Vitamin C Ethyl Ether, 4 parts of didextrose base gallate, 5 parts of zirconia ball, pearl powder 30
Part, 4 parts of tributyl phosphate.
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) it by after jellyfish desalting processing, is hydrolyzed using 105 parts of acidic hydrolysis agent and 105 parts of basic hydrolysis agent, In
Under the pressure of 0.4MPa, Hydrolysis At Room Temperature 1.2 hours, acid viscous fluid and alkaline viscous fluid are obtained;By the acid viscous fluid and
The alkalinity viscous fluid carries out separating treatment respectively, obtains acid clear liquid and alkaline clear liquid, by the acid clear liquid and the alkali
Property clear liquid merge, obtain mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, it is spare to obtain jellyfish extract;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and 20 times of volumes of addition are measured molten again thereto
Agent extracts at least 2 times, each 4h, and mixing extracts obtained extracting solution every time, obtains mixed extract;Obtained mixing is extracted
Liquid concentration, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1700rpm, and feed pressure starts grinding after being 0.2KPa, and pearl powder and ethyl alcohol are pressed to the quality volume of 1:15
After carrying out grinding 1.5h than addition distilled water after mixing and tributyl phosphate, pearl powder slurry is discharged, pearl powder slurry is cold
Be lyophilized it is dry after dried cake in an oven is washed with deionized after 3 times after, ground using ceramic mortar, cross 120 meshes obtain
Nano grade pearl powder is spare;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 120 meshes, 45% second of 8 times of quality of the two is added
Alcohol seals stir process 4h at 68 DEG C, then carries out microwave abstracting 40min, and it is spare to filter to take extract liquor;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 30min is stirred at 40 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 75 DEG C, after ultrasonic vibration 2h, then is cooled to 55 DEG C, continues to stir 4h, be cooled to 35 DEG C, stirred at 1700rpm
It mixes after 30min to obtain the final product.
Embodiment 4
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 45 parts of jellyfish, 35 parts of centella, 35 parts of ivy, spring
22 parts of yellow chrysanthemum, 4.5 parts of Coleus forskohlii, 5.5 parts of comfrey, 4.5 parts of multi-vitamins, 2.5 parts of apple polyphenol, ferulic acid 2.5
Part, 3.5 parts of arbutin, 4.5 parts of astringent, 2.5 parts of calamine, 6.5 parts of Vitamin C Ethyl Ether, 4.5 parts of didextrose base gallate,
5.5 parts of zirconia ball, 35 parts of pearl powder, 4.5 parts of tributyl phosphate.
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) it by after jellyfish desalting processing, is hydrolyzed using 110 parts of acidic hydrolysis agent and 110 parts of basic hydrolysis agent, In
Under the pressure of 0.5MPa, Hydrolysis At Room Temperature 1.5 hours, acid viscous fluid and alkaline viscous fluid are obtained;By the acid viscous fluid and
The alkalinity viscous fluid carries out separating treatment respectively, obtains acid clear liquid and alkaline clear liquid, by the acid clear liquid and the alkali
Property clear liquid merge, obtain mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, it is spare to obtain jellyfish extract;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and the solvent that 22 volumes are measured again is added thereto
Extraction at least 2 times, each 4.5h, mixing extract obtained extracting solution every time, obtain mixed extract;Obtained mixing is extracted
Liquid concentration, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1750rpm, and feed pressure starts grinding after being 0.25KPa, and pearl powder and ethyl alcohol are pressed to the mass body of 1:15
After product carries out grinding 1.8h than addition distilled water after mixing and tributyl phosphate, pearl powder slurry is discharged, by pearl powder slurry
It after dried cake in an oven is washed with deionized after 3 times after freeze-drying, is ground using ceramic mortar, crosses 120 meshes and obtain
It is spare to Nano grade pearl powder;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 140 meshes, the 45% of 8.5 times of quality of the two is added
Ethyl alcohol seals stir process 4.5h at 69 DEG C, then carries out microwave abstracting 45min, and it is spare to filter to take extract liquor;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 35min is stirred at 45 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 78 DEG C, after ultrasonic vibration 2.5h, then is cooled to 58 DEG C, continues to stir 4.5h, 38 DEG C are cooled to, in 1750rpm
After lower stirring 35min to obtain the final product.
Embodiment 5
A kind of cosmetic additive agent is made of the raw material of following parts by weight: 50 parts of jellyfish, 40 parts of centella, 40 parts of ivy, spring
25 parts of yellow chrysanthemum, 5 parts of Coleus forskohlii, 6 parts of comfrey, 5 parts of multi-vitamins, 3 parts of apple polyphenol, 3 parts of ferulic acid, arbutin 4
Part, 5 parts of astringent, 3 parts of calamine, 7 parts of Vitamin C Ethyl Ether, 5 parts of didextrose base gallate, 6 parts of zirconia ball, pearl powder 40
Part, 5 parts of tributyl phosphate.
The preparation method of the cosmetic additive agent, the specific steps are as follows:
(1) according to parts by weight at taking each raw material;
(2) it by after jellyfish desalting processing, is hydrolyzed using 120 parts of acidic hydrolysis agent and 120 parts of basic hydrolysis agent, In
Under the pressure of 0.6MPa, Hydrolysis At Room Temperature 2 hours, acid viscous fluid and alkaline viscous fluid are obtained;By the acid viscous fluid and institute
It states alkaline viscous fluid and carries out separating treatment respectively, obtain acid clear liquid and alkaline clear liquid, by the acid clear liquid and the alkalinity
Clear liquid merges, and obtains mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, it is spare to obtain jellyfish extract;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and the solvent that 25 volumes are measured again is added thereto
Extraction at least 2 times, each 5h, mixing extract obtained extracting solution every time, obtain mixed extract;The mixed extract that will be obtained
Concentration, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1800rpm, and feed pressure starts grinding after being 0.3KPa, and pearl powder and ethyl alcohol are pressed to the quality volume of 1:15
After carrying out grinding 2h than addition distilled water after mixing and tributyl phosphate, pearl powder slurry is discharged, pearl powder slurry is freezed
It after dried cake in an oven is washed with deionized after 3 times after drying, is ground using ceramic mortar, crosses 120 meshes and received
The other pearl powder of meter level is spare;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 150 meshes, 45% second of 9 times of quality of the two is added
Alcohol seals stir process 5h at 70 DEG C, then carries out microwave abstracting 50min, and it is spare to filter to take extract liquor;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 40min is stirred at 50 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 80 DEG C, after ultrasonic vibration 3h, then is cooled to 60 DEG C, continues to stir 5h, be cooled to 40 DEG C, stirred at 1800rpm
It mixes after 40min to obtain the final product.
The acidic hydrolysis agent is hydrochloric acid solution, sulfuric acid solution, nitric acid solution;The basic hydrolysis agent is that potassium hydroxide is molten
Liquid, sodium hydroxide solution, calcium hydroxide suspension.The acid W hydrolytic reagent and the concentration of basic hydrolysis agent are 2-3mol/L.
The present invention can lock the moisture of skin with depth, even in the lower environment of relative humidity, it also can be for a long time
Keep skin moisture, so that skin is not dried water shortage because of the influence of environment, thus keep for a long time skin moisture content and
Degree is moistened, and improves skin elasticity, is directly binded to tyrosinase and blocks the oxidation of tyrosinase and DOPA to make by itself
With accelerating the decomposition and excretion of melanin, the activity of the tyrosinase in skin can be effectively inhibited, block the shape of melanin
At to carry out white-skinned face function.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
Various changes can be made.
Claims (6)
1. a kind of cosmetic additive agent, which is characterized in that be made of the raw material of following parts by weight: 30-50 parts of jellyfish, centella
20-40 parts, 20-40 parts of ivy, 15-25 parts of yellow chamomile, 3-5 parts of Coleus forskohlii, 4-6 parts of comfrey, multi-vitamins 3-5
Part, 1-3 parts of apple polyphenol, 1-3 parts of ferulic acid, 2-4 parts of arbutin, 3-5 parts of astringent, 1-3 parts of calamine, vitamin C ethyl
5-7 parts of ether, 3-5 parts of didextrose base gallate, 4-6 parts of zirconia ball, 20-40 parts of pearl powder, 3-5 parts of tributyl phosphate.
2. cosmetic additive agent according to claim 1, which is characterized in that be made of the raw material of following parts by weight: jellyfish
35-45 parts, 25-35 parts of centella, 25-35 parts of ivy, 18-22 parts of yellow chamomile, 3.5-4.5 parts of Coleus forskohlii, comfrey
4.5-5.5 parts, 3.5-4.5 parts of multi-vitamins, 1.5-2.5 parts of apple polyphenol, 1.5-2.5 parts of ferulic acid, arbutin 2.5-3.5
Part, 3.5-4.5 parts of astringent, 1.5-2.5 parts of calamine, 5.5-6.5 parts of Vitamin C Ethyl Ether, didextrose base gallate 3.5-4.5
Part, 4.5-5.5 parts of zirconia ball, 25-35 parts of pearl powder, 3.5-4.5 parts of tributyl phosphate.
3. cosmetic additive agent according to claim 1, which is characterized in that be made of the raw material of following parts by weight: jellyfish
40 parts, 30 parts of centella, 30 parts of ivy, 20 parts of yellow chamomile, 4 parts of Coleus forskohlii, 5 parts of comfrey, 4 parts of multi-vitamins,
2 parts of apple polyphenol, 2 parts of ferulic acid, 3 parts of arbutin, 4 parts of astringent, 2 parts of calamine, 6 parts of Vitamin C Ethyl Ether, didextrose base
4 parts of gallate, 5 parts of zirconia ball, 30 parts of pearl powder, 4 parts of tributyl phosphate.
4. cosmetic additive agent according to claim 1 to 3, which is characterized in that the acidic hydrolysis agent is that hydrochloric acid is molten
Liquid, sulfuric acid solution, nitric acid solution;The basic hydrolysis agent is that potassium hydroxide solution, sodium hydroxide solution, calcium hydroxide are suspended
Liquid.
5. cosmetic additive agent according to claim 1 to 3, which is characterized in that the acidic hydrolysis agent and alkaline water
The concentration for solving agent is 2-3mol/L.
6. a kind of preparation method of cosmetic additive agent a method according to any one of claims 1-3, which is characterized in that specific steps are such as
Under:
(1) according to parts by weight at taking each raw material;
(2) by after jellyfish desalting processing, place is hydrolyzed using 90-120 parts of acidic hydrolysis agent and 90-120 parts of basic hydrolysis agent
Reason Hydrolysis At Room Temperature 0.5-2 hours, obtains acid viscous fluid and alkaline viscous fluid under the pressure of 0.1-0.6MPa;By the acid
Property viscous fluid and the alkaline viscous fluid carry out separating treatment respectively, obtain acid clear liquid and alkaline clear liquid, will be described acid clear
Liquid and the alkaline clear liquid merge, and obtain mixing clear liquid;Impurity will be removed after mixing clear liquid concentration, obtains jellyfish extract
It is spare;
(3) centella after taking cleaning smashes it through 10 meshes and obtains asiatic pennywort Herd, and addition 15-25 volume is measured molten again thereto
Agent extracts at least 2 times, each 3-5h, and mixing extracts obtained extracting solution every time, obtains mixed extract;Obtained mixing is mentioned
It takes liquid to be concentrated, obtains concentrate, the concentrate is that the Gotu Kola P.E is spare;
(4) zirconia ball is transferred in nano ceramics sand milling dispersion machine in backward feed paddle cylinder and dehydrated alcohol is added, controlled
Engine speed processed is 1600-1800rpm, and feed pressure starts grinding after being 0.1-0.3KPa, and pearl powder and ethyl alcohol are pressed 1:15
Mass volume ratio mixing after be added after distilled water and tributyl phosphate carry out grinding 1-2h, pearl powder slurry is discharged, will be precious
It is ground in an oven using ceramic mortar, mistake after dried cake after being washed with deionized 2-3 times after the freeze-drying of pearl slurry material
It is spare that 120 meshes obtain Nano grade pearl powder;
(5) ivy, yellow chamomile, Coleus forskohlii, comfrey are crushed, crosses 100-150 mesh, 7-9 times of quality of the two is added
45% ethyl alcohol, stir process 3-5h is sealed at 65-70 DEG C, then carries out microwave abstracting 30-50min, it is standby to filter to take extract liquor
With;
(6) multi-vitamins, apple polyphenol, ferulic acid, arbutin, astringent, calamine, Vitamin C Ethyl Ether, didextrose are taken
Deionized water is added in base gallate, and 20-40min is stirred at 30-50 DEG C and obtains mixture;
(7) jellyfish extract, Gotu Kola P.E, Nano grade pearl powder and extract liquor are added to the mixing of step (6)
In object, it is heated to 70-80 DEG C, after ultrasonic vibration 1-3h, then is cooled to 50-60 DEG C, continues to stir 3-5h, be cooled to 30-40 DEG C,
At 1600-1800rpm after stirring 20-40min to obtain the final product.
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CN113116955A (en) * | 2021-02-24 | 2021-07-16 | 中国药科大学 | Pharmaceutical composition containing plant extracts and application thereof |
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