CN110395855A - A kind of integrated conduct method of cotton dyeing waste water - Google Patents
A kind of integrated conduct method of cotton dyeing waste water Download PDFInfo
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- CN110395855A CN110395855A CN201910828645.7A CN201910828645A CN110395855A CN 110395855 A CN110395855 A CN 110395855A CN 201910828645 A CN201910828645 A CN 201910828645A CN 110395855 A CN110395855 A CN 110395855A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5281—Installations for water purification using chemical agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/308—Dyes; Colorants; Fluorescent agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/30—Nature of the water, waste water, sewage or sludge to be treated from the textile industry
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2203/00—Apparatus and plants for the biological treatment of water, waste water or sewage
- C02F2203/006—Apparatus and plants for the biological treatment of water, waste water or sewage details of construction, e.g. specially adapted seals, modules, connections
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/06—Controlling or monitoring parameters in water treatment pH
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/08—Chemical Oxygen Demand [COD]; Biological Oxygen Demand [BOD]
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/30—Aerobic and anaerobic processes
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Removal Of Specific Substances (AREA)
- Purification Treatments By Anaerobic Or Anaerobic And Aerobic Bacteria Or Animals (AREA)
Abstract
The present invention relates to a kind of integrated conduct methods of cotton dyeing waste water, carry out complexometry extraction concentration to cotton fabric dyeing residual liquid with high salt using extraction process ,-salt concentrated water extracted can be back to dyeing production.High concentration dye concentrated solution extracted is mixed with the organic pre-treatment waste water of high concentration, acidification is hydrolyzed by the way that resistance to sulfate is anaerobic fluidized bed in composite waste, it realizes the degradation of efficient anaerobic dyestuff and decoloration, guarantees the coloration and phenyl amines index qualified discharge of integrated printing and dyeing wastewater treatment.
Description
Technical field
The invention belongs to field of waste water treatment, in particular to a kind of integrated conduct method of cotton dyeing waste water.
Background technique
In dyeing production process, waste water caused by cotton dyeing usually contains higher COD and higher
Salinity causes residual dye concentration high since reactive dye dye-uptake is low, and coloration is high, and biodegradability is poor.It is general higher
Salinity will have a direct impact on the activity of microorganism in biochemical treatment system, salinity contained therein is mainly Na2SO4, due to SO4 2-
The presence of ion, excessively high sulfate concentration can inhibit anaerobic biological process, influence biochemical disposed of in its entirety effect.Therefore, cotton
There is decoloration hardly possible in dyeing waste water, salinity is high, and the phenomenon easily exceeded there are tail water phenyl amines index, and these problems will be that printing and dyeing are useless
Water process urgent problem to be solved.
Currently, the main method for treatment of dyeing wastewater has several techniques such as physico-chemical process, biochemical method, chemical method to combine
Combination treatment method.Part printing and dyeing enterprise also starts the method using shunting of removing contamination, dual treatment, and source of generation carries out waste water
High and low sub-prime is collected and is handled, and reduces processing cost to a certain extent, is recycled to effluent part, generally but
The thinking of end treatment is still continued, the recycling of material is not implemented.It is added especially to cotton dyeing waste water, in dyeing course a large amount of
Salt assitant finally by discharge of wastewater, result in waste of resources.The presence of salt residue and dyestuff simultaneously, to useless under a certain concentration
The biological production liveliness proof of water biochemical system inhibits, thus generally require by special bioreactor by bacteria selection with
The means such as domestication, activity activator carry out bioreactor performance promotion.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of integrated conduct method of cotton dyeing waste water, this method
It solves high chroma, the high salinity, the processing problem of biodegradability difference of dyeing waste water, breaches cotton fabric biological wastewater treatment work
The limitation of skill.
The present invention provides a kind of integrated conduct methods of cotton dyeing waste water, comprising:
(1) cotton fabric dyeing process raffinate is discharged into raffinate water tank and is extracted, the two-phase liquid flowed out from raffinate water tank is logical
Enter compressed air and is sent into three phase separation tank;Color oil of the three phase separation tank top discharge containing dyestuff, is sent into color oil collecting tank, color oil
Collecting tank recycles extractant by back extraction, and the dyestuff raffinate being concentrated is sent into conditioning tank I;The discharge of three phase separation tank lower part
High level salt solution, high level salt solution are sent into salting liquid collecting tank utilization (can be back to dyeing) to be recycled;
(2) high-concentration waste water in pre-treatment workshop section is discharged into conditioning tank I, the dyestuff raffinate with the concentration in step (1)
Mixing, and pH value is adjusted to neutrality;Waste water in low concentration wastewater and the remaining workshop section of dyeing in pre-treatment workshop section is discharged into tune
Save pond II;
(3) by the waste water in conditioning tank I be sent into resistance to sulfate it is anaerobic fluidized bed in degraded and decolourized, resistance to sulfate is detested
After the water outlet of oxygen fluidized bed is mixed with the waste water in conditioning tank II, it is sent into aerobic biochemical system and carries out biological treatment, through sedimentation basin
Biological aerated filter processing is re-fed into after coagulating sedimentation.
Extractant in the step (1) is complexing agent 15-45%, cosolvent 10-30%, surplus are diluent;Wherein,
Complexing agent is one or both of trioctylamine, benzoic acid, and cosolvent is one or both of isomery alcohol, n-octyl alcohol, dilution
Agent is petroleum ether or sulfonated kerosene.
The workshop section that pre-treatment generates high-concentration waste water in step (2) includes one or more of desizing, kiering, concise;
It includes one or more of bleaching, washing that pre-treatment, which generates the workshop section of low concentration wastewater, in step (2).
Dyeing residue workshop section in the step (2) includes one or more of rinsing/washing, fixation.
Dehydration waste liquid in cotton dyeing final finishing workshop section is discharged into conditioning tank II;In cotton dyeing final finishing workshop section
Discarded finishing fluid is discharged into conditioning tank I.
Resistance to sulfate in the step (3) is anaerobic fluidized bed using Mo-bearing Iron Ores as filler, granular size 200-400
Mesh, concentration 0.05-0.25kg/m3。
The anaerobic fluidized bed disengaging mode of resistance to sulfate in the step (3) is bottom in and top out formula, and upflow velocity is
0.8-1.2m/h, water outlet crest of weir arrange 60 mesh wire nettings, and Mo-bearing Iron Ores and mud granule is prevented to be lost;Hydraulic detention time is greater than
36h can realize extension hydraulic detention time by water outlet circulation and the concatenated mode of multiple reactor.
By Mo-bearing Iron Ores particle be placed in resistance to sulfate it is anaerobic fluidized bed in, pass through the anaerobic fluidized bed upflow velocity of control and top
Effluent weir flow velocity realizes that stop and fluidization of the Mo-bearing Iron Ores particle in anaerobic reactor are uniformly distributed, using molybdenum-iron element to hydrolysis
The effect that anaerobic fluidized bed resistance to sulfate inhibits is played in anaerobic bacteria activation in acidification.
The hydraulic detention time of aerobic biochemical system in the step (3) is greater than 24 hours.
The hydraulic detention time of biological aerated filter in the step (3) is greater than 8 hours.
The present invention for the higher cotton dyeing waste water of saliferous take be reasonable distribution and interflow waste water mechanism, will contain
The higher dense dyeing waste-water of salt after being stripped with cotton fabric desizing, that concise/kiering waste water is mixed into resistance to hydrolysis acidification with high salt is anti-
It answers device to handle, can be recycled after processing through staining solution with high salt extracted, solve the problems, such as that salt is difficult to remove.
Desized wastewater, kiering waste water in pre-treating technology section can also contain a large amount of organic matter, can use these organic matter tune in this way
The biodegradability for saving reactor for hydrolysis and acidification is avoided since the too low caused sludge of organic substrates cannot remain sufficiently high dense
Degree, influences effluent quality.The resistance to anaerobic fluidized bed middle packing layer of sulfate can not only filter some suspended materials, also have and inhibit
SO with high salt4 -2Effect.
Beneficial effect
(1) present invention realizes the resource utilization of cotton fabric dyeing process waste liquid salt and water, solves the high color of dyeing waste water
Degree, high salinity, the processing problem of biodegradability difference, breach the limitation of cotton fabric biological process of wastewater treatment.
(2) present invention has been achieved at low cost the recycling of salt in dyeing waste-water, in anaerobic fluidized bed hydrolysis acidification
Stage can remove the pollutants such as 60% or more residual dye.
(3) present invention does not have to change original dyeing production method, handles high chroma, high salinity dyeing waste-water at low cost,
And existing sewerage processing difficulty is significantly reduced, strengthen Hydrolysis Acidification microbiological treatment waste water efficiency under high salt,
The degradation and decoloration and phenyl amines processing up to standard of realization cotton dyeing waste water;High salinity solution extracted can recycle,
Avoid influence of the salt to aftertreatment systems.
Detailed description of the invention
Fig. 1 is the process flow diagram of embodiment 1;Arithemetic unit is m in figure3/d;
Fig. 2 is the process flow diagram of embodiment 2;Arithemetic unit is m in figure3/d。
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
Embodiment 1
To produce based on color cotton yarn, production waste water total amount is 1000m for certain cotton spun yarn dyeing textile enterprise3/ d, composite waste
Mean concentration CODCrFor 1500mg/L, often there is exceeded situation in the coloration of waste water disposal facility, phenyl amines.To meet discharge mark
Quasi- and save the cost resource, is handled dyeing waste water using method of the invention, carries out reuse, effluent color dilution of keeping under strict control to salt
With phenyl amines index.To guarantee to reduce biochemical treatment pressure, dyeing waste water needs effectively to be adjusted before entering biochemical treatment
Section, while salt reuse water quality being made to be protected.Specific implementation process is as follows, as shown in Figure 1:
(1) by cotton fabric dyeing process raffinate 100m3It is discharged into raffinate water tank and is extracted, the two-phase liquid flowed out from raffinate water tank
Body is passed through compressed air and is sent into three phase separation tank;Color oil of the three phase separation tank top discharge containing dyestuff, is sent into color oil collecting tank,
Color oil collecting tank recycles extractant, the dyestuff raffinate 10m being concentrated by back extraction3It is sent into conditioning tank I;Three phase separation tank
90m is discharged in lower part3High level salt solution, high level salt solution are sent into the utilization to be recycled of salting liquid collecting tank.
(2) the concise and desized wastewater 200m being discharged in pre-treatment workshop section3Fully enter conditioning tank I.In pre-treatment workshop section
Bleaching, washing, the washing waste water in dyeing workshop section, the dehydration in final finishing workshop section, amount to 700m3It is discharged into conditioning tank II, as
Lightweight contaminant water.
(3) 210m in conditioning tank I3High concentration COD and high-salt wastewater enter resistance to sulfate it is anaerobic fluidized bed, through 48 hours
Hydraulic detention time processing after and II waste water of conditioning tank mixing after enter aerobic treatment system, amount to 910m3.Wherein,
The resistance to anaerobic fluidized bed Mo-bearing Iron Ores granular size of sulfate is 300 mesh, Mo-bearing Iron Ores granule density 0.1kg/m3;Rise inside fluidized bed
Flow velocity is 0.1m/h, and water outlet crest of weir arranges 60 mesh wire nettings.Aerobic biochemical system hydraulic detention time is for 24 hours, through coagulating sedimentation
Afterwards, it is handled by the biological aerated filter of 8h hydraulic detention time, water 10m is during which lost3, remaining 900m3Tail water can reach
Related request to the direct emission of " textile dyeing and finishing industrial water pollution object discharge standard " (GB 4287) is as shown in table 1.
Embodiment 2
To produce based on dyed cotton fabric and chintz, production waste water total amount is 10000m for certain cotton dyeing textile enterprise3/
D, composite waste mean concentration CODCrFor 2000mg/L.Often there is exceeded situation in the coloration of waste water disposal facility, phenyl amines.Together
When, due to the rise in price of printing and dyeing assistant, enterprise requirements is caused to carry out reuse to salt.Using method of the invention to dyeing waste water
It is handled, specific implementation process is as follows, as shown in Figure 2:
(1) by cotton fabric dyeing process raffinate 500m3It is discharged into raffinate water tank and is extracted, the two-phase liquid flowed out from raffinate water tank
Body is passed through compressed air and is sent into three phase separation tank;Color oil of the three phase separation tank top discharge containing dyestuff, is sent into color oil collecting tank,
Color oil collecting tank recycles extractant, the dyestuff raffinate 50m being concentrated by back extraction3It is sent into conditioning tank I;Three phase separation tank
450m is discharged in lower part3High level salt solution, high level salt solution are sent into the utilization to be recycled of salting liquid collecting tank.
(2) the discarded finishing fluid in the waste water such as desizing, kiering being discharged in pre-treatment workshop section and final finishing is total
1000m3Fully enter conditioning tank I.It bleaches, wash in pre-treatment workshop section, the washing waste water in dyeing workshop section, amounting to 8500m3Row
Enter conditioning tank II, as lightweight contaminant water.
(3) 1050m in conditioning tank I3High concentration COD and high-salt wastewater enter resistance to sulfate it is anaerobic fluidized bed, it is small through 48
When hydraulic detention time processing after and II waste water 8500m of conditioning tank3Biochemical treatment system is arrived into aerobic after mixing, is amounted to
9550m3.Wherein, the anaerobic fluidized bed Mo-bearing Iron Ores granular size of resistance to sulfate is 300 mesh, Mo-bearing Iron Ores granule density inside fluidized bed
0.1kg/m3;Upflow velocity is 0.2m/h inside fluidized bed, and water outlet crest of weir arranges 60 mesh wire nettings.Aerobic biochemical system waterpower is stopped
Staying the time is 48h, and after coagulating sedimentation, water 250m is during which lost3, remaining 9300m3Tail water can achieve " textile dyeing and finishing work
Industry pollution discharge standard " (GB 4287) all related requests discharged indirectly it is as shown in table 1.
1 textile dyeing and finishing industrial water pollution object discharge standard of table
Unit: mg/L (in addition to coloration, pH)
Note:
(1) be suitable for garden (including industrial park, development zone, agglomeration of industries etc.) enterprise is to can be useless to textile dyeing and finishing
The situation that water is specially collected and concentrated the garden sewage treatment plant of pretreatment (not mixing with other waste water) to discharge is concentrated pre-
The water outlet of processing should meet emission limit required by (2).
(2) it is suitable for other indirect emission behaviours in addition to (1).
(3) batik industry executes the limit value.
Claims (9)
1. a kind of integrated conduct method of cotton dyeing waste water, comprising:
(1) cotton fabric dyeing process raffinate is discharged into raffinate water tank and is extracted, the two-phase liquid flowed out from raffinate water tank is passed through pressure
Contracting air is simultaneously sent into three phase separation tank;Color oil of the three phase separation tank top discharge containing dyestuff, is sent into color oil collecting tank, color oil is collected
Tank recycles extractant by back extraction, and the dyestuff raffinate being concentrated is sent into conditioning tank I;The discharge of three phase separation tank lower part is with high salt
Solution, high level salt solution are sent into the utilization to be recycled of salting liquid collecting tank;
(2) high-concentration waste water in pre-treatment workshop section is discharged into conditioning tank I, is mixed with the dyestuff raffinate of the concentration in step (1),
And pH value is adjusted to neutrality;Waste water in low concentration wastewater and the remaining workshop section of dyeing in pre-treatment workshop section is discharged into conditioning tank
Ⅱ;
(3) by the waste water in conditioning tank I be sent into resistance to sulfate it is anaerobic fluidized bed in degraded and decolourized, resistance to sulfate anaerobism stream
After the water outlet of change bed is mixed with the waste water in conditioning tank II, it is sent into aerobic biochemical system and carries out biological treatment, through sedimentation basin coagulation
Biological aerated filter processing is re-fed into after precipitating.
2. processing method according to claim 1, it is characterised in that: the extractant in the step (1) is complexing agent 15-
45%, cosolvent 10-30%, surplus are diluent;Wherein, complexing agent is one or both of trioctylamine, benzoic acid, hydrotropy
Agent is one or both of isomery alcohol, n-octyl alcohol, and diluent is petroleum ether or sulfonated kerosene.
3. processing method according to claim 1, it is characterised in that: pre-treatment generates high-concentration waste water in step (2)
Workshop section includes one or more of desizing, kiering, concise;The workshop section of pre-treatment generation low concentration wastewater includes in step (2)
One or more of bleaching, washing.
4. processing method according to claim 1, it is characterised in that: the dyeing residue workshop section in the step (2) includes
One or more of rinsing/washing, fixation.
5. processing method according to claim 1, it is characterised in that: the dehydration waste liquid in cotton dyeing final finishing workshop section
It is discharged into conditioning tank II;Discarded finishing fluid in cotton dyeing final finishing workshop section is discharged into conditioning tank I.
6. processing method according to claim 1, it is characterised in that: the resistance to sulfate anaerobism fluidisation in the step (3)
For bed using Mo-bearing Iron Ores as filler, granular size is 200-400 mesh, concentration 0.05-0.25kg/m3。
7. processing method according to claim 1, it is characterised in that: the resistance to sulfate anaerobism fluidisation in the step (3)
The disengaging mode of bed is bottom in and top out formula, upflow velocity 0.8-1.2m/h, water outlet crest of weir 60 mesh wire nettings of arrangement;Hydraulic retention
Time is greater than 36h.
8. processing method according to claim 1, it is characterised in that: the water of the aerobic biochemical system in the step (3)
The power residence time is greater than 24 hours.
9. processing method according to claim 1, it is characterised in that: the water of the biological aerated filter in the step (3)
The power residence time is greater than 8 hours.
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CN104211132A (en) * | 2014-09-05 | 2014-12-17 | 广东溢达纺织有限公司 | Extracting agent and method for treating reactive dyeing wastewater |
CN107021538A (en) * | 2017-03-28 | 2017-08-08 | 刘奎东 | A kind of efficient extraction decolouring system of reactive dyeing raffinate |
CN107235594A (en) * | 2017-07-05 | 2017-10-10 | 山东如意科技集团有限公司 | A kind of utilization process and system of reactive dyeing raffinate |
CN108373240A (en) * | 2018-04-11 | 2018-08-07 | 东华大学 | A kind of cotton dyeing waste water dual treatment and the integrated technique of reuse |
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2019
- 2019-09-03 CN CN201910828645.7A patent/CN110395855A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1231995A (en) * | 1999-03-17 | 1999-10-20 | 张秭昆 | Technique of separate treatment for purifying industrial effluent |
CN1309092A (en) * | 2001-03-16 | 2001-08-22 | 清华大学 | Complex extraction process for pre-treating waste water for intermediate of sulfornic dyes |
CN102603025A (en) * | 2012-03-31 | 2012-07-25 | 中国中化股份有限公司 | Method for processing wastewater produced in reactive dye production by utilizing complexing extraction technology |
CN103011516A (en) * | 2012-12-13 | 2013-04-03 | 杭州绿色环保技术开发有限公司 | Reactive printing wastewater treatment process and device |
CN104211132A (en) * | 2014-09-05 | 2014-12-17 | 广东溢达纺织有限公司 | Extracting agent and method for treating reactive dyeing wastewater |
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Application publication date: 20191101 |