CN110330668A - A kind of method and apparatus of agricultural and food and drink waste production humic acid - Google Patents

A kind of method and apparatus of agricultural and food and drink waste production humic acid Download PDF

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Publication number
CN110330668A
CN110330668A CN201910771149.2A CN201910771149A CN110330668A CN 110330668 A CN110330668 A CN 110330668A CN 201910771149 A CN201910771149 A CN 201910771149A CN 110330668 A CN110330668 A CN 110330668A
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CN
China
Prior art keywords
humic acid
food
separator
multiphase
high temperature
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Pending
Application number
CN201910771149.2A
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Chinese (zh)
Inventor
肖莹露
蒋遂安
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Sichuan Rui Yuanneng Ring Science And Technology Ltd
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Sichuan Rui Yuanneng Ring Science And Technology Ltd
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Priority to CN201910771149.2A priority Critical patent/CN110330668A/en
Publication of CN110330668A publication Critical patent/CN110330668A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00Other organic fertilisers
    • C05F11/02Other organic fertilisers from peat, brown coal, and similar vegetable deposits
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07GCOMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G99/00Subject matter not provided for in other groups of this subclass
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08HDERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00Macromolecular compounds derived from lignin, e.g. tannins, humic acids

Abstract

The invention discloses the equipment of a kind of agricultural and food and drink waste production humic acid, belong to technical field of fertilizer production, it includes crusher, multiphase mixer, high temperature anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor, multiphase separator and extraction separator, crusher, multiphase mixer, high temperature anaerobic biochemical reactor, pipeline is passed sequentially through between high temperature oxygen consumption biochemical reactor and multiphase separator is connected to setting, the liquid object output end of multiphase separator is connected to by pipeline with the input terminal of extraction separator, the output end that extraction separator is used to export humic acid is provided with and communicated with humic acid recyclable device, agricultural and food and drink waste are utilized and processing, therefrom extract humic acid, so that resource utilizes the reduction wasting of resources again;The landfill disposal of food garbage is reduced simultaneously, and reduce garbage loading embeading influences caused by environment.

Description

A kind of method and apparatus of agricultural and food and drink waste production humic acid
Technical field
The present invention relates to a kind of methods of technical field of fertilizer production more particularly to agricultural and food and drink waste production humic acid And equipment.
Background technique
Humic acid is the larger molecular organics matter being widely present in nature, is widely used in agriculture, woods, herds, petroleum, change The every field such as work, building materials, medical and health, environmental protection.Ecological agriculture construction is especially advocated now, pollution-less agriculture produces, is green Color food, pollution-free environmental protection etc., more make " humic acid " by high praise.
In the prior art, food and drink waste and agricultural wastes mostly carry out landfill disposal, and agricultural and food and drink waste exist Humic acid is directly filled so that the wasting of resources, is unfavorable for the long-run development of society.
Summary of the invention
The object of the invention is that provide it is a kind of agricultural and food and drink waste production humic acid method and apparatus, have pair The advantages of agricultural and food and drink waste utilize again, reduce the wasting of resources.
To achieve the goals above, the technical solution adopted by the present invention is that: it is a kind of agricultural and food and drink waste produce humic acid Equipment, including crusher, multiphase mixer, high temperature anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor, multiphase separator And extraction separator, crusher, multiphase mixer, high temperature anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor and multiphase point From passing sequentially through pipeline connection setting between device, the liquid object output end of the multiphase separator passes through pipeline and extraction separator Input terminal connection, the output end that the extraction separator is used to export humic acid are provided with and communicated with humic acid recyclable device.
Preferably, the crusher includes shell, is arranged in the intracorporal crushing wheel of shell, for driving crushing wheel to rotate Motor, the crushing wheel includes shaft and multiple cutterheads for being threaded through in shaft, is folded with and is arranged between the adjacent cutterhead Spring in shaft, the spring overcoat are equipped with bellows, and the crushing wheel sets at least to two, the different crushing Cutterhead interlaced setting on break bar offers feed inlet at the top of the shell, and the bottom of shell offers discharge port.
Preferably, the intracorporal top of the shell is provided with a circle water inlet pipe, and multiple hole for water sprayings are offered on water inlet pipe, described Water inlet pipe is in communication with the outside by pipeline.
Preferably, the solid content output end of the multiphase separator is provided with and communicated with carbonization machine by screw conveyor.
Preferably, the output end that the extraction separator is used to export waste material, which is connected to by screw conveyor with carbonization machine, to be set It sets.
Preferably, the pump for material in conveyance conduit is provided on the pipeline.
It preferably, further include control panel and multiple probes, multiple probes are separately positioned on crusher, multiphase mixing Device, high temperature anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor, multiphase separator, extraction separator, carbonization machine and recycling are rotten Phytic acid device, multiple probes are connect with control panel signal.
A kind of method of agricultural and food and drink waste production humic acid, comprising the following steps:
S1, by the food productions leftover bits and pieces waste such as grain, grain, fruits and vegetables, pig, ox, sheep, chicken and duck by pressure breaking machine into Row is broken;
S2, broken material is sent into multiphase mixer, and adds catalyst by stirring into multiphase mixer It mixes so that material and catalyst are homogenized;
S3, it mixture is successively carried out to high temperature anaerobic is reacted with high temperature oxygen consumption, the organic matter in mixture is converted;
S4, the mixture for completing reaction in S3 is delivered in multiphase separator and is separated, be separated into solid content with Liquid object;
S5, liquid object is conveyed into extracting in extraction separator, obtained extract is humic acid, and is used Humic acid is collected by humic acid recyclable device.
Preferably, the solid content in S4 is transported toward carbonization machine and carries out carburizing reagent.
Preferably, waste material remaining in S5 is transported toward carbonization machine and carries out carburizing reagent.
Compared with the prior art, the advantages of the present invention are as follows:
One, reduce and block the damage caused by crusher entirety of hard object between cutterhead;
Two, reduce and block hard object between cutterhead, what is occurred between adjacent cutterhead hits knife phenomenon;
Three, humic acid can be extracted from agricultural and food and drink waste, reduce the wasting of resources;
Four, the landfill phenomenon for reducing agricultural and food and drink waste, reduces the pollution of environment.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the embodiment of the present invention;
Fig. 2 is the schematic diagram of the section structure of the pulverizer of the embodiment of the present invention;
Fig. 3 is the structural schematic diagram of two crushing wheel of pulverizer of the embodiment of the present invention.
In figure: 1, shell;11, feed inlet;12, discharge port;2, crushing wheel;21, shaft;22, cutterhead;3, motor;4, Spring;5, bellows;6, water inlet pipe;61, hole for water spraying.
Specific embodiment
The invention will be further described below.
Embodiment:
As shown in Figure 1, the equipment of a kind of agricultural and food and drink waste production humic acid, including crusher, multiphase mixer, height Warm anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor, multiphase separator and extraction separator.
As shown in Figure 2,3, crusher includes shell 1, the crushing wheel being arranged in shell 12, for driving crushing wheel The motor 3 of 2 rotations.The top of shell 1 offers feed inlet 11, and the bottom of shell 1 offers discharge port 12.
As shown in Figure 2,3, crushing wheel 2 includes shaft 21 and multiple cutterheads 22 for being threaded through in shaft 21, shaft 21 with Motor 3 is sequentially connected.The spring 4 being set in shaft 21 is folded between adjacent cutterhead 22, both ends and the cutterhead 22 of spring 4 offset It connects, is arranged with bellows 5 outside spring 4, spring 4 is blocked, because there are a large amount of moisture, ripples in agricultural and food and drink waste Pipe 5 can preferably protect spring 4, and spring 4 is effectively prevent to get rusty, and extend the service life of spring 4.
As shown in Figure 2,3, crushing wheel 2 is set as two in the present embodiment, 22 phase of cutterhead in different crushing wheels 2 It is mutually staggered, and there are certain intervals between two adjacent cutterheads 22.When being crushed to agricultural wastes, in agricultural wastes inevitably The hard object such as stone can be mingled with, in the prior art, if the gap location that hard object is stuck between two cutterheads 22 will lead to crushing wheel 2 can not Rotation, causes motor 3 to burn.Spring 4 in the present invention between two cutterheads 22 makes cutterhead 22 with certain along 21 axis of shaft The mobile distance in direction, when so that stone being stuck in adjacent cutterhead 22, cutterhead 22 is able to carry out certain offset, to prevent The phenomenon that crushing wheel 2 can not rotate.Two crushing wheels 2 rotation it is contrary, and two crushing wheels 2 setting so that The amount of movement between cutterhead 22 in two different shafts 21 is larger, enables on reducing by two different shafts 21 between adjacent cutterhead 22 Apart from when do not reduce amount of movement between adjacent cutterhead 22.When hard object is stuck in adjacent cutterhead 22 on neither coaxial, coaxially Different degrees of compression is presented in spring 4 between upper two adjacent cutterhead 22, reduces pressure suffered on single spring 4, multiple cutterheads Occur different degrees of axial movement between 22, effectively reduces the collision in different shafts 21 between adjacent cutterhead 22.It reduces simultaneously Folding force suffered by cutterhead 22 prevents cutterhead 22 from fractureing.
As shown in Fig. 2, the top in shell 1 is provided with a circle water inlet pipe 6, water inlet pipe 6 passes through pipeline and extraneous water source Place's connection, may be configured as pond, pump being provided on pipeline in the present embodiment at water source, the water in pond is pumped into water inlet pipe In 6.Multiple hole for water sprayings 61 are offered on water inlet pipe 6, to spray water to crushing wheel 2 and 1 inner wall of shell.Agricultural wastes are mostly stalk The siccative of class, food and drink waste are mostly the remnants of fresh plant, when the two mixes it is broken when, the moisture in fresh plant easily makes The broken agglomerating agglomeration of stalk is obtained, or is covered on 1 inner wall of shell and crushing wheel 2, subsequent broken work is caused Certain influence, while the material that station covers on 1 inner wall of shell and crushing wheel 2 is difficult to clear up.Water is added into shell 1 to be made Broken material is in muddy, cover it is smaller, also to the inside of shell 1 and powder while water is ceaselessly rinsed material Broken break bar 2 is cleaned, and the influence to broken work is reduced.Crushing wheel 2 will appear fever phenomenon when being crushed, and water It can cool down to broken break bar, reduce the fever of broken break bar, extend the service life of cutterhead 22, in the present embodiment, Cutterhead 22 is made of stainless steel material, with certain antibiosis rust ability.
As shown in Figure 1, the discharge port 12 of crusher is connected to by pipeline with the feeding inlet of multiphase mixer, it will be broken Material is delivered in multiphase mixer and is mixed, and multiphase mixer is the auspicious LR-1000 type blender of dragon in the present embodiment.It is more It mixes and also passes through pipeline at device and be provided with and communicated with catalyst tank, the catalyst in catalyst tank is transported to multiphase mixing in material It is delivered to after in device in multiphase mixer, catalyst tank is mixed positioned at multiphase with the connectivity part of multiphase mixer in the present embodiment The roof of clutch, and the control valve whether control catalyst enters in multiphase mixer is provided on pipeline.Multiphase mixer will Catalyst is uniformly mixed with material, and material is homogenized, and is reached the fluctuation amplitude for reducing material chemical component, is made object The chemical component uniformity of material, in order to which the later period carries out biochemical reaction.
As shown in Figure 1, the output end of multiphase mixer is connected to by pipeline with high temperature anaerobic biochemical reactor input terminal, The present embodiment high temperature anaerobic biochemical reactor is that honor enjoys safe FYF-3000L type reaction kettle.After anaerobic reaction, by material from height The output end of warm anaerobic biochemical reactor is reacted in the input terminal by pipeline to high temperature oxygen consumption biochemical reactor, high temperature Material after being sterilized is absorbed by aerobic bacteria, is aoxidized, is decomposed by oxygen consumption biochemical reactor, absorbed is had a part of Machine object is oxidized to simple inorganic matter.The present embodiment high temperature oxygen consumption biochemical reactor is great FJG001 type fermentor.
As shown in Figure 1, the output end of high temperature oxygen consumption biochemical reactor is connected to by pipeline with the input terminal of multiphase separator, Multiphase separator is clear and rich science and technology QRUASB type gas, solid, liquid three phase separator in the present embodiment.The solid content of multiphase separator Output end setting is connected to carbonization machine, to solid content carry out carburizing reagent, recycle solid content in oil gas and activated carbon.At this Carbonization machine is Yunlong YL-150B type carbonizing apparatus in embodiment.
As shown in Figure 1, the liquid object output end of multiphase separator is connected to by pipeline with the input terminal of extraction separator, Extraction separator is global 2500 type seperator in the present embodiment.Extraction separator can be obtained humic acid and be remained after being extracted Under intermediate.Extraction separator, which is used to export the output end of humic acid, is provided with and communicated with humic acid recyclable device, to producing Humic acid be collected, complete humic acid from the extraction in agriculture food and drink waste.Intermediate, which is conveyed into carbonization machine, carries out carbon Change, the water for the generation that is carbonized may be recovered utilization, and final remaining product is active carbon after carbonization, can recycle herein.? Intermediate is delivered in carbonization machine by screw conveyor in the present embodiment.
As shown in Figure 1, being provided with pump and control valve on every root canal road in the present embodiment, pump mentions the liquid in pipeline For power, whether the liquid in control valve control pipeline flows.
As shown in Figure 1, multiple probes are separately positioned on crusher, multiphase mixer, high temperature anaerobic biochemical reactor, high temperature Oxygen consumption biochemical reactor, multiphase separator, extraction separator, humic acid recyclable device, catalyst oxidation reactor and hypergravity are anti- It answers in separator, multiple probes are connect with control panel signal, and the information in each setting is transferred to control panel by probe Interior, operator is in real time monitored the operating of equipment by the faceplate formation on control panel, to realize operating parameter control System and overall intelligence control.
The knot of the equipment of a kind of agricultural provided by the invention and food and drink waste production humic acid is described in detail in above content Structure, corresponding with above equipment system, the present invention also provides a kind of methods of agricultural and food and drink waste production humic acid.
A kind of method of agricultural and food and drink waste production humic acid, comprising the following steps:
S1, by the food productions leftover bits and pieces waste such as grain, grain, fruits and vegetables, pig, ox, sheep, chicken and duck by pressure breaking machine into Row is broken, reduces the body volume of material, in order to subsequent mixing, and reduces the time that material carries out biochemical reaction;
S2, broken material is sent into multiphase mixer, and adds catalyst by stirring into multiphase mixer It mixes so that material and catalyst homogenizing, reach the fluctuation amplitude for reducing material chemical component, make the chemical component of material uniform one It causes;
S3, it mixture is successively carried out to high temperature anaerobic is reacted with high temperature oxygen consumption, the organic matter in mixture is converted;
S4, the mixture for completing reaction in S3 is delivered in multiphase separator and is separated, be separated into solid content with Solid content is transported toward carbonization machine and carries out carburizing reagent, recycles the active carbon of generation by liquid object;
S5, liquid object is conveyed into extracting in extraction separator, obtained extract is humic acid, and is used Humic acid is collected by humic acid recyclable device, and waste material remaining after extraction is transported toward carbonization machine and carries out carburizing reagent, is returned Receive the active carbon generated.
Used herein a specific example illustrates the principle and implementation of the invention, and above embodiments are said It is bright to be merely used to help understand method and its core concept of the invention;At the same time, for those skilled in the art, foundation Thought of the invention, there will be changes in the specific implementation manner and application range, will to change and improvement of the invention It is possible, the conception and scope without exceeding accessory claim defined, in conclusion the content of the present specification should not manage Solution is limitation of the present invention.

Claims (10)

1. the equipment of a kind of agricultural and food and drink waste production humic acid, which is characterized in that including crusher, multiphase mixer, height Warm anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor, multiphase separator and extraction separator, crusher, multiphase mixer, Pipeline is passed sequentially through between high temperature anaerobic biochemical reactor, high temperature oxygen consumption biochemical reactor and multiphase separator is connected to setting, it is described The liquid object output end of multiphase separator is connected to by pipeline with the input terminal of extraction separator, and the extraction separator is for defeated The output end of humic acid is provided with and communicated with humic acid recyclable device out.
2. the equipment of a kind of agricultural according to claim 1 and food and drink waste production humic acid, which is characterized in that described broken Broken machine includes shell (1), the crushing wheel (2) being arranged in shell (1), the motor for driving crushing wheel (2) to rotate (3), the crushing wheel (2) includes shaft (21) and the multiple cutterheads (22) being threaded through on shaft (21), the adjacent cutterhead (22) it is folded with the spring (4) being set on shaft (21) between, bellows (5), the crushing knife are arranged with outside the spring (4) Wheel (2) sets at least to two, cutterhead (22) interlaced setting on the different crushing wheels (2), the shell (1) Top offers feed inlet (11), and the bottom of shell (1) offers discharge port (12).
3. the equipment of a kind of agricultural according to claim 2 and food and drink waste production humic acid, which is characterized in that the shell Top in body (1) is provided with a circle water inlet pipe (6), offers multiple hole for water sprayings (61), the water inlet pipe on water inlet pipe (6) (6) it is in communication with the outside by pipeline.
4. the equipment of a kind of agricultural according to claim 1 and food and drink waste production humic acid, which is characterized in that described more The solid content output end of phase separator is provided with and communicated with carbonization machine by screw conveyor.
5. the equipment of a kind of agricultural according to claim 4 and food and drink waste production humic acid, which is characterized in that the extraction Separator is taken to be connected to setting with carbonization machine by screw conveyor for exporting the output end of waste material.
6. a kind of equipment of agricultural and food and drink waste production humic acid, special described according to claim 1~any one of 5 Sign is, the pump for material in conveyance conduit is provided on the pipeline.
7. the equipment of a kind of agricultural according to claim 1 and food and drink waste production humic acid, which is characterized in that further include Control panel and multiple probes, multiple probes are separately positioned on crusher, multiphase mixer, high temperature anaerobic biochemical reaction Device, high temperature oxygen consumption biochemical reactor, multiphase separator, extraction separator, carbonization machine and recycling humic acid device, multiple spies Head is connect with control panel signal.
8. a kind of method of agricultural and food and drink waste production humic acid, which comprises the following steps:
S1, the food productions leftover bits and pieces waste such as grain, grain, fruits and vegetables, pig, ox, sheep, chicken and duck is carried out brokenly by pressure breaking machine It is broken;
S2, broken material is sent into multiphase mixer, and adds catalyst into multiphase mixer to make by stirring It obtains material and catalyst is homogenized;
S3, it mixture is successively carried out to high temperature anaerobic is reacted with high temperature oxygen consumption, the organic matter in mixture is converted;
S4, the mixture for completing reaction in S3 is delivered in multiphase separator and is separated, be separated into solid content and liquid Object;
S5, liquid object is conveyed into extracting in extraction separator, obtained extract is humic acid, and is planted using rotten Humic acid is collected by acid-restoring plant.
9. the method for a kind of agricultural according to claim 8 and food and drink waste production humic acid, which is characterized in that will be in S4 Solid content transport toward carbonization machine carry out carburizing reagent.
10. the method for a kind of agricultural according to claim 8 and food and drink waste production humic acid, which is characterized in that by S5 In remaining waste material transport toward carbonization machine carry out carburizing reagent.
CN201910771149.2A 2019-08-21 2019-08-21 A kind of method and apparatus of agricultural and food and drink waste production humic acid Pending CN110330668A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103626608A (en) * 2013-11-06 2014-03-12 北京博文合众生物科技有限公司 Technology and process for preparing biological humic acid fertilizer by use of pig manure
CN203649570U (en) * 2013-12-24 2014-06-18 重庆神工机械制造有限责任公司 Deburring device of machine tool
CN107201241A (en) * 2017-05-27 2017-09-26 大连理工大学 The technique that a kind of debirs hydrothermal carbonization produces humic acid coproduction energy gas and charcoal
CN107803259A (en) * 2017-11-28 2018-03-16 苏州拓洁环保工程有限公司 A kind of rubbish crushes crusher chamber
CN108658638A (en) * 2018-08-06 2018-10-16 北京开元信节能科技有限公司 A kind of device with anaerobic fermentation and medium temperature oxidization combination operation production organic fertilizer

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103626608A (en) * 2013-11-06 2014-03-12 北京博文合众生物科技有限公司 Technology and process for preparing biological humic acid fertilizer by use of pig manure
CN203649570U (en) * 2013-12-24 2014-06-18 重庆神工机械制造有限责任公司 Deburring device of machine tool
CN107201241A (en) * 2017-05-27 2017-09-26 大连理工大学 The technique that a kind of debirs hydrothermal carbonization produces humic acid coproduction energy gas and charcoal
CN107803259A (en) * 2017-11-28 2018-03-16 苏州拓洁环保工程有限公司 A kind of rubbish crushes crusher chamber
CN108658638A (en) * 2018-08-06 2018-10-16 北京开元信节能科技有限公司 A kind of device with anaerobic fermentation and medium temperature oxidization combination operation production organic fertilizer

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