CN110327933B - Catalyst for preparing methanol by carbon dioxide hydrogenation, preparation method and application thereof - Google Patents
Catalyst for preparing methanol by carbon dioxide hydrogenation, preparation method and application thereof Download PDFInfo
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- CN110327933B CN110327933B CN201910675995.4A CN201910675995A CN110327933B CN 110327933 B CN110327933 B CN 110327933B CN 201910675995 A CN201910675995 A CN 201910675995A CN 110327933 B CN110327933 B CN 110327933B
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- Prior art keywords
- catalyst
- carbon dioxide
- roasting
- filter cake
- pressure
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title claims abstract description 154
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title claims abstract description 129
- 239000003054 catalyst Substances 0.000 title claims abstract description 97
- 229910002092 carbon dioxide Inorganic materials 0.000 title claims abstract description 77
- 239000001569 carbon dioxide Substances 0.000 title claims abstract description 77
- 238000005984 hydrogenation reaction Methods 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title abstract description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 58
- 239000012065 filter cake Substances 0.000 claims abstract description 34
- 229910052751 metal Inorganic materials 0.000 claims abstract description 30
- 239000002184 metal Substances 0.000 claims abstract description 30
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 28
- 239000000243 solution Substances 0.000 claims abstract description 27
- 238000001556 precipitation Methods 0.000 claims abstract description 24
- 238000000034 method Methods 0.000 claims abstract description 22
- 238000001035 drying Methods 0.000 claims abstract description 19
- 239000012266 salt solution Substances 0.000 claims abstract description 18
- 238000001816 cooling Methods 0.000 claims abstract description 15
- 238000001914 filtration Methods 0.000 claims abstract description 15
- 238000011049 filling Methods 0.000 claims abstract description 14
- 230000008569 process Effects 0.000 claims abstract description 14
- 230000032683 aging Effects 0.000 claims abstract description 7
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000012018 catalyst precursor Substances 0.000 claims abstract description 7
- 150000001879 copper Chemical class 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 150000003751 zinc Chemical class 0.000 claims abstract description 7
- 239000007789 gas Substances 0.000 claims description 21
- 239000010949 copper Substances 0.000 claims description 17
- 230000002431 foraging effect Effects 0.000 claims description 13
- 229910052802 copper Inorganic materials 0.000 claims description 9
- 229910052739 hydrogen Inorganic materials 0.000 claims description 8
- 239000001257 hydrogen Substances 0.000 claims description 8
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 7
- 239000011701 zinc Substances 0.000 claims description 5
- 238000011065 in-situ storage Methods 0.000 claims description 4
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- 230000009467 reduction Effects 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 9
- 230000003197 catalytic effect Effects 0.000 abstract description 6
- 239000013078 crystal Substances 0.000 abstract description 4
- 239000008367 deionised water Substances 0.000 description 18
- 229910021641 deionized water Inorganic materials 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- 230000001276 controlling effect Effects 0.000 description 17
- 239000000047 product Substances 0.000 description 12
- 239000000203 mixture Substances 0.000 description 11
- 150000002739 metals Chemical class 0.000 description 10
- 238000000465 moulding Methods 0.000 description 10
- 239000002243 precursor Substances 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 9
- XIOUDVJTOYVRTB-UHFFFAOYSA-N 1-(1-adamantyl)-3-aminothiourea Chemical compound C1C(C2)CC3CC2CC1(NC(=S)NN)C3 XIOUDVJTOYVRTB-UHFFFAOYSA-N 0.000 description 8
- XNDZQQSKSQTQQD-UHFFFAOYSA-N 3-methylcyclohex-2-en-1-ol Chemical compound CC1=CC(O)CCC1 XNDZQQSKSQTQQD-UHFFFAOYSA-N 0.000 description 8
- SXTLQDJHRPXDSB-UHFFFAOYSA-N copper;dinitrate;trihydrate Chemical compound O.O.O.[Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O SXTLQDJHRPXDSB-UHFFFAOYSA-N 0.000 description 8
- 239000008188 pellet Substances 0.000 description 8
- 230000001105 regulatory effect Effects 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 6
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 238000000975 co-precipitation Methods 0.000 description 4
- 239000002131 composite material Substances 0.000 description 4
- 229910044991 metal oxide Inorganic materials 0.000 description 4
- 150000004706 metal oxides Chemical class 0.000 description 4
- 238000001179 sorption measurement Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical compound [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 229910000510 noble metal Inorganic materials 0.000 description 3
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 2
- 241000282414 Homo sapiens Species 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 238000001651 catalytic steam reforming of methanol Methods 0.000 description 1
- 239000007809 chemical reaction catalyst Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- -1 nitrate ions Chemical class 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 239000011941 photocatalyst Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000767 polyaniline Polymers 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/002—Mixed oxides other than spinels, e.g. perovskite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/80—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with zinc, cadmium or mercury
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/153—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the catalyst used
- C07C29/154—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the catalyst used containing copper, silver, gold, or compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910675995.4A CN110327933B (en) | 2019-07-25 | 2019-07-25 | Catalyst for preparing methanol by carbon dioxide hydrogenation, preparation method and application thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910675995.4A CN110327933B (en) | 2019-07-25 | 2019-07-25 | Catalyst for preparing methanol by carbon dioxide hydrogenation, preparation method and application thereof |
Publications (2)
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CN110327933A CN110327933A (en) | 2019-10-15 |
CN110327933B true CN110327933B (en) | 2022-09-20 |
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CN201910675995.4A Active CN110327933B (en) | 2019-07-25 | 2019-07-25 | Catalyst for preparing methanol by carbon dioxide hydrogenation, preparation method and application thereof |
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Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111167459A (en) * | 2020-02-12 | 2020-05-19 | 中国科学院上海高等研究院 | Catalyst for preparing methanol from mixed gas and preparation method and application thereof |
CN111389401B (en) * | 2020-03-27 | 2021-07-23 | 北京化工大学 | For the efficient catalytic conversion of CO2Preparation method of microorganism coupling catalytic system |
CN113559934B (en) * | 2021-07-21 | 2022-06-17 | 南京工业大学 | Preparation method of catalyst for preparing ethanol by carbon dioxide hydrogenation |
CN113842920B (en) * | 2021-09-24 | 2023-10-31 | 中国科学院上海高等研究院 | Catalyst for preparing methanol by hydrogenation of carbon dioxide, and forming method and application thereof |
CN113856688B (en) * | 2021-11-16 | 2023-11-10 | 扬州大学 | For CO 2 Preparation method of Cu-based catalyst for preparing methanol by hydrogenation |
CN114920623B (en) * | 2022-05-11 | 2023-09-01 | 太原工业学院 | CO (carbon monoxide) 2 Method for preparing methanol by hydrogenation |
CN114849718A (en) * | 2022-05-17 | 2022-08-05 | 山东亮剑环保新材料有限公司 | Rare earth doped CO 2 Preparation method of hydrogenation composite catalyst |
CN116173959A (en) * | 2022-12-12 | 2023-05-30 | 陕西科技大学 | Reverse ZrO 2 -Co catalyst and catalytic Co thereof 2 Hydrogenation synthesis C 5+ Use of alkanes |
CN117282432B (en) * | 2023-08-28 | 2024-06-18 | 中国科学院大连化学物理研究所 | Catalyst for synthesizing green methanol by biomass gasification coupling renewable energy source hydrogen production and preparation method and application thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1036711A (en) * | 1988-03-04 | 1989-11-01 | 纳幕尔杜邦公司 | The carbon dioxide roasting of preparing copper bearing methanol dissociation catalysts |
US5106810A (en) * | 1989-06-29 | 1992-04-21 | E. I. Du Pont De Nemours And Company | Methanol dissociation catalysts |
CN101530803A (en) * | 2009-04-08 | 2009-09-16 | 太原理工大学 | Method for preparing catalyst for methanol synthesis in slurry reactor and application thereof |
WO2012040977A1 (en) * | 2010-09-29 | 2012-04-05 | 大连理工大学 | Catalyst for catalytically hydrogenating co2 to methanol and preparation thereof |
CN104096566A (en) * | 2013-04-12 | 2014-10-15 | 中国石油化工股份有限公司 | Method for preparing copper series methanol synthesis catalyst through precipitation-impregnation process |
-
2019
- 2019-07-25 CN CN201910675995.4A patent/CN110327933B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1036711A (en) * | 1988-03-04 | 1989-11-01 | 纳幕尔杜邦公司 | The carbon dioxide roasting of preparing copper bearing methanol dissociation catalysts |
US5106810A (en) * | 1989-06-29 | 1992-04-21 | E. I. Du Pont De Nemours And Company | Methanol dissociation catalysts |
CN101530803A (en) * | 2009-04-08 | 2009-09-16 | 太原理工大学 | Method for preparing catalyst for methanol synthesis in slurry reactor and application thereof |
WO2012040977A1 (en) * | 2010-09-29 | 2012-04-05 | 大连理工大学 | Catalyst for catalytically hydrogenating co2 to methanol and preparation thereof |
CN104096566A (en) * | 2013-04-12 | 2014-10-15 | 中国石油化工股份有限公司 | Method for preparing copper series methanol synthesis catalyst through precipitation-impregnation process |
Non-Patent Citations (1)
Title |
---|
CO2制备甲醇催化剂研究进展;韩睿 等;《工业催化》;20150930;第23卷(第9期);第678页左栏第2-6段 * |
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CN110327933A (en) | 2019-10-15 |
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