CN110305377A - A kind of vibration isolator and preparation method thereof - Google Patents

A kind of vibration isolator and preparation method thereof Download PDF

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Publication number
CN110305377A
CN110305377A CN201910478490.9A CN201910478490A CN110305377A CN 110305377 A CN110305377 A CN 110305377A CN 201910478490 A CN201910478490 A CN 201910478490A CN 110305377 A CN110305377 A CN 110305377A
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rubber
vibration isolator
liquid
magnetic field
preparation
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CN201910478490.9A
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CN110305377B (en
Inventor
王广克
张燕秉
聂京凯
金文德
刘主光
龚烈谦
易永利
侯东
樊超
田一
刘晓圣
何强
陈新
韩钰
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State Grid Corp of China SGCC
State Grid Zhejiang Electric Power Co Ltd
Global Energy Interconnection Research Institute
Jinhua Power Supply Co of State Grid Zhejiang Electric Power Co Ltd
Wenzhou Power Supply Co of State Grid Zhejiang Electric Power Co Ltd
Original Assignee
State Grid Corp of China SGCC
State Grid Zhejiang Electric Power Co Ltd
Global Energy Interconnection Research Institute
Jinhua Power Supply Co of State Grid Zhejiang Electric Power Co Ltd
Wenzhou Power Supply Co of State Grid Zhejiang Electric Power Co Ltd
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    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K13/00Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
    • C08K13/04Ingredients characterised by their shape and organic or inorganic ingredients
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K13/00Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
    • C08K13/06Pretreated ingredients and ingredients covered by the main groups C08K3/00 - C08K7/00
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/04Carbon
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/08Metals
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00Use of ingredients characterised by shape
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00Use of ingredients characterised by shape
    • C08K7/02Fibres or whiskers
    • C08K7/04Fibres or whiskers inorganic
    • C08K7/06Elements
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00Use of pretreated ingredients
    • C08K9/10Encapsulated ingredients
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/08Metals
    • C08K2003/0856Iron
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/01Magnetic additives

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
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  • Moulding By Coating Moulds (AREA)

Abstract

The present invention relates to vibration isolator technical fields, and in particular to a kind of vibration isolator and preparation method thereof.The present invention provides a kind of vibration isolator, the raw material including following parts by weight: 100 parts and magnetic fillers 5-20 parts of liquid rubber.The present invention also provides a kind of preparation methods of vibration isolator described above, include the following steps: 1) under the action of impressed pressure and externally-applied magnetic field, and the mixture of liquid rubber and magnetic fillers is carried out preforming processing, obtains preforming rubber;2) the preforming rubber for obtaining step 1) carries out sulfidization molding processing, obtains the vibration isolator.Vibration isolator provided by the invention, under the action of externally-applied magnetic field, the microstructure of magnetic fillers will do it fine tuning, makes its orientation arrangement, to form " damping-constraining " structure on microcosmic, and then substantially increases the damping isolation performance of vibration isolator.

Description

A kind of vibration isolator and preparation method thereof
Technical field
The present invention relates to vibration isolator technical fields, and in particular to a kind of vibration isolator and preparation method thereof.
Background technique
With the rapid development of modern industry, construction industry and transportation, noise and vibration pollution is got worse.Noise The normal work and life of people is influenced, is detrimental to health, it is dirty with water pollution, atmosphere pollution, solid waste at present Dye and referred to as today's society four major public hazards.Noise is generated by the vibration of machinery equipment, and vibration influences mechanical machining accuracy And product quality, acceleration mechanical fatigue damage, shorten mechanical service life, and the noise caused by vibrating also endangers the strong of people Health.Therefore, to vibration equipment carry out control it is necessary to, common vibration control method be damping and vibration isolation, vibration isolation be to pass through It is different with the intrinsic frequency of vibratory equipment and damping ratio from the position that equipment is connected directly, and inhibit Vibration propagation;The work of damping With the damping action that principle is by material itself or structure, converts vibrational energy into heat and reach vibration damping purpose.Rubber It is a kind of special viscoelastic material, response lag has good damping characteristic in stress, and itself also has lower Intrinsic frequency, thus often be fabricated to vibration isolator or vibration isolator be used to vibration damping.
The existing method for improving rubber material damping capacity has very much, as blending and modifying, modification by copolymerization, filler filling change Property, form inierpeneirating network structure etc..However filler is arranged irregularly in rubber material in the above method, the resistance for vibration isolator Buddhist nun's anti-vibration performance improves limited.
Summary of the invention
It is an object of the invention to overcome the problems, such as that the damping isolation of vibration isolator in the prior art is ineffective, to provide A kind of vibration isolator and preparation method thereof.
In order to achieve the above objectives, the present invention adopts the following technical scheme:
A kind of vibration isolator, the raw material including following parts by weight: 100 parts and magnetic fillers 5-20 parts of liquid rubber.
Preferably, the magnetic fillers are 10-15 parts.
Preferably, the liquid rubber is selected from diene series liquid rubber, olefin-based liquid rubber, polyurethane series liquid rubber One or more of glue, silicon systems liquid rubber, fluorine system liquid rubber;
Preferably, the liquid rubber is selected from liquid nitrile rubber, liquid styrene butadiene rubber, liquid butyl rubber, LSR type liquid It is one or more of in body silicon rubber.
Preferably, the magnetic fillers are one-dimensional linear or two-dimensional slice stratiform magnetic fillers.
Preferably, the magnetic fillers are selected from one or more of nickel coated graphite powder, nickel packet carbon fiber, flake iron powder.
Preferably, the raw material further includes rubber chemicals.
Preferably, the additional amount of the rubber chemicals is 2-10 parts by weight.
Preferably, the rubber chemicals include the vulcanizing agent of 1-5 parts by weight and the promotor of 1-5 parts by weight.In the present invention In the type of rubber chemicals is not specifically limited, including but not limited to vulcanizing agent and promotor.
Preferably, the vulcanizing agent includes sulphur or peroxide vulcanizing agent;The promotor includes 2- mercapto benzo Thiazole, tetramethylthiuram disulfide, N- ring group -2-[4-morpholinodithio sulfenamide, diphenylguanidine, dimethyl dithiocarbamic acid One or more of zinc, hexa, ethylene thiourea.
The present invention also provides a kind of preparation methods of vibration isolator described above, include the following steps:
1) under the action of impressed pressure and externally-applied magnetic field, the mixture of liquid rubber and magnetic fillers is carried out preforming Processing, obtains preforming rubber;
2) the preforming rubber for obtaining step 1) carries out sulfidization molding processing, obtains the vibration isolator.
Preferably, the externally-applied magnetic field is parallel magnetic field, the magnetic induction intensity of the externally-applied magnetic field be 0.1-1.0 it is special this It draws, the impressed pressure is 3-8 megapascal, time of the mixture of the liquid rubber and magnetic fillers in the externally-applied magnetic field It is 5-20 minutes.
Preferably, further include the steps that rubber chemicals are added into the mixture of the liquid rubber and magnetic fillers.
Preferably, the preforming processing step are as follows: be placed in the mixture of liquid rubber, magnetic fillers and rubber chemicals In mold, then pre-molding under the action of impressed pressure and externally-applied magnetic field.
Preferably, the curing temperature is 150-173 DEG C.
Beneficial effects of the present invention:
1) present invention provides a kind of vibration isolator, the raw material including following parts by weight: 100 parts of liquid rubber and magnetic fillers 5- 20 parts.Vibration isolator provided by the invention, under the action of externally-applied magnetic field, the microstructure of magnetic fillers will do it fine tuning, make It is orientated arrangement, to form " damping-constraining " structure on microcosmic, and then substantially increases the damping isolation performance of vibration isolator.
2) present invention provides a kind of vibration isolator, and further, the liquid rubber is selected from diene series liquid rubber, olefin-based One or more of liquid rubber, polyurethane series liquid rubber, silicon systems liquid rubber, fluorine system liquid rubber;Preferably, described Liquid rubber is a kind of or several in liquid nitrile rubber, liquid styrene butadiene rubber, liquid butyl rubber, LSR type liquid silastic Kind.The magnetic fillers are selected from one or more of nickel coated graphite powder, nickel packet carbon fiber, flake iron powder.The present invention passes through upper The mutual cooperation for stating specific several components further improves the damping isolation performance of vibration isolator.
3) present invention provides a kind of preparation method of vibration isolator described above, includes the following steps: 1) in impressed pressure Under the action of externally-applied magnetic field, the mixture of liquid rubber and magnetic fillers is subjected to preforming processing, obtains preforming rubber; 2) the preforming rubber for obtaining step 1) carries out sulfidization molding processing, obtains the vibration isolator.The present invention passes through in liquid rubber Magnetic fillers are added in glue, is acted on by externally-applied magnetic field and adjusts magnetic fillers microstructure, makes its orientation arrangement, is formed on microcosmic " damping-constraining " structure, to substantially increase the damping isolation performance of vibration isolator.This method is easy to operate, for vibration isolator The promotion of damping isolation performance work well.
4) present invention provides a kind of preparation method of vibration isolator described above, and further, the externally-applied magnetic field is flat Row magnetic field, the magnetic induction intensity of the externally-applied magnetic field are 0.1-1.0 tesla, and the pressure is 3-8 megapascal, the liquid rubber It is 5-20 minutes with the time of the mixtures of magnetic fillers in the externally-applied magnetic field.The present invention is in above-mentioned magnetic induction intensity, pressure Power and under conditions of the time, further increases the promotion effect of the damping isolation performance of vibration isolator.
Detailed description of the invention
It, below will be to specific in order to illustrate more clearly of the specific embodiment of the invention or technical solution in the prior art Embodiment or attached drawing needed to be used in the description of the prior art be briefly described, it should be apparent that, it is described below Attached drawing is some embodiments of the present invention, for those of ordinary skill in the art, before not making the creative labor It puts, is also possible to obtain other drawings based on these drawings.
Fig. 1 is the schematic diagram for the vibration isolator that the embodiment of the present invention 1 obtains;
Fig. 2 is the stereoscan photograph for the vibration isolator that the embodiment of the present invention 1 obtains;
Fig. 3 is the stereoscan photograph for the vibration isolator that the embodiment of the present invention 2 obtains;
Fig. 4 is the stereoscan photograph for the vibration isolator that the embodiment of the present invention 3 obtains.
Appended drawing reference in Fig. 1: 1, rubber material;2, magnetic fillers;3, constrained damping structure.
Specific embodiment
There is provided following embodiments is to preferably further understand the present invention, it is not limited to the best embodiment party Formula is not construed as limiting the contents of the present invention and protection scope, anyone under the inspiration of the present invention or by the present invention and its The feature of his prior art is combined and any and identical or similar product of the present invention for obtaining, all falls within of the invention Within protection scope.
Specific experiment step or condition person are not specified in embodiment, according to the literature in the art described routine experiment The operation of step or condition can carry out.Reagents or instruments used without specified manufacturer, being can be by commercially available acquisition Conventional reagent product.
Liquid nitrile rubber -40 described in following embodiment of the present invention is purchased from Shanghai low coverage International Trading Company Ltd, institute Liquid nitrile rubber -26 is stated purchased from Nanjing Jia Rui Chemical trade Co., Ltd;The liquid styrene butadiene rubber SN-307R is purchased from Foshan Shi Cheng New Energy Technology Co., Ltd.;The liquid butyl rubber model SH-1WJ, winning great plastic material purchased from Dongguan City has Limit company;The LSR type liquid silastic model LSR-9650A/B is purchased from Guangdong Chao Te new material Co., Ltd.
Embodiment 1
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel coated graphite powder filler, sulphur and hexa are added in liquid nitrile rubber -40, are sufficiently stirred Uniformly, it is then placed in the bubble extracted out in liquid nitrile rubber in vacuum tank, obtains nickel coated graphite powder filler, sulphur, six methylenes The mixture of urotropine and liquid nitrile rubber -40;
(2) mixture of nickel coated graphite powder filler, sulphur, hexa and liquid nitrile rubber -40 is poured into poly- In the mold of tetrafluoroethene preparation, the pressure of 5 megapascal is kept in mold, it is 0.1 tesla that mold, which is put into magnetic induction intensity, 10min is kept in parallel magnetic field environment, is carried out pre-molding processing, is made filler segregation in magnetic field, obtain preforming rubber;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in vulcanizing press together with mold, 150 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment is unloaded Mould inner pressure is removed, the vibration isolator can be obtained.
Fig. 1 is the schematic diagram for the vibration isolator that the present embodiment obtains, as shown in Figure 1, in the obtained vibration isolator of the present embodiment, The magnetic fillers form constrained damping structure as shown in the figure in rubber material, substantially increase the damping isolation of vibration isolator Performance.
Embodiment 2
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber filler, sulphur and hexa are added in liquid nitrile rubber -26, are sufficiently stirred Uniformly, it is then placed in the bubble extracted out in liquid nitrile rubber in vacuum tank, obtains nickel packet carbon fiber filler, sulphur, six methylenes The mixture of urotropine and liquid nitrile rubber -26;
(2) mixture of nickel packet carbon fiber filler, sulphur, hexa and liquid nitrile rubber -26 is poured into poly- In the mold of tetrafluoroethene preparation, the pressure of 5 megapascal is kept in mold, it is 0.3 tesla that mold, which is put into magnetic induction intensity, 10min is kept in parallel magnetic field environment, is carried out pre-molding processing, is made filler segregation in magnetic field, obtain preforming rubber;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in vulcanizing press together with mold, 160 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment is unloaded Mould inner pressure is removed, the vibration isolator can be obtained.
Embodiment 3
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber filler, sulphur and hexa are added in liquid styrene butadiene rubber SN-307R, sufficiently It stirs evenly, is then placed in the bubble extracted out in liquid styrene butadiene rubber in vacuum tank, obtains nickel packet carbon fiber filler, sulphur, six The mixture of methenamine and liquid styrene butadiene rubber SN-307R;
(2) mixture of nickel packet carbon fiber filler, sulphur, hexa and liquid styrene butadiene rubber SN-307R are fallen In the mold for entering polytetrafluoroethylene (PTFE) preparation, the pressure of 5 megapascal is kept in mold, by mold be put into magnetic induction intensity be 0.8 it is special this 10min is kept in the parallel magnetic field environment of drawing, is carried out pre-molding processing, is made filler segregation in magnetic field, obtain preforming rubber Glue;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in vulcanizing press together with mold, 165 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment is unloaded Mould inner pressure is removed, the vibration isolator can be obtained.
Embodiment 4
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) flake iron powder filler, sulphur and ethylene thiourea are added in liquid butyl rubber, are stirred, so It is put into the bubble extracted out in liquid butyl rubber in vacuum tank afterwards, obtains flake iron powder filler, sulphur, ethylene thiourea and liquid The mixture of butyl rubber;
(2) mixture of flake iron powder filler, sulphur, ethylene thiourea and liquid butyl rubber is poured into polytetrafluoroethylene (PTFE) In the mold of preparation, the pressure of 8 megapascal is kept in mold, and mold is put into the parallel magnetic field that magnetic induction intensity is 1.0 teslas 5min is kept in environment, is carried out pre-molding processing, is made filler segregation in magnetic field, obtain preforming rubber;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in vulcanizing press together with mold, 170 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment is unloaded Mould inner pressure is removed, the vibration isolator can be obtained.
Embodiment 5
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber, sulphur and ethylene thiourea are added in liquid styrene butadiene rubber SN-307R, are sufficiently stirred It is even, it is then placed in the bubble extracted out in liquid styrene butadiene rubber SN-307R in vacuum tank, obtains nickel packet carbon fiber, sulphur, ethylidene The mixture of thiocarbamide and liquid styrene butadiene rubber SN-307R;
(2) mixture of nickel packet carbon fiber, sulphur, ethylene thiourea and liquid styrene butadiene rubber SN-307R are poured into poly- four In the mold of vinyl fluoride preparation, the pressure of 3 megapascal is kept in mold, it is the flat of 0.5 tesla that mold, which is put into magnetic induction intensity, 20min is kept in row magnetic field environment, is carried out pre-molding processing, is made filler segregation in magnetic field, obtain preforming rubber;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in vulcanizing press together with mold, 173 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment is unloaded Mould inner pressure is removed, the vibration isolator can be obtained.
Embodiment 6
Present embodiments provide a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber, sulphur and ethylene thiourea are added in LSR type liquid silastic, are stirred, so It is put into the bubble extracted out in LSR type liquid silastic in vacuum tank afterwards, obtains nickel packet carbon fiber, sulphur, ethylene thiourea and LSR The mixture of type liquid silastic;
(2) mixture of nickel packet carbon fiber, sulphur, ethylene thiourea and LSR type liquid silastic is poured into polytetrafluoroethyl-ne In the mold of alkene preparation, the pressure of 6 megapascal is kept in mold, and mold is put into the parallel magnetic that magnetic induction intensity is 0.2 tesla 12min is kept in the environment of field, pre-molding processing is carried out, makes filler segregation in magnetic field, obtain preforming rubber;
(3) the preforming rubber that step (2) obtains is put into progress sulfidization molding processing in baking oven, vulcanization temperature together with mold 169 DEG C of degree, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and sulfidization molding after treatment sheds mold The vibration isolator can be obtained in interior pressure.
Comparative example 1
This comparative example provides a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel coated graphite powder filler, sulphur and hexa are added in liquid nitrile rubber -40, are sufficiently stirred Uniformly, it is then placed in the bubble extracted out in liquid nitrile rubber in vacuum tank, obtains nickel coated graphite powder filler, sulphur, six methylenes The mixture of urotropine and liquid nitrile rubber -40;
(2) mixture of nickel coated graphite powder filler, sulphur, hexa and liquid nitrile rubber -40 is poured into poly- In the mold of tetrafluoroethene preparation, the pressure of 5 megapascal is kept in mold, mold is put into vulcanizing press and carries out sulfidization molding Processing, 150 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and processing terminate for sulfidization molding Afterwards, mould inner pressure is shed, the vibration isolator can be obtained.
Comparative example 2
This comparative example provides a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber filler, sulphur and hexa are added in liquid nitrile rubber -26, are sufficiently stirred Uniformly, it is then placed in the bubble extracted out in liquid nitrile rubber in vacuum tank, obtains nickel packet carbon fiber filler, sulphur, six methylenes The mixture of urotropine and liquid nitrile rubber -26;
(2) mixture of nickel packet carbon fiber filler, sulphur, hexa and liquid nitrile rubber -26 is poured into poly- In the mold of tetrafluoroethene preparation, the pressure of 5 megapascal is kept in mold, mold is put into vulcanizing press and carries out sulfidization molding Processing, 160 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, and processing terminate for sulfidization molding Afterwards, mould inner pressure is shed, the vibration isolator can be obtained.
Comparative example 3
This comparative example provides a kind of vibration isolator, including the following raw material:
The preparation method of vibration isolator described above, includes the following steps:
(1) nickel packet carbon fiber filler, sulphur and hexa are added in liquid styrene butadiene rubber SN-307R, sufficiently It stirs evenly, is then placed in the bubble extracted out in liquid styrene butadiene rubber in vacuum tank, obtains nickel packet carbon fiber filler, sulphur, six The mixture of methenamine and liquid styrene butadiene rubber SN-307R;
(2) mixture of nickel packet carbon fiber filler, sulphur, hexa and liquid styrene butadiene rubber SN-307R are fallen In the mold for entering polytetrafluoroethylene (PTFE) preparation, the pressure of 5 megapascal is kept in mold, mold is put into vulcanizing press and is vulcanized Forming processes, 165 DEG C of curing temperature, vulcanization time is the technique sulfurizing time t90 determined by vulcameter, sulfidization molding processing After, mould inner pressure is shed, the vibration isolator can be obtained.
Performance test
It is tested for the property to by embodiment 1-6 and the preparation-obtained vibration isolator of comparative example 1-3, as a result such as 1 institute of table Show.
The preparation-obtained vibration isolator performance of table 1 embodiment 1-6 and comparative example 1-3
Damping ratio Vibration isolation efficiency (%)
Embodiment 1 0.93 96.4
Embodiment 2 0.89 95.7
Embodiment 3 0.91 94.7
Embodiment 4 0.88 95.1
Embodiment 5 0.90 95.9
Embodiment 6 0.92 96.2
Comparative example 1 0.85 87.3
Comparative example 2 0.81 84.5
Comparative example 3 0.83 85.8
Obviously, the above embodiments are merely examples for clarifying the description, and does not limit the embodiments.It is right For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of variation or It changes.There is no necessity and possibility to exhaust all the enbodiments.And it is extended from this it is obvious variation or It changes still within the protection scope of the invention.

Claims (10)

1. a kind of vibration isolator, which is characterized in that the raw material including following parts by weight: 100 parts of liquid rubber and magnetic fillers 5-20 Part.
2. vibration isolator according to claim 1, which is characterized in that the magnetic fillers are 10-15 parts.
3. vibration isolator according to claim 1 or 2, which is characterized in that the liquid rubber be selected from diene series liquid rubber, One or more of olefin-based liquid rubber, polyurethane series liquid rubber, silicon systems liquid rubber, fluorine system liquid rubber;
Preferably, the liquid rubber is selected from liquid nitrile rubber, liquid styrene butadiene rubber, liquid butyl rubber, LSR type liquid silicon One or more of rubber.
4. vibration isolator according to claim 1-3, which is characterized in that the magnetic fillers are one-dimensional linear or two Tie up sheet magnetic fillers.
5. vibration isolator according to claim 4, which is characterized in that the magnetic fillers are selected from nickel coated graphite powder, nickel packet carbon One or more of fiber, flake iron powder.
6. vibration isolator according to claim 1, which is characterized in that the raw material further includes rubber chemicals.
7. a kind of preparation method of vibration isolator described in any one of claims 1-6, which comprises the steps of:
1) under the action of impressed pressure and externally-applied magnetic field, the mixture of liquid rubber and magnetic fillers is subjected to preforming place Reason, obtains preforming rubber;
2) the preforming rubber for obtaining step 1) carries out sulfidization molding processing, obtains the vibration isolator.
8. preparation method according to claim 7, which is characterized in that the externally-applied magnetic field is parallel magnetic field, described additional The magnetic induction intensity in magnetic field is 0.1-1.0 tesla, and the impressed pressure is 3-8 megapascal, the liquid rubber and magnetic fillers Time of the mixture in the externally-applied magnetic field be 5-20 minutes.
9. preparation method according to claim 7 or 8, which is characterized in that further include being filled out to the liquid rubber and magnetism The step of rubber chemicals are added in the mixture of material.
10. preparation method according to claim 9, which is characterized in that the preforming processing step are as follows: by liquid rubber The mixture of glue, magnetic fillers and rubber chemicals is placed in mold, then precompressed under the action of impressed pressure and externally-applied magnetic field Molding.
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