CN110286067A - A kind of method of Equivalent boundary layer thickness in quantitatively characterizing porous media - Google Patents

A kind of method of Equivalent boundary layer thickness in quantitatively characterizing porous media Download PDF

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CN110286067A
CN110286067A CN201910600220.0A CN201910600220A CN110286067A CN 110286067 A CN110286067 A CN 110286067A CN 201910600220 A CN201910600220 A CN 201910600220A CN 110286067 A CN110286067 A CN 110286067A
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boundary layer
layer thickness
water
pore throat
porous media
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CN110286067B (en
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郑自刚
李兆国
张永强
熊维亮
杨金龙
张庆洲
周晋
曾山
张晓斌
袁颖婕
赵向宏
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China Petroleum and Natural Gas Co Ltd
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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    • G01N13/04Investigating osmotic effects
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/088Investigating volume, surface area, size or distribution of pores; Porosimetry

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Abstract

The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps: step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and porosity calculation theory pore throat radius and flowing pore throat radius, wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream move pore throat radius, water boundary layer thickness and oily boundary layer thickness are calculated by theoretical pore throat radius and flowing pore throat radius, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by theoretical pore throat radius and flowing pore throat radius;Step 3) judges influence of the porous media inner boundary layer to be measured to seepage flow according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness.

Description

A kind of method of Equivalent boundary layer thickness in quantitatively characterizing porous media
Technical field
The invention belongs to reservoir physics core analysis technical fields, and in particular to equivalent in a kind of quantitatively characterizing porous media The method of boundary layer thickness.
Background technique
The pore radius for being mainly characterized by fluid flowing of low-permeability oil deposit is small, and flow resistance is big, solid liquid interface and liquid liquid Interaction between interface is affected to seepage flow, causes its percolation law to deviate classical Darcy linear seepage flow, belongs to non- Darcy flow.The feature of non linear fluid flow through porous medium is mainly characterized with starting pressure gradient at present, but to causing starting pressure gradient The reason of --- boundary layer research is less.Boundary layer is intermolecular in interface interaction and boundary layer due to solid and liquid Interaction, blowhole inner surface there are a motionless layer, boundary layer thickness is bigger, more unfavorable to the flowing of fluid. For high permeable cement, the thickness in boundary layer is smaller compared with pore throat radius, and the influence to seepage flow is little;But for low For infiltration, extra-low permeability oil reservoirs, boundary layer thickness be can not ignore.
Boundary layer quantitative measuring method includes micro- round tube method and check weighing method at present.Wherein, micro- round tube test usually utilizes one The annular microchamber of a known internal diameter carries out flowing experiment, according to the practical radius flowed of poiseuille theoretical calculation fluid, with true The difference of internal diameter and flow radius calculates boundary layer thickness, but since rock porous media is not isodiametric round tube, but one The various sizes of pore throat composition of series, so, this method is not suitable with the measurement of porous media inner boundary layer thickness.Weight method is pair Weight than rock core before and after water drive is calculated, and not only error is big for this method, and due to the remaining oil type multiplicity after water drive, and The non-inner surface for being present in porous media in the form of single oil film causes method to lack certain science, while this method It cannot achieve the boundary layer quantitatively characterizing of different fluid.
Summary of the invention
It is an object of the invention to overcome above-mentioned the deficiencies in the prior art, provide equivalent in a kind of quantitatively characterizing porous media The method of boundary layer thickness overcomes in the prior art 1: micro- round tube test is usually opened using the annular microchamber of a known internal diameter Flowing experiment is opened up, according to the practical radius flowed of poiseuille theoretical calculation fluid, in terms of the difference of true internal diameter and flow radius Boundary layer thickness is calculated, but since rock porous media is not isodiametric round tube, but a series of various sizes of pore throat compositions, So this method is not suitable with the measurement of porous media inner boundary layer thickness;2: weight method is the weight of rock core before and after comparing water drive It is calculated, not only error is big for this method, and due to the remaining oil type multiplicity after water drive, is not deposited in the form of single oil film It is the inner surface of porous media, causes method to lack certain science, while this method cannot achieve the side of different fluid Interlayer quantitatively characterizing;3: being unable to characterize porous media inner boundary layer thickness and different types of fluid in the prior art in porous Jie The characterization of boundary layer thickness in matter, at the same the prior art measurement porous media in Equivalent boundary layer thickness efficiency it is lower, accidentally The problems such as difference is larger.
In order to solve technical problem, the technical scheme is that Equivalent Boundary thickness in a kind of quantitatively characterizing porous media The method of degree, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Preferably, theoretical pore throat radius is calculated by gas permeability in the step 2), wherein flowing pore throat radius Permeability is surveyed by water or oil is surveyed computing permeability and obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius With the difference of flowing pore throat radius, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness Or the ratio of oily boundary layer thickness and theoretical pore throat radius.
Preferably, theoretical pore throat radius, flowing pore throat radius, water boundary layer thickness and oily boundary thickness in the step 2) The calculation formula of degree are as follows:
Theoretical pore throat radius isFlowing pore throat radius isOr
Wherein:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
hw- water boundary layer thickness, um;
Ho-oil boundary layer thickness, um;
φ-porous media porosity, %.
Preferably, in the step 2) zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness calculation formula Are as follows:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
φ-porous media porosity, %;
εwThe reasonable ratio by pore throat radius of-zero dimension water boundary layer thickness, i.e. water boundary layer thickness, %;
ε0- zero dimension oil boundary layer thickness, the i.e. reasonable ratio by pore throat radius of oily boundary layer thickness, %.
Preferably, when zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are less than 30% in the step 3) When, porous media inner boundary layer to be measured is rudimentary to the influence degree of seepage flow;When zero dimension water boundary layer thickness or zero dimension oil Boundary layer thickness be 30%~60% when, porous media inner boundary layer to be measured to the influence degree of seepage flow be in it is rudimentary;When it is no because When secondary water boundary layer thickness or zero dimension oil boundary layer thickness are 60%~80%, porous media inner boundary layer to be measured is to seepage flow Influence degree is middle-and-high-ranking;It is to be measured porous when zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are greater than 80% Medium inner boundary layer is advanced to the influence degree of seepage flow.
Compared with the existing technology, the present invention has the advantages that
(1) present invention is to propose a kind of survey with rock core porous media gas on the basis of analyzing Liquid Flow difference and seep The difference that the theoretical pore throat radius that saturating rate calculates surveys the flowing pore throat radius that permeability (water phase and oily phase) calculates with liquid quantifies table The method for levying Equivalent boundary layer thickness in rock core porous media, and according to boundary layer thickness accounting size (the i.e. zero dimension of calculating Water boundary layer thickness or zero dimension oil boundary layer thickness) boundary layer quickly judges seepage effect degree, work as zero dimension When water boundary layer thickness or zero dimension oil boundary layer thickness are less than 30%, influence journey of the porous media inner boundary layer to be measured to seepage flow Degree is rudimentary;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are 30%~60%, porous media to be measured Inner boundary layer to the influence degree of seepage flow be in it is rudimentary;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are When 60%~80%, porous media inner boundary layer to be measured is middle-and-high-ranking to the influence degree of seepage flow;When zero dimension water boundaries thickness When degree or zero dimension oil boundary layer thickness are greater than 80%, porous media inner boundary layer to be measured is advanced to the influence degree of seepage flow;
(2) present invention can Equivalent boundary layer thickness and its accounting in quantitatively characterizing porous media, while can also quantitatively characterizing The boundary layer thickness and its accounting of different types of fluid can be used for evaluating different permeabilities, different physical property fluids, different wetting With the Equivalent boundary layer thickness under different pressures;
(3) for the present invention due to the Basic Physical Properties parameter that calculating parameter is rock core porous media, calculating process is simple, can be pair Difference than studying different type flow through oil reservoir rule provides foundation, while being easy to carry out boundary layer to the fast of seepage effect degree Speed judgement, and judge that accurately efficiency is higher, and error is smaller.
Specific embodiment
The specific embodiment of the invention is described below with reference to embodiment:
It should be noted that structure, ratio, the size etc. of this specification signal, only to cooperate disclosed in specification Content, for those skilled in the art understand and read, be not intended to limit the invention enforceable qualifications, it is any The modification of structure, the change of proportionate relationship or the adjustment of size are not influencing the effect of present invention can be generated and can reach Purpose under, should all still fall in the range of disclosed technology contents can cover.
Meanwhile cited such as "upper" in this specification, "lower", "left", "right", " centre " and " one " term, also Only being illustrated convenient for narration, rather than to limit the scope of the invention, relativeness is altered or modified, in nothing Under essence change technology contents, when being also considered as the enforceable scope of the present invention.
" two-phase fluid is opposite in rock permeates by SY/T5336 " core analysis method " of the present invention, SY/T5345-2007 Rate test method " it is the prior art.
Embodiment 1
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Embodiment 2
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Embodiment 3
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Preferably, theoretical pore throat radius is calculated by gas permeability in the step 2), wherein flowing pore throat radius Permeability is surveyed by water or oil is surveyed computing permeability and obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius With the difference of flowing pore throat radius, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness Or the ratio of oily boundary layer thickness and theoretical pore throat radius.
Embodiment 4
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Preferably, theoretical pore throat radius is calculated by gas permeability in the step 2), wherein flowing pore throat radius Permeability is surveyed by water or oil is surveyed computing permeability and obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius With the difference of flowing pore throat radius, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness Or the ratio of oily boundary layer thickness and theoretical pore throat radius.
Preferably, theoretical pore throat radius, flowing pore throat radius, water boundary layer thickness and oily boundary thickness in the step 2) The calculation formula of degree are as follows:
Theoretical pore throat radius isFlowing pore throat radius isOr
Wherein:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
hw- water boundary layer thickness, um;
ho- oil boundary layer thickness, um;
φ-porous media porosity, %.
Embodiment 5
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Preferably, theoretical pore throat radius is calculated by gas permeability in the step 2), wherein flowing pore throat radius Permeability is surveyed by water or oil is surveyed computing permeability and obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius With the difference of flowing pore throat radius, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness Or the ratio of oily boundary layer thickness and theoretical pore throat radius.
Preferably, theoretical pore throat radius, flowing pore throat radius, water boundary layer thickness and oily boundary thickness in the step 2) The calculation formula of degree are as follows:
Theoretical pore throat radius isFlowing pore throat radius isOr
Wherein:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
hw- water boundary layer thickness, um;
ho- oil boundary layer thickness, um;
φ-porous media porosity, %.
Preferably, in the step 2) zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness calculation formula Are as follows:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
φ-porous media porosity, %;
εwThe reasonable ratio by pore throat radius of-zero dimension water boundary layer thickness, i.e. water boundary layer thickness, %;
ε0- zero dimension oil boundary layer thickness, the i.e. reasonable ratio by pore throat radius of oily boundary layer thickness, %.
Embodiment 6
The invention discloses a kind of methods of Equivalent boundary layer thickness in quantitatively characterizing porous media, comprising the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and hole Porosity calculates theoretical pore throat radius and flowing pore throat radius, and wherein flowing pore throat radius includes that water flowing pore throat radius and oil stream are dynamic Pore throat radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through reason Zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are calculated by pore throat radius and flowing pore throat radius;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness Influence of the porous media inner boundary layer to be measured to seepage flow is judged with zero dimension oil boundary layer thickness, wherein water boundary layer thickness, oil Boundary layer thickness, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
Preferably, gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
Preferably, water surveys permeability in the step 1) and oil surveys permeability and passes through SY/T5345-2007 " two-phase in rock Fluid relative permeability test method " measurement.
Preferably, theoretical pore throat radius is calculated by gas permeability in the step 2), wherein flowing pore throat radius Permeability is surveyed by water or oil is surveyed computing permeability and obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius With the difference of flowing pore throat radius, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness Or the ratio of oily boundary layer thickness and theoretical pore throat radius.
Preferably, theoretical pore throat radius, flowing pore throat radius, water boundary layer thickness and oily boundary thickness in the step 2) The calculation formula of degree are as follows:
Theoretical pore throat radius isFlowing pore throat radius isOr
Wherein:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
hw- water boundary layer thickness, um;
ho- oil boundary layer thickness, um;
φ-porous media porosity, %.
Preferably, in the step 2) zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness calculation formula Are as follows:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
φ-porous media porosity, %;
εwThe reasonable ratio by pore throat radius of-zero dimension water boundary layer thickness, i.e. water boundary layer thickness, %;
ε0- zero dimension oil boundary layer thickness, the i.e. reasonable ratio by pore throat radius of oily boundary layer thickness, %.
Preferably, when zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are less than 30% in the step 3) When, porous media inner boundary layer to be measured is rudimentary to the influence degree of seepage flow;When zero dimension water boundary layer thickness or zero dimension oil Boundary layer thickness be 30%~60% when, porous media inner boundary layer to be measured to the influence degree of seepage flow be in it is rudimentary;When it is no because When secondary water boundary layer thickness or zero dimension oil boundary layer thickness are 60%~80%, porous media inner boundary layer to be measured is to seepage flow Influence degree is middle-and-high-ranking;It is to be measured porous when zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are greater than 80% Medium inner boundary layer is advanced to the influence degree of seepage flow.
Embodiment 7
Fine and close oil rock heart porous media is selected, wherein core diameter 2.508cm, length 4.309cm, porosity 10.8%, Gas permeability is 0.143mD, and it is 0.0051mD that water, which surveys permeability, and oil is surveyed permeability 0.0014mD, calculated according to the method described above, Obtaining theoretical pore throat radius is 0.1029 μm, and it is 0.01943 μm that water flow measurement, which moves pore throat radius, and water boundary layer is with a thickness of 0.08348 μ M, zero dimension water boundary layer is with a thickness of 81.11%;It is 0.01018 μm that oily flow measurement, which moves pore throat radius, and oily bound thickness is 0.09273 μm, zero dimension oil boundary layer thickness is 90.11%, and the influence according to porous media inner boundary layer to seepage flow obtains fine and close oil rock Heart porous media water boundary layer thickness and oily boundary layer thickness are advanced, water boundary layer thickness and oil to the influence degree of seepage flow Boundary layer thickness is high to seepage effect degree.
Embodiment 8
Ultra-low penetration rock core porous media is selected, wherein core diameter 2.492cm, length 5.210cm, porosity 13.67%, gas permeability 0.5705mD, it is 0.1347mD that water, which surveys permeability, and oil surveys permeability 0.1056mD, according to above-mentioned Method calculates, and obtaining theoretical pore throat radius is 0.1827 μm, and it is 0.08875 μm that water flow measurement, which moves pore throat radius, water boundary layer thickness It is 0.09397 μm, zero dimension water boundary layer is with a thickness of 51.43%;It is 0.0786 μm that oily flow measurement, which moves pore throat radius, oily bound thickness It is 0.1041 μm, zero dimension oil boundary layer thickness is 56.98%, and the influence according to porous media inner boundary layer to seepage flow obtains Ultra-low penetration rock core water boundary layer thickness and oily boundary layer thickness are middle-and-high-ranking, water boundary layer thickness to the influence degree of seepage flow It is higher to seepage effect with oily boundary layer thickness.
Embodiment 9
Flow in low permeability core porous media is selected, wherein core diameter 2.49cm, length 8.89cm, porosity 13.6%, gas Survey permeability is 29.49mD, and it is 11.51mD that water, which surveys permeability, and oil surveys permeability 9.46mD, calculates, obtain according to the method described above Theoretical pore throat radius be 1.3170 μm, water flow measurement move pore throat radius be 0.8228 μm, water boundary layer with a thickness of 0.4992 μm, it is no because Secondary water boundary layer is with a thickness of 37.53%;It is 0.746 μm that oily flow measurement, which moves pore throat radius, and oily bound thickness is 0.571 μm, zero dimension Oily boundary layer thickness is 43.36%, and the influence according to porous media inner boundary layer to seepage flow obtains flow in low permeability core water boundary layer Thickness and oily boundary layer thickness to the influence degree of seepage flow be in it is rudimentary, water boundary layer thickness and oily boundary layer thickness are to seepage flow Slightly influence.
Embodiment 10
Medium to high permeable rock core porous media is selected, wherein core diameter 2.502cm, length 5.76cm, porosity 14.9%, Gas permeability is 209.5mD, and it is 118.73mD that water, which surveys permeability, and oil is surveyed permeability 90.98mD, calculated according to the method described above, Obtain theoretical pore throat radius be 3.3538 μm, water flow measurement move pore throat radius be 2.5249 μm, water boundary layer with a thickness of 0.8289 μm, Zero dimension water boundary layer is with a thickness of 24.72%;It is 2.4078 μm that oily flow measurement, which moves pore throat radius, and oily bound thickness is 0.9460 μm, Zero dimension oil boundary layer thickness is 28.21%, and the influence according to porous media inner boundary layer to seepage flow obtains medium to high permeable rock core Water boundary layer thickness and oily boundary layer thickness are rudimentary, water boundary layer thickness and oily boundary layer thickness to the influence degree of seepage flow It is negligible to seepage effect.
From embodiment 7~10 as can be seen that influence of the Equivalent boundary layer thickness to seepage flow in different rock core porous medias Difference, ultra-low penetration rock core water boundary layer thickness and oily boundary layer thickness be to the influence degree of seepage flow it is middle-and-high-ranking, to seepage flow Influence degree is high;Ultra-low penetration rock core water boundary layer thickness and oily boundary layer thickness be to the influence degree of seepage flow it is middle-and-high-ranking, It is higher to seepage effect;Flow in low permeability core water boundary layer thickness and oily boundary layer thickness to the influence degree of seepage flow be in it is low Grade slightly influences seepage flow;Medium to high permeable rock core water boundary layer thickness and oily boundary layer thickness are to the influence degree of seepage flow It is rudimentary, it is negligible to seepage effect.
The principle of the present invention is as follows:
The present invention is to propose one kind on the basis of analyzing Liquid Flow difference with rock core porous media gas permeability The theoretical pore throat radius of calculating surveys the difference quantitatively characterizing rock for the flowing pore throat radius that permeability (water phase and oily phase) calculates with liquid The method of Equivalent boundary layer thickness in heart porous media, and according to boundary layer thickness accounting size (the i.e. zero dimension waterside of calculating Thickness of boundary layer or zero dimension oil boundary layer thickness) boundary layer quickly judges seepage effect degree, when zero dimension waterside When thickness of boundary layer or zero dimension oil boundary layer thickness are less than 30%, porous media inner boundary layer to be measured is to the influence degree of seepage flow It is rudimentary;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are 30%~60%, porous media inner edge to be measured Interlayer to the influence degree of seepage flow be in it is rudimentary;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness be 60%~ When 80%, porous media inner boundary layer to be measured is middle-and-high-ranking to the influence degree of seepage flow;When zero dimension water boundary layer thickness or nothing When dimension oil boundary layer thickness is greater than 80%, porous media inner boundary layer to be measured is advanced to the influence degree of seepage flow.
The present invention can Equivalent boundary layer thickness and its accounting in quantitatively characterizing porous media, while can also quantitatively characterizing it is different The boundary layer thickness and its accounting of type of fluid can be used for evaluating different permeabilities, different physical property fluid, different wetting and not With the Equivalent boundary layer thickness under pressure.
For the present invention due to the Basic Physical Properties parameter that calculating parameter is rock core porous media, calculating process is simple, can be comparison The difference for studying different type flow through oil reservoir rule provides foundation, while being easy to carry out boundary layer to the quick of seepage effect degree Judgement, and judge that accurately efficiency is higher, and error is smaller.
The preferred embodiment for the present invention is explained in detail above, but the present invention is not limited to the above embodiments, Those of ordinary skill in the art within the scope of knowledge, can also make various without departing from the purpose of the present invention Variation.
Many other changes and remodeling can be made by not departing from the spirit and scope of the present invention.It should be appreciated that the present invention is not It is limited to specific embodiment, the scope of the present invention is defined by the following claims.The component that the present embodiment does not describe in detail With the well-known components and common structure or conventional means of the structure category industry, do not describe one by one here.

Claims (7)

1. a kind of method of Equivalent boundary layer thickness in quantitatively characterizing porous media, which comprises the following steps:
Step 1) measures the gas permeability of porous media to be measured, water surveys permeability, oil surveys permeability and porosity;
The gas permeability for the porous media that step 2) is measured by step 1), water survey permeability, oil surveys permeability and porosity Theoretical pore throat radius and flowing pore throat radius are calculated, wherein flowing pore throat radius includes water flowing pore throat radius and oily flowing pore throat Radius calculates water boundary layer thickness and oily boundary layer thickness by theoretical pore throat radius and flowing pore throat radius, passes through theoretical hole Larynx radius and flowing pore throat radius calculate zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness;
Step 3) is according to the water boundary layer thickness calculated in step 2), oily boundary layer thickness, zero dimension water boundary layer thickness and nothing Dimension oil boundary layer thickness judges influence of the porous media inner boundary layer to be measured to seepage flow, wherein water boundary layer thickness, oily boundary Thickness degree, zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are directly proportional to the influence to seepage flow.
2. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 1 In gas permeability and porosity are measured by SY/T5336 " core analysis method " in the step 1).
3. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 1 In " two-phase fluid permeates relatively in rock by SY/T5345-2007 for water survey permeability and oil survey permeability in the step 1) Rate test method " measurement.
4. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 1 In theoretical pore throat radius is calculated by gas permeability in the step 2), and wherein flowing pore throat radius surveys permeability by water Or oil is surveyed computing permeability and is obtained, wherein water boundary layer thickness and oily boundary layer thickness are theoretical pore throat radius and flowing pore throat half The difference of diameter, wherein zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness are water boundary layer thickness or oily boundary thickness The ratio of degree and theoretical pore throat radius.
5. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 4 In the calculation formula of theoretical pore throat radius, flowing pore throat radius, water boundary layer thickness and oily boundary layer thickness in the step 2) Are as follows:
Theoretical pore throat radius isFlowing pore throat radius isOr
Wherein:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
hw- water boundary layer thickness, um;
ho- oil boundary layer thickness, um;
φ-porous media porosity, %.
6. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 4 In the calculation formula of zero dimension water boundary layer thickness and zero dimension oil boundary layer thickness in the step 2) are as follows:
Kg-porous media gas permeability, mD;
Kw-porous media water surveys permeability, mD;
Ko-porous media oil surveys permeability, mD;
φ-porous media porosity, %;
εwThe reasonable ratio by pore throat radius of-zero dimension water boundary layer thickness, i.e. water boundary layer thickness, %;
ε0- zero dimension oil boundary layer thickness, the i.e. reasonable ratio by pore throat radius of oily boundary layer thickness, %.
7. the method for Equivalent boundary layer thickness, feature exist in a kind of quantitatively characterizing porous media according to claim 1 In: in the step 3) when zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are less than 30%, porous Jie to be measured Matter inner boundary layer is rudimentary to the influence degree of seepage flow;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are When 30%~60%, porous media inner boundary layer to be measured to the influence degree of seepage flow be in it is rudimentary;When zero dimension water boundaries thickness When degree or zero dimension oil boundary layer thickness are 60%~80%, during porous media inner boundary layer to be measured is to the influence degree of seepage flow It is advanced;When zero dimension water boundary layer thickness or zero dimension oil boundary layer thickness are greater than 80%, porous media inner boundary layer to be measured Influence degree to seepage flow is advanced.
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