CN110277212A - A kind of preparation method of high magnetic conductivity cream - Google Patents
A kind of preparation method of high magnetic conductivity cream Download PDFInfo
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- CN110277212A CN110277212A CN201910592473.8A CN201910592473A CN110277212A CN 110277212 A CN110277212 A CN 110277212A CN 201910592473 A CN201910592473 A CN 201910592473A CN 110277212 A CN110277212 A CN 110277212A
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- preparation
- pretreatment material
- magnetic conductivity
- high magnetic
- magnaglo
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
- B22F1/102—Metallic powder coated with organic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/16—Metallic particles coated with a non-metal
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/147—Alloys characterised by their composition
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/20—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
Abstract
The invention discloses a kind of preparation methods of high magnetic conductivity cream, comprising the following steps: Magnaglo one is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;Magnaglo two is handled under an inert gas and obtains pretreatment material two;Pretreatment material one and pretreatment material two are surface-treated respectively;Pretreatment material one after surface treatment is carried out being mixed to get middle material according to mass percent 1:9~4:6 with pretreatment material two;Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;Mixture is mediated, obtains magnetic cream after rolling, the present invention has preferable magnetic conductivity performance.
Description
Technical field
The present invention relates to the technical field of magnetically soft alloy material preparation, the preparation methods of specifically a kind of high magnetic conductivity cream.
Background technique
With the increase of electronic product degree of integration, electronic product has more demands for electric power, and requires power supply system
System has reliable electric current and voltage protection and lower fever in the case where high current.
Alloy soft magnetic material direct current biasing is had excellent performance, but resistivity is low, and eddy-current loss is high under high frequency, fever seriously to
It limits and is used under its high frequency, and the trend of high frequency and high power now with electronic device, to the resistance for promoting material
Rate and the calorific value for reducing material are very crucial.Meanwhile the work that alloy soft magnetic inductance generally uses coil and magnetic powder integrally to suppress
Skill mode is realized, and interiors of products copper wire will appear damage if material surface difference excessive compared with sharp or pressing pressure in pressing process
Hurt phenomenon, the bad phenomenon of short circuit is easily caused in device use process, but the inductance value of hypotony product is unable to reach and makes
With requiring.To overcome the weakness, insulating wrapped need to be carried out to alloy powder surface to promote its resistivity, and by improve at
Type reduces the risk of the pressure reduction copper wire damage during production using the compacting stress of material, promotes the property of product
Energy.
So carrying out insulating wrapped to alloy powder promotes pressure required for the insulation of material and the molding of reduction material
Play a significant role to product development, therefore it is very necessary to develop soft magnetic materials magnetism cream technology.
Application publication number CN102942886 Magneto-conductivitygluewater gluewater and its application, be related to a kind of glue with magnetic conductivity and its
Using can use and can obtain more preferable permeability characteristics and reliable in magnetic core gap bonds more particularly to one kind
The application of the glue of adhesion strength and the glue in magnetic core gap bonds.Comprising chemosetting glue, magnetic-particle and
Optional nano-dispersed additive, wherein the total weight relative to the Magneto-conductivitygluewater gluewater, the loading of magnetic-particle is not less than
50% total weight.The Magneto-conductivitygluewater gluewater of this high filler loading capacity has good magnetic conduction effect, thus for bonding magnetic core seam
When gap, can have the function of increasing magnetic flux effect.The invention passes through in bi-component acrylic ester type structure glue and bi-component ring
The Mn-Zn ferrite magnetic particle of addition weight percent 80% or so in oxygen resin type structure glue, Ni-Zn ferrite particle,
Iron sial powder and FeCuNbSiB powder etc., and point of the magnetic-particle in glue is improved by addition nano-dispersed additive
Effect is dissipated, but homogenous material is extremely difficult to higher magnetic conductivity, the high inside of glue content there are a large amount of air gaps to cause power consumption higher, nothing
Method reaches design requirement.
A kind of magnetic glue of application publication number CN 106590345 includes magnetism for the magnetic glue-line of wire-wound inductor device
The mixture of substrate and bonding substrates, the magnetic base material be NiZn ferrite, MnZn ferrite it is one such or it is a variety of with
The FeNi of metal system, carbonyl iron dust, one or more mixtures mixed in FeSiCr, FeSi.A kind of inductance component, including
Coil windings on magnetic core and magnetic core are coated with the magnetic glue on the magnetic core and cover the coil windings, Gu
The magnetic glue after change forms the magnetic glue-line with the magnetic core tight bond.It is compared with ordinary inductor device, using the magnetic
The mechanical impact resistance of the inductance component of property glue is stronger, and is formed by closed-flux structure and can reduce leakage field, anti-electromagnetism
Interference performance is strong.But the ratio that the materials such as NiZn ferrite, MnZn ferrite, FeNi, FeSiCr add under the system is low, leads
Cause magnetic conductivity relatively low, (such as high temperature and humidity) magnet can generate phenomena such as getting rusty under conditions of slightly harsh, so as to cause
Reducing power consumption rises under the insulation of product.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of high magnetic conductivity cream, to solve to propose in above-mentioned background technique
The problem of.
To achieve the above object, the invention provides the following technical scheme:
A kind of preparation method of high magnetic conductivity cream.The following steps are included:
Magnaglo one is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
Magnaglo two is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment mix according to mass percent 1:9~4:6 with pretreatment material two
To middle material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
As a further solution of the present invention: the Magnaglo one be specially Fe, FeSi, FeSiCr, FeNi, FeSi and
At least one of FeSiAl.
As a further solution of the present invention: the Magnaglo two be specially FeSiCrBC, FeSiAlBNbC and
At least one of FeNiCrAlBC.
As a further solution of the present invention: the partial size of the Magnaglo one and Magnaglo two is 1-70 μm.
As a further solution of the present invention: processing when Magnaglo one to coat to phosphoric acid class glass under cyclone
Temperature is 300 DEG C~500 DEG C.
As a further solution of the present invention: described that pretreatment material one and pretreatment material two are subjected to surface treatment tool respectively
Body is to be carried out by surface treating agent when treatment temperature is 50~90 DEG C processing 30~60 minutes.
As a further solution of the present invention: the surface treating agent be specially silane coupling agent, titanate esters, aluminic acid lipoprotein and
At least one of zirconic acid rouge.
As a further solution of the present invention: the phosphoric acid class glass is specially P2O5-Na2O-ZnO、ZnO-Al2O3-P2O5
And P2O5-Na2One of O-BaO.
As a further solution of the present invention: the curing agent is aliphatic diamine and polyamines, aromatic polyamine, glue are
At least one of epoxy resin, phenolic resin, silicone resin;
The filler is nano silicon oxide.
As a further solution of the present invention: described that mixture is mediated, obtains magnetic cream after rolling specifically:
It obtains mediating material after mixture is mediated in high-speed kneading machine;
Material rod in roller mill will be mediated to roll to obtain magnetic cream.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
Fe is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeNiCrAlBC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 1:9 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 320 DEG C;
FeNiCrAlBC is handled under a nitrogen, 400 DEG C for the treatment of temperature, is handled the time 60 minutes;Surface treating agent selects silane coupling agent;
Curing agent is aliphatic diamine;The filler is nano silicon oxide.
Embodiment 2
FeSi is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeSiAlBNbC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 2:8 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 350 DEG C;
FeSiAlBNbC is handled under a nitrogen, 320 DEG C for the treatment of temperature, is handled the time 120 minutes;Surface treating agent selects titanate esters;Gu
Agent is aliphatic diamine;The filler is nano silicon oxide.
Embodiment 3
FeSiCr is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeSiAlBNbC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 3:7 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 500 DEG C;
FeSiAlBNbC is handled under a nitrogen, 220 DEG C for the treatment of temperature, is handled the time 180 minutes;Surface treating agent selects titanate esters;Gu
Agent is aliphatic diamine;The filler is nano silicon oxide.
Embodiment 4
FeSi is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeNiCrAlBC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 4:6 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 450 DEG C;
FeSiAlBNbC is handled under a nitrogen, 220 DEG C for the treatment of temperature, is handled the time 180 minutes;Surface treating agent selects titanate esters;Gu
Agent is aliphatic diamine;The filler is nano silicon oxide.
Embodiment 5
FeNi is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeSiAlBNbC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 4:6 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 350 DEG C;
FeSiAlBNbC is handled under a nitrogen, 320 DEG C for the treatment of temperature, is handled the time 120 minutes;Surface treating agent selects titanate esters;Gu
Agent is aliphatic diamine;The filler is nano silicon oxide.
Embodiment 6
FeSiAl is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
FeSiCrBC is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
Pretreatment material one after surface treatment is carried out being mixed to get centre according to mass percent 3:7 with pretreatment material two
Material;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
Wherein treatment temperature when Magnaglo one to coat to phosphoric acid class glass under cyclone is 450 DEG C;
FeSiAlBNbC is handled under a nitrogen, 400 DEG C for the treatment of temperature, is handled the time 60 minutes;Surface treating agent selects titanate esters;Solidification
Agent is aliphatic diamine;The filler is nano silicon oxide.
Comparative example 1
Powder is selected to choose MnZn, powder particle 10um, and epoxy resin: phenolic resin=3:1 hybrid resin, filler
For granularity be 1um silica after evenly mixing, mixed magnetic powder: glue mixture weight ratio be 80:20, by high-speed kneading
It rolls to obtain magnetic cream with rod.
Comparative example 2
Powder is selected to choose Fe, powder particle 10um, with epoxy resin: phenolic resin=3:1 hybrid resin, filler are
Granularity be 1um silica after evenly mixing, mixed magnetic powder: glue mixture weight ratio is 85:15, by high-speed kneading and
Rod rolls to obtain magnetic cream.
Comparative example 3
Powder is selected to choose FeSiCr, powder particle 10um, with epoxy resin: phenolic resin=3:1 hybrid resin is filled
Agent be granularity be 1um silica after evenly mixing, mixed magnetic powder: glue mixture weight ratio be 85:15, by pinching at a high speed
It closes and rod rolls to obtain magnetic cream.
Embodiment and comparative example is infused into magnet ring by fixing mould tank, pressed density is controlled in 6.0g/cm3, the ruler of magnet ring
Very little is outer diameter (OD) * internal diameter (ID) * thickness (TH)=15mm*5.0mm*2.0mm;It is dried using a conventional oven, sintering temperature control
System is at 180 DEG C, soaking time 2h.Performance Evaluation is carried out to the magnet ring after baking, number of turns N=10Ts circle uses 3260B
The initial permeability μ i (1V/1MHz) of type LCR tester test magnet ring sample;It is surveyed with IWATSU-SY-8218 type hysteresiscope
Try the power consumption (10mT&1MHz) of magnet ring.
1. embodiment and comparative example performance comparison of table
The permeability and power consumption that comparing embodiment and comparative example obtain, it is seen that the obtained material power consumption side of embodiment
Face will be significantly lower than comparative example, this shows that clad and surface treatment low-power consumption are particularly significant, while knowing with filling proportion
Raising, implement resulting magnetic conductivity requirement and be apparently higher than comparative example.
Although this specification is described in terms of embodiments, but not each embodiment only includes an independent skill
Art scheme, this description of the specification is merely for the sake of clarity, and those skilled in the art should be using specification as one
A entirety, the technical solutions in the various embodiments may also be suitably combined, formed it will be appreciated by those skilled in the art that other
Embodiment.
Therefore the foregoing is merely the preferred embodiments of the application, not are used to limit the practical range of the application;It is i.e. all according to
The various equivalents that claims hereof range is done are the protection scope of the claim of this application.
Claims (10)
1. a kind of preparation method of high magnetic conductivity cream, it is characterised in that: the following steps are included:
Magnaglo one is coated to phosphoric acid class glass under cyclone and obtains pretreatment material one;
Magnaglo two is handled under an inert gas and obtains pretreatment material two;
Pretreatment material one and pretreatment material two are surface-treated respectively;
By the pretreatment material one after surface treatment and during pretreatment material two is mixed to get according to mass percent 1:9~4:6
Between expect;
Middle material is added in glue, curing agent and filler and is uniformly mixed to get mixture;
Mixture is mediated, obtains magnetic cream after rolling.
2. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that the Magnaglo one has
Body is at least one of Fe, FeSi, FeSiCr, FeNi, FeSi and FeSiAl.
3. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that the Magnaglo two has
Body is at least one of FeSiCrBC, FeSiAlBNbC and FeNiCrAlBC.
4. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that one He of Magnaglo
The partial size of Magnaglo two is 1-70 μm.
5. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that described by Magnaglo one
Treatment temperature when coating phosphoric acid class glass under cyclone is 300 DEG C~500 DEG C.
6. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that described to pre-process respectively
Material one and pretreatment material two be surface-treated specifically by surface treating agent treatment temperature be 50~90 DEG C when at
Reason 30~60 minutes.
7. a kind of preparation method of high magnetic conductivity cream according to claim 6, which is characterized in that the surface treating agent tool
Body is at least one of silane coupling agent, titanate esters, aluminic acid lipoprotein and zirconic acid rouge.
8. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that the phosphoric acid class glass tool
Body is P2O5-Na2O-ZnO、ZnO-Al2O3-P2O5And P2O5-Na2One of O-BaO.
9. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that the curing agent is fat
Race's diamines and polyamines, aromatic polyamine;Glue is at least one of epoxy resin, phenolic resin, silicone resin;
The filler is nano silicon oxide.
10. a kind of preparation method of high magnetic conductivity cream according to claim 1, which is characterized in that it is described by mixture into
Row is mediated, obtains magnetic cream after rolling specifically:
It obtains mediating material after mixture is mediated in high-speed kneading machine;
Material rod in roller mill will be mediated to roll to obtain magnetic cream.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN113674979A (en) * | 2021-07-06 | 2021-11-19 | 浙江东睦科达磁电有限公司 | Preparation method and material of metal soft magnetic core applied to ultrahigh frequency |
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Application publication date: 20190924 |