CN110270286A - A kind of high-purity MPE heat-sensitive paper color developing agent condensation system - Google Patents

A kind of high-purity MPE heat-sensitive paper color developing agent condensation system Download PDF

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Publication number
CN110270286A
CN110270286A CN201910529264.9A CN201910529264A CN110270286A CN 110270286 A CN110270286 A CN 110270286A CN 201910529264 A CN201910529264 A CN 201910529264A CN 110270286 A CN110270286 A CN 110270286A
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China
Prior art keywords
reactor tank
welded
purity
tank
connect
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CN201910529264.9A
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Chinese (zh)
Inventor
姚振锋
陈剑栋
李松
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Jiangyin Changsheng Chemical Co Ltd
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Jiangyin Changsheng Chemical Co Ltd
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Priority to CN201910529264.9A priority Critical patent/CN110270286A/en
Publication of CN110270286A publication Critical patent/CN110270286A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a kind of high-purity MPE heat-sensitive paper color developing agents to be condensed system, including reactor tank and supporting leg, one week of the lower end of the reactor tank is each provided with three supporting legs, the supporting leg is by being welded to connect in the lower end of reactor tank, the reactor tank and supporting leg pass through welded connecting, having heaters is arranged in the intersection of the supporting leg and reactor tank, by being internally provided with plugboard in top plate, and perforative axis hole is internally provided in plugboard, can make can to allow in the case where the movement of plugboard in this way axis hole inside plugboard and the axis hole inside reactor tank gradually be aligned, so that the phenomenon that axis hole inside axis hole and reactor tank inside plugboard misplaces, the outflow for more preferably carrying out the solution inside reactor tank is allowed in this way, solves existing high-purity MPE condensation system The incomplete phenomenon that may make internal solution reaction due to there is the gap of height between discharge nozzle and reactor tank.

Description

A kind of high-purity MPE heat-sensitive paper color developing agent condensation system
Technical field
The invention belongs to chemical industry synthesis correlative technology fields, and in particular to a kind of high-purity MPE heat-sensitive paper color developing agent condensation System.
Background technique
Chemically refer to a kind of chemical reaction, the often referred to chemical reaction of organic matter, identical or different organic compound The mutual chemical combination of molecule, be precipitated one or several molecules water or other compounds and form the process of new substance, two sometimes Organic compound molecule interacts and at a biggish molecule does not release simple molecules, is also referred to as condensed, reaction kettle it is wide Reason and good sense solution has the container physically or chemically reacted, by the structure design and parameter configuration to container, realizes what technique required Heating, evaporation, cooling and low high speed mixed function, reaction kettle are widely used in petroleum, chemical industry, rubber, pesticide, dyestuff, doctor Medicine, food, for completing the pressure vessel of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, Reaction pot, decomposition pot, polymeric kettle etc., material generally has carbon manganese steel, stainless steel, zirconium, nickel-base alloy and other composite materials.
MPE heat-sensitive paper color developing agent, abbreviation MPE, existing high-purity MPE condensation systems technology have the following problems: existing High-purity MPE condensation system during carrying out MPE condensation, need carry out heat when ceaselessly stirred, Such that internal solution can preferably be reacted, but it is existing when being condensed, because of discharge nozzle Typically there are the gaps of certain height between lower end, discharge nozzle and reactor tank for setting, may be such that accumulation in this way Solution inside discharge nozzle cannot be reacted and be processed well, such that there are the difference after some reactions, It may be such that solution content difference occur leads to the problem of reacting incomplete phenomenon.
Summary of the invention
The purpose of the present invention is to provide a kind of high-purity MPE heat-sensitive paper color developing agents to be condensed system, to solve above-mentioned background The existing high-purity MPE condensation system proposed in technology may be due to the gap between discharge nozzle and reactor tank there are height So that the problem of incomplete phenomenon of internal solution reaction.
To achieve the above object, the invention provides the following technical scheme: a kind of high-purity MPE heat-sensitive paper color developing agent condensation system System, including reactor tank and supporting leg, one week of the lower end of the reactor tank are each provided with three supporting legs, and the supporting leg passes through It is welded to connect in the lower end of reactor tank, the reactor tank and supporting leg by being welded to connect, the phase of the supporting leg and reactor tank At friendship be arranged having heaters, the heater by be welded to connect the lower end of reactor tank table side, the heater with react Tank is by being welded to connect, and the table side of the front end of the reactor tank is provided with visual window, and the visual window is connected by screw to anti- The table side of the front end of tank is answered, the reactor tank is fixedly connected with visual window by screw, and the visual window is socketed in reactor tank Inside, the front end of the heater are provided with discharge nozzle, and the discharge nozzle is bolted to connection in the lower end of reactor tank, institute It states discharge nozzle to be bolted to connection with reactor tank, conduction oil outlet is provided on the right side of the lower end of the reactor tank, it is described Conduction oil outlet is connected in the right side of the lower end of reactor tank, the reactor tank and conduction oil outlet by welding by being welded to connect It connects, the table side of the right end of the upside of the reactor tank is provided with heat conductive oil inlet, and the heat conductive oil inlet is by being welded to connect The table side of the right end of the upside of reactor tank, the reactor tank and heat conductive oil inlet are by being welded to connect, the upper end of the reactor tank It is provided with end cap, the end cap is bolted in the upper end of reactor tank, and the reactor tank and end cap are bolted company It connecing, feed pipe is provided on the left of the upper end of the end cap, the feed pipe, which passes through, to be welded to connect in the left side of the upper end of end cap, The feed pipe and end cap are by being welded to connect, and the upper end on the right side of the end cap is provided with cleaning pipe, and the cleaning pipe passes through It is welded to connect in the upper end on the right side of end cap, the cleaning pipe and end cap by being welded to connect, the left end setting of the feed pipe There is electric cabinet, it is solid by bolt that the upper end in the left side of end cap, the electric cabinet and end cap is bolted in the electric cabinet Fixed to connect, the upper end at the axle center of the end cap is provided with speed reducer, and the speed reducer is bolted in the upper end of end cap Axle center at, the speed reducer is bolted to connection with end cap, and the upper end of the speed reducer is provided with motor, the electricity The upper end of speed reducer is arranged in by bolt for motivation, and the motor is bolted to connection with speed reducer, the motor The table side of left end be provided with terminal box, the terminal box is connected by screw to the table side in the left end of motor, the wiring Box is fixedly connected with motor by screw, and the motor and power switch are electrically connected, the speed reducer and power switch It is electrically connected, the electric cabinet and power switch are electrically connected, and the heater and power switch are electrically connected.
Preferably, the composition of the discharge nozzle includes plugboard, threaded hole, top plate, side plate, discharge port and support base, The left and right ends of the inside of the top plate are each provided with two threaded holes, the threaded hole and top plate through connection, the top plate Inside axle center at a plugboard is provided with by socket, the plugboard is the structure of strip, under the top plate End is provided with support base, the support base and top plate by being welded to connect, and the table side of the left end of the support base is provided with side plate, The table end of the left end of the side plate is provided with discharge port, and the discharge port is the cylindrical structure of inner hollow, the discharge nozzle It is bolted to connection by top plate and reactor tank.
Preferably, the composition of the heater includes main body, heating tube, binding post, logical spool and vertical line pipe, the master Successively spaced set has three to pass through interior spiral shell with heating tube, three heating tubes and main body to the table side of the front end of body from left to right Groove rotation connection, the lower end of three heating tubes are each provided with a binding post, and the binding post and heating tube pass through set It connects in succession, the lower end of the binding post is provided with logical spool, and the logical spool is connect with binding post by twining in succession, the logical spool Right end be provided with vertical line pipe, the heater passes through welded connecting by main body and reactor tank.
Preferably, the composition of the heating tube includes heating pole, thread groove, end and protective plate, a left side for the end It is provided with protective plate, the end and protective plate on the downside of end, connection is rotated by internal thread groove, the left end of the protective plate Downside is provided with thread groove, and heating pole is provided on the downside of the left end of the thread groove, and the heating pole and thread groove pass through set It connects in succession, the heating tube, which is rotated by thread groove and main body by internal thread groove, to be connected.
Preferably, the composition of the reactor tank includes blender, stull, tank body and interlocking lever, the inside of the tank body Upper end be provided with interlocking lever, the left and right ends of the lower end of the interlocking lever are each provided with a stull, the lower end of the stull It is provided with blender, the blender is fixedly connected with interlocking lever by sealing flange, and the reactor tank is by tank body and visually Window is fixedly connected by screw.
Preferably, the composition of the electric cabinet includes thermometer, setting table, cabinet, heater switch, stirring switch, bottom Frame, terminals and lock core, the upper end of the chassis are provided with cabinet, heating are provided on the left of the bottom end of the inside of the cabinet Switch, the right end of the heater switch are provided with stirring switch, and the table side of the right end of the cabinet is provided with terminals, the case Setting table is provided on the left of the upper end of the inside of body, the right end of the setting table is provided with thermometer, and the electric cabinet passes through Chassis is bolted to connection with end cap.
Preferably, the heating tube is cylindrical structure, and the heating tube is provided with three altogether, three heating tubes point It is not symmetrical set being successively equally spaced from left to right in main body, three heating tubes are logical by internal thread groove and main body Rotation connection is crossed, the lower end of three heating tubes is successively each provided with a binding post, and three heating tubes are opened with power supply It closes and is electrically connected.
Preferably, the reactor tank is the cylindrical structure of inner hollow, and the diameter of section of the reactor tank is 80 lis Rice, the height of the reactor tank are 60 centimetres, and the volume of the reactor tank is three hectolitres, and the operating temperature of the reactor tank is low In 160 degrees Celsius, the hole for being internally provided with a rectangle of the table side of the front end of the reactor tank.
Preferably, the heat conductive oil inlet is flat cylindrical structure, the section of the outer circle of the heat conductive oil inlet Diameter is ten centimetres, and the diameter of section of the inner circle of the heat conductive oil inlet is eight centimetres, the shape of the inside of the heat conductive oil inlet Shape is funnel-shaped structure, and the heat conductive oil inlet and reactor tank pass through welded connecting.
Preferably, the supporting leg is the cylindrical structure of inner hollow, and the supporting leg is provided with three altogether, three institutes Stating supporting leg respectively is at one week of the lower end for being symmetrically set in qually spaced in reactor tank, and the height of three supporting legs is 20 Centimetre, the table side of the lower end of three supporting legs is provided with antiskid plate, under the antiskid plate of three supporting leg lower ends End is provided with skid resistance strip.
Compared with prior art, the present invention provides a kind of high-purity MPE heat-sensitive paper color developing agents to be condensed system, has following The utility model has the advantages that
(1), high-purity MPE is condensed system, by the way that traditional discharge nozzle to be modified, so that the top of existing discharge nozzle The height of size of bottom end of size and reactor tank at end is identical, the solution inside reactor tank can be allowed better in this way It is reacted;
(2), high-purity MPE is condensed system and can be made under the action of threaded hole in this way under the action of threaded hole Top plate can be allowed preferably preferably to connect with the outside table end of the bottom end of reactor tank, can discharge nozzle be connected in this way What is connect is more stable;
(3), high-purity MPE is condensed system, and by the setting of support base, can make in this way can under the action of support base So that discharge nozzle will not be made in this way because the active force of flowing makes under the action of the discharge nozzle can have preferably support Obtain the phenomenon that discharge nozzle shakes;
(4), high-purity MPE is condensed system, by the plugboard that is internally provided in top plate, and in the inside of plugboard Be provided with perforative axis hole, can make make in the case where the movement of plugboard in this way axis hole inside plugboard with Axis hole inside reactor tank can gradually carry out being aligned, and can thus preferably to carry out the solution inside reactor tank Outflow, so that solving existing high-purity MPE condensation system may be since there are height between discharge nozzle and reactor tank Gap makes the problem of incomplete phenomenon of internal solution reaction;
(5), high-purity MPE is condensed system, through the axis hole inside plugboard in plugboard grafting complete with top plate, makes The phenomenon that axis hole and the axis hole inside reactor tank inside plugboard misplace is obtained, in the movement of plugboard progress side It waits, the phenomenon that axis hole inside plugboard is successively overlapped with the axis hole inside reactor tank, can preferably carry out so interior The control of the flow velocity of the solution in portion can preferably work in this way.
Detailed description of the invention
Fig. 1 is that high-purity MPE of the invention is condensed system structure diagram;
Fig. 2 is discharge nozzle structural schematic diagram of the invention;
Fig. 3 is heater structure schematic diagram of the invention;
Fig. 4 is heating-pipe structure schematic diagram of the invention;
Fig. 5 is reactor tank structural schematic diagram of the invention;
Fig. 6 is electric cabinet structure schematic diagram of the invention;
In figure: 1, supporting leg;2, discharge nozzle;21, plugboard;22, threaded hole;23, top plate;24, side plate;25, discharge port; 26, support base;3, heater;31, main body;32, heating tube;321, heating pole;322, thread groove;323, end;324, it protects Plate;33, binding post;34, lead to spool;35, vertical line pipe;4, visual window;5, reactor tank;51, blender;52, stull;53, tank body; 54, interlocking lever;6, electric cabinet;61, thermometer;62, table is set;63, cabinet;64, heater switch;65, stirring switch;66, bottom Frame;67, terminals;68, lock core;7, feed pipe;8, terminal box;9, motor;10, speed reducer;11, cleaning pipe;12, end cap; 13, heat conductive oil inlet;14, conduction oil outlet.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Fig. 1-6 is please referred to, the present invention provides a kind of technical solution: a kind of high-purity MPE heat-sensitive paper color developing agent condensation system, Including reactor tank 5 and supporting leg 1, one week of the lower end of reactor tank 5 is each provided with three supporting legs 1, and supporting leg 1 is inner hollow Cylindrical structure, supporting leg 1 is provided with three altogether, by the setting of three supporting legs 1, can make in this way through three branch The effect that the setting of support leg 1 can be preferably supported, three supporting legs 1 are set in qually spaced in reactor tank 5 in symmetrical respectively One week of lower end at, the height of three supporting legs 1 is 20 centimetres, and the table side of the lower end of three supporting legs 1 is provided with anti- Slide plate, the lower end of the antiskid plate of three 1 lower ends of supporting leg are provided with skid resistance strip, and supporting leg 1 is being reacted by being welded to connect By being welded to connect, having heaters 3 is arranged in the intersection of supporting leg 1 and reactor tank 5 for the lower end of tank 5, reactor tank 5 and supporting leg 1, The composition of heater 3 includes main body 31, heating tube 32, binding post 33, leads to spool 34 and vertical line pipe 35, the front end of main body 31 Successively spaced set has three to rotate with heating tube 32, three heating tubes 32 and main body 31 by internal thread groove to table side from left to right Connection, the lower end of three heating tubes 32 is each provided with a binding post 33, by the setting of binding post 33, can make so more The connection of good progress route, so as to preferably work, binding post 33 and heating tube 32 pass through socket connection, heating The composition of pipe 32 includes heating pole 321, thread groove 322, end 323 and protective plate 324, is set on the downside of the left end of end 323 It is equipped with protective plate 324, end 323 and protective plate 324 and connection is rotated by internal thread groove, set on the downside of the left end of protective plate 324 It is equipped with thread groove 322, heating pole 321 is provided on the downside of the left end of thread groove 322, by the setting of heating pole 321, in this way may be used So that the effect that can be preferably heated under the action of heating pole 321, heating pole 321 and thread groove 322 pass through set It connects in succession, heating tube 32, which is rotated by thread groove 322 and main body 31 by internal thread groove, to be connected, and heating tube 32 is cylindrical body knot Structure,
A kind of high-purity MPE heat-sensitive paper color developing agent condensation system, including heating tube 32 are provided with three altogether, are added by three The setting of heat pipe 32, can make the effect preferably heated in this way, and three heating tubes 32 are symmetrical set respectively in master Body 31 is successively equally spaced from left to right, and three heating tubes 32 are connected by internal thread groove and main body 31 by rotation, and three The lower end of root heating tube 32 is successively each provided with a binding post 33, and three heating tubes 32 and power switch are electrically connected, wiring The lower end of column 33 is provided with logical spool 34, and logical spool 34 is connect with binding post 33 by twining in succession, and the right end of logical spool 34 is provided with Vertical line pipe 35, heater 3 is by main body 31 and reactor tank 5 by being welded to connect, and heater 3 is by being welded to connect in reactor tank 5 Lower end table side, by being welded to connect, the table side of the front end of reactor tank 5 is provided with visual window 4 for heater 3 and reactor tank 5, can Form 4 is connected by screw to the table side in the front end of reactor tank 5, and reactor tank 5 is fixedly connected with visual window 4 by screw, visually Window 4 is socketed in the inside of reactor tank 5, and the front end of heater 3 is provided with discharge nozzle 2, and the composition of discharge nozzle 2 includes plugboard 21, threaded hole 22, top plate 23, side plate 24, discharge port 25 and support base 26, the left and right ends of the inside of top plate 23 are each provided with two A threaded hole 22, threaded hole 22 and top plate 23 are provided with one by socket at connection, the axle center of the inside of top plate 23 and insert Fishplate bar 21, plugboard 21 are the structure of strip, and the lower end of top plate 23 is provided with support base 26, and support base 26 passes through with top plate 23 It is welded to connect, by being welded to connect, so that integrally-built stability is preferably fixed, a left side for support base 26 The table side at end is provided with side plate 24, and the table end of the left end of side plate 24 is provided with discharge port 25, and discharge port 25 is the circle of inner hollow Column structure, discharge nozzle 2 are bolted to connection by top plate 23 with reactor tank 5, and discharge nozzle 2 is bolted to connection The lower end of reactor tank 5, reactor tank 5 are the cylindrical structure of inner hollow, and the diameter of section of reactor tank 5 is 80 centimetres,
A kind of high-purity MPE heat-sensitive paper color developing agent condensation system, the height including reactor tank 5 is 60 centimetres, by anti- The setting of tank 5 is answered, the solution inside preferably carrying out can be made to be reacted in this way, so that preferably react More sufficiently, the volume of reactor tank 5 is three hectolitres, and the operating temperature of reactor tank 5 is lower than 160 degrees Celsius, reactor tank 5 Front end table side the hole for being internally provided with a rectangle, discharge nozzle 2 is bolted to connection with reactor tank 5, reacts Conduction oil outlet 14 is provided on the right side of the lower end of tank 5, conduction oil outlet 14 is by being welded to connect on the right side of the lower end of reactor tank 5 Side, reactor tank 5 and conduction oil outlet 14 by being welded to connect, the table side of the right end of the upside of reactor tank 5 be provided with conduction oil into Mouth 13, heat conductive oil inlet 13 are flat cylindrical structure, and the diameter of section of the outer circle of heat conductive oil inlet 13 is ten centimetres, are led The diameter of section of the inner circle of hot oil inlet 13 is eight centimetres, and the shape of the inside of heat conductive oil inlet 13 is funnel-shaped structure, is passed through By the setting of heat conductive oil inlet 13, the addition for preferably carrying out conduction oil can be made, in this way so as to preferably carry out work Make, heat conductive oil inlet 13 and reactor tank 5 are by being welded to connect, and heat conductive oil inlet 13 is by being welded to connect in the upside of reactor tank 5 Right end table side, by being welded to connect, the upper end of reactor tank 5 is provided with end cap 12, end cap for reactor tank 5 and heat conductive oil inlet 13 12 are bolted in the upper end of reactor tank 5, and the composition of reactor tank 5 includes blender 51, stull 52, tank body 53 and interlocks Bar 54, the upper end of the inside of tank body 53 are provided with interlocking lever 54, and the left and right ends of the lower end of interlocking lever 54 are each provided with a cross Support 52, the lower end of stull 52 is provided with blender 51, by the setting of blender 51, can make preferably to be stirred in this way It mixes, so as to preferably work, blender 51 is fixedly connected with interlocking lever 54 by sealing flange, and reactor tank 5 passes through Tank body 53 is fixedly connected with visual window 4 by screw, and reactor tank 5 is bolted to connection with end cap 12, the upper end of end cap 12 Left side be provided with feed pipe 7,
A kind of high-purity MPE heat-sensitive paper color developing agent condensation system, including feed pipe 7 by being welded to connect in the upper of end cap 12 By being welded to connect, the upper end on the right side of end cap 12 is provided with cleaning pipe 11, cleaning pipe for the left side at end, feed pipe 7 and end cap 12 11 by being welded to connect in the upper end on the right side of end cap 12, cleaning pipe 11 and end cap 12 by being welded to connect, the left end of feed pipe 7 It is provided with electric cabinet 6, the composition of electric cabinet 6 includes thermometer 61, setting table 62, cabinet 63, heater switch 64, stirring switch 65, chassis 66, terminals 67 and lock core 68, the upper end of chassis 66 are provided with cabinet 63, the left side of the bottom end of the inside of cabinet 63 It is provided with heater switch 64, by the setting of heater switch 64, the effect preferably heated can be made in this way, heating is opened The right end for closing 64 is provided with stirring switch 65, and the table side of the right end of cabinet 63 is provided with terminals 67, the inside of cabinet 63 it is upper Setting table 62 is provided on the left of end, the right end of setting table 62 is provided with thermometer 61, and electric cabinet 6 passes through chassis 66 and end cap 12 It is bolted to connection, the upper end in the left side of end cap 12 is bolted in electric cabinet 6, and electric cabinet 6 passes through with end cap 12 Bolt is fixedly connected, and the upper end at the axle center of end cap 12 is provided with speed reducer 10, and speed reducer 10 is bolted in end cap 12 Upper end axle center at, speed reducer 10 is bolted to connection with end cap 12, and the upper end of speed reducer 10 is provided with motor 9, The upper end of speed reducer 10 is arranged in by bolt for motor 9, and motor 9 is bolted to connection with speed reducer 10, motor 9 The table side of left end be provided with terminal box 8, terminal box 8 is connected by screw to the table side in the left end of motor 9, terminal box 8 with Motor 9 is fixedly connected by screw, and motor 9 and power switch are electrically connected, and speed reducer 10 and power switch are electrically connected, Electric cabinet 6 and power switch are electrically connected, and heater 3 and power switch are electrically connected.
The working principle of the invention and process for using: it after the present invention installs, first checks for such machine and whether can It works normally, checks that the plug on electric wire is finished with whether socket connect, if there is abnormal noise, should close immediately such Machine waits the maintenance of professional, when the reaction for the condensation to carry out the MPE, takes out the solution of the MPE first, The solution of the MPE is placed on to the side of the equipment later, by the setting of three supporting legs 1, can be made by three in this way The effect that the setting of root supporting leg 1 can be preferably supported, three supporting legs 1 are set in qually spaced in reaction in symmetrical respectively At one week of the lower end of tank 5, then by the equipment power-on, the MPE solution is added to instead from the mouth end of feed pipe 7 later The inside for answering tank 5 after MPE solution addition finishes carries out that heating oil is added later by the inside of heat conductive oil inlet 13, Then make to heat the heating oil being added by the heater switch 64 inside electric cabinet 6, Heater 3 is preferably heated by three internal heating tubes 32, and the wiring that three heating tubes 32 pass through lower end Column 33 can be electrically connected under the action of vertical line pipe 35 with electric cabinet 6, and the route of the flowing of heating oil With the lateral ends for being wrapped in reactor tank 5, the temperature of heating can be set by the setting table 62 inside electric cabinet 6, works as inside Temperature be heated to setting temperature after, can preferably carry out the temperature inside observing response tank 5 in thermometer 61 in this way, By the setting of reactor tank 5, the solution inside preferably carrying out can be made to be reacted in this way, so that preferably That reacts is more abundant, and after internal heating is oily heated, at this moment the MPE solution inside reactor tank 5 carries out tentatively anti- It answers, later by the stirring switch 65 inside electric cabinet 6, so that the device works, and 6 electricity of motor 9 and electric cabinet Property connection, the model Y355 of motor 9 uses F class B insulation, voltage rating 380V, rated frequency 50Hz, in this way can be with So that rotating the interlocking lever 54 inside reactor tank 5, and in the rotation of interlocking lever 54 In the case of make that blender 51 is driven to be stirred, while motor 9 can be made in rotation under the action of speed reducer 10 When preferably carry out work at the uniform velocity, the model PL60 of speed reducer 10 in this way can for the MPE solution inside reactor tank 5 Preferably to be reacted, after the time enough of the MPE solution reaction inside reactor tank 5, can by visual window 4 into The case where stirring inside row reactor tank 5, is preferably observed, and so as to be observed in real time, closes electric cabinet later 6 so that motor 9 stops operating, the blender 51 inside reactor tank 5 stop rotating one end time after, at this moment by going out Expects pipe 2 flows out the solution inside reactor tank 5, and grasps plugboard 21 by user, and firmly will Plugboard 21 is pulled toward side, and the through-hole in the inside of plugboard 21 will gradually be carried out with the through-hole inside reactor tank 5 in this way Alignment, through the axis hole inside plugboard 21 in plugboard 21 and 23 complete grafting of top plate, so that the axis inside plugboard 21 The phenomenon that axis hole inside hole and reactor tank 5 misplaces, when plugboard 21 carries out the movement of side, in plugboard 21 The phenomenon that axis hole in portion is successively overlapped with the axis hole inside reactor tank 5 can preferably carry out internal solution in this way The control of flow velocity, so that solve existing high-purity MPE condensation system may be due to depositing between discharge nozzle 2 and reactor tank 5 The problem of making the incomplete phenomenon of internal solution reaction in the gap of height, can thus make will be in reactor tank 5 The solution in portion is flowed out, and at the same time opening conduction oil outlet 14, the heating oil of 5 outer end of reactor tank is passed through thermally conductive Oil export 14 is flowed out, and can make preferably to work in this way, after the MPE solution inside reactor tank 5 flows out, is at this moment led to Over cleaning pipe 11 opens electric cabinet 6, can to react under the action of blender 51 to the inside injected clear water of reactor tank 5 Tank 5 can clean more clean, and this completes the condensation reactions of the MPE solution, finally close electric cabinet 6, make It obtains the equipment and disconnects power supply.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (10)

1. a kind of high-purity MPE heat-sensitive paper color developing agent is condensed system, including reactor tank (5) and supporting leg (1), it is characterised in that: The lower end of the reactor tank (5) is each provided with three supporting legs (1) for one week, and the supporting leg (1) is by being welded to connect anti- The lower end of tank (5) is answered, the reactor tank (5) and supporting leg (1) are by being welded to connect, the supporting leg (1) and reactor tank (5) Having heaters (3) are arranged in intersection, and the heater (3) is described to add by being welded to connect the table side in the lower end of reactor tank (5) By being welded to connect, the table side of the front end of the reactor tank (5) is provided with visual window (4), described for hot device (3) and reactor tank (5) Visual window (4) is connected by screw to the table side in the front end of reactor tank (5), and the reactor tank (5) and visual window (4) pass through screw It is fixedly connected, the visual window (4) is socketed in the inside of reactor tank (5), and the front end of the heater (3) is provided with discharge nozzle (2), the discharge nozzle (2) is bolted to connection in the lower end of reactor tank (5), and the discharge nozzle (2) and reactor tank (5) are logical It crosses bolt to be fixedly connected, is provided with conduction oil outlet (14), the conduction oil outlet on the right side of the lower end of the reactor tank (5) (14) by being welded to connect on the right side of the lower end of reactor tank (5), the reactor tank (5) and conduction oil outlet (14) pass through welding Connection, the table side of the right end of the upside of the reactor tank (5) are provided with heat conductive oil inlet (13), and the heat conductive oil inlet (13) is logical The table side being welded to connect in the right end of the upside of reactor tank (5) is crossed, the reactor tank (5) and heat conductive oil inlet (13) pass through welding Connection, the upper end of the reactor tank (5) are provided with end cap (12), and the end cap (12) is bolted in reactor tank (5) Upper end, the reactor tank (5) are bolted to connection with end cap (12), be provided on the left of the upper end of the end cap (12) into Expects pipe (7), the feed pipe (7) is by being welded to connect in the left side of the upper end of end cap (12), the feed pipe (7) and end cap (12) by being welded to connect, the upper end on the right side of the end cap (12) is provided with cleaning pipe (11), and the cleaning pipe (11) passes through It is welded to connect in the upper end on the right side of end cap (12), the cleaning pipe (11) and end cap (12) are by being welded to connect, the charging The left end of pipe (7) is provided with electric cabinet (6), and the electric cabinet (6) is bolted in the upper end in the left side of end cap (12), institute It states electric cabinet (6) to be bolted to connection with end cap (12), the upper end at the axle center of the end cap (12) is provided with speed reducer (10), the speed reducer (10) is bolted at the axle center of the upper end of end cap (12), the speed reducer (10) and end cap (12) it is bolted to connection, the upper end of the speed reducer (10) is provided with motor (9), and the motor (9) passes through spiral shell Bolt is arranged in the upper end of speed reducer (10), and the motor (9) is bolted to connection with speed reducer (10), the motor (9) table side of left end is provided with terminal box (8), and the terminal box (8) is connected by screw to the table in the left end of motor (9) Side, the terminal box (8) are fixedly connected with motor (9) by screw, and the motor (9) and power switch are electrically connected, The speed reducer (10) and power switch are electrically connected, and the electric cabinet (6) and power switch are electrically connected, the heater (3) it is electrically connected with power switch.
2. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: it is described go out The composition of expects pipe (2) includes plugboard (21), threaded hole (22), top plate (23), side plate (24), discharge port (25) and support base (26), the left and right ends of the inside of the top plate (23) are each provided with two threaded holes (22), the threaded hole (22) and top plate (23) plugboard (21), the grafting are provided with by socket at connection, the axle center of the inside of the top plate (23) Plate (21) is the structure of strip, and the lower end of the top plate (23) is provided with support base (26), the support base (26) and top plate (23) by being welded to connect, the table side of the left end of the support base (26) is provided with side plate (24), the left end of the side plate (24) Table end be provided with discharge port (25), the discharge port (25) is the cylindrical structure of inner hollow, and the discharge nozzle (2) passes through Top plate (23) is bolted to connection with reactor tank (5).
3. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: described to add The composition of hot device (3) includes main body (31), heating tube (32), binding post (33), leads to spool (34) and vertical line pipe (35), described Successively spaced set has three with heating tube (32), three heating tubes (32) table side of the front end of main body (31) from left to right It is rotated and is connected by internal thread groove with main body (31), the lower end of three heating tubes (32) is each provided with a binding post (33), by socket connection, the lower end of the binding post (33) is provided with logical spool for the binding post (33) and heating tube (32) (34), the logical spool (34) is connect with binding post (33) by twining in succession, and the right end of the logical spool (34) is provided with vertical line pipe (35), the heater (3) passes through welded connecting by main body (31) and reactor tank (5).
4. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 3 is condensed system, it is characterised in that: described to add The composition of heat pipe (32) includes heating pole (321), thread groove (322), end (323) and protective plate (324), the end (323) it is provided on the downside of left end protective plate (324), the end (323) and protective plate (324) are rotated by internal thread groove It connects, is provided with thread groove (322) on the downside of the left end of the protective plate (324), the downside of the left end of the thread groove (322) It is provided with heating pole (321), by socket connection, the heating tube (32) passes through for the heating pole (321) and thread groove (322) Thread groove (322) and main body (31) are rotated by internal thread groove to be connected.
5. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: described anti- The composition for answering tank (5) includes blender (51), stull (52), tank body (53) and interlocking lever (54), the tank body (53) it is interior The upper end in portion is provided with interlocking lever (54), and the left and right ends of the lower end of the interlocking lever (54) are each provided with a stull (52), The lower end of the stull (52) is provided with blender (51), and the blender (51) is fixed with interlocking lever (54) by sealing flange Connection, the reactor tank (5) are fixedly connected with visual window (4) by screw by tank body (53).
6. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: the electricity Control case (6) composition include thermometer (61), setting table (62), cabinet (63), heater switch (64), stirring switch (65), The upper end of chassis (66), terminals (67) and lock core (68), the chassis (66) is provided with cabinet (63), the cabinet (63) It being provided with heater switch (64) on the left of internal bottom end, the right end of the heater switch (64) is provided with stirring switch (65), The table side of the right end of the cabinet (63) is provided with terminals (67), is provided on the left of the upper end of the inside of the cabinet (63) It sets table (62), the right end of setting table (62) is provided with thermometer (61), and the electric cabinet (6) passes through chassis (66) and end Lid (12) is bolted to connection.
7. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 3 is condensed system, it is characterised in that: described to add Heat pipe (32) is cylindrical structure, and the heating tube (32) is provided with three altogether, and three heating tubes (32) are respectively in symmetrical Being successively equally spaced from left to right in main body (31) is set, and three heating tubes (32) pass through internal thread groove and main body (31) by rotation connection, the lower end of three heating tubes (32) is successively each provided with a binding post (33), described in three Heating tube (32) and power switch are electrically connected.
8. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: described anti- Answering tank (5) is the cylindrical structure of inner hollow, and the diameter of section of the reactor tank (5) is 80 centimetres, the reactor tank (5) Height be 60 centimetres, the volume of the reactor tank (5) is three hectolitres, and the operating temperature of the reactor tank (5) is lower than 100 60 degrees Celsius, the hole for being internally provided with a rectangle of the table side of the front end of the reactor tank (5).
9. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: described to lead Hot oil inlet (13) is flat cylindrical structure, and the diameter of section of the outer circle of the heat conductive oil inlet (13) is ten centimetres, The diameter of section of the inner circle of the heat conductive oil inlet (13) is eight centimetres, and the shape of the inside of the heat conductive oil inlet (13) is leakage Bucket-shaped structure, the heat conductive oil inlet (13) and reactor tank (5) pass through welded connecting.
10. a kind of high-purity MPE heat-sensitive paper color developing agent according to claim 1 is condensed system, it is characterised in that: the branch Support leg (1) is the cylindrical structure of inner hollow, and the supporting leg (1) is provided with three altogether, and three supporting legs (1) are respectively At one week of the lower end for being symmetrically set in qually spaced in reactor tank (5), the height of three supporting legs (1) is 20 centimetres, The table side of the lower end of three supporting legs (1) is provided with antiskid plate, under the antiskid plate of three supporting leg (1) lower ends End is provided with skid resistance strip.
CN201910529264.9A 2019-06-19 2019-06-19 A kind of high-purity MPE heat-sensitive paper color developing agent condensation system Pending CN110270286A (en)

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CN202310155U (en) * 2011-10-31 2012-07-04 中国矿业大学 Quick heater with protection sleeve
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