CN110261425A - A kind of visualization high pressure property condensation analytical equipment - Google Patents

A kind of visualization high pressure property condensation analytical equipment Download PDF

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Publication number
CN110261425A
CN110261425A CN201910664024.XA CN201910664024A CN110261425A CN 110261425 A CN110261425 A CN 110261425A CN 201910664024 A CN201910664024 A CN 201910664024A CN 110261425 A CN110261425 A CN 110261425A
Authority
CN
China
Prior art keywords
condensation
viewer module
autoclave body
high pressure
cap
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910664024.XA
Other languages
Chinese (zh)
Inventor
马凤鸣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HAIAN HUADA PETROLEUM DEVICES CO Ltd
Original Assignee
HAIAN HUADA PETROLEUM DEVICES CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HAIAN HUADA PETROLEUM DEVICES CO Ltd filed Critical HAIAN HUADA PETROLEUM DEVICES CO Ltd
Priority to CN201910664024.XA priority Critical patent/CN110261425A/en
Publication of CN110261425A publication Critical patent/CN110261425A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/02Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering
    • G01N25/12Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering of critical point; of other phase change
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/56Investigating or analyzing materials by the use of thermal means by investigating moisture content
    • G01N25/66Investigating or analyzing materials by the use of thermal means by investigating moisture content by investigating dew-point
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N2021/8411Application to online plant, process monitoring

Abstract

The present invention relates to a kind of visualization high pressure property condensation analytical equipments, it is characterised in that: including condensation autoclave body, viewer module and detection bar;The viewer module is arranged on condensation autoclave body;It can be widely used in exploration and development field in the present invention, the general experiment that condensation under object high pressure dew point is converted can be completed;More importantly: scientific research personnel can intuitive observation place carry out relevant state observation and record related data, the physical property high pressure condensation visualized experiment carried out with technology provided by the invention under different pressure, pressure and state of temperature physical property condensation relationship have important practical significance and application value;Using the detection rod structure of adjustable detection range, in the case where guaranteeing leakproofness, the real-time detection of internal environment can be carried out by detection bar.

Description

A kind of visualization high pressure property condensation analytical equipment
Technical field
The present invention relates to high pressure property condensation analytical equipment fields more particularly to a kind of visualization high pressure property condensation to analyze Device.
Background technique
The condensation analytical equipment of general physical property does not have visualization function, and it is entirely logical that the detection of data is carried out in dew point It crosses and protrudes into intracavitary probe or the relevant Data Detection of detection device progress;External staff can not observe physical property in dew point Related particular state;Therefore a kind of visual condensation device is needed to carry out the physical property state of intuitive observation dew point;This Outer common physical property condensation analytical equipment poor sealing performance, pressure fluctuating in inner range is big during test.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of visualization high pressure property condensation analytical equipments, are able to solve one As physical property condensation analytical equipment cannot achieve the problem of visual observation and leakproofness difference.
In order to solve the above technical problems, the technical solution of the present invention is as follows: a kind of visualization high pressure property condensation analytical equipment, Its innovative point is: including condensation autoclave body, viewer module and detection bar;The viewer module is arranged on condensation autoclave body;
The viewer module is cylindrical to be connect and respectively about horizontal central line and axisymmetrical, among the circumferential side wall of viewer module Position is recessed inwardly to form groove, and groove is symmetric about the axis and is located at axis two sides, and intermediate position is provided with a level and runs through Hole;The viewer module is provided with the observation cavity through clamp body in the axial direction, is located on the inner wall of viewer module Viewer module both ends are provided with transparent glass limit table top;Observation cavity pressure cap card is provided on the outer wall of the viewer module Slot;
The condensation autoclave body includes autoclave body unit and autoclave body end plug;The autoclave body unit is horizontally disposed high pressure resistant transparent knot Structure;The autoclave body unit is embedded among viewer module in the through hole at position and autoclave body unit is closed at one end open at one end;Institute State the open end that autoclave body end plug is located at autoclave body unit;The autoclave body end plug includes end cap and end socket;The end cap and end socket along Axis direction, which is coaxially arranged with, accommodates the through-hole that detection bar passes through, and the detection bar passes through end cap and end socket extends to condensation kettle In body unit, the detection bar is locked on end cap by end socket;It is located at axis two sides on the end cap and is respectively arranged with medium Into pipeline and medium effuser road.
Further, it is provided with a cylindric transparent glass in the observation cavity, and transparent glass is placed on form mould On the limit table top of block;Several washers are provided between the transparent glass and the inner wall of viewer module;The viewer module End be provided with observation cavity pressure cap.
Further, the observation cavity pressure cap is in annulus tubular, and centre is provided with the cavity for accommodating viewer module end, The center of observation cavity pressure cap is provided with light-transmitting opening;It observes and is provided with bayonet on the inner wall of end of cavity pressure cap, the bayonet and form Transparent glass is fastened in the observation cavity of viewer module by the observation cavity pressure cap card slot cooperation on module outer wall.
Further, the through-hole wall on the end cap is provided with locking internal screw thread, is provided with lock on the end socket outer wall Tight external screw thread;The end cap and end socket are by being threadedly engaged the detection rod locking for passing through end socket and end cap on end cap.
The present invention has the advantages that
1) it can be widely used in exploration and development field in the present invention, can completes what condensation under object high pressure dew point was converted Generality experiment;More importantly: scientific research personnel intuitively observation place can carry out relevant state observation and record dependency number According to the physical property high pressure condensation visualized experiment carried out with technology provided by the invention is in different pressure, pressure and temperature Physical property condensation relationship has important practical significance and application value under degree state;Using the detection bar knot of adjustable detection range Structure can carry out the real-time detection of internal environment in the case where guaranteeing leakproofness by detection bar.
Detailed description of the invention
The present invention will be further described in detail below with reference to the accompanying drawings and specific embodiments.
Fig. 1 is a kind of structural schematic diagram of visualization high pressure property condensation analytical equipment of the invention.
Specific embodiment
The following examples can make professional and technical personnel that the present invention be more fully understood, but therefore not send out this It is bright to be limited among the embodiment described range.
A kind of visualization high pressure property condensation analytical equipment as shown in Figure 1, including condensation autoclave body 1, viewer module 2 and spy Measuring staff 3;The viewer module 2 is arranged on condensation autoclave body 1.
Viewer module 2 is cylindrical to be connect and respectively about horizontal central line and axisymmetrical, in the circumferential side wall of viewer module 2 Between position be recessed inwardly to form groove, groove it is symmetric about the axis and be located at axis two sides, intermediate position is provided with a level and passes through Perforation 21;The viewer module 2 is provided with the observation cavity 22 through clamp body in the axial direction, viewer module 2 it is interior It is located at 2 both ends of viewer module on wall and is provided with transparent glass limit table top;Observation is provided on the outer wall of the viewer module 2 22 pressure cap card slot of cavity.
Condensation autoclave body 1 includes autoclave body unit 11 and autoclave body end plug 12;The autoclave body unit 11 is horizontally disposed high pressure resistant Transparent configuration;The autoclave body unit 11 is embedded in the through hole 21 at the intermediate position of viewer module 2 and 11 1 end seal of autoclave body unit It closes open at one end;The autoclave body end plug 12 is located at the open end of autoclave body unit 11;The autoclave body end plug 12 includes end cap 13 and envelope First 14;The end cap 13 is coaxially arranged with the through-hole for accommodating detection bar 3 and passing through, the detection with end socket 14 along axis direction Bar 3 passes through end cap 13 and end socket 14 extends in condensation autoclave body unit 11, and the detection bar 3 is locked at end cap 13 by end socket 14 On;Medium, which is respectively arranged with, positioned at axis two sides on the end cap 13 enters pipeline 15 and medium effuser road 16.
It is provided with a cylindric transparent glass 4 in observation cavity 22, and transparent glass 4 is placed on the limit of viewer module 2 On table top;Several washers are provided between the transparent glass 4 and the inner wall of viewer module 2;The end of the viewer module 2 It is provided with observation cavity pressure cap 23.
Observing cavity pressure cap 23 is in annulus tubular, and centre is provided with the cavity for accommodating 2 end of viewer module, observes cavity pressure The center of cap 23 is provided with light-transmitting opening;It observes and is provided with bayonet on the inner wall of end of cavity pressure cap 23, outside the bayonet and viewer module 2 Transparent glass 4 is fastened in the observation cavity 22 of viewer module 2 by the observation cavity pressure cap card slot cooperation on wall.
Through-hole wall on end cap 13 is provided with locking internal screw thread, is provided with locking external thread on 14 outer wall of end socket; The end cap 13 passes through with end socket 14 to be threadedly engaged the detection bar 4 for passing through end socket 14 and end cap 13 and is locked on end cap 13.
It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, above-described embodiment and explanation It is merely illustrated the principles of the invention described in book, without departing from the spirit and scope of the present invention, the present invention also has Various changes and modifications, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention It is defined by the appending claims and its equivalent thereof.

Claims (4)

1. a kind of visualization high pressure property condensation analytical equipment, it is characterised in that: including condensation autoclave body, viewer module and detection Bar;The viewer module is arranged on condensation autoclave body;
The viewer module is cylindrical to be connect and respectively about horizontal central line and axisymmetrical, among the circumferential side wall of viewer module Position is recessed inwardly to form groove, and groove is symmetric about the axis and is located at axis two sides, and intermediate position is provided with a level and runs through Hole;The viewer module is provided with the observation cavity through clamp body in the axial direction, is located on the inner wall of viewer module Viewer module both ends are provided with transparent glass limit table top;Observation cavity pressure cap card is provided on the outer wall of the viewer module Slot;
The condensation autoclave body includes autoclave body unit and autoclave body end plug;The autoclave body unit is horizontally disposed high pressure resistant transparent knot Structure;The autoclave body unit is embedded among viewer module in the through hole at position and autoclave body unit is closed at one end open at one end;Institute State the open end that autoclave body end plug is located at autoclave body unit;The autoclave body end plug includes end cap and end socket;The end cap and end socket along Axis direction, which is coaxially arranged with, accommodates the through-hole that detection bar passes through, and the detection bar passes through end cap and end socket extends to condensation kettle In body unit, the detection bar is locked on end cap by end socket;It is located at axis two sides on the end cap and is respectively arranged with medium Into pipeline and medium effuser road.
2. a kind of visualization high pressure property condensation analytical equipment according to claim 1, it is characterised in that: the observation is empty It is intracavitary to be provided with a cylindric transparent glass, and transparent glass is placed on the limit table top of viewer module;The transparent glass Several washers are provided between the inner wall of viewer module;The end of the viewer module is provided with observation cavity pressure cap.
3. a kind of visualization high pressure property condensation analytical equipment according to claim 2, it is characterised in that: the observation is empty Chamber pressure cap is in annulus tubular, and centre is provided with the cavity for accommodating viewer module end, and the center of observation cavity pressure cap is provided with light transmission Mouthful;It observes and is provided with bayonet on the inner wall of end of cavity pressure cap, the observation cavity pressure cap card on the bayonet and viewer module outer wall Transparent glass is fastened in the observation cavity of viewer module by slot cooperation.
4. a kind of visualization high pressure property condensation analytical equipment according to claim 1, it is characterised in that: on the end cap Through-hole wall be provided with locking internal screw thread, be provided with locking external thread on the end socket outer wall;The end cap passes through with end socket The detection rod locking for passing through end socket and end cap is threadedly engaged on end cap.
CN201910664024.XA 2019-07-23 2019-07-23 A kind of visualization high pressure property condensation analytical equipment Pending CN110261425A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910664024.XA CN110261425A (en) 2019-07-23 2019-07-23 A kind of visualization high pressure property condensation analytical equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910664024.XA CN110261425A (en) 2019-07-23 2019-07-23 A kind of visualization high pressure property condensation analytical equipment

Publications (1)

Publication Number Publication Date
CN110261425A true CN110261425A (en) 2019-09-20

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CN201910664024.XA Pending CN110261425A (en) 2019-07-23 2019-07-23 A kind of visualization high pressure property condensation analytical equipment

Country Status (1)

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CN (1) CN110261425A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112682013A (en) * 2021-01-04 2021-04-20 西南石油大学 Experimental test method for high-temperature high-pressure visual exploitation of fracture-cavity condensate gas reservoir

Citations (8)

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DE10230857A1 (en) * 2002-07-09 2004-02-12 Bayer Ag Optical port, for plant control, e.g. of pressurized chemical plant, comprises measurement cell body containing threaded insert, with radiation transparent window, and shell between window and cover holding window in insert
WO2004048952A1 (en) * 2002-11-27 2004-06-10 Obschestvo S Ogranichennoi Otvetstvennostju 'orenburggasprom' Equilibrium bomb for studying phase behaviour of hydrocarbons
CN201273903Y (en) * 2008-10-15 2009-07-15 中国石油天然气股份有限公司 Clamping device for high temperature high pressure microscopic experiment
CN105545271A (en) * 2015-12-22 2016-05-04 中国石油化工股份有限公司 Low-permeability condensate gas reservoir fracturing fluid flowback control method
CN106404778A (en) * 2016-08-27 2017-02-15 南通华兴石油仪器有限公司 Visual rock core holder microscopic test model
CN106679757A (en) * 2017-02-22 2017-05-17 扬州华宝石油仪器有限公司 Visual volume metering device for high pressure physical property analyzer
CN109613113A (en) * 2018-04-08 2019-04-12 江苏联友科研仪器有限公司 A kind of high-temperature, high pressure fluid test kettle
CN210322860U (en) * 2019-07-23 2020-04-14 海安华达石油仪器有限公司 Visual high-pressure physical property condensation analysis device

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10230857A1 (en) * 2002-07-09 2004-02-12 Bayer Ag Optical port, for plant control, e.g. of pressurized chemical plant, comprises measurement cell body containing threaded insert, with radiation transparent window, and shell between window and cover holding window in insert
WO2004048952A1 (en) * 2002-11-27 2004-06-10 Obschestvo S Ogranichennoi Otvetstvennostju 'orenburggasprom' Equilibrium bomb for studying phase behaviour of hydrocarbons
CN201273903Y (en) * 2008-10-15 2009-07-15 中国石油天然气股份有限公司 Clamping device for high temperature high pressure microscopic experiment
CN105545271A (en) * 2015-12-22 2016-05-04 中国石油化工股份有限公司 Low-permeability condensate gas reservoir fracturing fluid flowback control method
CN106404778A (en) * 2016-08-27 2017-02-15 南通华兴石油仪器有限公司 Visual rock core holder microscopic test model
CN106679757A (en) * 2017-02-22 2017-05-17 扬州华宝石油仪器有限公司 Visual volume metering device for high pressure physical property analyzer
CN109613113A (en) * 2018-04-08 2019-04-12 江苏联友科研仪器有限公司 A kind of high-temperature, high pressure fluid test kettle
CN210322860U (en) * 2019-07-23 2020-04-14 海安华达石油仪器有限公司 Visual high-pressure physical property condensation analysis device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112682013A (en) * 2021-01-04 2021-04-20 西南石油大学 Experimental test method for high-temperature high-pressure visual exploitation of fracture-cavity condensate gas reservoir
CN112682013B (en) * 2021-01-04 2021-12-21 西南石油大学 Experimental test method for high-temperature high-pressure visual exploitation of fracture-cavity condensate gas reservoir

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